View source for ZS-2020-0001, Restoration Project Termination Plan FSS Final Report for Phase 4, A41 FSS Release Record - Survey Unit 10221C, Revision 1

{{Adams
| number = ML20133K019
| issue date = 07/29/2020
| title = Restoration Project Termination Plan FSS Final Report for Phase 4, A41 FSS Release Record - Survey Unit 10221C, Revision 1
| author name = Yetter R
| author affiliation = ZionSolutions, LLC
| addressee name = 
| addressee affiliation = NRC/NMSS
| docket = 05000295, 05000304
| license number = DPR-039, DPR-048
| contact person = 
| case reference number = ZS-2020-0001
| package number = ML20133J975
| document type = Report, Technical
| page count = 510
}}

=Text=
{{#Wiki_filter:ZION STATION RESTORATION PROJECT FINAL STATUS SURVEY RELEASE RECORD SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C REVISION 1

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C PREPARED BY / DATE:   Robert Yetter III Final Status Survey Specialist REVIEWED BY / DATE:   Robert Yetter Director, Radiological Site Closure APPROVED BY / DATE:   Sarah Roberts Vice President, Radiological Programs
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C TABLE OF CONTENTS
: 1. EXECUTIVE 

==SUMMARY==
 ................................................................................................... 7
: 2. SURVEY UNIT DESCRIPTION ......................................................................................... 7
: 3. CLASSIFICATION BASIS .................................................................................................. 8
: 4. DATA QUALITY OBJECTIVES (DQO) ......................................................................... 10
: 5. SURVEY DESIGN .............................................................................................................. 15
: 6. SURVEY IMPLEMENTATION........................................................................................ 22
: 7. SURVEY RESULTS............................................................................................................ 23
: 8. QUALITY CONTROL ....................................................................................................... 32
: 9. INVESTIGATIONS AND RESULTS ............................................................................... 33
: 10. REMEDIATION AND RESULTS ..................................................................................... 33
: 11. CHANGES FROM THE SURVEY PLAN ....................................................................... 33
: 12. DATA QUALITY ASSESSMENT (DQA) ........................................................................ 34
: 13. ANOMALIES....................................................................................................................... 34
: 14. CONCLUSION .................................................................................................................... 34
: 15. REFERENCES .................................................................................................................... 35
: 16. ATTACHMENTS ................................................................................................................ 36 ATTACHMENT 1 - FIGURE AND MAPS ............................................................................... 37 ATTACHMENT 2 - SCAN DATA ........................................................................................... 43 ATTACHMENT 3 - CONSULTATION TRIGGERS FOR RESIDENTIAL AND COMMERCIAL/INDUSTRIAL SOIL CONTAMINATION ............................... 52 ATTACHMENT 4 - SIGN TEST ............................................................................................. 54 ATTACHMENT 5 - QC SAMPLE ASSESSMENT ..................................................................... 56 ATTACHMENT 6 - GRAPHICAL PRESENTATIONS ................................................................ 59 ATTACHMENT 7 - SAMPLE ANALYTICAL REPORTS ............................................................ 66 ATTACHMENT 8 - EBERLINE ANALYTICAL REPORTS ................................................... 393
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C LIST OF TABLES Table 1 - Dose Significant Radionuclides and Mixture.......................................................................... 12 Table 2 - Base Case DCGLs for Surface Soils (BcDCGLSS) ................................................................ 13 Table 3 - Base Case DCGLs for Subsurface Soils (BcDCGLSB) .......................................................... 13 Table 4 - Operational DCGLs for Surface Soils (OpDCGLSS) ............................................................. 14 Table 5 - Operational DCGLs for Subsurface Soils (OpDCGLSB) ....................................................... 14 Table 6 - Surrogate Ratios ...................................................................................................................... 15 Table 7 - Investigation Levels ................................................................................................................ 17 Table 8 - Systematic Sample Measurement Locations ........................................................................... 19 Table 9 - Synopsis of Survey Design ..................................................................................................... 21 Table 10 - Instruments and Detectors ..................................................................................................... 23 Table 11 - Synopsis of Scan Results....................................................................................................... 24 Table 12 - Summary of Gamma Spectroscopy Results for Surface Soil Samples Comprising the Statistical Sample Population ............................................................................................... 26 Table 13 - Summary of Gamma Spectroscopy Results for Investigation/Judgmental Surface Soil Samples ................................................................................................................................. 27 Table 14 - Summary of Gamma Spectroscopy Results for Subsurface Soil Samples............................ 27 Table 15 - Off-Site Analysis Results ...................................................................................................... 28 Table 16 - Summary of Gamma Spectroscopy Results for QC Soil Samples ........................................ 30 Table 17 - Sum of Fractions for Individual Systematic Surface Soil Samples, when compared to the OpDCGLs ................................................................................................................... 30 Table 18 - Sum of Fractions for Investigation/Judgmental Surface Soil Samples, when compared to the OpDCGLs ................................................................................................................... 31 Table 19 - Sum of Fractions for Individual Subsurface Soil Samples, when compared to the OpDCGLs ............................................................................................................................. 32 Table 20 - Sum of Fractions for Individual QC Soil Samples, when compared to the OpDCGLs ........ 32 Table 21 - Basic Statistical Properties of Systematic Sample Population .............................................. 32 Table 22  Relocated Systematic Sample Locations............................................................................... 34 LIST OF FIGURES Figure 1 - Class 3 Open Land Survey Units from Figure 2-6 of the LTP ................................................ 8 Figure 2 - The Four Class 1 Open Land Survey Units Created from the Original Class 3 Survey Unit 10221B .............................................................................................................. 10
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C LIST OF ACRONYMS AND ABBREVIATIONS ALARA      As Low As Reasonably Achievable AMCG       Average Member of the Critical Group BcDCGL     Base Case Derived Concentration Guideline Level BcSOF      Base Case Sum of Fractions C/LT       Characterization/License Termination cpm        Counts per minute DQO        Data Quality Objective DCGL       Derived Concentration Guideline Level EMC        Elevated Measurement Comparison FSS        Final Status Survey GPS        Global Positioning System HTD        Hard-to-Detect HSA        Historical Site Assessment IC         Insignificant Contributor LBGR       Lower Bound of the Gray Region LTP        License Termination Plan MARSSIM    Multi-Agency Radiation Survey and Site Investigation Manual MDC        Minimum Detectable Concentration MDCR       Minimum Detectable Count Rate NAD        North American Datum NaI        Sodium Iodide OpDCGL     Operational Derived Concentration Guideline Level OpSOF      Operational Sum of Fractions QC         Quality Control RA         Radiological Assessment RE         Radiological Engineer ROC        Radionuclides of Concern SOF        Sum of Fractions
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C TEDE       Total Effective Dose Equivalent TSD        Technical Support Document UBGR       Upper Bound of the Gray Region VSP        Visual Sample Plan ZNPS       Zion Nuclear Power Station ZSRP       Zion Station Restoration Project
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
: 1. EXECUTIVE 

==SUMMARY==

This Final Status Survey (FSS) Release Record for Survey Unit 10221C, South of Protected Area - Inland, has been generated for the Zion Station Restoration Project (ZSRP) in accordance with ZionSolutions procedure ZS-LT-300-001-005, Final Status Survey Data Reporting (Reference 1) and satisfies the requirements of Section 5.11 of the Zion Station Restoration Project License Termination Plan (LTP) (Reference 2).
An FSS package (L1-10221C-F) was developed in accordance with ZionSolutions procedure ZS-LT-300-001-001, Final Status Survey Package Development (Reference 3), the ZSRP LTP, and guidance from NUREG-1575, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM) (Reference 4).
This open land survey unit has a MARSSIM classification of one. A survey plan was designed based upon use of the Sign Test as the nonparametric statistical test for compliance. Both the Type I () and Type II () decision error rates were set at 0.05. Seventeen (17) systematic surface soil samples were acquired from the survey unit. In addition, surface scanning was performed on 100% of the total surface area in the survey unit under the FSS Sample Plan. No areas of elevated activity were detected during the scans under the FSS Sample Plan. However, scans were performed earlier under a Radiological Assessment (RA) on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas one meter beyond the ballast gravel. The RA survey identified two (2) small areas of elevated activity (see Section 9 for further discussion). The analytical results for all soil samples (systematic and investigation) taken in survey unit 10221C indicated that the Sum of Fractions (SOF) for each sample, when compared to the Operational Derived Concentration Guideline Levels (OpDCGL), was less than 1.0. For the systematic samples, the maximum Operational SOF (OpSOF) was 0.262 with a mean OpSOF of 0.067. For the systematic samples, the mean Base Case SOF (BcSOF), when the analytical results were compared to the Base Case DCGLs (BcDCGL), was 0.017, which results in a dose assigned to the survey unit of 0.427 mrem/year Total Effective Dose Equivalent (TEDE).
Therefore, the null hypothesis is rejected and survey unit 10221C is acceptable for unrestricted release.
: 2. SURVEY UNIT DESCRIPTION Survey unit 10221C, South of Protected Area - Inland, is a Class 1 open land survey unit and is 1,959 m2 in size. It is bounded on the west by survey unit 10221B, the east by survey unit 10221D, the north by survey units 10209C thru 10209E, and the south by survey units 10220H and 10220I.
The topography of the survey unit is mainly flat with some small dips and depressions. The soil is mostly loam. A rail spur, with a ballast made up of gravel, runs through the southern half of the survey unit.
[7]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Illinois State Plane System North American Datum (NAD) 1983 East. The reference coordinates associated with the sample locations in this survey unit are presented in Table 8.
: 3. CLASSIFICATION BASIS Survey unit 10221C was classified in accordance with ZionSolutions procedure ZS-LT-300-001-002, Survey Unit Classification (Reference 5).
The area encompassing this survey unit was described as South of Fenced Area - Lakeshore and was located within survey unit 10221 as identified in Figure 4 of the Zion Station Historical Site Assessment (HSA) (Reference 6). Subsequently, this area was described as South of Protected Area - Inland (survey unit 10221B) in Table 2-29 and Figure 2-6 of the ZSRP LTP which is replicated below as Figure 1. This area was initially classified in both the HSA and LTP as Class 3.
Figure 1 - Class 3 Open Land Survey Units from Figure 2-6 of the LTP
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The HSA states that this area contained a parking area. It also discusses the potential for low levels of radiological contamination due to elevated environmental sample results from the 1970s. The elevated environmental samples appeared to have consisted primarily of tritium with the highest concentration (80 pCi/ml) found in the south ditch. The source was believed to be backup from storm drains that tied into the south Oil Separator and the Fire Sump system.
A Characterization Survey was performed in May and June of 2013 for the Class 3 survey unit 10221B. The following data was obtained:
* Five (5) judgmental surface samples taken in the drainage ditch on the east side of the survey unit.
* Twenty (20) random surface samples and two (2) random subsurface samples.
* One (1) investigation surface sample and one (1) investigation subsurface sample taken in an area identified by a scan alarm.
* NaI walkover scans of approximately 26% of the survey unit.
The results of the characterization survey were:
* Two (2) of the five (5) judgmental surface samples were positive for Cs-137 with the highest activity being 0.068 pCi/g.
* All twenty (20) of the random surface samples and the two (2) random subsurface samples were less than the Minimum Detectable Concentration (MDC) for the Radionuclides of Concern (ROC).
* The one (1) investigation surface sample and one (1) investigation subsurface sample were both <MDC for the ROC.
On July 15, 2016, due to changing radiological and operational conditions brought about by site decommissioning activities inside or adjacent to this area, survey unit 10221B was reclassified as a Class 1 open land survey unit, and divided into 4 survey units: 10221A, 10221B, 10221C and 10221D to comply with the survey unit size recommendations from MARSSIM Section 4.6.
The following figure shows the boundaries of the resulting Class 1 survey units. The change in classification was a conservative response which ensured that the survey unit was surveyed with the appropriate rigor.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Figure 2 - The Four Class 1 Open Land Survey Units Created from the Original Class 3 Survey Unit 10221B A Radiological Engineer (RE) and a Characterization/License Termination (C/LT) Supervisor performed a visual inspection and walk-down of the survey unit on July 24, 2019, prior to performing FSS. The purpose of the walk-down was to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions.
A final classification assessment was performed in accordance with procedure ZS-LT-300-001-002, Survey Unit Classification as part of the survey design for FSS. The assessment confirmed that survey unit 10221C was correctly classified as Class 1.
: 4. DATA QUALITY OBJECTIVES FSS planning and design hinges on coherence with the Data Quality Objective (DQO) process to ensure, through compliance with explicitly defined inputs and boundaries, that the primary objective of the survey is satisfied. The DQO process, utilized in accordance with MARSSIM, is described in the ZSRP LTP. The appropriate design for a given survey is developed using the DQO process as outlined in Appendix D of MARSSIM.
The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline
[10]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis, was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria.
Therefore, the survey unit would satisfy the primary objective of the FSS sample plan.
The primary objective of the FSS sample plan is to demonstrate that the level of residual radioactivity in survey unit 10221C does not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).
ZionSolutions Technical Support Document (TSD) 11-001, Technical Support Document for Potential Radionuclides of Concern During the Decommissioning of the Zion Station (Reference 7), established the basis for an initial suite of potential ROC for the decommissioning of the Zion Nuclear Power Station (ZNPS).
ZionSolutions TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms (Reference 8), was written to refine the initial selection of ROC for decommissioning at the ZSRP. The list of ROC was evaluated using Containment and Auxiliary Building concrete core analysis data to evaluate the dose significance of each radionuclide in the end state model.
Section 4.4 of TSD 14-019 evaluated the results of the characterization data of surveys taken of soils. The following conclusion was reached: The results of surface and subsurface soil characterization in the impacted area surrounding Zion indicate that there is minimal residual radioactivity in soil. Essentially all of the soil results were reported as non-detectable. Other than Cs-137 at very low levels, and Co-60 at a concentration of 0.24 pCi/g in one sample, the results for all radionuclides were less than MDC. Therefore, the direct determination of radionuclide mixture fractions for initial suite radionuclides in soil is not technically feasible due to the MDC biasing issues discussed above. Based on a generalized assumption that the contaminated water that caused concrete contamination would be similar to the source of soil contamination, the ROC and radionuclide mixture derived for the Auxiliary Building concrete was considered to be reasonably representative of soils for FSS planning and implementation.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The ROC for surface soils are listed in Table 1 below (from Table 5-2 of the LTP):
Table 1 - Dose Significant Radionuclides and Mixture Auxiliary Building Radionuclide                                       % of Total Activity (normalized)(1)(2)
Co-60                                                         0.92%
Ni-63                                                        23.71%
Sr-90                                                         0.05%
Cs-134                                                        0.01%
Cs-137                                                       75.32%
(1)  Based on maximum percent of total activity from Table 20 of TSD 14-019, normalized to one for the dose significant radionuclides (2)  Does not include dose significant radionuclides for activated concrete (H-3, Eu-152, Eu-154).
A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of DCGLs. The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soils.
Surface soil is defined as soil residing in the first 0.15 m (6 inches) layer of soil. A subsurface soil category, which is defined as a layer of soil beginning at the surface but extending to a depth of 1 m, is also assessed to allow for flexibility in compliance demonstration if contamination deeper than 0.15 m is encountered. Site-specific DCGLs for soil were calculated for both the 0.15 m and 1 m thicknesses. Based on characterization data and historical information, there are no expectations of encountering a source term geometry that is comprised of a clean surface layer of soil over a contaminated subsurface soil layer. ZionSolutions TSD 14-011, Soil Area Factors (Reference 9) and LTP, Section 6.8 provide the exposure scenarios and modeling parameters that were used to calculate the site-specific DCGLs for soils (referred to as BcDCGL in this Release Record).
At ZNPS, compliance is demonstrated through the summation of dose from four distinct source terms (basements, soils, buried pipe and groundwater) for the end-state. Basements are comprised of the summation of four structural source terms (surfaces, embedded pipe, penetrations and fill). When applied to soil, the DCGLs are expressed in units of activity per unit of mass (pCi/g). The unity rule is applied when there is more than one ROC. The measurement results for each singular ROC present in the mixture are compared against their respective DCGL to derive a dose fraction.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The surface and subsurface soil BcDCGLs for the unrestricted release of open land survey units are listed in Tables 5-5 and 5-6 of the LTP and are reproduced below in Table 2 and Table 3, respectively. The Insignificant Contributor (IC) dose percentage of 10% was used to adjust the DCGLs in soils to account for the dose from the eliminated IC radionuclides.
Table 2 - Base Case DCGLs for Surface Soils (BcDCGLSS)
Surface Soil DCGL Radionuclide (pCi/g)
Co-60                       4.26 Cs-134                      6.77 Cs-137                     14.18 Ni-63                    3,572.10 Sr-90                      12.09 Table 3 - Base Case DCGLs for Subsurface Soils (BcDCGLSB)
Subsurface Soil Radionuclide DCGL (pCi/g)
Co-60                       3.44 Cs-134                      4.44 Cs-137                      7.75 Ni-63                     763.02 Sr-90                       1.66 Each radionuclide-specific BcDCGL is equivalent to the level of residual radioactivity (above background levels) that could, when considered independently, result in a TEDE of 25 mrem/year to an Average Member of the Critical Group (AMCG). To ensure that the summation of dose from each source term is 25 mrem/year or less after all FSS is completed, the BcDCGLs are reduced based on an expected, or a priori, fraction of the 25 mrem/year dose limit from each source term. The reduced DCGLs, or Operational DCGLs, can be related to the BcDCGLs as an expected fraction of dose based on an a priori assessment of what the expected dose should be based on the results of site characterization, process knowledge and the extent of planned remediation. The OpDCGL is then used as the DCGL for the FSS design of the survey unit (calculation of surrogate DCGLs, investigations levels, etc.). Details of the OpDCGLs derived for each dose component and the basis for the applied a priori dose fractions are provided in ZionSolutions TSD 17-004, Operational Derived Concentration Guideline Levels for Final Status Survey (Reference 10).
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The OpDCGLs for the FSS of surface and subsurface soils are listed in Tables 5-7 and 5-8 of the LTP and are reproduced below in Table 4 and Table 5, respectively.
Table 4 - Operational DCGLs for Surface Soils (OpDCGLSS)
Surface Soil DCGL Radionuclide (pCi/g)
Co-60                      1.091 Cs-134                     1.733 Cs-137                     3.630 Ni-63                    914.458 Sr-90                      3.095 Table 5 - Operational DCGLs for Subsurface Soils (OpDCGLSB)
Subsurface Soil Radionuclide DCGL (pCi/g)
Co-60                      0.881 Cs-134                     1.137 Cs-137                     1.984 Ni-63                    195.333 Sr-90                      0.425 In accordance with NUREG-1757, Appendix G, if the HSA indicates that there is no likelihood of substantial subsurface residual radioactivity, subsurface surveys are not necessary. The HSA, as well as the results of the extensive characterization of subsurface soils in the impacted area surrounding the Zion facility have shown that there is minimal residual radioactivity in subsurface soil. Consequently, the ZSRP performed minimal subsurface sampling during FSS.
Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest at the required scan MDC, which for Class 1 open land survey units, is the a priori DCGL Elevated Measurement Comparison (DCGLEMC). Survey instrument response checks were required prior to issuance and after the instrument had been used. Control and accountability of survey instruments was required to ensure the quality and prevent the loss of data.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. The actual recorded value was used as the recorded FSS result for measurement and/or sample values that are less than MDC. Negative values were recorded as zero. For radionuclides less than MDC, the value representing the highest abundance was selected. Results were not reported as less than MDC. Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty, laboratory data qualifiers, units, and the observed MDC.
In accordance with the LTP, for laboratory analysis, MDCs less than 10% of the OpDCGL were preferable while MDCs up to 50% of the OpDCGL were acceptable. The maximum acceptable MDC for measurements obtained using field instruments was the a priori DCGLEMC, which was calculated using the methodology described in the LTP, Section 5.6.4.3.
: 5. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in ZS-LT-300-001-001, Final Status Survey Package Development.
The DQO process determined that Co-60, Ni-63, Sr-90, Cs-134 and Cs-137 would be the ROC in survey unit 10221C. During FSS, concentrations for Hard-to-Detect (HTD) ROC Ni-63 and Sr-90 were inferred using a surrogate approach. Cs-137 is the principle surrogate radionuclide for Sr-90 and Co-60 is the principle surrogate radionuclide for Ni-63. The mean, maximum and 95% Upper Confidence Level (UCL) of the surrogate ratios for concrete core samples taken in the Auxiliary Building basement were calculated in TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms, and are presented in Table 6. The maximum ratios will be used in the surrogate calculations during FSS unless area specific ratios are determined by continuing characterization.
Table 6 - Surrogate Ratios Auxiliary Building Ratios Mean         Max        95%UCL Ni-63/Co-60      44.143       180.450       154.632 Sr-90/Cs-137      0.001        0.002         0.002 For the FSS of survey unit 10221C, the surrogate OpDCGLs for Co-60 and Cs-137 were computed based on the maximum ratios from Table 6.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The equation for calculating a surrogate DCGL is as follows:
Equation 1 1
                         =
1                  2         3                
                                                       +   +         +
2            3 Where:          DCGLSur               =    Surrogate radionuclide DCGL DCGL2,3n             =    DCGL for radionuclides to be represented by the surrogate Rn                    =    Ratio of concentration (or nuclide mixture fraction) of radionuclide n to surrogate radionuclide Using the OpDCGLs for surface soils presented in Table 4 and the maximum ratios from Table 6, the following surrogate calculations for surface soils were performed:
Equation 2 1
(137) =                                                     = 3.622 /
1                 0.002 3.630                  +
(137)      3.095  (90)
The surrogate OpDCGL for surface soils that was used for Cs-137 in this survey unit for direct comparison of surface soil sample results to demonstrate compliance is 3.622 pCi/g.
Equation 3 1
(60) =                                                       = 0.898 /
1                   180.45 1.091                 +
(60)       914.458   (63)
The surrogate OpDCGL for surface soils that was used for Co-60 in this survey unit for direct comparison of surface soil sample results to demonstrate compliance is 0.898 pCi/g.
Using the BcDCGLs presented in Table 2 and the maximum ratios from Table 6, the following surrogate calculations were performed:
Equation 4 1
(137) =                                                    = 14.15 /
1                  0.002 14.18                  +
(137)      12.09  (90)
The surrogate BcDCGL for surface soils that was used for Cs-137 in this survey unit for calculating the DCGLEMC is 14.15 pCi/g.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Equation 5 1
(60) =                                         = 3.51 /
1               180.45 4.26          +
(60)     3572.10(63)
The surrogate BcDCGL for surface soils that was used for Co-60 in this survey unit for calculating the DCGLEMC is 3.51 pCi/g.
For this Class 1 open land survey unit, the Investigation Levels for area scanning and soil sample measurement results are those levels specified in LTP, Table 5-25, and are reproduced below in Table 7.
Table 7 - Investigation Levels Direct Investigation Classification                        Scan Investigation Levels Levels
                                     >Operational DCGL or >MDCscan if Class 1                                                                   > Operational DCGL MDCscan is greater than Operational DCGL The MDCscan for the 2350-1/44-10 was calculated using the methodology of ZionSolutions TSD-11-004, Ludlum Model 44-10 Detector Sensitivity (Reference 11) with the following parameters:
* background count rate of 5,000 counts per minute (cpm)
* scan speed of 0.5 m/sec
* distance from detector to surface of 2 inches
* isotopic mix of 95% Cs-137 and 5% Co-60 The calculated MDCscan value was 3.75 pCi/g, which was greater than the calculated surrogate DCGLs, therefore the scan investigation level was set at the MDCscan of the 2350-1/44-10. The collimator was used during the scan surveys to lower the background count rate.
The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.
The number of soil samples for FSS was determined in accordance with ZS-LT-300-001-001.
The relative shift (/) for the survey unit data set is defined as shift (), which is the Upper Bound of the Gray Region (UBGR), or the DCGL (SOF of 1.0), minus the Lower Bound of the Gray Region (LBGR) (SOF of 0.5), divided by sigma (), which is the standard deviation of the data set used for survey design. The optimal value for / should range between one and three.
The largest value the / can have is three. If the / exceeds three, then the value of three will
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C be used for /. For this survey design, a conservative estimate of the sample variability of 0.30 was used as the coefficient of variation to calculate /.
The calculated relative shift was 1.67. Both the Type I error, or  value, and the Type II error, or  value, was set at 0.05. The sample size from Table 5.5 of MARSSIM that equates to the Type I and Type II error of 0.05 for use with the Sign Test is an N value of 17.
The computer program Visual Sample Plan (VSP) was used to generate the sample map, in accordance with ZS-LT-300-001-001.             The map used was provided by the Survey Mapping/Computer Assisted Design Specialist, with coordinates based on the Illinois State Plane NAD 1983 standard topographical grid coordinate system. The number of samples generated by VSP for a systematic triangular grid was 17. The Prospective Power Curve generated by VSP showed adequate power for the survey design.
In accordance with section 5.6.4.3 of the LTP, the a priori DCGLEMC values were calculated for the gamma emitting ROC to ensure that the MDCscan of the selected instrument was sufficient to detect small areas of elevated activity in the survey unit. The calculations were:
1959
* To calculate the area bounded by the systematic samples:  =            =  17
                                                                                          = 115.2 2
* From the LTP, Table 5-16, the Area Factors for the next larger area (300 m2) were used:
o Cs-137 - 1.46 o Cs-134 - 1.30 o Co 1.16
* The DCGLEMC is the Surrogate Base Case DCGL times the Area Factor:
o The DCGLEMC for Cs-137 = 1.46  14.15 = 20.66 /
o The DCGLEMC for Cs-134 = 1.30  6.77 = 8.80 /
o The DCGLEMC for Co-60 = 1.16  3.51 = 4.07 /
The calculated MDCscan, 3.75 pCi/g, is less than the DCGLEMC values calculated above, therefore, the spacing of the statistical systematic sampling and measurement locations was adequate to detect small areas of elevated radioactivity. No adjustment to the sample number was required.
The implementation of quality control (QC) measures as referenced by LTP, Section 5.9 and ZionSolutions procedure ZS-LT-01, Quality Assurance Project Plan (for Characterization and FSS) (QAPP) (Reference 12) includes the collection of a soil sample for split sample analysis on 5% of the soil samples taken in a survey unit with the locations selected at random.
One (1) surface soil sample (L1-10221C-FQGS-012-SS) was selected randomly for split sample analysis for the FSS of this survey unit.
In accordance with section 5.7.1.6.2 of the LTP, a subsurface soil sample was taken at 10%
of the systematic surface soil sample locations in the survey unit with the location(s) selected at random. Locations L1-10221C-FSGS-005-SB and L1-10221C-FSGS-013-SB were
[18]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C selected for this survey unit.
The locations of the seventeen (17) systematic samples are listed in Table 8. Also included are the locations of the two (2) subsurface samples. A map of the systematic sample locations is included in Attachment 1.
Table 8 - Systematic Sample Measurement Locations NORTHING              EASTING MEASUREMENT ID (meters)             (meters)
L1-10221C-FSGS-001-SS              641486.29            343565.68 L1-10221C-FSGS-002-SS              641486.29            343577.21 L1-10221B-FSGS-003-SS              641496.28            343559.91 L1-10221B-FSGS-004-SS              641496.28            343571.45 L1-10221B-FSGS-005-SS              641496.28            343582.98 L1-10221B-FSGS-006-SS              641506.27            343565.68 L1-10221B-FSGS-007-SS              641506.27            343577.21 L1-10221B-FSGS-008-SS              641506.27            343588.75 L1-10221B-FSGS-009-SS              641516.26            343571.45 L1-10221B-FSGS-010-SS              641516.26            343582.98 L1-10221B-FSGS-011-SS              641526.25            343565.68 L1-10221B-FSGS-012-SS              641526.25            343577.21 L1-10221B-FSGS-013-SS              641526.25            343588.75 L1-10221B-FSGS-014-SS              641536.24            343571.45 L1-10221B-FSGS-015-SS              641536.24            343582.98 L1-10221B-FSGS-016-SS              641536.24            343594.52 L1-10221B-FSGS-017-SS              641546.23            343577.21 L1-10221B-FSGS-005-SB              641496.28            343582.98 L1-10221B-FSGS-013-SB              641526.25            343588.75 ZSRP LTP, Section 5.1 states that soil samples will be collected during FSS to confirm the HTD to surrogate radionuclide ratios (provided in Table 6). Ten percent (10%) of the FSS samples collected from open land survey units will be analyzed for HTD ROC. Only HTD radionuclides included as ROC (Ni-63 and Sr-90 for soils) will be analyzed in the FSS confirmatory samples. For soil samples with positive results for both a HTD ROC and the corresponding surrogate radionuclide (Cs-137 or Co-60), the HTD surrogate ratio will be derived and compared against the maximum ratio. The maximum ratios will be used unless specific survey information supports the use of a surrogate ratio that is specific to the area. In these cases, the survey unit-specific radiological data and the derived surrogate ratios will be submitted to the NRC for approval. If approved, then the survey unit-specific ratios used and the survey data serving as the basis for the surrogate ratios will be documented in the release record for the survey unit.
[19]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C In addition, LTP Chapter 5, Section 5.1 states that if levels of residual gamma radioactivity in an individual soil sample exceed an OpSOF of 0.1, then the sample(s) will be analyzed for HTD ROC. Six (6) samples: L1-10221C-FSGS-012-SS, L1-10221C-FSGS-013-SS, L1-10221C-FSGS-014-SS, L1-10221C-FSGS-013-SB, L1-10221C-FIGS-101-SS and L1-10221C-FIGS-103-SS exceeded an OpSOF of 0.1 during the FSS of survey unit 10221C.
These samples satisfy the requirement that 10% of the samples collected for the FSS of survey unit 10221C be analyzed for HTD ROC. Each selected sample was sent off-site (Eberline Analytical) for analysis of the HTD ROC as specified in LTP, Section 5.1. Eberline analytical reports are provided in Attachment 8.
Table 9 provides a synopsis of the survey design for survey unit 10221C.
[20]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 9 - Synopsis of Survey Design FEATURE                   DESIGN CRITERIA                              BASIS Survey Unit Area                   1,959 m2                   GPS measurements of area
                                                               *  = 0.30
* UBGR = SOF of 1
* LBGR = SOF of 0.5 Number of Surface 17 (Systematic)
* Type I error = 0.05 Soil Samples
* Type II error = 0.05
                                                               * / = 1.67 (MARSSIM Table 5.5)
Grid Spacing                      11.5 m                     (LTP, Section 5.6.4.5.2)
* Co 1.091 pCi/g
* Cs-134 - 1.733 pCi/g Operational DCGLs for Surface DCGLs
* Cs-137 - 3.630 pCi/g Soils, (LTP, Table 5-7)
* Ni 914.458 pCi/g
* Sr 3.095 pCi/g A minimum of two (2) soil samples HTD ROC Analysis                                                   (LTP, Section 5.1) selected for HTD ROC analysis Measurement Operational DCGL                     (LTP, Table 5-25)
Investigation Level Scan Survey Area 100%                         (LTP, Table 5-24)
Coverage One (1) surface soil sample selected QC                                                         (LTP, Section 5.9) randomly for split sample analysis Number of Two (2) - systematic surface soil sample Subsurface Soil                                               (LTP, Section 5.7.1.6.2) locations 5 and 13 Samples
[21]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
: 6. SURVEY IMPLEMENTATION Survey instructions for this FSS were incorporated into and performed in accordance with FSS sample plan L1-10221C-F, which was developed in accordance with ZS-LT-300-001-001. The FSS unit was inspected and controlled in accordance with ZionSolutions procedure ZS-LT-300-001-003, Isolation and Control for Final Status Survey (Reference 13).
For survey unit 10221C, compliance with the unrestricted release criteria was demonstrated through a combination of surface scanning with a Ludlum Model 44-10 gamma detector and the sampling of surface soil for isotopic analysis. In accordance with the LTP Chapter 5, two (2) subsurface samples were obtained and analyzed. Also, if during the performance of FSS, the analysis of a surface soil sample, or the results of a surface gamma scan indicated the potential presence of residual radioactivity at a concentration of 75% of the subsurface Operational DCGL, then a biased subsurface soil sample(s) would be taken to the appropriate depth within the area of concern as part of the investigation. This threshold was encountered during a RA survey on June 17, 2019. While performing a gamma scan of the railroad ballast located in survey unit 10221C, and the soil areas 1 meter beyond the ballast gravel, two (2) small areas of elevated activity were identified. A small radioactive particle was identified in one of the areas and was captured. Surface and subsurface investigation soil samples were taken at these locations (L1-10221C-FIGS-100-SS thru L1-10221C-FIGS-113-SS, L1-10221C-FIGS-100-SB and L1-10221C-FIGS-101-SB).
FSS field activities were conducted under FSS sample plan L1-10221C-F. A Field Log (ZS-LT-300-001-001, Attachment 14) was used to document field activities and other information pertaining to the performance of the FSS. FSS field activities were projected to take four (4) working days to complete. Daily briefings were conducted to discuss the expectations for job performance and to review safety aspects of the job. The survey required field activities were performed during normal working hours starting on June 11, 2019, and concluding September 17, 2019.
The seventeen (17) systematic surface soil sample locations were marked with flags based on GPS coordinates provided by VSP. Three (3) samples were relocated because they fell on the railroad ballast, which consists of gravel and not soil. The relocated sample points are listed in Table 22 and are shown on the systematic sample map in Attachment 1 and the posting plot in Attachment 6.
Under the FSS sample plan, gamma scans were performed on 100% of the surface area of the survey unit using a Ludlum 2350-1 paired with a Model 44-10 (2 x 2) NaI detector operated in the rate-meter mode and using audio response. The probe was positioned within 2-inches to the ground and was moved at a scan speed of approximately 0.5 meters per second. No areas of elevated activity were detected during the scans under the FSS Sample Plan. However, scans were performed at an earlier date under an RA on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas 1 meter beyond the ballast gravel. The RA survey
[22]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C identified two (2) small areas of elevated activity (see Section 9 for further discussion). Each detector was subjected to an Operation Response Check daily, prior to and following use, in accordance with ZionSolutions procedure ZS-RP-108-004-011, Operation of the Ludlum Model 2350-1 Data Logger (Reference 14). The daily Operational Response Check compared the background response and the response to check sources ranges, established for normal background and detector source response, to ensure that the detector was working properly.
The instruments and detectors used for this survey are presented in Table 10. The instruments and detectors were verified to be properly calibrated prior to use.
Table 10 - Instruments and Detectors Instrument/Detector Type                     Serial #               Calibration Due Date Ludlum 2350-1/Ludlum 44-10               293136/PR316938                   06/18/20 Ludlum 2350-1/Ludlum 44-10               304712/PR372143                    09/9/20 Ludlum 2350-1/Ludlum 44-10               266657/PR308037                   05/13/20 Ludlum 2350-1/Ludlum 44-10               304718/PR363311                   12/13/19 Ludlum 2350-1/Ludlum 44-10               304730/PR375273                   01/16/20 Ludlum 2350-1/Ludlum 44-10               304711/PR321902                   01/18/20 Ludlum 2350-1/Ludlum 44-10               304726/PR363452                   09/06/19 In accordance with the survey design, seventeen (17) surface soil samples were collected at the designated systematic sample points along with two (2) subsurface samples taken at randomly selected locations. In addition, fourteen (14) surface samples and two (2) subsurface samples were collected as part of the investigation of two (2) areas of elevated activity identified during surface scans performed under an RA; and eight (8) judgmental surface samples were taken adjacent to the railroad ballast on both sides.
Six (6) samples (L1-10221C-FSGS-012-SS, L1-10221C-FSGS-013-SS, L1-10221C-FSGS-014-SS, L1-10221C-FSGS-013-SB, L1-10221C-FIGS-101-SS and L1-10221C-FIGS-103-SS) were selected for HTD radionuclide analysis. One (1) surface soil sample (L1-10221C-FQGS-012-SS) was selected randomly for QC sample analysis.
: 7. SURVEY RESULTS One hundred percent (100%) of the surface of the survey unit was scanned for elevated radiation levels. Sixty-eight (68) 1-meter wide scan rows, as shown on the map in Attachment 1, were marked in the field and scanned with the 2350-1/44-10 using latching mode. Readings were recorded at approximately 10-meter intervals during the scans. No elevated measurements locations were identified by surface scan under the FSS Sample Plan. However, scans were performed at an earlier date under an RA on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas 1 meter beyond the ballast gravel. The RA survey
[23]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C identified two (2) small areas of elevated activity (see Section 9 for further discussion). Table 11 provides an overview of the scan results. Complete scan results are provided in Attachment 2.
Table 11 - Synopsis of Scan Results Highest Logged Scan                         Action Level(1) # of Scan Reading                                          Investigation Samples Area                                             Alarms (cpm)              (cpm)
Row 1            2090               2285           None                  None Row 2            2178               2285           None                  None Row 3            2198               2285           None                  None Row 4            1996               2285           None                  None Row 5            1815               2285           None                  None Row 6            1767               2285           None                  None Row 7            1840               2285           None                  None Row 8            1939               2285           None                  None Row 9            1875               2244           None                  None Row 10            1806               2244           None                  None Row 11            1943               2244           None                  None Row 12            2049               2244           None                  None Row 13            1946               2244           None                  None Row 14            1984               2244           None                  None Row 15            1972               2244           None                  None Row 16            1923               2244           None                  None Row 17            2070               2456           None                  None Row 18            2345               2456           None                  None Row 19            2292               2456           None                  None Row 20            2197               2456           None                  None Row 21            2408               2456           None                  None Row 22            2246               2456           None                  None Row 23            2340               2456           None                  None Row 24            2258               2456           None                  None Row 25            2359               2771           None                  None Row 26            2472               2771           None                  None Row 27            2349               2771           None                  None Row 28            2261               2771           None                  None Row 29            2227               2771           None                  None Row 30            2426               2771           None                  None Row 31            2554               2771           None                  None Row 32            2520               2771           None                  None Row 33            2574               3120           None                  None
[24]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 11 (continued) - Synopsis of Scan Results Scan       Highest Logged Action Level(1) # of Scan Reading                                                           Investigation Samples Area                                                            Alarms (cpm)                      (cpm)
Row 34               2765                       3120               None                         None Row 35               2813                       3120               None                         None Row 36               2718                       3120               None                         None Row 37               3011                       3120               None                         None Row 38               3109                       3120               None                         None Row 39               2928                       3120               None                         None Row 40               3057                       3120               None                         None Row 41               3103                       3566               None                         None Row 42               3275                       3566               None                         None Row 43               3067                       3566               None                         None Row 44               3252                       3566               None                         None Row 45               3063                       3566               None                         None Row 46               3063                       3566               None                         None Row 47               3109                       3566               None                         None Row 48               3188                       3566               None                         None Row 49               3359                       3576               None                         None Row 50               3076                       3576               None                         None Row 51               3544                       3576               None                         None Row 52               3316                       3576               None                         None Row 53               3337                       3576               None                         None Row 54               3054                       3576               None                         None Row 55               3202                       3576               None                         None Row 56               3198                       3576               None                         None Row 57               3059                       3327               None                         None Row 58               3276                       3327               None                         None Row 59               3128                       3327               None                         None Row 60               3000                       3327               None                         None Row 61               3024                       3463               None                         None Row 62               3053                       3463               None                         None Row 63               3188                       3463               None                         None Row 64               2971                       3463               None                         None Row 65               2799                       3463               None                         None Row 66               2729                       3463               None                         None Row 67               2929                       3463               None                         None Row 68               2712                       3463               None                         None
: 1)  The action level is based on the measurement Minimum Detectable Count Rate (MDCR) plus background in accordance with the FSS plan
[25]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The seventeen (17) systematic surface soil samples taken for non-parametric statistical testing, the twenty-two (22) biased surface soil samples (investigation and judgmental) and the four (4) subsurface soil samples were analyzed using the on-site gamma spectroscopy system.
Summaries of the sample analysis results are provided in Tables 12, 13 and 14, respectively. The basic statistics for the systematic sample population are summarized in Table 21. For the systematic samples, the gamma spectroscopy results revealed seven (7) samples with activity levels above MDC for Cs-137, two (2) samples with activity levels above MDC for Co-60 and no samples with activity levels above MDC for Cs-134. The concentrations for Ni-63 and Sr-90 were inferred based on the maximum ratios as specified in Table 6. The mean of the gamma spectroscopic analysis results for the sample population indicated that Cs-137 was present at levels lower than the concentrations of Cs-137 expected to be found in off-site soil in the vicinity of the ZNPS as presented in ZionSolutions TSD 13-004, Examination of Cs-137 Global Fallout In Soils At Zion Station (Reference 15). The complete gamma spectroscopy reports are presented in Attachment 7.
Table 12 - Summary of Gamma Spectroscopy Results for Surface Soil Samples Comprising the Statistical Sample Population Co-60(1)            Cs-134(1)            Cs-137(1)  Ni-63(2)  Sr-90(2)
MEASUREMENT ID (pCi/g)              (pCi/g)              (pCi/g)   (pCi/g)   (pCi/g)
L1-10221C-FSGS-001-SS                       1.95E-02             1.05E-02             1.71E-02  3.52E+00  3.42E-05 L1-10221C-FSGS-002-SS                       2.85E-02             1.31E-02             2.68E-02  5.14E+00  5.36E-05 L1-10221C-FSGS-003-SS                       9.10E-03             0.00E+00             3.65E-02  1.64E+00  7.30E-05 L1-10221C-FSGS-004-SS                       6.14E-03             5.33E-03            0.00E+00   1.11E+00  0.00E+00 L1-10221C-FSGS-005-SS                       4.16E-02             4.82E-03             7.47E-02  7.51E+00  1.49E-04 L1-10221C-FSGS-006-SS                       2.46E-02             1.30E-03             5.20E-02  4.44E+00  1.04E-04 L1-10221C-FSGS-007-SS                       3.26E-02             0.00E+00             9.37E-02  5.88E+00  1.87E-04 L1-10221C-FSGS-008-SS                       1.02E-02             1.12E-02            0.00E+00   1.84E+00  0.00E+00 L1-10221C-FSGS-009-SS                       2.92E-02             1.66E-02             1.61E-02  5.27E+00  3.22E-05 L1-10221C-FSGS-010-SS                       0.00E+00             0.00E+00             1.43E-02  0.00E+00  2.86E-05 L1-10221C-FSGS-011-SS                       5.21E-02             3.65E-02             4.53E-03  9.40E+00  9.06E-06 L1-10221C-FSGS-012-SS                       2.59E-02             5.26E-02             3.18E-01  4.67E+00  6.36E-04 L1-10221C-FSGS-013-SS                       9.66E-02             2.34E-02             1.41E-01  1.74E+01  2.82E-04 L1-10221C-FSGS-014-SS                       1.05E-01             4.43E-02             4.32E-01  1.89E+01  8.64E-04 L1-10221C-FSGS-015-SS                       2.33E-02             2.28E-02             4.24E-02  4.20E+00  8.48E-05 L1-10221C-FSGS-016-SS                       2.67E-02             3.22E-02             5.17E-02  4.82E+00  1.03E-04 L1-10221C-FSGS-017-SS                       1.06E-02             1.20E-02             9.70E-04  1.91E+00  1.94E-06 Note: (1) Bold font indicates ROC positively detected at concentration greater than MDC.
(2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
[26]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 13 - Summary of Gamma Spectroscopy Results for Investigation/Judgmental Surface Soil Samples Co-60    (1)        Cs-134(1)            Cs-137(1)  Ni-63(2)  Sr-90(2)
MEASUREMENT ID (pCi/g)              (pCi/g)              (pCi/g)   (pCi/g)   (pCi/g)
L1-10221C-FIGS-100-SS                      4.22E-03             5.24E-03             1.97E-02  7.61E-01  3.94E-05 L1-10221C-FIGS-101-SS                      1.09E-01             3.79E-02             5.69E-01  1.97E+01  1.14E-03 L1-10221C-FIGS-102-SS                      2.60E-02             1.53E-02             9.16E-02  4.69E+00  1.83E-04 L1-10221C-FIGS-103-SS                      5.84E-02             5.71E-03             1.58E-01  1.05E+01  3.16E-04 L1-10221C-FIGS-104-SS                      2.70E-02             6.48E-03             7.55E-03  4.87E+00  1.51E-05 L1-10221C-FIGS-105-SS                      4.93E-02             0.00E+00             2.82E-02  8.90E+00  5.64E-05 L1-10221C-FIGS-106-SS                      2.97E-02             0.00E+00             4.60E-02  5.36E+00  9.20E-05 L1-10221C-FIGS-107-SS                      8.24E-03             5.03E-02             1.39E-02  1.49E+00  2.78E-05 L1-10221C-FIGS-108-SS                      2.41E-02             6.42E-04             1.17E-02  4.35E+00  2.34E-05 L1-10221C-FIGS-109-SS                      8.17E-03             0.00E+00             5.13E-02  1.47E+00  1.03E-04 L1-10221C-FIGS-110-SS                      1.75E-02             3.92E-03             2.51E-02  3.16E+00  5.02E-05 L1-10221C-FIGS-111-SS                      0.00E+00             0.00E+00             3.55E-02  0.00E+00  7.10E-05 L1-10221C-FIGS-112-SS                      1.37E-02             4.34E-03             8.17E-03  2.47E+00  1.63E-05 L1-10221C-FIGS-113-SS                      2.82E-02             0.00E+00            0.00E+00   5.09E+00  0.00E+00 L1-10221C-FJGS-001-SS                      8.17E-04             1.74E-02             1.28E-02  1.47E-01  2.56E-05 L1-10221C-FJGS-002-SS                      4.26E-02             0.00E+00             7.32E-02  7.69E+00  1.46E-04 L1-10221C-FJGS-003-SS                      1.50E-02             0.00E+00            0.00E+00   2.71E+00  0.00E+00 L1-10221C-FJGS-004-SS                      1.97E-02             1.13E-02             5.00E-02  3.55E+00  1.00E-04 L1-10221C-FJGS-005-SS                      4.25E-03             3.06E-02            0.00E+00   7.67E-01  0.00E+00 L1-10221C-FJGS-006-SS                      0.00E+00             0.00E+00             4.68E-02  0.00E+00  9.36E-05 L1-10221C-FJGS-007-SS                      3.55E-02             1.03E-02             3.26E-02  6.41E+00  6.52E-05 L1-10221C-FJGS-008-SS                      3.28E-02             1.36E-03             1.34E-02  5.92E+00  2.68E-05 Note: (1) Bold font indicates ROC positively detected at concentration greater than MDC.
(2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
Table 14 - Summary of Gamma Spectroscopy Results for Subsurface Soil Samples Co-60(1)            Cs-134(1)            Cs-137(1)  Ni-63(2)  Sr-90(2)
MEASUREMENT ID (pCi/g)              (pCi/g)              (pCi/g)   (pCi/g)   (pCi/g)
L1-10221C-FSGS-005-SB                      1.25E-02             3.85E-03             4.63E-03  2.26E+00  9.26E-06 L1-10221C-FSGS-013-SB                      6.59E-02             3.57E-03             1.49E-01  1.19E+01  2.98E-04 L1-10221C-FIGS-100-SB                      0.00E+00             1.00E-02             3.56E-02  0.00E+00  7.12E-05 L1-10221C-FIGS-101-SB                      0.00E+00             4.49E-02             2.18E-02  0.00E+00  4.36E-05 Note: (1) Bold font indicates ROC positively detected at concentration greater than MDC.
(2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
[27]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The off-site laboratory, Eberline Analytical, processed the six (6) samples selected for HTD ROC analysis. Samples L1-10221C-FSGS-012-SS, L1-10221C-FSGS-013-SS, L1-10221C-FSGS-014-SS, L1-10221C-FSGS-013-SB, L1-10221C-FIGS-101-SS and L1-10221C-FIGS-103-SS were selected. Only HTD radionuclides included as ROC (Ni-63 and Sr-90 for soils) were included in the analysis. All analyses met the required MDC. Co-60 and Ni-63 were positively detected in only one (1) of the samples at a concentration greater than MDC. The HTD to surrogate ratio for this sample was 6.10 (see sample L1-10221A-FSGS-014SS-A) which is well below the maximum Ni-63/Co-60 ratio of 180.450 listed in Table 6. The off-site analysis results are provided in Table 15.
Table 15 - Off-Site Analysis Results Sample # L1-10221C-FSGS-012-SS-A Result          Uncertainty            MDC ROC                                                                         >MDC (pCi/g)            (pCi/g)           (pCi/g)
Co-60             -1.16E-02           1.07E-01          1.34E-01               No Cs-134            -2.28E-01           1.38E-01          1.27E-01               No Cs-137             1.78E-01           1.04E-01          1.62E-01              Yes Ni-63             -9.66E-01          2.02E+00           3.54E+00               No Sr-90             1.12E-01           3.71E-01          7.80E-01               No Sample # L1-10221C -FSGS-013-SS-A Result          Uncertainty            MDC ROC                                                                         >MDC (pCi/g)            (pCi/g)            (pCi/g)
Co-60              1.80E-02           9.42E-02           1.55E-01               No Cs-134             9.24E-03           2.70E-02           1.17E-01               No Cs-137             1.76E-01           9.04E-02           1.39E-01              Yes Ni-63             -1.38E+00          2.05E+00            3.61E+00               No Sr-90             2.71E-01           2.71E-01           5.48E-01               No Sample # L1-10221C -FSGS-014-SS-A Result          Uncertainty            MDC ROC                                                                         >MDC (pCi/g)            (pCi/g)            (pCi/g)
Co-60              5.93E-01           9.00E-02           1.17E-01              Yes Cs-134             7.28E-03           2.90E-02           5.86E-02               No Cs-137             2.29E+00           2.83E-01           1.47E-01              Yes Ni-63              3.62E+00          2.18E+00            3.58E+00              Yes Sr-90             7.79E-02           3.72E-01           7.86E-01               No
[28]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 15 (Continued) - Off-Site Analysis Results Sample # L1-10221C-FSGS-013-SB-A Result              Uncertainty        MDC ROC                                                                       >MDC (pCi/g)                (pCi/g)        (pCi/g)
Co-60              5.71E-02               5.36E-02       7.05E-02            No Cs-134              1.11E-02               2.59E-02       5.16E-02            No Cs-137              8.93E-02               5.74E-02       9.00E-02            No Ni-63             -6.98E-01               1.83E+00       3.19E+00            No (1)
Sr-90               4.90E-02               3.43E-02       6.77E-02            No Sample # L1-10221C-FIGS-101-SS-A Result              Uncertainty        MDC ROC                                                                       >MDC (pCi/g)                (pCi/g)        (pCi/g)
Co-60              2.45E-01               5.59E-02       6.76E-02           Yes Cs-134              1.30E-02               2.24E-02       5.57E-02            No Cs-137             1.06E+00                1.48E-01       1.07E-01           Yes Ni-63              6.32E-01               2.03E+00       3.46E+00            No Sr-90              3.55E-01               3.07E-01       7.39E-01            No Sample # L1-10221C-FIGS-103-SS-A Result              Uncertainty        MDC ROC                                                                       >MDC (pCi/g)                (pCi/g)        (pCi/g)
Co-60              9.13E-02               6.23E-02       1.12E-01            No Cs-134              1.66E-02               2.41E-02       1.04E-01            No Cs-137              1.73E-01               8.28E-02       1.26E-01           Yes Ni-63             2.41E+00                1.96E+00       3.26E+00            No Sr-90              3.73E-01               3.20E-01       6.40E-01            No (1) Sr-90 recounted February 19, 2020, to achieve adequate MDC The implementation of survey specific QC measures included the collection of one (1) systematic sample (L1-10221C-FQGS-012-SS) and two (2) biased samples (L1-10221C-QJGS-001-SS and L1-10221C-QIGS-110-SS) for split sample analysis. The on-site laboratory analyzed the QC samples using the on-site gamma spectroscopy system. Gamma spectroscopy results are summarized in Table 16. The concentrations for Ni-63 and Sr-90 were inferred based on the maximum ratios as specified in Table 6.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 16 - Summary of Gamma Spectroscopy Results for QC Soil Samples Co-60(1)            Cs-134(1)            Cs-137(1)      Ni-63(2)    Sr-90(2)
MEASUREMENT ID (pCi/g)              (pCi/g)              (pCi/g)       (pCi/g)     (pCi/g)
L1-10221C-FQGS-012-SS                       1.35E-04             6.96E-02             1.52E-01      2.44E-02    3.04E-04 L1-10221C-QJGS-001-SS                       1.80E-02             0.00E+00             1.26E-02     3.25E+00     2.52E-05 L1-10221C-QIGS-110-SS                       2.05E-02             3.01E-02             5.65E-02     3.70E+00     1.13E-04 Note:  (1) Bold font indicates ROC positively detected at concentration greater than MDC.
(2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
The SOF or unity rule is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The equation for the unity rule is:
Equation 6 C1              C2                      Cn
                               +               +............         1 DCGL1 DCGL 2                               DCGL n Where:         Cn               = concentration of radionuclide n DCGLn            = DCGL of radionuclide n.
The results of the unity rule calculations for the ROC in the systematic sample population when compared against the OpDCGLs for surface soils for survey unit 10221C are presented in Table 17. The results of the unity rule calculations for the ROC for the biased surface samples are presented in Table 18, the results for the subsurface samples are presented in Table 19, and the results for the QC samples are presented in Table 20.
Table 17 - Sum of Fractions for Systematic Surface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID                                                                                                      OpSOF Co-60              Cs-134            Cs-137          Ni-63      Sr-90 L1-10221C-FSGS-001-SS 1.79E-02 6.06E-03 4.71E-03 3.85E-03 1.11E-05                                                   0.033 L1-10221C-FSGS-002-SS 2.61E-02 7.56E-03 7.38E-03 5.62E-03 1.73E-05                                                   0.047 L1-10221C-FSGS-003-SS 8.34E-03 0.00E+00 1.01E-02 1.80E-03 2.36E-05                                                   0.020 L1-10221C-FSGS-004-SS 5.63E-03 3.08E-03 0.00E+00 1.21E-03 0.00E+00                                                   0.010 L1-10221C-FSGS-005-SS 3.81E-02 2.78E-03 2.06E-02 8.21E-03 4.83E-05                                                   0.070 L1-10221C-FSGS-006-SS 2.25E-02 7.50E-04 1.43E-02 4.85E-03 3.36E-05                                                   0.043 L1-10221C-FSGS-007-SS 2.99E-02 0.00E+00 2.58E-02 6.43E-03 6.05E-05                                                   0.062 L1-10221C-FSGS-008-SS 9.35E-03 6.46E-03 0.00E+00 2.01E-03 0.00E+00                                                   0.018 L1-10221C-FSGS-009-SS 2.68E-02 9.58E-03 4.44E-03 5.76E-03 1.04E-05                                                   0.047 L1-10221C-FSGS-010-SS 0.00E+00 0.00E+00 3.94E-03 0.00E+00 9.24E-06                                                   0.004 L1-10221C-FSGS-011-SS 4.78E-02 2.11E-02 1.25E-03 1.03E-02 2.93E-06                                                   0.080
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 17 (continued) - Sum of Fractions for Systematic Surface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID                                                                         OpSOF Co-60       Cs-134      Cs-137       Ni-63       Sr-90 L1-10221C-FSGS-012-SS 2.37E-02 3.04E-02 8.76E-02 5.11E-03 2.05E-04                      0.147 L1-10221C-FSGS-013-SS 8.85E-02 1.35E-02 3.88E-02 1.91E-02 9.11E-05                      0.160 L1-10221C-FSGS-014-SS 9.62E-02 2.56E-02 1.19E-01 2.07E-02 2.79E-04                      0.262 L1-10221C-FSGS-015-SS 2.14E-02 1.32E-02 1.17E-02 4.60E-03 2.74E-05                      0.051 L1-10221C-FSGS-016-SS 2.45E-02 1.86E-02 1.42E-02 5.27E-03 3.34E-05                      0.063 L1-10221C-FSGS-017-SS 9.72E-03 6.92E-03 2.67E-04 2.09E-03 6.27E-07                      0.019 Systematic Measurements Number of Systematic Measurements =   17
                                          # of Systematic Measurements with OpSOF > 1 =    0
                      # of Systematic Measurements with OpSOF > 0.1 (HTD Assessment) =     3 Max Individual Systematic Measurement OpSOF =   0.262 Mean Systematic Measurement OpSOF =    0.067 Table 18 - Sum of Fractions for Investigation/Judgmental Surface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID                                                                         OpSOF Co-60       Cs-134      Cs-137       Ni-63       Sr-90 L1-10221C-FIGS-100-SS       3.87E-03 3.02E-03 5.43E-03 8.33E-04 1.27E-05                0.013 L1-10221C-FIGS-101-SS       9.99E-02 2.19E-02 1.57E-01 2.15E-02 3.68E-04                0.300 L1-10221C-FIGS-102-SS       2.38E-02 8.83E-03 2.52E-02 5.13E-03 5.92E-05                0.063 L1-10221C-FIGS-103-SS       5.35E-02 3.29E-03 4.35E-02 1.15E-02 1.02E-04                0.112 L1-10221C-FIGS-104-SS       2.47E-02 3.74E-03 2.08E-03 5.33E-03 4.88E-06                0.036 L1-10221C-FIGS-105-SS       4.52E-02 0.00E+00 7.77E-03 9.73E-03 1.82E-05                0.063 L1-10221C-FIGS-106-SS       2.72E-02 0.00E+00 1.27E-02 5.86E-03 2.97E-05                0.046 L1-10221C-FIGS-107-SS       7.55E-03 2.90E-02 3.83E-03 1.63E-03 8.98E-06                0.042 L1-10221C-FIGS-108-SS       2.21E-02 3.70E-04 3.22E-03 4.76E-03 7.56E-06                0.030 L1-10221C-FIGS-109-SS       7.49E-03 0.00E+00 1.41E-02 1.61E-03 3.32E-05                0.023 L1-10221C-FIGS-110-SS       1.60E-02 2.26E-03 6.91E-03 3.45E-03 1.62E-05                0.029 L1-10221C-FIGS-111-SS 0.00E+00 0.00E+00 9.78E-03 0.00E+00 2.29E-05                      0.010 L1-10221C-FIGS-112-SS       1.26E-02 2.50E-03 2.25E-03 2.70E-03 5.28E-06                0.020 L1-10221C-FIGS-113-SS       2.58E-02 0.00E+00 0.00E+00 5.56E-03 0.00E+00 0.031 L1-10221C-FJGS-001-SS       7.49E-04 1.00E-02 3.53E-03 1.61E-04 8.27E-06                0.014 L1-10221C-FJGS-002-SS       3.90E-02 0.00E+00 2.02E-02 8.41E-03 4.73E-05                0.068 L1-10221C-FJGS-003-SS       1.37E-02 0.00E+00 0.00E+00 2.96E-03 0.00E+00 0.017 L1-10221C-FJGS-004-SS       1.81E-02 6.52E-03 1.38E-02 3.89E-03 3.23E-05                0.042 L1-10221C-FJGS-005-SS       3.90E-03 1.77E-02 0.00E+00 8.39E-04 0.00E+00 0.022 L1-10221C-FJGS-006-SS 0.00E+00 0.00E+00 1.29E-02 0.00E+00 3.02E-05                      0.013
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID                                                                                   OpSOF Co-60      Cs-134         Cs-137        Ni-63         Sr-90 L1-10221C-FJGS-007-SS          3.25E-02 5.94E-03 8.98E-03 7.01E-03 2.11E-05                        0.054 L1-10221C-FJGS-008-SS          3.01E-02 7.85E-04 3.69E-03 6.47E-03 8.66E-06                        0.041 Table 19 - Sum of Fractions for Subsurface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Subsurface Soils MEASUREMENT ID                                                                                   OpSOF Co-60      Cs-134         Cs-137        Ni-63         Sr-90 L1-10221C-FSGS-005-SB 1.42E-02 3.39E-03 2.33E-03 1.15E-02 2.18E-05                                 0.031 L1-10221C-FSGS-013-SB 7.48E-02 3.14E-03 7.51E-02 6.09E-02 7.01E-04                                 0.215 L1-10221C-FIGS-100-SB 0.00E+00 8.80E-03 1.79E-02 0.00E+00 1.68E-04                                 0.027 L1-10221C-FIGS-101-SB 0.00E+00 3.95E-02 1.10E-02 0.00E+00 1.03E-04                                 0.051 Table 20 - Sum of Fractions for QC Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID                                                                                   OpSOF Co-60      Cs-134         Cs-137        Ni-63         Sr-90 L1-10221C-FQGS-012-SS          1.24E-04 4.02E-02 4.19E-02 2.66E-05 9.82E-05                        0.082 L1-10221C-QJGS-001-SS          1.65E-02 0.00E+00 3.47E-03 3.55E-03 8.14E-06                        0.024 L1-10221C-QIGS-110-SS          1.88E-02 1.74E-02 1.56E-02 4.05E-03 3.65E-05                        0.056 Table 21 - Basic Statistical Properties of Systematic Sample Population Mean       Median      Max           Min       Std. Dev. BcDCGL       Avg. SOF  Avg. Dose ROC (pCi/g)     (pCi/g)    (pCi/g)      (pCi/g)      (pCi/g)    (pCi/g)     per ROC    Per ROC Co-60     3.19E-02    2.59E-02   1.05E-01     0.00E+00       0.029      4.26       7.48E-03   1.87E-01 Cs-134    1.69E-02    1.20E-02   5.26E-02     0.00E+00       0.016      6.77       2.49E-03   6.23E-02 Cs-137    7.78E-02 3.65E-02 4.32E-01 0.00E+00                0.120      14.18      5.48E-03   1.37E-01 Ni-63     5.75E+00 4.67E+00 1.89E+01 0.00E+00                5.246     3572.1      1.61E-03   4.02E-02 Sr-90    1.56E-04 7.30E-05 8.64E-04 0.00E+00                0.000      12.09      1.29E-05   3.22E-04 The mean BcSOF for survey unit 10221C is 0.017, which equates to a dose of 0.427 mrem/year TEDE.
The mean of all identified isotopes is less than the Consultation Triggers for Residential and Commercial/Industrial Soil Contamination depicted in Table H.1 of NUREG 1757, Vol. 1, (MOU Table 1). The full table is included in Attachment 3 of this Release Record.
: 8.      QUALITY CONTROL The on-site laboratory processed three (3) split samples, L1-10221C-FQGS-012-SS, L1-10221C-QJGS-001-SS and L1-10221C-QIGS-110-SS, using gamma spectroscopy analysis. The data was evaluated using acceptance criteria specified in ZS-LT-01.
For L1-10221C-FQGS-012-SS, there was not acceptable agreement between field split results when using Cs-137 due to the fact that it is present in the samples at relatively low concentrations.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C However, when using K-40, which is present in the samples at higher concentrations, there was acceptable agreement. No further action was deemed necessary For the remaining samples, there was acceptable agreement between the field split results. Refer to Attachment 5 for data and QC analysis results.
: 9. INVESTIGATIONS AND RESULTS An investigation was performed based on the results of gamma scans performed under an RA on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas 1- meter beyond the ballast gravel. The RA identified two (2) small areas of elevated activity (a map of these areas is included in Attachment 1). One area was less than 100 cm2 with a reading of 4,000 cpm. One (1) surface soil sample was taken at this location: L1-10221C-FIGS-101-SS. Four (4) additional samples were taken in the immediate vicinity (within 0.5 meters): L1-10221C-FIGS-102-SS through L1-10221C-FIGS-105-SS. The second location was a 1-meter by 2-meter area with a maximum reading of 7,000 cpm. A small radioactive particle was captured in this area and one (1) surface soil sample was taken at the location: L1-10221C-FIGS-100-SS. Eight (8) additional samples were taken in the immediate vicinity (within 1.0 meter): L1-10221C-FIGS-106-SS through L1-10221C-FIGS-113-SS. Gamma spectroscopy results revealed five (5) samples with activity levels above MDC for Cs-137 and no samples with activity levels above MDC for Co-60 and Cs-134. Since the OpSOF for the investigation samples were all less than 1.0, with a maximum OpSOF of 0.300, no further action was necessary. The investigation is documented in an Attachment 13 (from ZS- LT-300-001-004), Final Status Survey Investigation. The gamma spectroscopy results are summarized in Table 13, and the OpSOFs summarized in Table 18.
Also included in Table 13 and Table 18 are the results of the eight (8) judgmental surface soil samples that were taken adjacent to the railroad ballast. Maps of the judgmental sample locations are included in Attachment 1.
: 10. REMEDIATION AND RESULTS The small radioactive particle identified in the previous investigation was captured. No other remediation was performed in this survey unit.
: 11. CHANGES FROM THE SURVEY PLAN Three (3) systematic samples were relocated to the closest adjacent suitable location due to the original locations falling on the railroad ballast which is made up of gravel and not soil. The coordinates of the relocated samples are listed in the table below. The map included in Attachment 1 shows the original and relocated sample points.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 22  Relocated Systematic Sample Locations NORTHING             EASTING MEASUREMENT ID (meters)             (meters)
L1-10221C-FSGS-002-SS                641482.36            343575.98 L1-10221C-FSGS-003-SS                641491.28            343558.46 L1-10221C-FSGS-004-SS                641499.50            343573.75
: 12. DATA QUALITY ASSESSMENT The DQO sample design and data were reviewed in accordance with ZionSolutions procedure ZS-LT-300-001-004, Final Status Survey Data Assessment (Reference 16) for completeness and consistency. Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs. The sampling design had adequate power as indicated by the Retrospective Power Curve.
The analytical results of all samples were less than an OpSOF of one when compared to the OpDCGLs.
Although MARSSIM states that the Sign Test need not be performed in the instance that no measurements surpass the DCGL, the test was conducted to demonstrate coherence to the statistical principles of the DQO process. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results clearly demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected. The Sign Test is included in Attachment 4.
The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). All data were considered valid including negative values, zeros, values reported below the MDC, and values with uncertainties greater than two standard deviations. The mean and median values for each ROC were well below the respective OpDCGLs. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs.
The data for Co-60 and Cs-137 are represented graphically through a frequency plot and a quantile plot. All graphical representations are provided in Attachment 6.
: 13. ANOMALIES No anomalies were observed during the performance or analyses of the survey.
: 14. CONCLUSION Survey unit 10221C has met the DQOs of the FSS plan. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved. The EMC for soils was not needed for this survey unit.
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C All identified ROC were used for statistical testing to determine the adequacy of the survey unit for FSS. Evaluation of the data shows that none of the ROC concentration values exceed the OpDCGL or any investigational levels; therefore, in accordance with the LTP Section 5.10, the survey unit meets the release criterion.
The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve showed that adequate power was achieved.
The mean BcSOF, when the analytical results were compared to the BcDCGLs, was 0.017, which results in a dose contribution from soil in survey unit 10221C of 0.427 mrem/year TEDE, based on the average concentration of the ROC in samples used for non-parametric statistical sampling.
The conclusion of this Release Record is that survey unit 10221C is acceptable for unrestricted release.
: 15. REFERENCES
: 1. ZionSolutions procedure ZS-LT-300-001-005, Final Status Survey Data Reporting
: 2. Zion Station Restoration Project License Termination Plan
: 3. ZionSolutions procedure ZS-LT-300-001-001, Final Status Survey Package Development
: 4. NUREG-1575, Multi-Agency Radiation Survey and Site Investigation Manual
: 5. ZionSolutions procedure ZS-LT-300-001-002, Survey Unit Classification
: 6. Zion Station Historical Site Assessment
: 7. ZionSolutions TSD 11-001, Technical Support Document for Potential Radionuclides of Concern During the Decommissioning of the Zion Station
: 8. ZionSolutions TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms
: 9. ZionSolutions TSD 14-011, Soil Area Factors
: 10. ZionSolutions TSD 17-004, Operational Derived Concentration Guideline Levels for Final Status Survey
: 11. ZionSolutions TSD 11-004, Ludlum Model 44-10 Detector Sensitivity
: 12. ZionSolutions procedure ZS-LT-01, Quality Assurance Project Plan (for Characterization and FSS)
: 13. ZionSolutions procedure ZS-LT-300-001-003, Isolation and Control for Final Status Survey
: 14. ZionSolutions procedure ZS-RP-108-004-011, Operation of the Ludlum Model 2350-1 Data Logger
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
: 15. ZionSolutions TSD 13-004, Examination of Cs-137 Global Fallout In Soils At Zion Station
: 16. ZionSolutions procedure ZS-LT-300-001-004, Final Status Survey Data Assessment
: 16. ATTACHMENTS
: 1. Attachment 1 - Figures and Map
: 2. Attachment 2 - Scan Data
: 3. Attachment 3 - Consultation Triggers for Residential and Commercial/Industrial Soil Contamination
: 4. Attachment 4 - Sign Test
: 5. Attachment 5 - QC Sample Assessment
: 6. Attachment 6 - Graphical Presentations
: 7. Attachment 7 - Sample Analytical Reports
: 8. Attachment 8 - Eberline Analytical Reports
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ATTACHMENT 1 FIGURES AND MAP
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Final Status Survey Boundaries and Systematic Sample Points
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Final Status Survey Boundaries with Relocated Systematic Sample Points
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Elevated Areas Discovered during Radiological Assessment
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Judgmental Sample Points taken Adjacent to Railroad Ballast
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FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Final Status Survey Scan Rows
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ATTACHMENT 2 SCAN DATA
[43]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR363311  304718 10221C  GS001     7/24/2019 13:17  2090     1668     2285    No 44-10   PR363311  304718 10221C  GS001     7/24/2019 13:19  1975     1668     2285    No 44-10   PR363311  304718 10221C  GS001     7/24/2019 13:21  1917     1668     2285    No 44-10   PR363311  304718 10221C  GS001     7/24/2019 13:23  1955     1668     2285    No 44-10   PR363311  304718 10221C  GS002     7/24/2019 13:25  2035     1668     2285    No 44-10   PR363311  304718 10221C  GS002     7/24/2019 13:27  2178     1668     2285    No 44-10   PR363311  304718 10221C  GS002     7/24/2019 13:29  2063     1668     2285    No 44-10   PR363311  304718 10221C  GS003     7/24/2019 13:33  2198     1668     2285    No 44-10   PR363311  304718 10221C  GS003     7/24/2019 13:35  1967     1668     2285    No 44-10   PR363311  304718 10221C  GS003     7/24/2019 13:37  2022     1668     2285    No 44-10   PR363311  304718 10221C  GS003     7/24/2019 13:39  1979     1668     2285    No 44-10   PR363311  304718 10221C  GS004     7/24/2019 13:41  1931     1668     2285    No 44-10   PR363311  304718 10221C  GS004     7/24/2019 13:43  1996     1668     2285    No 44-10   PR363311  304718 10221C  GS004     7/24/2019 13:45  1909     1668     2285    No 44-10   PR363311  304718 10221C  GS004     7/24/2019 13:47  1871     1668     2285    No 44-10   PR363311  304718 10221C  GS005     7/24/2019 13:49  1704     1668     2285    No 44-10   PR363311  304718 10221C  GS005     7/24/2019 13:51  1815     1668     2285    No 44-10   PR363311  304718 10221C  GS005     7/24/2019 13:53  1800     1668     2285    No 44-10   PR363311  304718 10221C  GS005     7/24/2019 13:55  1692     1668     2285    No 44-10   PR363311  304718 10221C  GS006     7/24/2019 14:13  1767     1668     2285    No 44-10   PR363311  304718 10221C  GS006     7/24/2019 14:15  1740     1668     2285    No 44-10   PR363311  304718 10221C  GS006     7/24/2019 14:17  1745     1668     2285    No 44-10   PR363311  304718 10221C  GS006     7/24/2019 14:19  1760     1668     2285    No 44-10   PR363311  304718 10221C  GS007     7/24/2019 14:21  1744     1668     2285    No 44-10   PR363311  304718 10221C  GS007     7/24/2019 14:23  1840     1668     2285    No 44-10   PR363311  304718 10221C  GS007     7/24/2019 14:25  1685     1668     2285    No 44-10   PR363311  304718 10221C  GS007     7/24/2019 14:27  1712     1668     2285    No 44-10   PR363311  304718 10221C  GS008     7/24/2019 14:29  1706     1668     2285    No 44-10   PR363311  304718 10221C  GS008     7/24/2019 14:31  1939     1668     2285    No 44-10   PR363311  304718 10221C  GS008     7/24/2019 14:33  1839     1668     2285    No 44-10   PR363311  304718 10221C  GS008     7/24/2019 14:35  1716     1668     2285    No 44-10   PR321902  304711 10221C  GS033     7/24/2019 12:56  2574     2382     3120    No 44-10   PR321902  304711 10221C  GS033     7/24/2019 12:58  2481     2382     3120    No 44-10   PR321902  304711 10221C  GS033     7/24/2019 13:00  2113     2382     3120    No 44-10   PR321902  304711 10221C  GS033     7/24/2019 13:03  2467     2382     3120    No
[44]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR321902  304711 10221C  GS034     7/24/2019 13:06  2039     2382     3120    No 44-10   PR321902  304711 10221C  GS034     7/24/2019 13:09  2380     2382     3120    No 44-10   PR321902  304711 10221C  GS034     7/24/2019 13:12  2620     2382     3120    No 44-10   PR321902  304711 10221C  GS034     7/24/2019 13:14  2765     2382     3120    No 44-10   PR321902  304711 10221C  GS035     7/24/2019 13:17  2813     2382     3120    No 44-10   PR321902  304711 10221C  GS035     7/24/2019 13:19  2544     2382     3120    No 44-10   PR321902  304711 10221C  GS035     7/24/2019 13:21  2215     2382     3120    No 44-10   PR321902  304711 10221C  GS035     7/24/2019 13:23  2464     2382     3120    No 44-10   PR321902  304711 10221C  GS036     7/24/2019 13:26  2127     2382     3120    No 44-10   PR321902  304711 10221C  GS036     7/24/2019 13:29  2674     2382     3120    No 44-10   PR321902  304711 10221C  GS036     7/24/2019 13:31  2718     2382     3120    No 44-10   PR321902  304711 10221C  GS036     7/24/2019 13:35  2565     2382     3120    No 44-10   PR321902  304711 10221C  GS037     7/24/2019 13:38  3011     2382     3120    No 44-10   PR321902  304711 10221C  GS037     7/24/2019 13:40  2804     2382     3120    No 44-10   PR321902  304711 10221C  GS037     7/24/2019 13:42  2775     2382     3120    No 44-10   PR321902  304711 10221C  GS037     7/24/2019 13:45  2405     2382     3120    No 44-10   PR321902  304711 10221C  GS038     7/24/2019 13:48  2420     2382     3120    No 44-10   PR321902  304711 10221C  GS038     7/24/2019 13:50  2642     2382     3120    No 44-10   PR321902  304711 10221C  GS038     7/24/2019 13:52  2881     2382     3120    No 44-10   PR321902  304711 10221C  GS038     7/24/2019 13:57  3109     2382     3120    No 44-10   PR321902  304711 10221C  GS039     7/24/2019 14:02  2928     2382     3120    No 44-10   PR321902  304711 10221C  GS039     7/24/2019 14:05  2889     2382     3120    No 44-10   PR321902  304711 10221C  GS039     7/24/2019 14:08  2808     2382     3120    No 44-10   PR321902  304711 10221C  GS039     7/24/2019 14:10  2686     2382     3120    No 44-10   PR321902  304711 10221C  GS040     7/24/2019 14:13  2944     2382     3120    No 44-10   PR321902  304711 10221C  GS040     7/24/2019 14:16  3057     2382     3120    No 44-10   PR321902  304711 10221C  GS040     7/24/2019 14:18  2933     2382     3120    No 44-10   PR321902  304711 10221C  GS040     7/24/2019 14:21  2972     2382     3120    No 44-10   PR375273  304730 10221C  GS009     7/24/2019 12:50  1875     1633     2244    No 44-10   PR375273  304730 10221C  GS009     7/24/2019 12:52  1689     1633     2244    No 44-10   PR375273  304730 10221C  GS009     7/24/2019 12:54  1658     1633     2244    No 44-10   PR375273  304730 10221C  GS009     7/24/2019 13:03  1693     1633     2244    No 44-10   PR375273  304730 10221C  GS010     7/24/2019 13:05  1680     1633     2244    No 44-10   PR375273  304730 10221C  GS010     7/24/2019 13:07  1679     1633     2244    No 44-10   PR375273  304730 10221C  GS010     7/24/2019 13:09  1772     1633     2244    No 44-10   PR375273  304730 10221C  GS010     7/24/2019 13:11  1806     1633     2244    No
[45]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR375273  304730 10221C  GS011     7/24/2019 13:13  1943     1633     2244    No 44-10   PR375273  304730 10221C  GS011     7/24/2019 13:15  1938     1633     2244    No 44-10   PR375273  304730 10221C  GS011     7/24/2019 13:17  1788     1633     2244    No 44-10   PR375273  304730 10221C  GS011     7/24/2019 13:19  1754     1633     2244    No 44-10   PR375273  304730 10221C  GS012     7/24/2019 13:21  1772     1633     2244    No 44-10   PR375273  304730 10221C  GS012     7/24/2019 13:23  2049     1633     2244    No 44-10   PR375273  304730 10221C  GS012     7/24/2019 13:25  1763     1633     2244    No 44-10   PR375273  304730 10221C  GS012     7/24/2019 13:27  1830     1633     2244    No 44-10   PR375273  304730 10221C  GS013     7/24/2019 13:29  1753     1633     2244    No 44-10   PR375273  304730 10221C  GS013     7/24/2019 13:31  1946     1633     2244    No 44-10   PR375273  304730 10221C  GS013     7/24/2019 13:33  1946     1633     2244    No 44-10   PR375273  304730 10221C  GS013     7/24/2019 13:35  1871     1633     2244    No 44-10   PR375273  304730 10221C  GS014     7/24/2019 13:37  1911     1633     2244    No 44-10   PR375273  304730 10221C  GS014     7/24/2019 13:39  1984     1633     2244    No 44-10   PR375273  304730 10221C  GS014     7/24/2019 13:41  1741     1633     2244    No 44-10   PR375273  304730 10221C  GS014     7/24/2019 13:43  1775     1633     2244    No 44-10   PR375273  304730 10221C  GS015     7/24/2019 13:45  1850     1633     2244    No 44-10   PR375273  304730 10221C  GS015     7/24/2019 13:47  1972     1633     2244    No 44-10   PR375273  304730 10221C  GS015     7/24/2019 13:52  1864     1633     2244    No 44-10   PR375273  304730 10221C  GS015     7/24/2019 14:03  1885     1633     2244    No 44-10   PR375273  304730 10221C  GS016     7/24/2019 14:06  1674     1633     2244    No 44-10   PR375273  304730 10221C  GS016     7/24/2019 14:08  1669     1633     2244    No 44-10   PR375273  304730 10221C  GS016     7/24/2019 14:10  1728     1633     2244    No 44-10   PR375273  304730 10221C  GS016     7/24/2019 14:12  1923     1633     2244    No 44-10   PR308037  266657 10221C  GS025     7/24/2019 12:56  2359     2082     2771    No 44-10   PR308037  266657 10221C  GS025     7/24/2019 13:00  2163     2082     2771    No 44-10   PR308037  266657 10221C  GS025     7/24/2019 13:02  1980     2082     2771    No 44-10   PR308037  266657 10221C  GS025     7/24/2019 13:04  1925     2082     2771    No 44-10   PR308037  266657 10221C  GS026     7/24/2019 13:09  2082     2082     2771    No 44-10   PR308037  266657 10221C  GS026     7/24/2019 13:12  2181     2082     2771    No 44-10   PR308037  266657 10221C  GS026     7/24/2019 13:14  2318     2082     2771    No 44-10   PR308037  266657 10221C  GS026     7/24/2019 13:16  2472     2082     2771    No 44-10   PR308037  266657 10221C  GS027     7/24/2019 13:18  2277     2082     2771    No 44-10   PR308037  266657 10221C  GS027     7/24/2019 13:20  2349     2082     2771    No 44-10   PR308037  266657 10221C  GS027     7/24/2019 13:22  2031     2082     2771    No 44-10   PR308037  266657 10221C  GS027     7/24/2019 13:25  2055     2082     2771    No
[46]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR308037  266657 10221C  GS028     7/24/2019 13:29  2011     2082     2771    No 44-10   PR308037  266657 10221C  GS028     7/24/2019 13:32  2134     2082     2771    No 44-10   PR308037  266657 10221C  GS028     7/24/2019 13:35  2244     2082     2771    No 44-10   PR308037  266657 10221C  GS028     7/24/2019 13:37  2261     2082     2771    No 44-10   PR308037  266657 10221C  GS029     7/24/2019 13:40  2227     2082     2771    No 44-10   PR308037  266657 10221C  GS029     7/24/2019 13:42  2196     2082     2771    No 44-10   PR308037  266657 10221C  GS029     7/24/2019 13:44  2055     2082     2771    No 44-10   PR308037  266657 10221C  GS029     7/24/2019 13:47  1926     2082     2771    No 44-10   PR308037  266657 10221C  GS030     7/24/2019 13:51  2103     2082     2771    No 44-10   PR308037  266657 10221C  GS030     7/24/2019 13:54  2158     2082     2771    No 44-10   PR308037  266657 10221C  GS030     7/24/2019 13:56  2282     2082     2771    No 44-10   PR308037  266657 10221C  GS030     7/24/2019 13:59  2426     2082     2771    No 44-10   PR308037  266657 10221C  GS031     7/24/2019 14:03  2554     2082     2771    No 44-10   PR308037  266657 10221C  GS031     7/24/2019 14:06  2336     2082     2771    No 44-10   PR308037  266657 10221C  GS031     7/24/2019 14:08  2118     2082     2771    No 44-10   PR308037  266657 10221C  GS031     7/24/2019 14:11  2051     2082     2771    No 44-10   PR308037  266657 10221C  GS032     7/24/2019 14:13  1998     2082     2771    No 44-10   PR308037  266657 10221C  GS032     7/24/2019 14:16  2304     2082     2771    No 44-10   PR308037  266657 10221C  GS032     7/24/2019 14:18  2520     2082     2771    No 44-10   PR316938  293136 10221C  GS049     7/24/2001 13:49  3019     2779     3576    No 44-10   PR316938  293136 10221C  GS049     7/24/2001 13:52  3080     2779     3576    No 44-10   PR316938  293136 10221C  GS049     7/24/2001 13:54  3320     2779     3576    No 44-10   PR316938  293136 10221C  GS049     7/24/2001 13:56  3359     2779     3576    No 44-10   PR316938  293136 10221C  GS050     7/24/2001 14:00  2986     2779     3576    No 44-10   PR316938  293136 10221C  GS050     7/24/2001 14:02  3076     2779     3576    No 44-10   PR316938  293136 10221C  GS050     7/24/2001 14:07  3060     2779     3576    No 44-10   PR316938  293136 10221C  GS050     7/24/2001 14:09  3055     2779     3576    No 44-10   PR316938  293136 10221C  GS051     7/24/2001 14:13  2989     2779     3576    No 44-10   PR316938  293136 10221C  GS051     7/24/2001 14:16  3069     2779     3576    No 44-10   PR316938  293136 10221C  GS051     7/24/2001 14:18  3162     2779     3576    No 44-10   PR316938  293136 10221C  GS051     7/24/2001 14:21  3544     2779     3576    No 44-10   PR316938  293136 10221C  GS052     7/24/2001 14:26  2945     2779     3576    No 44-10   PR316938  293136 10221C  GS052     7/24/2001 14:29  3251     2779     3576    No 44-10   PR316938  293136 10221C  GS052     7/24/2001 14:31  3168     2779     3576    No 44-10   PR316938  293136 10221C  GS052     7/24/2001 14:33  3316     2779     3576    No 44-10   PR316938  293136 10221C  GS053     7/24/2001 14:37  2976     2779     3576    No
[47]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR316938  293136 10221C  GS053     7/24/2001 14:39  3264     2779     3576    No 44-10   PR316938  293136 10221C  GS053     7/24/2001 14:41  3174     2779     3576    No 44-10   PR316938  293136 10221C  GS053     7/24/2001 14:43  3337     2779     3576    No 44-10   PR316938  293136 10221C  GS054     7/24/2001 14:47  3035     2779     3576    No 44-10   PR316938  293136 10221C  GS054     7/24/2001 14:50  2987     2779     3576    No 44-10   PR316938  293136 10221C  GS054     7/24/2001 14:52  3054     2779     3576    No 44-10   PR316938  293136 10221C  GS054     7/24/2001 14:54  2804     2779     3576    No 44-10   PR316938  293136 10221C  GS055     7/24/2001 14:58  3037     2779     3576    No 44-10   PR316938  293136 10221C  GS055     7/24/2001 15:00  2983     2779     3576    No 44-10   PR316938  293136 10221C  GS055     7/24/2001 15:02  3202     2779     3576    No 44-10   PR316938  293136 10221C  GS055     7/24/2001 15:05  3188     2779     3576    No 44-10   PR316938  293136 10221C  GS056     7/24/2001 15:08  2981     2779     3576    No 44-10   PR316938  293136 10221C  GS056     7/24/2001 15:10  2959     2779     3576    No 44-10   PR316938  293136 10221C  GS056     7/24/2001 15:12  3198     2779     3576    No 44-10   PR316938  293136 10221C  GS056     7/24/2001 15:15  2875     2779     3576    No 44-10   PR363452  304726 10221C  GS041     7/24/2019 13:49  3021     2770     3566    No 44-10   PR363452  304726 10221C  GS041     7/24/2019 13:53  2951     2770     3566    No 44-10   PR363452  304726 10221C  GS041     7/24/2019 13:56  2866     2770     3566    No 44-10   PR363452  304726 10221C  GS041     7/24/2019 13:59  3103     2770     3566    No 44-10   PR363452  304726 10221C  GS042     7/24/2019 14:02  2794     2770     3566    No 44-10   PR363452  304726 10221C  GS042     7/24/2019 14:04  3064     2770     3566    No 44-10   PR363452  304726 10221C  GS042     7/24/2019 14:08  3275     2770     3566    No 44-10   PR363452  304726 10221C  GS042     7/24/2019 14:10  3061     2770     3566    No 44-10   PR363452  304726 10221C  GS043     7/24/2019 14:12  3023     2770     3566    No 44-10   PR363452  304726 10221C  GS043     7/24/2019 14:14  3067     2770     3566    No 44-10   PR363452  304726 10221C  GS043     7/24/2019 14:16  3027     2770     3566    No 44-10   PR363452  304726 10221C  GS043     7/24/2019 14:18  2809     2770     3566    No 44-10   PR363452  304726 10221C  GS044     7/24/2019 14:21  2908     2770     3566    No 44-10   PR363452  304726 10221C  GS044     7/24/2019 14:23  3050     2770     3566    No 44-10   PR363452  304726 10221C  GS044     7/24/2019 14:25  3252     2770     3566    No 44-10   PR363452  304726 10221C  GS044     7/24/2019 14:27  2983     2770     3566    No 44-10   PR363452  304726 10221C  GS045     7/24/2019 14:29  3007     2770     3566    No 44-10   PR363452  304726 10221C  GS045     7/24/2019 14:31  3063     2770     3566    No 44-10   PR363452  304726 10221C  GS045     7/24/2019 14:33  2866     2770     3566    No 44-10   PR363452  304726 10221C  GS045     7/24/2019 14:35  2944     2770     3566    No 44-10   PR363452  304726 10221C  GS046     7/24/2019 14:37  2995     2770     3566    No
[48]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR363452  304726 10221C  GS046     7/24/2019 14:39  3011     2770     3566    No 44-10   PR363452  304726 10221C  GS046     7/24/2019 14:41  3063     2770     3566    No 44-10   PR363452  304726 10221C  GS046     7/24/2019 14:43  2831     2770     3566    No 44-10   PR363452  304726 10221C  GS047     7/24/2019 14:45  2970     2770     3566    No 44-10   PR363452  304726 10221C  GS047     7/24/2019 14:47  3109     2770     3566    No 44-10   PR363452  304726 10221C  GS047     7/24/2019 14:49  2881     2770     3566    No 44-10   PR363452  304726 10221C  GS047     7/24/2019 14:51  2854     2770     3566    No 44-10   PR363452  304726 10221C  GS048     7/24/2019 14:53  2851     2770     3566    No 44-10   PR363452  304726 10221C  GS048     7/24/2019 14:55  3094     2770     3566    No 44-10   PR363452  304726 10221C  GS048     7/24/2019 14:57  3188     2770     3566    No 44-10   PR363452  304726 10221C  GS048     7/24/2019 14:59  2982     2770     3566    No 44-10   PR308037  266657 10221C  GS032      7/25/2019 7:12  2616     2353     3087    No 44-10   PR363311  304718 10221C  GS002     7/25/2019 13:06  2407     1801     2443    No 44-10   PR316938  293136 10221C  GS057      7/25/2001 8:10  3002     2562     3327    No 44-10   PR316938  293136 10221C  GS057      7/25/2001 8:13  3044     2562     3327    No 44-10   PR316938  293136 10221C  GS057      7/25/2001 8:15  2922     2562     3327    No 44-10   PR316938  293136 10221C  GS057      7/25/2001 8:17  3059     2562     3327    No 44-10   PR316938  293136 10221C  GS058      7/25/2001 8:20  2985     2562     3327    No 44-10   PR316938  293136 10221C  GS058      7/25/2001 8:23  3030     2562     3327    No 44-10   PR316938  293136 10221C  GS058      7/25/2001 8:25  2826     2562     3327    No 44-10   PR316938  293136 10221C  GS058      7/25/2001 8:27  3276     2562     3327    No 44-10   PR316938  293136 10221C  GS059      7/25/2001 8:32  2803     2562     3327    No 44-10   PR316938  293136 10221C  GS059      7/25/2001 8:34  2918     2562     3327    No 44-10   PR316938  293136 10221C  GS059      7/25/2001 8:36  2982     2562     3327    No 44-10   PR316938  293136 10221C  GS059      7/25/2001 8:38  3128     2562     3327    No 44-10   PR316938  293136 10221C  GS060      7/25/2001 8:42  2653     2562     3327    No 44-10   PR316938  293136 10221C  GS060      7/25/2001 8:45  2886     2562     3327    No 44-10   PR316938  293136 10221C  GS060      7/25/2001 8:47  2917     2562     3327    No 44-10   PR316938  293136 10221C  GS060      7/25/2001 8:49  3000     2562     3327    No 44-10   PR363452  304726 10221C  GS061      7/25/2019 8:06  3024     2680     3463    No 44-10   PR363452  304726 10221C  GS061      7/25/2019 8:09  2858     2680     3463    No 44-10   PR363452  304726 10221C  GS061      7/25/2019 8:11  2752     2680     3463    No 44-10   PR363452  304726 10221C  GS062      7/25/2019 8:14  2732     2680     3463    No 44-10   PR363452  304726 10221C  GS062      7/25/2019 8:16  2890     2680     3463    No 44-10   PR363452  304726 10221C  GS062      7/25/2019 8:18  3053     2680     3463    No 44-10   PR363452  304726 10221C  GS063      7/25/2019 8:20  3188     2680     3463    No
[49]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR363452  304726 10221C  GS063      7/25/2019 8:22  2950     2680     3463    No 44-10   PR363452  304726 10221C  GS063      7/25/2019 8:24  2816     2680     3463    No 44-10   PR363452  304726 10221C  GS064      7/25/2019 8:27  2971     2680     3463    No 44-10   PR363452  304726 10221C  GS064      7/25/2019 8:29  2810     2680     3463    No 44-10   PR363452  304726 10221C  GS065      7/25/2019 8:32  2799     2680     3463    No 44-10   PR363452  304726 10221C  GS065      7/25/2019 8:34  2788     2680     3463    No 44-10   PR363452  304726 10221C  GS066      7/25/2019 8:37  2729     2680     3463    No 44-10   PR363452  304726 10221C  GS067      7/25/2019 8:40  2929     2680     3463    No 44-10   PR363452  304726 10221C  GS068      7/25/2019 8:44  2712     2680     3463    No 44-10   PR372143  304712 10221C  GS017      9/17/2019 9:12  1905     1812     2456    No 44-10   PR372143  304712 10221C  GS017      9/17/2019 9:14  1906     1812     2456    No 44-10   PR372143  304712 10221C  GS017      9/17/2019 9:16  1927     1812     2456    No 44-10   PR372143  304712 10221C  GS017      9/17/2019 9:18  2070     1812     2456    No 44-10   PR372143  304712 10221C  GS018      9/17/2019 9:20  2345     1812     2456    No 44-10   PR372143  304712 10221C  GS018      9/17/2019 9:23  2091     1812     2456    No 44-10   PR372143  304712 10221C  GS018      9/17/2019 9:25  1913     1812     2456    No 44-10   PR372143  304712 10221C  GS018      9/17/2019 9:27  1861     1812     2456    No 44-10   PR372143  304712 10221C  GS019      9/17/2019 9:29  1946     1812     2456    No 44-10   PR372143  304712 10221C  GS019      9/17/2019 9:31  1985     1812     2456    No 44-10   PR372143  304712 10221C  GS019      9/17/2019 9:33  2263     1812     2456    No 44-10   PR372143  304712 10221C  GS019      9/17/2019 9:36  2292     1812     2456    No 44-10   PR372143  304712 10221C  GS020      9/17/2019 9:38  2197     1812     2456    No 44-10   PR372143  304712 10221C  GS020      9/17/2019 9:40  2156     1812     2456    No 44-10   PR372143  304712 10221C  GS020      9/17/2019 9:42  2020     1812     2456    No 44-10   PR372143  304712 10221C  GS020      9/17/2019 9:44  1873     1812     2456    No 44-10   PR372143  304712 10221C  GS021      9/17/2019 9:47  1966     1812     2456    No 44-10   PR372143  304712 10221C  GS021      9/17/2019 9:49  1987     1812     2456    No 44-10   PR372143  304712 10221C  GS021      9/17/2019 9:51  2353     1812     2456    No 44-10   PR372143  304712 10221C  GS021      9/17/2019 9:53  2408     1812     2456    No 44-10   PR372143  304712 10221C  GS022      9/17/2019 9:56  2246     1812     2456    No 44-10   PR372143  304712 10221C  GS022      9/17/2019 9:58  2180     1812     2456    No 44-10   PR372143  304712 10221C  GS022     9/17/2019 10:00  1976     1812     2456    No 44-10   PR372143  304712 10221C  GS022     9/17/2019 10:02  1931     1812     2456    No 44-10   PR372143  304712 10221C  GS023     9/17/2019 10:04  1834     1812     2456    No 44-10   PR372143  304712 10221C  GS023     9/17/2019 10:07  2158     1812     2456    No 44-10   PR372143  304712 10221C  GS023     9/17/2019 10:09  2180     1812     2456    No
[50]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg     Action Detector  Detector M2350- Survey                            Logged                    Scan Location      Date/Time           Background Level Type       ID      1 ID   Unit                             Result                   Alarms (cpm)    (cpm)    (cpm) 44-10   PR372143  304712 10221C  GS023     9/17/2019 10:11  2340     1812     2456    No 44-10   PR372143  304712 10221C  GS024     9/17/2019 10:13  2258     1812     2456    No 44-10   PR372143  304712 10221C  GS024     9/17/2019 10:15  2099     1812     2456    No 44-10   PR372143  304712 10221C  GS024     9/17/2019 10:17  2168     1812     2456    No 44-10   PR372143  304712 10221C  GS024     9/17/2019 10:19  1946     1812     2456    No
[51]

ATTACHMENT 3 CONSULTATION TRIGGERS FOR RESIDENTIAL AND COMMERCIAL/INDUSTRIAL SOIL CONTAMINATION
[52]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
[53]

ATTACHMENT 4 SIGN TEST
[54]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
[55]

ATTACHMENT 5 QC SAMPLE ASSESSMENT
[56]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
[57]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
[58]

ATTACHMENT 6 GRAPHICAL PRESENTATIONS
[59]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Posting Plot
[60]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C QUANTILE PLOT FOR Co-60 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 3.19E-02 pCi/g Quantile Plot For Co-60 1.20E-01 1.00E-01 Concentration (pCi/g) 8.00E-02 6.00E-02 4.00E-02 2.00E-02 0.00E+00 0%       20%          40%             60%   80%   100%
Percentage
[61]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C QUANTILE PLOT FOR Cs-137 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 7.78E-02 pCi/g Quantile Plot For Cs-137 5.00E-01 4.50E-01 4.00E-01 Concentration (pCi/g) 3.50E-01 3.00E-01 2.50E-01 2.00E-01 1.50E-01 1.00E-01 5.00E-02 0.00E+00 0%       20%          40%            60%   80%   100%
Percentage
[62]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C HISTOGRAM FOR Co-60 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 3.19E-02 pCi/g Median: 2.59E-02 pCi/g ST DEV:      0.029 Skew:     1.694 Frequency Plot For Co-60 10 9                   8 8
7 Frequency 6      5 5
4 3                               2                                2 2
1                                          0          0 0
1.75E-02     3.50E-02    5.25E-02   7.00E-02   8.75E-02   1.05E-01 Upper End Value (pCi/g)
Observation Observation Upper Value Frequency       %
1.75E-02         5         29%
3.50E-02         8         47%
5.25E-02         2         12%
7.00E-02         0          0%
8.75E-02         0          0%
1.05E-01         2         12%
TOTAL          17        100%
[63]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C HISTOGRAM FOR Cs-137 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 7.78E-02 pCi/g Median: 3.65E-02 pCi/g ST DEV:      0.120 Skew:     2.305 Frequency Plot For Cs-137 14     12 12 10 Frequency 8
6 4                   3 2                                                         1          1 0           0 0
7.20E-02     1.44E-01     2.16E-01   2.88E-01      3.60E-01   4.32E-01 Upper End Value (pCi/g)
Observation Observation Upper Value Frequency       %
7.20E-02       12         71%
1.44E-01        3         18%
2.16E-01        0          0%
2.88E-01        0          0%
3.60E-01        1          6%
4.32E-01        1          6%
TOTAL         17        100%
[64]

FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Prospective and Retrospective Power Curves for Survey Unit 10221C
[65]

ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS
[66]

6/12/2019 12:23:23PM Page 1 of 6 Analysis Report for    12-Jun-19-10014 L1-10221C-FSGS-001SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10014 Sample Description                           : L1-10221C-FSGS-001SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.582E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:15:00AM Acquisition Started                          : 6/12/2019 12:08:14PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77295 Fill Height                                  : 1581.63 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:23:16PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[67]

6/12/2019   12:23:23PM         Page 2 of 6 Analysis Report for    12-Jun-19-10014 L1-10221C-FSGS-001SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.60               472 - 480             477.38          4.91E+01               15.30      8.59E+01           0.83 2       352.00               699 - 708             703.94          6.39E+01               11.58      3.11E+01           1.45 3       609.26             1212 - 1223           1218.09           6.68E+01                9.50      9.16E+00           1.60 4      1461.04             2915 - 2928           2922.14           1.49E+02               12.97      7.00E+00           1.84 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              2.78E+00              2.70E-01 Bi-211                   0.87           351.07
* 13.02              3.80E-01              7.55E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              6.85E-02              2.20E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.64E-01              2.54E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83 1280.98                    1.43                                               [68]

6/12/2019   12:23:23PM         Page 3 of 6 Analysis Report for    12-Jun-19-10014 L1-10221C-FSGS-001SS Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Bi-214                   1.00        1377.67                     3.99 1385.31                     0.79 1401.52                     1.33 1407.99                     2.39 1509.21                     2.13 1661.27                     1.05 1729.59                     2.88 1764.49                   15.30 1847.43                     2.03 2118.51                     1.16 Pb-214                   1.00          241.99                    7.25 295.22                  18.42 351.93
* 35.60              1.39E-01              2.76E-02 785.96                    1.06
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
K-40                                0.992                     2.78E+00                2.70E-01
      ?       Bi-211                              0.871                     3.80E-01                7.55E-02 Pb-212                              1.000                     6.85E-02                2.20E-02 Bi-214                              1.000                     1.64E-01                2.54E-02
      ?       Pb-214                              1.000                     1.39E-01                2.76E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[69]

6/12/2019  12:23:23PM       Page 4 of 6 Analysis Report for    12-Jun-19-10014 L1-10221C-FSGS-001SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:23:16PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.30E-02          5.00E-02        5.00E-02 BE-7            477.60              10.44       1.67E-01          3.28E-01        3.28E-01
+         K-40          1460.82
* 10.66       2.78E+00          3.31E-01        3.31E-01 Mn-54           834.85              99.98       5.17E-03          3.70E-02        3.70E-02 Co-60         1173.23               99.85       5.95E-03          3.87E-02        3.98E-02 1332.49               99.98       1.95E-02                          3.87E-02 Nb-94           702.65              99.81       2.69E-03          2.66E-02        2.93E-02 871.09              99.89       2.12E-03                          2.66E-02 Ag-108m          79.13                6.60    -5.35E-02           2.88E-02        9.13E-01 433.94              90.50       3.75E-03                          2.88E-02 614.28              89.80     -2.46E-02                           4.21E-02 722.94              90.80     -1.83E-02                           3.12E-02 Sb-125          176.31                6.84      5.57E-02          9.11E-02        4.22E-01 380.45                1.52      1.10E-01                          1.75E+00 427.87              29.60     -3.28E-02                           9.11E-02 463.36              10.49       4.71E-02                          2.86E-01 600.60              17.65     -9.94E-02                           1.53E-01 606.71                4.98    -2.05E-01                           1.04E+00 635.95              11.22       1.41E-02                          2.55E-01            [70]

6/12/2019  12:23:23PM Page 5 of 6 Analysis Report for 12-Jun-19-10014 L1-10221C-FSGS-001SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.54E-01      9.11E-02        1.76E+00 Ba-133        79.61            2.65   -2.55E-01      5.63E-02        2.16E+00 81.00           32.90   -1.27E-01                      1.52E-01 276.40            7.16    1.04E-01                      4.00E-01 302.85           18.34    4.68E-02                      1.53E-01 356.01           62.05   -2.35E-02                      5.63E-02 383.85            8.94    3.93E-02                      3.13E-01 Cs-134       475.36            1.48    1.28E+00      3.88E-02        2.26E+00 563.25            8.34   -3.85E-02                      3.61E-01 569.33           15.37    3.13E-02                      1.73E-01 604.72           97.62   -1.42E-02                      4.57E-02 795.86           85.46    1.05E-02                      3.88E-02 801.95            8.69    4.13E-02                      4.07E-01 1038.61             0.99    1.85E-01                      3.81E+00 1167.97             1.79   -1.27E-01                      2.05E+00 1365.19             3.02    2.71E-01                      9.76E-01 Cs-137       661.66           85.10    1.71E-02      4.11E-02        4.11E-02 Eu-152       121.78           28.67   -3.07E-02      9.76E-02        9.76E-02 244.70            7.61    4.31E-02                      3.95E-01 295.94            0.45    3.06E+00                      6.90E+00 344.28           26.60   -1.08E-04                      1.15E-01 367.79            0.86    7.47E-01                      3.48E+00 411.12            2.24    1.60E-01                      1.16E+00 443.96            2.83    1.34E-01                      9.90E-01 488.68            0.42    3.96E-02                      6.91E+00 563.99            0.49   -3.93E-01                      6.03E+00 586.26            0.46    7.77E+00                      8.73E+00 678.62            0.47    3.25E+00                      6.96E+00 688.67            0.86    7.52E-01                      3.20E+00 719.35            0.28   -2.34E+00                      9.87E+00 778.90           12.96    6.84E-02                      2.62E-01 810.45            0.32    6.77E+00                      1.28E+01 867.37            4.26   -1.09E-01                      6.89E-01 919.33            0.43   -2.78E+00                      9.36E+00 964.08           14.65   -4.93E-02                      2.67E-01 1085.87            10.24    2.43E-01                      3.95E-01 1089.74             1.73   -4.48E-01                      2.02E+00 1112.07            13.69   -5.26E-02                      2.87E-01 1212.95             1.43   -4.29E-02                      3.29E+00 1249.94             0.19   -2.95E+00                      2.02E+01 1299.14             1.63   -4.87E-02                      2.41E+00 1408.01            21.07   -2.20E-02                      1.25E-01 1457.64             0.50   -2.17E+00                      2.50E+01 1528.10             0.28   -3.28E+00                      7.04E+00 Eu-154       123.07           40.40   -3.92E-02      6.79E-02        6.79E-02 247.93            6.89   -1.89E-01                      3.50E-01 591.76            4.95    2.05E-01                      6.75E-01 692.42            1.78    5.14E-02                      1.63E+00 723.30           20.06   -2.16E-03                      1.55E-01 756.80            4.52   -1.60E-01                      6.30E-01 873.18           12.08    9.59E-02                      2.36E-01
[71]

6/12/2019  12:23:23PM Page 6 of 6 Analysis Report for     12-Jun-19-10014 L1-10221C-FSGS-001SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        2.45E-02      6.79E-02        3.58E-01 1004.76                  18.01        1.91E-01                      2.43E-01 1274.43                  34.80       -3.89E-02                      1.08E-01 1596.48                   1.80       -1.97E-01                      1.73E+00 Eu-155            45.30                  1.31        2.38E+00      1.53E-01        8.99E+00 60.01                  1.22        1.76E+00                      1.09E+01 86.55                 30.70        1.36E-02                      1.53E-01 105.31                 21.10        4.67E-03                      1.57E-01 Ra-226           186.21                  3.64        3.81E-01      8.50E-01        8.50E-01 Pa-231            27.36                 10.30        7.17E-01      1.06E+00        1.06E+00 283.69                  1.70        6.26E-01                      1.47E+00 300.07                  2.47       -4.03E-01                      1.14E+00 302.65                  2.20        3.90E-01                      1.27E+00 330.06                  1.40       -1.98E-01                      1.98E+00 U-235            143.76                 10.96       -1.60E-02      5.46E-02        2.58E-01 163.33                  5.08        4.60E-02                      6.21E-01 185.71                 57.20        3.54E-02                      5.46E-02 202.11                  1.08       -8.96E-01                      2.73E+00 205.31                  5.01       -1.69E-01                      5.93E-01 Am-241            59.54                 35.90        1.07E-01      3.90E-01        3.90E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[72]

6/12/2019 12:23:34PM Page 1 of 6 Analysis Report for    12-Jun-19-10015 L1-10221C-FSGS-002SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10015 Sample Description                           : L1-10221C-FSGS-002SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.800E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:20:00AM Acquisition Started                          : 6/12/2019 12:08:21PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.0 seconds Dead Time                                    : 0.11 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77296 Fill Height                                  : 1799.83 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:23:24PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[73]

6/12/2019   12:23:34PM         Page 2 of 6 Analysis Report for    12-Jun-19-10015 L1-10221C-FSGS-002SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.85               948 - 961             955.51          6.17E+01               14.34      5.13E+01           0.78 2       295.30             1176 - 1185           1181.09           1.61E+01                7.97      2.09E+01           0.50 3       352.01             1402 - 1413           1407.76           4.26E+01                9.55      1.94E+01           0.62 4      1460.83             5835 - 5852           5843.14           1.20E+02               12.22      9.00E+00           1.42 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     1.00          1460.82
* 10.66              2.87E+00              3.18E-01 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.08E-01              2.65E-02 300.09                    3.30 Pb-214                   0.99           241.99                    7.25 295.22
* 18.42              7.46E-02              3.74E-02 351.93
* 35.60              1.16E-01              2.76E-02 785.96                    1.06
[74]

6/12/2019 12:23:34PM         Page 3 of 6 Analysis Report for    12-Jun-19-10015 L1-10221C-FSGS-002SS
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                1.000                     2.87E+00              3.18E-01 X       Bi-211                              0.869 Pb-212                              0.993                     1.08E-01              2.65E-02 Pb-214                              0.999                     1.01E-01              2.22E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[75]

6/12/2019  12:23:34PM       Page 4 of 6 Analysis Report for    12-Jun-19-10015 L1-10221C-FSGS-002SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:23:24PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.53E-02          5.58E-02        5.58E-02 BE-7            477.60              10.44       2.98E-01          4.16E-01        4.16E-01
+         K-40          1460.82
* 10.66       2.87E+00          5.08E-01        5.08E-01 Mn-54           834.85              99.98       7.74E-03          4.25E-02        4.25E-02 Co-60         1173.23               99.85       2.23E-02          4.64E-02        4.96E-02 1332.49               99.98       2.85E-02                          4.64E-02 Nb-94           702.65              99.81     -9.07E-03           3.74E-02        4.19E-02 871.09              99.89       1.55E-02                          3.74E-02 Ag-108m          79.13                6.60      1.27E+00          3.52E-02        1.70E+00 433.94              90.50     -1.71E-02                           3.87E-02 614.28              89.80     -8.05E-03                           5.55E-02 722.94              90.80     -4.20E-03                           3.52E-02 Sb-125          176.31                6.84    -4.91E-01           1.25E-01        4.69E-01 380.45                1.52    -6.81E-01                           2.00E+00 427.87              29.60     -3.21E-02                           1.25E-01 463.36              10.49     -1.04E-01                           3.26E-01 600.60              17.65     -1.44E-01                           1.80E-01 606.71                4.98      1.36E+00                          1.05E+00 635.95              11.22       2.32E-03                          2.70E-01            [76]

6/12/2019  12:23:34PM Page 5 of 6 Analysis Report for 12-Jun-19-10015 L1-10221C-FSGS-002SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    4.85E-01      1.25E-01        1.91E+00 Ba-133        79.61            2.65    3.56E+00      6.95E-02        4.13E+00 81.00           32.90   -2.17E-01                      2.72E-01 276.40            7.16    5.71E-02                      4.71E-01 302.85           18.34    7.32E-02                      1.87E-01 356.01           62.05   -4.88E-03                      6.95E-02 383.85            8.94    2.13E-01                      3.60E-01 Cs-134       475.36            1.48    7.87E-01      4.51E-02        2.89E+00 563.25            8.34   -2.04E-01                      3.64E-01 569.33           15.37   -2.75E-02                      1.94E-01 604.72           97.62   -5.18E-02                      4.51E-02 795.86           85.46    1.31E-02                      4.60E-02 801.95            8.69   -7.39E-02                      4.43E-01 1038.61             0.99   -5.36E-01                      3.98E+00 1167.97             1.79   -2.65E+00                      2.62E+00 1365.19             3.02    4.82E-01                      1.17E+00 Cs-137       661.66           85.10    2.68E-02      5.12E-02        5.12E-02 Eu-152       121.78           28.67   -2.76E-02      1.16E-01        1.33E-01 244.70            7.61    4.20E-01                      5.50E-01 295.94            0.45    7.55E+00                      8.90E+00 344.28           26.60    8.07E-02                      1.16E-01 367.79            0.86    7.18E-01                      4.06E+00 411.12            2.24    1.01E+00                      1.53E+00 443.96            2.83   -6.33E-01                      1.19E+00 488.68            0.42    7.60E-01                      7.64E+00 563.99            0.49   -1.37E-01                      6.35E+00 586.26            0.46    9.67E+00                      1.08E+01 678.62            0.47    3.37E+00                      7.83E+00 688.67            0.86   -2.26E+00                      3.60E+00 719.35            0.28   -1.18E+01                      1.06E+01 778.90           12.96    1.64E-01                      3.33E-01 810.45            0.32   -7.77E+00                      1.04E+01 867.37            4.26   -1.11E+00                      8.47E-01 919.33            0.43    3.94E+00                      8.78E+00 964.08           14.65    2.55E-02                      3.40E-01 1085.87            10.24   -2.91E-01                      4.36E-01 1089.74             1.73   -2.71E-01                      2.66E+00 1112.07            13.69    5.01E-02                      3.31E-01 1212.95             1.43    1.71E-01                      3.46E+00 1249.94             0.19    6.03E+00                      2.18E+01 1299.14             1.63   -1.33E+00                      2.70E+00 1408.01            21.07    1.06E-01                      2.03E-01 1457.64             0.50    7.08E+01                      3.02E+01 1528.10             0.28    7.02E-01                      1.05E+01 Eu-154       123.07           40.40   -4.92E-03      9.53E-02        9.53E-02 247.93            6.89    4.32E-01                      5.48E-01 591.76            4.95    1.52E-01                      7.25E-01 692.42            1.78    2.93E-01                      2.06E+00 723.30           20.06   -1.66E-02                      1.59E-01 756.80            4.52   -4.61E-01                      8.40E-01 873.18           12.08    1.93E-01                      3.00E-01
[77]

6/12/2019  12:23:34PM Page 6 of 6 Analysis Report for     12-Jun-19-10015 L1-10221C-FSGS-002SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -2.98E-02      9.53E-02        3.91E-01 1004.76                  18.01       -3.27E-02                      2.29E-01 1274.43                  34.80        3.79E-02                      1.29E-01 1596.48                   1.80       -3.80E-02                      1.70E+00 Eu-155            45.30                  1.31        5.15E+00      2.32E-01        2.78E+01 60.01                  1.22        2.49E+00                      2.64E+01 86.55                 30.70        1.42E-01                      2.32E-01 105.31                 21.10        1.04E-01                      2.51E-01 Ra-226           186.21                  3.64        8.62E-01      1.04E+00        1.04E+00 Pa-231            27.36                 10.30        8.21E-01      1.36E+00        2.42E+00 283.69                  1.70       -2.88E-01                      1.91E+00 300.07                  2.47       -6.38E-01                      1.36E+00 302.65                  2.20        9.76E-02                      1.53E+00 330.06                  1.40       -3.92E-02                      2.39E+00 U-235            143.76                 10.96       -1.77E-01      6.43E-02        3.30E-01 163.33                  5.08       -1.70E-01                      6.41E-01 185.71                 57.20        1.27E-02                      6.43E-02 202.11                  1.08        9.98E-01                      3.29E+00 205.31                  5.01        3.55E-02                      6.86E-01 Am-241            59.54                 35.90        2.80E-02      9.36E-01        9.36E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[78]

6/12/2019 12:23:49PM Page 1 of 7 Analysis Report for    12-Jun-19-10016 L1-10221C-FSGS-003SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10016 Sample Description                           : L1-10221C-FSGS-003SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.805E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:25:00AM Acquisition Started                          : 6/12/2019 12:08:31PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77297 Fill Height                                  : 1804.99 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:23:40PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[79]

6/12/2019   12:23:49PM         Page 2 of 7 Analysis Report for    12-Jun-19-10016 L1-10221C-FSGS-003SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.76               950 -    960          954.63          1.01E+02               13.04      2.87E+01           1.13 2       338.40             1349 -   1356         1352.68           1.07E+01                6.65      1.53E+01           0.53 3       351.89             1400 -   1415         1406.58           7.80E+01               12.76      2.80E+01           1.09 4       583.20             2326 -   2336         2330.90           1.78E+01                6.12      8.25E+00           0.71 5       609.27             2429 -   2441         2435.13           4.76E+01                9.66      1.74E+01           0.85 6       661.75             2640 -   2650         2644.88           2.30E+01                5.69      3.96E+00           0.40 7      1460.41             5828 -   5849         5839.58           1.86E+02               13.64      0.00E+00           1.48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.97          1460.82
* 10.66              4.00E+00              3.41E-01 Cs-137                   0.99           661.66
* 85.10              3.65E-02              9.27E-03 Tl-208                   1.00           583.19
* 85.00              2.58E-02              9.04E-03 Bi-211                   0.89           351.07
* 13.02              5.21E-01              9.50E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.57E-01              2.38E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.33E-01              2.82E-02 768.36                    4.89 806.18                    1.26                                               [80]

6/12/2019   12:23:49PM        Page 3 of 7 Analysis Report for    12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00         934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00         241.99                  7.25 295.22                 18.42 351.93
* 35.60  1.91E-01              3.47E-02 785.96                  1.06 Ac-228                   1.00         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32
* 11.27  8.00E-02              5.04E-02 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20                 25.80 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[81]

6/12/2019 12:23:49PM         Page 4 of 7 Analysis Report for   12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.973                     4.00E+00              3.41E-01 Cs-137                              0.999                     3.65E-02              9.27E-03 Tl-208                              1.000                     2.58E-02              9.04E-03
     ?       Bi-211                              0.898                     5.21E-01              9.50E-02 Pb-212                              0.997                     1.57E-01              2.38E-02 Bi-214                              1.000                     1.33E-01              2.82E-02
     ?       Pb-214                              1.000                     1.91E-01              3.47E-02 Ac-228                              1.000                     8.00E-02              5.04E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[82]

6/12/2019  12:23:49PM       Page 5 of 7 Analysis Report for    12-Jun-19-10016 L1-10221C-FSGS-003SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:23:40PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.58E-02          4.66E-02        4.66E-02 BE-7            477.60              10.44       1.68E-01          3.40E-01        3.40E-01
+         K-40          1460.82
* 10.66       4.00E+00          6.19E-02        6.19E-02 Mn-54           834.85              99.98       3.17E-03          4.38E-02        4.38E-02 Co-60         1173.23               99.85       6.93E-03          4.85E-02        4.90E-02 1332.49               99.98       9.10E-03                          4.85E-02 Nb-94           702.65              99.81     -7.02E-04           3.34E-02        3.34E-02 871.09              99.89       7.69E-03                          3.47E-02 Ag-108m          79.13                6.60    -1.52E-01           3.44E-02        1.03E+00 433.94              90.50       1.46E-02                          3.44E-02 614.28              89.80     -2.61E-02                           5.05E-02 722.94              90.80     -4.24E-02                           3.83E-02 Sb-125          176.31                6.84      1.15E-01          1.03E-01        4.06E-01 380.45                1.52    -9.03E-01                           1.90E+00 427.87              29.60       4.54E-02                          1.03E-01 463.36              10.49       4.42E-02                          3.15E-01 600.60              17.65       1.72E-03                          1.92E-01 606.71                4.98      1.48E+00                          1.22E+00 635.95              11.22       6.43E-02                          2.58E-01            [83]

6/12/2019  12:23:49PM Page 6 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.01E+00      1.03E-01        1.97E+00 Ba-133        79.61            2.65   -9.89E-01      6.13E-02        2.48E+00 81.00           32.90   -1.84E-01                      1.64E-01 276.40            7.16    4.45E-02                      4.05E-01 302.85           18.34    5.84E-02                      1.58E-01 356.01           62.05   -1.36E-02                      6.13E-02 383.85            8.94   -1.96E-02                      3.24E-01 Cs-134       475.36            1.48    1.39E+00      4.43E-02        2.39E+00 563.25            8.34   -7.52E-01                      3.75E-01 569.33           15.37   -4.59E-03                      2.01E-01 604.72           97.62   -3.45E-02                      5.48E-02 795.86           85.46   -3.18E-04                      4.43E-02 801.95            8.69    1.37E-01                      4.10E-01 1038.61             0.99    1.38E+00                      3.83E+00 1167.97             1.79   -1.33E-01                      2.73E+00 1365.19             3.02    3.57E-01                      1.41E+00
+         Cs-137       661.66
* 85.10    3.65E-02      2.10E-02        2.10E-02 Eu-152       121.78           28.67    2.30E-02      9.39E-02        1.04E-01 244.70            7.61    3.56E-01                      4.20E-01 295.94            0.45    9.97E-01                      8.42E+00 344.28           26.60   -1.52E-01                      9.39E-02 367.79            0.86    1.13E+00                      3.80E+00 411.12            2.24   -2.45E-01                      1.44E+00 443.96            2.83   -3.98E-01                      9.56E-01 488.68            0.42   -1.63E+00                      7.13E+00 563.99            0.49   -1.18E+01                      5.86E+00 586.26            0.46    5.05E+00                      8.86E+00 678.62            0.47    1.76E-01                      6.90E+00 688.67            0.86   -9.09E-01                      3.83E+00 719.35            0.28   -5.90E+00                      1.24E+01 778.90           12.96   -3.17E-02                      3.11E-01 810.45            0.32    2.18E-02                      9.02E+00 867.37            4.26    2.52E-01                      8.35E-01 919.33            0.43    1.48E+00                      9.55E+00 964.08           14.65    2.96E-02                      3.18E-01 1085.87            10.24   -4.57E-02                      4.55E-01 1089.74             1.73   -5.08E-01                      2.75E+00 1112.07            13.69   -4.84E-02                      3.30E-01 1212.95             1.43   -5.25E-01                      3.86E+00 1249.94             0.19   -1.56E+01                      2.40E+01 1299.14             1.63   -2.30E+00                      2.70E+00 1408.01            21.07   -5.54E-02                      2.14E-01 1457.64             0.50    8.34E+01                      3.12E+01 1528.10             0.28    3.37E+00                      1.05E+01 Eu-154       123.07           40.40    1.67E-02      7.27E-02        7.27E-02 247.93            6.89   -4.75E-02                      4.20E-01 591.76            4.95   -2.46E-01                      5.86E-01 692.42            1.78   -1.50E-01                      1.81E+00 723.30           20.06   -1.31E-01                      1.77E-01 756.80            4.52    2.07E-01                      6.99E-01 873.18           12.08    3.89E-02                      2.88E-01
[84]

6/12/2019  12:23:49PM Page 7 of 7 Analysis Report for     12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -5.59E-02      7.27E-02        3.93E-01 1004.76                  18.01       -7.42E-02                      2.12E-01 1274.43                  34.80       -2.84E-02                      1.12E-01 1596.48                   1.80        2.05E+00                      2.93E+00 Eu-155            45.30                  1.31        2.07E+00      1.56E-01        1.02E+01 60.01                  1.22        7.93E-01                      1.11E+01 86.55                 30.70        6.60E-02                      1.69E-01 105.31                 21.10        4.46E-02                      1.56E-01 Ra-226           186.21                  3.64        7.13E-01      9.01E-01        9.01E-01 Pa-231            27.36                 10.30        5.84E-01      1.16E+00        1.16E+00 283.69                  1.70        2.44E-01                      1.72E+00 300.07                  2.47       -1.50E+00                      1.24E+00 302.65                  2.20        8.74E-01                      1.34E+00 330.06                  1.40       -3.65E-01                      2.06E+00 U-235            143.76                 10.96        6.12E-02      5.58E-02        2.74E-01 163.33                  5.08        1.08E-01                      5.38E-01 185.71                 57.20        2.60E-02                      5.58E-02 202.11                  1.08       -7.82E-01                      2.79E+00 205.31                  5.01       -1.11E-01                      5.90E-01 Am-241            59.54                 35.90       -6.17E-02      3.74E-01        3.74E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[85]

6/12/2019 12:23:55PM Page 1 of 6 Analysis Report for    12-Jun-19-10017 L1-10221C-FSGS-004SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10017 Sample Description                           : L1-10221C-FSGS-004SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.640E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:30:00AM Acquisition Started                          : 6/12/2019 12:08:37PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77298 Fill Height                                  : 1640.39 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:23:43PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[86]

6/12/2019   12:23:55PM         Page 2 of 6 Analysis Report for    12-Jun-19-10017 L1-10221C-FSGS-004SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.68               948 - 961             955.18          5.89E+01               12.48      3.51E+01           0.88 2       295.18             1173 - 1187           1180.93           2.54E+01                9.53      2.26E+01           0.62 3       583.18             2328 - 2337           2332.05           2.79E+01                6.85      7.14E+00           0.93 4      1460.44             5833 - 5854           5842.15           1.34E+02               12.30      4.91E+00           0.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.97          1460.82
* 10.66              2.76E+00              2.80E-01 Tl-208                   1.00           583.19
* 85.00              3.93E-02              9.94E-03 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              9.13E-02              2.07E-02 300.09                    3.30 Pb-214                   1.00           241.99                    7.25 295.22
* 18.42              1.05E-01              4.00E-02 351.93                  35.60 785.96                    1.06
[87]

6/12/2019 12:23:55PM         Page 3 of 6 Analysis Report for    12-Jun-19-10017 L1-10221C-FSGS-004SS
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.978                     2.76E+00              2.80E-01 Tl-208                              1.000                     3.93E-02              9.94E-03 Pb-212                              1.000                     9.13E-02              2.07E-02 Pb-214                              1.000                     1.05E-01              4.00E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[88]

6/12/2019  12:23:55PM       Page 4 of 6 Analysis Report for    12-Jun-19-10017 L1-10221C-FSGS-004SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:23:43PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        4.18E-02          4.39E-02        4.39E-02 BE-7            477.60              10.44     -1.71E-01           3.02E-01        3.02E-01
+         K-40          1460.82
* 10.66       2.76E+00          3.49E-01        3.49E-01 Mn-54           834.85              99.98       1.18E-02          3.61E-02        3.61E-02 Co-60         1173.23               99.85       6.14E-03          4.28E-02        4.28E-02 1332.49               99.98       5.70E-03                          4.52E-02 Nb-94           702.65              99.81     -3.21E-02           2.56E-02        3.64E-02 871.09              99.89     -1.36E-02                           2.56E-02 Ag-108m          79.13                6.60    -8.44E-01           2.98E-02        1.12E+00 433.94              90.50     -1.95E-02                           2.98E-02 614.28              89.80     -2.96E-04                           4.69E-02 722.94              90.80     -2.13E-02                           3.77E-02 Sb-125          176.31                6.84    -5.34E-02           9.48E-02        3.64E-01 380.45                1.52      2.13E+00                          2.00E+00 427.87              29.60     -6.52E-02                           9.48E-02 463.36              10.49     -4.03E-03                           2.05E-01 600.60              17.65       9.27E-02                          1.83E-01 606.71                4.98    -1.26E-01                           8.84E-01 635.95              11.22       2.38E-01                          2.81E-01            [89]

6/12/2019  12:23:55PM Page 5 of 6 Analysis Report for 12-Jun-19-10017 L1-10221C-FSGS-004SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.49E+00      9.48E-02        1.53E+00 Ba-133        79.61            2.65    1.02E+00      5.34E-02        2.80E+00 81.00           32.90   -1.42E-01                      1.94E-01 276.40            7.16    1.73E-01                      3.96E-01 302.85           18.34   -5.72E-03                      1.50E-01 356.01           62.05   -9.40E-03                      5.34E-02 383.85            8.94   -1.31E-01                      2.92E-01 Cs-134       475.36            1.48    1.40E+00      3.89E-02        2.33E+00 563.25            8.34   -3.44E-01                      3.10E-01 569.33           15.37   -2.64E-02                      1.95E-01 604.72           97.62   -2.97E-03                      4.27E-02 795.86           85.46    5.33E-03                      3.89E-02 801.95            8.69    3.34E-02                      3.54E-01 1038.61             0.99   -2.13E+00                      3.05E+00 1167.97             1.79   -1.04E+00                      2.44E+00 1365.19             3.02   -7.37E-01                      1.14E+00 Cs-137       661.66           85.10   -8.75E-03      4.11E-02        4.11E-02 Eu-152       121.78           28.67    1.36E-03      1.02E-01        1.02E-01 244.70            7.61   -6.38E-02                      3.49E-01 295.94            0.45    6.31E+00                      7.80E+00 344.28           26.60   -2.52E-02                      1.05E-01 367.79            0.86    1.93E+00                      3.28E+00 411.12            2.24   -1.06E-02                      1.22E+00 443.96            2.83   -4.45E-02                      9.83E-01 488.68            0.42   -1.90E-01                      7.40E+00 563.99            0.49   -5.60E+00                      5.27E+00 586.26            0.46    4.63E+00                      1.01E+01 678.62            0.47    5.61E+00                      6.82E+00 688.67            0.86   -1.54E+00                      3.03E+00 719.35            0.28   -4.80E+00                      1.30E+01 778.90           12.96   -2.83E-01                      2.89E-01 810.45            0.32   -2.76E+00                      7.60E+00 867.37            4.26   -7.61E-02                      7.58E-01 919.33            0.43   -1.58E+01                      8.54E+00 964.08           14.65    6.57E-03                      3.41E-01 1085.87            10.24   -3.10E-01                      3.03E-01 1089.74             1.73    1.46E+00                      2.17E+00 1112.07            13.69   -1.66E-02                      2.60E-01 1212.95             1.43   -1.75E-01                      2.98E+00 1249.94             0.19    1.12E+01                      2.35E+01 1299.14             1.63   -1.81E+00                      2.50E+00 1408.01            21.07   -2.57E-02                      1.58E-01 1457.64             0.50    6.39E+01                      2.65E+01 1528.10             0.28    4.02E+00                      1.09E+01 Eu-154       123.07           40.40   -2.39E-02      7.01E-02        7.01E-02 247.93            6.89   -6.20E-02                      3.36E-01 591.76            4.95    2.32E-01                      6.45E-01 692.42            1.78    2.17E-01                      1.95E+00 723.30           20.06   -1.97E-02                      1.71E-01 756.80            4.52   -1.10E-01                      7.64E-01 873.18           12.08   -2.37E-01                      1.75E-01
[90]

6/12/2019  12:23:55PM Page 6 of 6 Analysis Report for     12-Jun-19-10017 L1-10221C-FSGS-004SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        1.32E-01      7.01E-02        3.48E-01 1004.76                  18.01       -8.99E-02                      2.09E-01 1274.43                  34.80       -7.15E-02                      1.23E-01 1596.48                   1.80       -1.08E+00                      1.91E+00 Eu-155            45.30                  1.31       -1.43E+00      1.68E-01        1.55E+01 60.01                  1.22        1.03E+00                      1.83E+01 86.55                 30.70        1.17E-02                      1.68E-01 105.31                 21.10        2.10E-02                      1.77E-01 Ra-226           186.21                  3.64       -7.89E-02      8.17E-01        8.17E-01 Pa-231            27.36                 10.30        9.92E-01      1.11E+00        1.74E+00 283.69                  1.70        5.45E-02                      1.53E+00 300.07                  2.47       -3.38E-01                      1.11E+00 302.65                  2.20        3.74E-01                      1.26E+00 330.06                  1.40       -4.46E-01                      1.96E+00 U-235            143.76                 10.96       -1.70E-01      5.27E-02        2.69E-01 163.33                  5.08       -2.42E-01                      4.87E-01 185.71                 57.20        1.50E-02                      5.27E-02 202.11                  1.08        1.82E+00                      2.71E+00 205.31                  5.01        6.08E-02                      5.74E-01 Am-241            59.54                 35.90        3.42E-01      6.49E-01        6.49E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[91]

6/12/2019 12:47:23PM Page 1 of 7 Analysis Report for    12-Jun-19-10018 L1-10221C-FSGS-005SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10018 Sample Description                           : L1-10221C-FSGS-005SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.690E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:35:00AM Acquisition Started                          : 6/12/2019 12:32:11PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77299 Fill Height                                  : 1689.99 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:47:14PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[92]

6/12/2019   12:47:23PM         Page 2 of 7 Analysis Report for    12-Jun-19-10018 L1-10221C-FSGS-005SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.46               472 -    481          477.10          6.79E+01               16.71      8.91E+01           1.23 2       295.25               588 -    595          590.56          3.67E+01               10.92      3.93E+01           1.10 3       351.92               699 -    708          703.79          4.71E+01               11.63      3.89E+01           1.49 4       583.24             1162 -   1170         1166.09           3.13E+01                8.71      2.08E+01           1.24 5       609.25             1213 -   1223         1218.08           5.85E+01                8.92      8.45E+00           1.59 6       661.65             1319 -   1328         1322.83           5.45E+01                9.10      1.25E+01           1.58 7      1460.89             2916 -   2928         2921.84           1.64E+02               13.63      8.24E+00           2.05 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              3.00E+00              2.82E-01 Cs-137                   1.00           661.66
* 85.10              7.47E-02              1.33E-02 Tl-208                   1.00           583.19
* 85.00              3.95E-02              1.13E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              9.36E-02              2.43E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.42E-01              2.33E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11                                               [93]

6/12/2019   12:47:23PM         Page 3 of 7 Analysis Report for    12-Jun-19-10018 L1-10221C-FSGS-005SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   1.00        1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00         241.99                  7.25 295.22
* 18.42       1.35E-01              4.16E-02 351.93
* 35.60       1.01E-01              2.63E-02 785.96                  1.06
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean                Wt mean     Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
K-40                              0.999               3.00E+00               2.82E-01 Cs-137                            1.000               7.47E-02               1.33E-02 Tl-208                            1.000               3.95E-02               1.13E-02 X       Bi-211                            0.890 Pb-212                            0.996               9.36E-02               2.43E-02 Bi-214                            1.000               1.42E-01               2.33E-02 Pb-214                            1.000               1.11E-01               2.22E-02
[94]

6/12/2019 12:47:23PM Page 4 of 7 Analysis Report for   12-Jun-19-10018 L1-10221C-FSGS-005SS
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[95]

6/12/2019  12:47:23PM       Page 5 of 7 Analysis Report for    12-Jun-19-10018 L1-10221C-FSGS-005SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:47:14PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        5.27E-02          4.81E-02        4.81E-02 BE-7            477.60              10.44       1.13E-01          3.17E-01        3.17E-01
+         K-40          1460.82
* 10.66       3.00E+00          3.43E-01        3.43E-01 Mn-54           834.85              99.98       1.49E-02          3.96E-02        3.96E-02 Co-60         1173.23               99.85       4.16E-02          4.24E-02        5.72E-02 1332.49               99.98       1.60E-02                          4.24E-02 Nb-94           702.65              99.81     -2.81E-03           3.20E-02        3.20E-02 871.09              99.89       4.88E-03                          3.54E-02 Ag-108m          79.13                6.60      3.22E-01          2.97E-02        9.38E-01 433.94              90.50     -2.00E-03                           2.97E-02 614.28              89.80     -5.11E-03                           4.51E-02 722.94              90.80       1.30E-02                          3.08E-02 Sb-125          176.31                6.84    -2.98E-01           9.48E-02        4.29E-01 380.45                1.52      6.67E-01                          1.85E+00 427.87              29.60       1.46E-02                          9.48E-02 463.36              10.49       1.20E-01                          2.71E-01 600.60              17.65       5.20E-02                          1.78E-01 606.71                4.98    -2.00E-01                           9.77E-01 635.95              11.22       1.47E-01                          2.91E-01            [96]

6/12/2019  12:47:23PM Page 6 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    2.08E-01      9.48E-02        1.67E+00 Ba-133        79.61            2.65    5.30E-01      5.90E-02        2.24E+00 81.00           32.90   -7.30E-02                      1.56E-01 276.40            7.16   -1.46E-01                      3.65E-01 302.85           18.34    7.13E-02                      1.65E-01 356.01           62.05   -1.56E-02                      5.90E-02 383.85            8.94   -4.23E-02                      3.02E-01 Cs-134       475.36            1.48    7.20E-01      3.90E-02        2.32E+00 563.25            8.34   -4.13E-02                      3.94E-01 569.33           15.37    5.69E-02                      2.07E-01 604.72           97.62   -1.47E-02                      4.19E-02 795.86           85.46    4.82E-03                      3.90E-02 801.95            8.69   -1.20E-01                      3.26E-01 1038.61             0.99    1.81E+00                      4.08E+00 1167.97             1.79   -2.05E+00                      2.61E+00 1365.19             3.02   -3.64E-01                      1.11E+00
+         Cs-137       661.66
* 85.10    7.47E-02      2.87E-02        2.87E-02 Eu-152       121.78           28.67    1.95E-02      9.93E-02        9.93E-02 244.70            7.61   -2.04E-02                      4.00E-01 295.94            0.45    6.48E+00                      7.82E+00 344.28           26.60   -1.49E-02                      1.02E-01 367.79            0.86   -3.99E-01                      2.90E+00 411.12            2.24    1.84E-01                      1.39E+00 443.96            2.83    2.27E-01                      9.37E-01 488.68            0.42    1.76E+00                      7.02E+00 563.99            0.49    6.82E-01                      6.77E+00 586.26            0.46   -3.47E+00                      1.01E+01 678.62            0.47    1.07E+00                      6.24E+00 688.67            0.86    4.78E-01                      3.53E+00 719.35            0.28   -5.51E-01                      8.90E+00 778.90           12.96    2.25E-02                      2.73E-01 810.45            0.32    5.59E+00                      1.07E+01 867.37            4.26   -1.83E-01                      7.19E-01 919.33            0.43   -5.21E+00                      8.21E+00 964.08           14.65    8.15E-02                      2.82E-01 1085.87            10.24   -4.06E-02                      3.89E-01 1089.74             1.73    2.54E-01                      2.31E+00 1112.07            13.69   -7.28E-02                      2.62E-01 1212.95             1.43   -6.28E-01                      3.12E+00 1249.94             0.19   -2.18E+00                      2.21E+01 1299.14             1.63   -2.26E+00                      1.72E+00 1408.01            21.07   -8.38E-02                      1.40E-01 1457.64             0.50   -2.16E+00                      2.61E+01 1528.10             0.28   -2.35E+00                      1.11E+01 Eu-154       123.07           40.40   -1.68E-02      6.77E-02        6.77E-02 247.93            6.89   -1.27E-01                      3.79E-01 591.76            4.95    1.75E-01                      7.02E-01 692.42            1.78   -1.41E-01                      1.71E+00 723.30           20.06    5.88E-02                      1.39E-01 756.80            4.52   -2.31E-02                      6.99E-01 873.18           12.08    9.34E-02                      3.10E-01
[97]

6/12/2019  12:47:23PM Page 7 of 7 Analysis Report for     12-Jun-19-10018 L1-10221C-FSGS-005SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        1.11E-01      6.77E-02        3.75E-01 1004.76                  18.01       -1.04E-01                      1.77E-01 1274.43                  34.80        4.35E-02                      1.16E-01 1596.48                   1.80       -1.67E+00                      1.91E+00 Eu-155            45.30                  1.31       -2.99E+00      1.57E-01        9.40E+00 60.01                  1.22        1.92E+00                      1.05E+01 86.55                 30.70        7.49E-02                      1.57E-01 105.31                 21.10        2.88E-02                      1.67E-01 Ra-226           186.21                  3.64       -1.05E-01      8.17E-01        8.17E-01 Pa-231            27.36                 10.30        3.10E-01      9.45E-01        9.45E-01 283.69                  1.70       -4.84E-01                      1.50E+00 300.07                  2.47        2.26E-01                      1.26E+00 302.65                  2.20        5.94E-01                      1.38E+00 330.06                  1.40        5.76E-01                      2.10E+00 U-235            143.76                 10.96       -4.45E-02      5.33E-02        2.32E-01 163.33                  5.08        9.39E-03                      5.87E-01 185.71                 57.20        9.96E-03                      5.33E-02 202.11                  1.08        1.23E+00                      2.83E+00 205.31                  5.01       -1.36E-01                      5.92E-01 Am-241            59.54                 35.90        5.14E-02      3.60E-01        3.60E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[98]

6/12/2019 12:47:30PM Page 1 of 6 Analysis Report for    12-Jun-19-10019 L1-10221C-FSGS-006SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10019 Sample Description                           : L1-10221C-FSGS-006SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.723E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:40:00AM Acquisition Started                          : 6/12/2019 12:32:18PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.2 seconds Dead Time                                    : 0.14 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77300 Fill Height                                  : 1722.60 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:47:21PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[99]

6/12/2019   12:47:30PM         Page 2 of 6 Analysis Report for    12-Jun-19-10019 L1-10221C-FSGS-006SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.64               946 -    960          954.67          1.36E+02               17.49      5.93E+01           0.78 2       295.16             1176 -   1185         1180.53           2.17E+01                8.49      2.23E+01           1.03 3       352.08             1401 -   1412         1408.05           3.55E+01               10.70      3.15E+01           1.02 4       583.27             2327 -   2337         2332.30           3.30E+01                7.67      1.00E+01           0.37 5       661.63             2641 -   2651         2645.62           2.94E+01                7.56      1.16E+01           0.59 6       911.33             3638 -   3650         3644.26           3.28E+01                7.38      8.19E+00           1.03 7      1460.90             5833 -   5854         5843.44           2.32E+02               15.88      5.50E+00           1.88 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              5.59E+00              4.54E-01 Cs-137                   1.00           661.66
* 85.10              5.20E-02              1.38E-02 Tl-208                   0.99           583.19
* 85.00              5.37E-02              1.29E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              2.38E-01              3.62E-02 300.09                    3.30 Pb-214                   0.99           241.99                    7.25 295.22
* 18.42              1.01E-01              4.04E-02 351.93
* 35.60              9.72E-02              3.03E-02 785.96                    1.06                                              [100]

6/12/2019   12:47:30PM         Page 3 of 6 Analysis Report for    12-Jun-19-10019 L1-10221C-FSGS-006SS Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Ac-228                   0.99          129.07                    2.42 209.25                    3.89 270.24                    3.46 328.00                    2.95 338.32                  11.27 409.46                    1.92 463.00                    4.40 794.95                    4.25 911.20
* 25.80              2.38E-01              5.44E-02 964.77                    4.99 968.97                  15.80 1588.20                     3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
K-40                                0.999                     5.59E+00                4.54E-01 Cs-137                              1.000                     5.20E-02                1.38E-02 Tl-208                              0.999                     5.37E-02                1.29E-02 Pb-212                              1.000                     2.38E-01                3.62E-02 Pb-214                              0.998                     9.86E-02                2.43E-02 Ac-228                              0.999                     2.38E-01                5.44E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[101]

6/12/2019  12:47:30PM       Page 4 of 6 Analysis Report for    12-Jun-19-10019 L1-10221C-FSGS-006SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:47:21PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        7.44E-02          6.17E-02        6.17E-02 BE-7            477.60              10.44       1.84E-01          4.84E-01        4.84E-01
+         K-40          1460.82
* 10.66       5.59E+00          4.42E-01        4.42E-01 Mn-54           834.85              99.98     -3.28E-03           4.10E-02        4.10E-02 Co-60         1173.23               99.85       2.05E-02          6.05E-02        6.05E-02 1332.49               99.98       2.46E-02                          6.22E-02 Nb-94           702.65              99.81     -1.87E-02           4.41E-02        4.91E-02 871.09              99.89       3.62E-02                          4.41E-02 Ag-108m          79.13                6.60      1.22E+00          3.85E-02        1.75E+00 433.94              90.50       3.37E-03                          3.85E-02 614.28              89.80       3.96E-02                          6.49E-02 722.94              90.80     -1.30E-02                           5.05E-02 Sb-125          176.31                6.84      1.40E-01          1.27E-01        5.48E-01 380.45                1.52      2.28E+00                          2.50E+00 427.87              29.60     -4.35E-02                           1.27E-01 463.36              10.49       6.28E-02                          3.95E-01 600.60              17.65     -3.92E-02                           2.30E-01 606.71                4.98      1.03E+00                          1.24E+00 635.95              11.22     -8.65E-02                           3.39E-01          [102]

6/12/2019  12:47:30PM Page 5 of 6 Analysis Report for 12-Jun-19-10019 L1-10221C-FSGS-006SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -2.34E+00      1.27E-01        2.28E+00 Ba-133        79.61            2.65    1.10E+00      7.75E-02        4.12E+00 81.00           32.90   -1.64E-01                      2.81E-01 276.40            7.16    2.25E-01                      5.11E-01 302.85           18.34   -1.98E-03                      2.10E-01 356.01           62.05   -6.73E-02                      7.75E-02 383.85            8.94    2.45E-01                      4.27E-01 Cs-134       475.36            1.48    3.79E+00      5.59E-02        3.36E+00 563.25            8.34    2.07E-01                      5.13E-01 569.33           15.37   -1.23E-01                      2.66E-01 604.72           97.62   -1.67E-02                      5.59E-02 795.86           85.46    1.30E-03                      5.82E-02 801.95            8.69    1.64E-01                      5.58E-01 1038.61             0.99    2.89E+00                      5.64E+00 1167.97             1.79    1.54E+00                      3.64E+00 1365.19             3.02   -6.55E-01                      1.52E+00
+         Cs-137       661.66
* 85.10    5.20E-02      3.68E-02        3.68E-02 Eu-152       121.78           28.67   -5.23E-03      1.43E-01        1.54E-01 244.70            7.61    2.54E-01                      5.42E-01 295.94            0.45    5.98E-01                      9.01E+00 344.28           26.60    7.59E-02                      1.43E-01 367.79            0.86    2.61E+00                      3.97E+00 411.12            2.24   -9.13E-02                      1.81E+00 443.96            2.83    1.56E-03                      1.33E+00 488.68            0.42    2.74E+00                      9.69E+00 563.99            0.49    2.08E+00                      8.72E+00 586.26            0.46    4.17E+00                      1.20E+01 678.62            0.47   -3.00E+00                      7.90E+00 688.67            0.86    3.72E+00                      5.63E+00 719.35            0.28   -2.93E+00                      1.51E+01 778.90           12.96    1.07E-02                      2.94E-01 810.45            0.32    2.69E-01                      1.34E+01 867.37            4.26   -1.92E+00                      9.35E-01 919.33            0.43   -1.19E+01                      1.02E+01 964.08           14.65   -2.41E-01                      3.43E-01 1085.87            10.24   -2.51E-01                      4.52E-01 1089.74             1.73   -2.00E-01                      2.53E+00 1112.07            13.69    1.39E-01                      4.61E-01 1212.95             1.43   -3.03E+00                      4.25E+00 1249.94             0.19   -1.01E+01                      2.90E+01 1299.14             1.63   -2.07E-01                      3.29E+00 1408.01            21.07    1.19E-01                      2.14E-01 1457.64             0.50    1.16E+02                      3.97E+01 1528.10             0.28   -2.36E+00                      1.38E+01 Eu-154       123.07           40.40   -2.91E-02      1.09E-01        1.09E-01 247.93            6.89    1.90E-01                      5.13E-01 591.76            4.95    7.76E-02                      8.47E-01 692.42            1.78   -2.77E-01                      2.66E+00 723.30           20.06    1.01E-01                      2.29E-01 756.80            4.52   -1.73E-01                      9.97E-01 873.18           12.08   -1.46E-01                      3.57E-01
[103]

6/12/2019  12:47:30PM Page 6 of 6 Analysis Report for     12-Jun-19-10019 L1-10221C-FSGS-006SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.62E-01      1.09E-01        4.61E-01 1004.76                  18.01        1.91E-01                      2.81E-01 1274.43                  34.80       -1.16E-01                      1.67E-01 1596.48                   1.80       -7.29E-01                      2.65E+00 Eu-155            45.30                  1.31       -3.61E+00      2.54E-01        2.82E+01 60.01                  1.22        2.22E+01                      3.04E+01 86.55                 30.70       -1.64E-01                      2.54E-01 105.31                 21.10       -1.41E-01                      2.54E-01 Ra-226           186.21                  3.64        2.51E-01      1.04E+00        1.04E+00 Pa-231            27.36                 10.30        6.10E-01      1.55E+00        3.17E+00 283.69                  1.70        1.17E+00                      2.18E+00 300.07                  2.47       -1.10E+00                      1.55E+00 302.65                  2.20       -3.01E-01                      1.75E+00 330.06                  1.40       -1.05E+00                      2.76E+00 U-235            143.76                 10.96        1.84E-01      6.73E-02        3.77E-01 163.33                  5.08       -1.69E-02                      7.78E-01 185.71                 57.20        3.23E-02                      6.73E-02 202.11                  1.08        1.04E+00                      3.31E+00 205.31                  5.01       -4.01E-01                      7.25E-01 Am-241            59.54                 35.90        7.36E-01      1.10E+00        1.10E+00
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[104]

6/12/2019 12:47:53PM Page 1 of 7 Analysis Report for    12-Jun-19-10020 L1-10221C-FSGS-007SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10020 Sample Description                           : L1-10221C-FSGS-007SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.679E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:45:00AM Acquisition Started                          : 6/12/2019 12:32:25PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77301 Fill Height                                  : 1678.91 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:47:44PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[105]

6/12/2019   12:47:53PM         Page 2 of 7 Analysis Report for    12-Jun-19-10020 L1-10221C-FSGS-007SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.72               949 -    962          954.45          1.12E+02               15.33      4.40E+01           1.15 2       338.47             1349 -   1358         1352.95           2.85E+01                9.07      2.35E+01           0.82 3       351.92             1402 -   1412         1406.69           3.30E+01                9.51      2.40E+01           0.79 4       609.39             2429 -   2442         2435.59           4.27E+01                8.43      1.03E+01           0.30 5       661.53             2636 -   2650         2644.02           5.84E+01                8.64      5.64E+00           0.63 6       964.40             3851 -   3860         3855.01           9.00E+00                4.52      5.00E+00           0.52 7      1460.33             5829 -   5850         5839.24           1.95E+02               14.30      2.53E+00           1.80 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.96          1460.82
* 10.66              4.28E+00              3.64E-01 Cs-137                   0.99           661.66
* 85.10              9.37E-02              1.50E-02 Bi-211                   0.89           351.07
* 13.02              2.23E-01              6.68E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.75E-01              2.78E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.21E-01              2.50E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11                                              [106]

6/12/2019   12:47:53PM        Page 3 of 7 Analysis Report for    12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00        1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00         241.99                  7.25 295.22                 18.42 351.93
* 35.60  8.15E-02              2.44E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32
* 11.27  2.16E-01              7.11E-02 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20                 25.80 964.77
* 4.99  3.18E-01              1.60E-01 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[107]

6/12/2019 12:47:53PM         Page 4 of 7 Analysis Report for   12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.961                     4.28E+00              3.64E-01 Cs-137                              0.997                     9.37E-02              1.50E-02 X       Eu-152                              0.593
     ?       Bi-211                              0.891                     2.23E-01              6.68E-02 Pb-212                              0.999                     1.75E-01              2.78E-02 Bi-214                              1.000                     1.21E-01              2.50E-02
     ?       Pb-214                              1.000                     8.15E-02              2.44E-02 Ac-228                              0.998                     2.33E-01              6.50E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[108]

6/12/2019  12:47:53PM       Page 5 of 7 Analysis Report for    12-Jun-19-10020 L1-10221C-FSGS-007SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:47:44PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        4.79E-02          4.76E-02        4.76E-02 BE-7            477.60              10.44       1.68E-01          4.38E-01        4.38E-01
+         K-40          1460.82
* 10.66       4.28E+00          2.85E-01        2.85E-01 Mn-54           834.85              99.98     -1.30E-02           3.81E-02        3.81E-02 Co-60         1173.23               99.85       3.26E-02          5.30E-02        6.18E-02 1332.49               99.98       5.17E-03                          5.30E-02 Nb-94           702.65              99.81     -2.20E-03           3.69E-02        3.69E-02 871.09              99.89     -4.11E-03                           3.82E-02 Ag-108m          79.13                6.60    -2.03E-01           3.83E-02        1.07E+00 433.94              90.50       8.71E-03                          3.83E-02 614.28              89.80     -4.85E-02                           5.22E-02 722.94              90.80     -1.62E-02                           4.36E-02 Sb-125          176.31                6.84      2.48E-02          1.14E-01        3.76E-01 380.45                1.52      6.15E-02                          1.90E+00 427.87              29.60       3.01E-03                          1.14E-01 463.36              10.49       2.31E-01                          3.86E-01 600.60              17.65     -5.01E-02                           1.68E-01 606.71                4.98      1.40E+00                          1.07E+00 635.95              11.22       8.09E-02                          3.51E-01          [109]

6/12/2019  12:47:53PM Page 6 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.46E+00      1.14E-01        1.83E+00 Ba-133        79.61            2.65    7.20E-02      5.55E-02        2.62E+00 81.00           32.90   -2.06E-01                      1.69E-01 276.40            7.16    7.06E-02                      3.99E-01 302.85           18.34    9.31E-02                      1.75E-01 356.01           62.05   -2.29E-02                      5.55E-02 383.85            8.94    0.00E+00                      3.19E-01 Cs-134       475.36            1.48    1.64E+00      4.12E-02        3.06E+00 563.25            8.34   -3.56E-01                      4.65E-01 569.33           15.37   -4.34E-02                      1.86E-01 604.72           97.62   -3.49E-02                      4.12E-02 795.86           85.46   -9.05E-04                      4.40E-02 801.95            8.69    6.58E-02                      4.05E-01 1038.61             0.99    1.68E+00                      4.01E+00 1167.97             1.79   -7.59E-01                      3.25E+00 1365.19             3.02   -1.07E-01                      1.58E+00
+         Cs-137       661.66
* 85.10    9.37E-02      2.66E-02        2.66E-02 Eu-152       121.78           28.67   -5.50E-02      9.32E-02        9.32E-02 244.70            7.61   -2.56E-02                      3.99E-01 295.94            0.45    2.88E-01                      7.92E+00 344.28           26.60   -2.57E-03                      1.22E-01 367.79            0.86   -1.51E+00                      3.03E+00 411.12            2.24    5.01E-01                      1.54E+00 443.96            2.83    2.54E-01                      1.13E+00 488.68            0.42   -4.03E+00                      7.09E+00 563.99            0.49   -1.52E+01                      6.58E+00 586.26            0.46    7.14E+00                      1.03E+01 678.62            0.47    2.72E+00                      7.00E+00 688.67            0.86    2.71E-01                      3.70E+00 719.35            0.28    8.65E+00                      1.58E+01 778.90           12.96    8.89E-02                      2.29E-01 810.45            0.32   -1.26E+01                      9.50E+00 867.37            4.26   -2.60E-01                      9.14E-01 919.33            0.43   -2.99E+00                      8.55E+00 964.08
* 14.65    1.08E-01                      1.73E-01 1085.87            10.24    9.76E-02                      4.21E-01 1089.74             1.73    2.97E-01                      2.96E+00 1112.07            13.69    5.52E-02                      3.58E-01 1212.95             1.43   -1.66E+00                      3.85E+00 1249.94             0.19    6.35E+00                      2.56E+01 1299.14             1.63    6.75E-01                      2.91E+00 1408.01            21.07   -4.17E-02                      2.10E-01 1457.64             0.50    9.26E+01                      3.27E+01 1528.10             0.28   -9.63E+00                      8.27E+00 Eu-154       123.07           40.40   -5.68E-03      7.04E-02        7.04E-02 247.93            6.89   -6.01E-02                      4.18E-01 591.76            4.95   -3.54E-02                      6.99E-01 692.42            1.78   -1.64E-01                      1.80E+00 723.30           20.06    1.60E-03                      1.98E-01 756.80            4.52   -4.58E-01                      8.39E-01 873.18           12.08    1.19E-01                      3.31E-01
[110]

6/12/2019  12:47:53PM Page 7 of 7 Analysis Report for     12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.51E-01      7.04E-02        3.68E-01 1004.76                  18.01        8.81E-02                      2.16E-01 1274.43                  34.80       -9.92E-02                      1.34E-01 1596.48                   1.80        8.34E-01                      2.03E+00 Eu-155            45.30                  1.31       -2.53E-01      1.53E-01        9.98E+00 60.01                  1.22        1.41E+00                      1.08E+01 86.55                 30.70       -7.71E-02                      1.53E-01 105.31                 21.10       -2.22E-02                      1.57E-01 Ra-226           186.21                  3.64        7.00E-01      8.05E-01        8.05E-01 Pa-231            27.36                 10.30        9.39E-01      1.21E+00        1.21E+00 283.69                  1.70       -6.50E-01                      1.77E+00 300.07                  2.47       -2.43E+00                      1.25E+00 302.65                  2.20        3.23E-01                      1.45E+00 330.06                  1.40        7.70E-01                      2.25E+00 U-235            143.76                 10.96       -2.94E-02      5.11E-02        2.62E-01 163.33                  5.08        1.64E-01                      5.57E-01 185.71                 57.20        5.05E-02                      5.11E-02 202.11                  1.08       -1.54E+00                      2.40E+00 205.31                  5.01       -4.45E-01                      5.11E-01 Am-241            59.54                 35.90        1.58E-01      3.84E-01        3.84E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[111]

6/12/2019 12:47:45PM Page 1 of 7 Analysis Report for    12-Jun-19-10021 L1-10221C-FSGS-008SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10021 Sample Description                           : L1-10221C-FSGS-008SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.674E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:50:00AM Acquisition Started                          : 6/12/2019 12:32:33PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77302 Fill Height                                  : 1674.19 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 12:47:36PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[112]

6/12/2019   12:47:45PM         Page 2 of 7 Analysis Report for    12-Jun-19-10021 L1-10221C-FSGS-008SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       186.02               739 -    748          744.82          2.93E+01                9.62      2.77E+01           0.54 2       238.61               949 -    961          954.90          6.68E+01               14.52      5.02E+01           0.88 3       351.83             1401 -   1414         1407.32           4.07E+01               10.37      2.43E+01           0.99 4       477.44             1905 -   1914         1909.32           2.20E+01                6.72      1.00E+01           0.67 5       583.01             2326 -   2337         2331.37           3.06E+01                7.01      7.41E+00           0.66 6       609.02             2429 -   2442         2435.34           3.36E+01                8.28      1.24E+01           1.51 7      1460.53             5830 -   5853         5842.49           1.70E+02               15.16      1.47E+01           2.03 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty BE-7                     0.99           477.60
* 10.44              2.24E-01              7.04E-02 K-40                     0.98          1460.82
* 10.66              3.48E+00              3.45E-01 Tl-208                   0.99           583.19
* 85.00              4.30E-02              1.02E-02 Bi-211                   0.91           351.07
* 13.02              2.66E-01              7.12E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              1.03E-01              2.39E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              9.08E-02              2.30E-02 768.36                    4.89 806.18                    1.26                                              [113]

6/12/2019   12:47:45PM         Page 3 of 7 Analysis Report for    12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   0.99         934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22                 18.42 351.93
* 35.60       9.74E-02              2.60E-02 785.96                  1.06 Ra-226                   0.99         186.21
* 3.64       4.85E-01              1.64E-01 U-235                    0.98         143.76                 10.96 163.33                  5.08 185.71
* 57.20       3.09E-02              1.04E-02 202.11                  1.08 205.31                  5.01
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean                Wt mean     Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
BE-7                              0.995               2.24E-01               7.04E-02 K-40                              0.986               3.48E+00               3.45E-01      [114]

6/12/2019 12:47:45PM         Page 4 of 7 Analysis Report for   12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
Tl-208                              0.995                     4.30E-02              1.02E-02
     ?       Bi-211                              0.912                     2.66E-01              7.12E-02 Pb-212                              1.000                     1.03E-01              2.39E-02 Bi-214                              0.994                     9.08E-02              2.30E-02
     ?       Pb-214                              0.999                     9.74E-02              2.60E-02
     ?       Ra-226                              0.994                     4.85E-01              1.64E-01
     ?       U-235                               0.989                     3.09E-02              1.04E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[115]

6/12/2019  12:47:45PM       Page 5 of 7 Analysis Report for    12-Jun-19-10021 L1-10221C-FSGS-008SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 12:47:36PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        5.25E-02          4.85E-02        4.85E-02
+         BE-7            477.60
* 10.44       2.24E-01          1.96E-01        1.96E-01
+         K-40          1460.82
* 10.66       3.48E+00          5.93E-01        5.93E-01 Mn-54           834.85              99.98       2.67E-02          4.34E-02        4.34E-02 Co-60         1173.23               99.85       1.02E-02          4.37E-02        4.57E-02 1332.49               99.98       4.76E-04                          4.37E-02 Nb-94           702.65              99.81       5.94E-03          3.28E-02        3.28E-02 871.09              99.89       3.09E-02                          4.72E-02 Ag-108m          79.13                6.60      5.45E-01          2.81E-02        1.30E+00 433.94              90.50     -6.79E-03                           2.81E-02 614.28              89.80     -2.49E-02                           5.50E-02 722.94              90.80       3.86E-02                          5.30E-02 Sb-125          176.31                6.84    -1.25E-02           1.03E-01        4.28E-01 380.45                1.52    -2.63E-01                           1.99E+00 427.87              29.60       4.93E-02                          1.03E-01 463.36              10.49       1.42E-01                          3.03E-01 600.60              17.65       1.07E-01                          2.18E-01 606.71                4.98      1.22E+00                          1.06E+00 635.95              11.22     -2.13E-01                           3.38E-01          [116]

6/12/2019  12:47:45PM Page 6 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    6.30E-01      1.03E-01        1.48E+00 Ba-133        79.61            2.65    1.24E+00      6.19E-02        3.07E+00 81.00           32.90   -3.64E-01                      2.00E-01 276.40            7.16    3.95E-01                      4.24E-01 302.85           18.34    5.74E-02                      1.63E-01 356.01           62.05   -3.42E-02                      6.19E-02 383.85            8.94    1.68E-01                      3.66E-01 Cs-134       475.36            1.48    1.39E+00      4.51E-02        2.68E+00 563.25            8.34   -9.81E-02                      4.32E-01 569.33           15.37   -3.87E-02                      2.13E-01 604.72           97.62   -4.66E-03                      5.13E-02 795.86           85.46    1.12E-02                      4.51E-02 801.95            8.69    1.73E-01                      4.29E-01 1038.61             0.99    1.39E+00                      4.28E+00 1167.97             1.79    1.92E+00                      2.81E+00 1365.19             3.02   -4.21E-01                      1.43E+00 Cs-137       661.66           85.10   -4.65E-03      4.44E-02        4.44E-02 Eu-152       121.78           28.67   -8.18E-02      1.06E-01        1.11E-01 244.70            7.61    2.31E-01                      4.14E-01 295.94            0.45    8.08E-01                      8.11E+00 344.28           26.60   -1.01E-01                      1.06E-01 367.79            0.86    6.42E-01                      3.31E+00 411.12            2.24   -4.85E-01                      1.29E+00 443.96            2.83   -4.25E-01                      1.06E+00 488.68            0.42    4.84E+00                      7.82E+00 563.99            0.49    3.67E+00                      7.53E+00 586.26            0.46    5.87E+00                      9.76E+00 678.62            0.47    2.79E+00                      5.04E+00 688.67            0.86   -1.14E+00                      3.93E+00 719.35            0.28   -5.29E+00                      1.41E+01 778.90           12.96   -2.21E-01                      2.45E-01 810.45            0.32    8.75E+00                      1.10E+01 867.37            4.26    7.84E-02                      1.09E+00 919.33            0.43   -1.94E+00                      1.04E+01 964.08           14.65    1.28E-01                      3.40E-01 1085.87            10.24   -1.61E-01                      3.95E-01 1089.74             1.73    1.55E+00                      2.63E+00 1112.07            13.69    2.39E-01                      3.08E-01 1212.95             1.43   -2.04E+00                      3.27E+00 1249.94             0.19    4.54E+00                      2.78E+01 1299.14             1.63    1.70E+00                      3.00E+00 1408.01            21.07    8.33E-02                      2.16E-01 1457.64             0.50    8.35E+01                      3.01E+01 1528.10             0.28   -4.30E+00                      9.97E+00 Eu-154       123.07           40.40    1.07E-02      7.92E-02        7.92E-02 247.93            6.89   -1.72E-01                      4.16E-01 591.76            4.95    1.58E-01                      6.77E-01 692.42            1.78    6.36E-01                      2.05E+00 723.30           20.06    1.61E-01                      2.42E-01 756.80            4.52    7.82E-02                      8.55E-01 873.18           12.08    2.30E-01                      4.01E-01
[117]

6/12/2019  12:47:45PM Page 7 of 7 Analysis Report for     12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        2.95E-02      7.92E-02        3.66E-01 1004.76                  18.01        1.04E-01                      1.78E-01 1274.43                  34.80       -6.88E-02                      1.03E-01 1596.48                   1.80       -7.13E-01                      1.90E+00 Eu-155            45.30                  1.31        5.11E+00      1.75E-01        1.74E+01 60.01                  1.22       -1.65E+01                      1.69E+01 86.55                 30.70        9.70E-02                      1.95E-01 105.31                 21.10       -9.10E-02                      1.75E-01
+         Ra-226           186.21
* 3.64        4.85E-01      4.94E-01        4.94E-01 Pa-231            27.36                 10.30        9.15E-01      1.26E+00        1.78E+00 283.69                  1.70       -2.55E-01                      1.65E+00 300.07                  2.47       -1.29E+00                      1.26E+00 302.65                  2.20        8.46E-01                      1.36E+00 330.06                  1.40       -8.48E-01                      2.23E+00
+         U-235            143.76                 10.96       -1.34E-01      3.14E-02        2.68E-01 163.33                  5.08       -1.06E-01                      6.20E-01 185.71
* 57.20        3.09E-02                      3.14E-02 202.11                  1.08       -1.53E+00                      2.67E+00 205.31                  5.01        1.20E-02                      6.05E-01 Am-241            59.54                 35.90       -3.86E-01      5.98E-01        5.98E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[118]

6/12/2019 1:12:57PM Page 1 of 7 Analysis Report for    12-Jun-19-10022 L1-10221C-FSGS-009SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10022 Sample Description                           : L1-10221C-FSGS-009SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.767E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 8:55:00AM Acquisition Started                          : 6/12/2019 12:57:45PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77303 Fill Height                                  : 1766.91 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:12:48PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[119]

6/12/2019   1:12:57PM         Page 2 of 7 Analysis Report for    12-Jun-19-10022 L1-10221C-FSGS-009SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       238.67               473 -    481          477.52          1.33E+02              18.79      9.87E+01           1.21 2       295.39               587 -    593          590.84          4.59E+01              10.20      3.01E+01           1.37 3       338.18               673 -    680          676.33          3.24E+01                9.85     3.16E+01           1.27 4       351.95               698 -    708          703.85          7.71E+01              12.84      3.69E+01           0.85 5       583.11             1160 -   1171         1165.82           7.00E+01              10.00      1.20E+01           0.78 6       609.43             1212 -   1222         1218.45           5.25E+01                9.82     1.85E+01           1.27 7       911.15             1818 -   1828         1821.74           3.53E+01                8.07     1.17E+01           1.54 8      1460.89             2914 -   2928         2921.83           2.59E+02              16.43      3.75E+00           1.77 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              4.70E+00             3.61E-01 Tl-208                   0.99           583.19
* 85.00              8.77E-02             1.36E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              1.83E-01             2.97E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              1.27E-01             2.48E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11                                             [120]

6/12/2019   1:12:57PM         Page 3 of 7 Analysis Report for    12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99        1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42  1.68E-01             3.97E-02 351.93
* 35.60  1.65E-01             3.05E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32
* 11.27  2.13E-01             6.70E-02 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.95E-01             4.53E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[121]

6/12/2019 1:12:57PM          Page 4 of 7 Analysis Report for   12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.999                     4.70E+00              3.61E-01 Tl-208                              0.999                     8.77E-02              1.36E-02 X       Bi-211                              0.882 Pb-212                              1.000                     1.83E-01              2.97E-02 Bi-214                              0.999                     1.27E-01              2.48E-02 Pb-214                              0.999                     1.66E-01              2.42E-02 Ac-228                              0.999                     2.00E-01              3.75E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[122]

6/12/2019   1:12:57PM       Page 5 of 7 Analysis Report for    12-Jun-19-10022 L1-10221C-FSGS-009SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:12:48PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        5.89E-02          4.72E-02        4.72E-02 BE-7            477.60              10.44       2.97E-01          3.49E-01        3.49E-01
+         K-40          1460.82
* 10.66       4.70E+00          2.54E-01        2.54E-01 Mn-54           834.85              99.98       1.44E-03          3.42E-02        3.42E-02 Co-60         1173.23               99.85       2.92E-02          3.99E-02        5.79E-02 1332.49               99.98     -5.65E-04                           3.99E-02 Nb-94           702.65              99.81     -1.48E-02           2.26E-02        2.26E-02 871.09              99.89       5.18E-03                          3.21E-02 Ag-108m          79.13                6.60      5.65E-01          3.43E-02        1.08E+00 433.94              90.50     -2.02E-02                           3.43E-02 614.28              89.80     -2.85E-02                           4.68E-02 722.94              90.80       1.14E-03                          4.04E-02 Sb-125          176.31                6.84      2.42E-01          1.10E-01        4.89E-01 380.45                1.52      2.26E-01                          1.86E+00 427.87              29.60       5.87E-02                          1.10E-01 463.36              10.49       1.12E-01                          3.00E-01 600.60              17.65       4.51E-03                          1.74E-01 606.71                4.98    -8.78E-02                           9.99E-01 635.95              11.22     -7.75E-02                           2.75E-01          [123]

6/12/2019   1:12:57PM Page 6 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.05E+00      1.10E-01        1.72E+00 Ba-133        79.61            2.65    8.93E-01      6.29E-02        2.55E+00 81.00           32.90   -1.29E-01                      1.72E-01 276.40            7.16    1.60E-03                      4.03E-01 302.85           18.34   -3.01E-02                      1.52E-01 356.01           62.05   -1.26E-02                      6.29E-02 383.85            8.94   -3.84E-02                      2.90E-01 Cs-134       475.36            1.48    1.92E+00      4.26E-02        2.51E+00 563.25            8.34    1.07E-02                      3.85E-01 569.33           15.37    1.45E-02                      1.99E-01 604.72           97.62   -1.96E-03                      4.26E-02 795.86           85.46    1.66E-02                      4.51E-02 801.95            8.69   -3.16E-01                      3.50E-01 1038.61             0.99   -3.05E-01                      3.35E+00 1167.97             1.79    2.17E+00                      3.16E+00 1365.19             3.02    6.71E-01                      1.15E+00 Cs-137       661.66           85.10    1.61E-02      4.41E-02        4.41E-02 Eu-152       121.78           28.67    2.06E-02      1.01E-01        1.04E-01 244.70            7.61   -6.65E-02                      4.42E-01 295.94            0.45    5.16E+00                      7.77E+00 344.28           26.60   -1.24E-01                      1.01E-01 367.79            0.86   -1.15E+00                      3.13E+00 411.12            2.24    2.05E-01                      1.27E+00 443.96            2.83   -9.91E-02                      9.83E-01 488.68            0.42   -1.10E+00                      6.28E+00 563.99            0.49   -1.24E+00                      6.28E+00 586.26            0.46   -4.04E+00                      1.12E+01 678.62            0.47    3.80E+00                      6.92E+00 688.67            0.86    1.90E-01                      3.64E+00 719.35            0.28   -4.85E-01                      1.17E+01 778.90           12.96   -3.20E-01                      2.66E-01 810.45            0.32   -3.18E+00                      9.05E+00 867.37            4.26    1.34E-01                      7.12E-01 919.33            0.43   -3.34E-01                      8.65E+00 964.08           14.65   -2.20E-01                      3.19E-01 1085.87            10.24   -2.07E-01                      3.60E-01 1089.74             1.73    3.25E-01                      2.43E+00 1112.07            13.69   -1.83E-01                      3.33E-01 1212.95             1.43    1.16E+00                      3.32E+00 1249.94             0.19    2.98E+00                      2.42E+01 1299.14             1.63   -8.99E-01                      2.41E+00 1408.01            21.07    1.07E-01                      1.74E-01 1457.64             0.50   -2.07E+00                      3.12E+01 1528.10             0.28    6.38E+00                      1.22E+01 Eu-154       123.07           40.40   -3.19E-02      7.17E-02        7.17E-02 247.93            6.89   -1.27E-01                      4.04E-01 591.76            4.95   -2.36E-01                      6.14E-01 692.42            1.78    2.51E-01                      1.77E+00 723.30           20.06    1.15E-02                      1.86E-01 756.80            4.52    3.54E-02                      5.81E-01 873.18           12.08    2.93E-02                      2.52E-01
[124]

6/12/2019   1:12:57PM Page 7 of 7 Analysis Report for     12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -6.92E-02      7.17E-02        3.42E-01 1004.76                  18.01        6.59E-02                      2.09E-01 1274.43                  34.80        6.97E-02                      1.33E-01 1596.48                   1.80        8.94E-02                      1.98E+00 Eu-155            45.30                  1.31       -3.65E-01      1.56E-01        1.00E+01 60.01                  1.22        4.32E+00                      1.14E+01 86.55                 30.70       -1.69E-02                      1.56E-01 105.31                 21.10        7.88E-02                      1.72E-01 Ra-226           186.21                  3.64        4.31E-01      9.09E-01        9.09E-01 Pa-231            27.36                 10.30        1.07E+00      1.15E+00        1.21E+00 283.69                  1.70       -2.38E-01                      1.52E+00 300.07                  2.47       -1.21E+00                      1.15E+00 302.65                  2.20       -2.50E-01                      1.27E+00 330.06                  1.40        8.31E-01                      2.29E+00 U-235            143.76                 10.96       -1.33E-01      5.69E-02        2.37E-01 163.33                  5.08        1.02E-02                      6.39E-01 185.71                 57.20        9.17E-03                      5.69E-02 202.11                  1.08        1.39E+00                      2.87E+00 205.31                  5.01       -5.95E-01                      5.49E-01 Am-241            59.54                 35.90        9.19E-02      3.99E-01        3.99E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[125]

6/12/2019 1:13:04PM Page 1 of 7 Analysis Report for    12-Jun-19-10023 L1-10221C-FSGS-010SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10023 Sample Description                           : L1-10221C-FSGS-010SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.763E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:00:00AM Acquisition Started                          : 6/12/2019 12:57:52PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.3 seconds Dead Time                                    : 0.15 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77304 Fill Height                                  : 1762.74 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:12:55PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[126]

6/12/2019   1:13:04PM         Page 2 of 7 Analysis Report for    12-Jun-19-10023 L1-10221C-FSGS-010SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       238.77               946 -    961          955.17          1.47E+02              18.90      7.04E+01           0.84 2       295.16             1175 -   1188         1180.53           4.99E+01              12.37      3.71E+01           0.66 3       352.04             1400 -   1415         1407.90           8.93E+01              11.42      1.37E+01           1.27 4       583.26             2327 -   2338         2332.27           3.52E+01                7.95     1.08E+01           1.20 5       609.33             2432 -   2445         2436.47           4.79E+01                9.76     1.71E+01           0.40 6       911.43             3638 -   3653         3644.67           4.36E+01                8.37     8.38E+00           0.33 7      1460.90             5832 -   5855         5843.42           3.07E+02              17.88      3.13E+00           1.65 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              7.37E+00             5.36E-01 Tl-208                   0.99           583.19
* 85.00              5.71E-02             1.33E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              2.56E-01             3.90E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.49E-01             3.17E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92                                              [127]

6/12/2019   1:13:04PM         Page 3 of 7 Analysis Report for    12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00        1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42  2.32E-01             6.05E-02 351.93
* 35.60  2.44E-01             3.68E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  3.14E-01             6.18E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[128]

6/12/2019 1:13:04PM          Page 4 of 7 Analysis Report for   12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.999                     7.37E+00              5.36E-01 Tl-208                              0.999                     5.71E-02              1.33E-02 X       Bi-211                              0.860 Pb-212                              0.997                     2.56E-01              3.90E-02 Bi-214                              1.000                     1.49E-01              3.17E-02 Pb-214                              0.999                     2.41E-01              3.14E-02 Ac-228                              0.998                     3.14E-01              6.18E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[129]

6/12/2019   1:13:04PM       Page 5 of 7 Analysis Report for    12-Jun-19-10023 L1-10221C-FSGS-010SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:12:55PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        7.39E-02          5.67E-02        5.67E-02 BE-7            477.60              10.44       3.01E-01          4.38E-01        4.38E-01
+         K-40          1460.82
* 10.66       7.37E+00          3.63E-01        3.63E-01 Mn-54           834.85              99.98     -1.15E-02           5.04E-02        5.04E-02 Co-60         1173.23               99.85     -5.67E-02           5.27E-02        6.51E-02 1332.49               99.98     -4.74E-02                           5.27E-02 Nb-94           702.65              99.81       1.40E-02          4.39E-02        5.25E-02 871.09              99.89     -3.16E-02                           4.39E-02 Ag-108m          79.13                6.60      1.09E+00          4.53E-02        2.06E+00 433.94              90.50     -4.82E-04                           4.53E-02 614.28              89.80     -1.47E-03                           6.36E-02 722.94              90.80     -1.86E-02                           6.14E-02 Sb-125          176.31                6.84      5.92E-02          1.25E-01        5.83E-01 380.45                1.52    -1.74E+00                           2.45E+00 427.87              29.60     -4.59E-02                           1.25E-01 463.36              10.49       3.65E-02                          4.01E-01 600.60              17.65       8.39E-02                          2.65E-01 606.71                4.98    -6.57E-01                           1.42E+00 635.95              11.22       1.93E-01                          3.96E-01          [130]

6/12/2019   1:13:04PM Page 6 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.63E+00      1.25E-01        2.61E+00 Ba-133        79.61            2.65    5.31E+00      7.56E-02        5.04E+00 81.00           32.90   -3.22E-01                      3.34E-01 276.40            7.16    3.55E-02                      5.03E-01 302.85           18.34    2.78E-02                      2.09E-01 356.01           62.05   -7.61E-03                      7.56E-02 383.85            8.94   -2.91E-01                      4.05E-01 Cs-134       475.36            1.48    4.18E-01      5.34E-02        2.93E+00 563.25            8.34    3.73E-01                      4.56E-01 569.33           15.37   -6.62E-03                      2.45E-01 604.72           97.62   -5.48E-02                      6.47E-02 795.86           85.46   -2.19E-02                      5.34E-02 801.95            8.69   -4.43E-01                      4.67E-01 1038.61             0.99    1.63E+00                      5.61E+00 1167.97             1.79    2.40E+00                      3.97E+00 1365.19             3.02   -3.83E-01                      1.33E+00 Cs-137       661.66           85.10    1.43E-02      5.22E-02        5.22E-02 Eu-152       121.78           28.67    5.75E-02      1.46E-01        1.77E-01 244.70            7.61    5.08E-01                      6.04E-01 295.94            0.45    2.10E+00                      1.08E+01 344.28           26.60   -2.66E-02                      1.46E-01 367.79            0.86   -4.24E-01                      4.47E+00 411.12            2.24   -2.15E+00                      1.65E+00 443.96            2.83   -5.14E-01                      1.42E+00 488.68            0.42    2.45E+00                      9.43E+00 563.99            0.49    9.19E-01                      7.62E+00 586.26            0.46    6.23E+00                      1.27E+01 678.62            0.47    4.93E+00                      8.68E+00 688.67            0.86    6.43E-01                      4.99E+00 719.35            0.28    4.12E+00                      1.84E+01 778.90           12.96   -1.06E-01                      3.65E-01 810.45            0.32   -4.01E-01                      1.56E+01 867.37            4.26    3.27E-01                      1.00E+00 919.33            0.43   -3.97E+00                      1.27E+01 964.08           14.65   -2.32E-01                      3.73E-01 1085.87            10.24    2.96E-01                      6.46E-01 1089.74             1.73    5.12E-01                      3.47E+00 1112.07            13.69    7.75E-03                      4.09E-01 1212.95             1.43    9.04E-01                      5.05E+00 1249.94             0.19    1.93E+01                      3.74E+01 1299.14             1.63    7.76E-01                      3.88E+00 1408.01            21.07   -5.02E-02                      2.38E-01 1457.64             0.50    1.59E+02                      4.48E+01 1528.10             0.28   -2.27E+00                      1.05E+01 Eu-154       123.07           40.40    3.68E-02      1.24E-01        1.24E-01 247.93            6.89   -1.76E-01                      5.50E-01 591.76            4.95   -2.56E-01                      9.01E-01 692.42            1.78   -3.93E-01                      2.72E+00 723.30           20.06    1.17E-02                      2.84E-01 756.80            4.52    1.15E-01                      9.39E-01 873.18           12.08   -2.31E-01                      4.01E-01
[131]

6/12/2019   1:13:04PM Page 7 of 7 Analysis Report for     12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        6.41E-02      1.24E-01        4.58E-01 1004.76                  18.01        1.63E-01                      3.01E-01 1274.43                  34.80       -1.61E-02                      1.91E-01 1596.48                   1.80       -2.78E+00                      1.47E+00 Eu-155            45.30                  1.31       -3.25E-01      2.67E-01        3.08E+01 60.01                  1.22       -3.65E+00                      2.87E+01 86.55                 30.70        9.27E-02                      2.86E-01 105.31                 21.10       -1.49E-01                      2.67E-01 Ra-226           186.21                  3.64        7.94E-01      1.21E+00        1.21E+00 Pa-231            27.36                 10.30        3.89E+00      1.66E+00        3.96E+00 283.69                  1.70        8.77E-01                      2.15E+00 300.07                  2.47       -3.56E-01                      1.66E+00 302.65                  2.20        3.57E-01                      1.74E+00 330.06                  1.40        1.80E+00                      3.00E+00 U-235            143.76                 10.96       -1.48E-01      7.50E-02        3.94E-01 163.33                  5.08        9.19E-04                      7.82E-01 185.71                 57.20        1.41E-02                      7.50E-02 202.11                  1.08        2.79E-02                      3.51E+00 205.31                  5.01       -4.56E-01                      7.02E-01 Am-241            59.54                 35.90       -1.19E-01      1.03E+00        1.03E+00
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[132]

6/12/2019 1:13:27PM Page 1 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10024 Sample Description                           : L1-10221C-FSGS-011SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.687E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:05:00AM Acquisition Started                          : 6/12/2019 12:57:59PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.04 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77305 Fill Height                                  : 1686.99 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:13:20PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[133]

6/12/2019   1:13:27PM         Page 2 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1         77.33              306 -    314          309.83          5.73E+01              16.04      9.28E+01           0.48 2       238.76               948 -    961          954.63          1.64E+02              21.36      1.02E+02           1.01 3       295.23             1173 -   1186         1180.21           8.42E+01              14.30      4.38E+01           0.38 4       338.29             1346 -   1358         1352.26           4.04E+01              11.23      3.26E+01           0.82 5       351.93             1398 -   1413         1406.74           1.38E+02              14.71      2.61E+01           0.93 6       582.94             2324 -   2337         2329.88           5.73E+01                9.89     1.47E+01           0.78 7       609.17             2428 -   2441         2434.74           9.94E+01              11.93      1.56E+01           1.07 8       910.83             3634 -   3648         3640.76           5.69E+01                8.45     5.10E+00           1.11 9      1460.33             5828 -   5851         5839.28           3.86E+02              20.18      5.52E+00           1.90 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.96          1460.82
* 10.66              8.44E+00             5.73E-01 Tl-208                   0.99           583.19
* 85.00              8.44E-02             1.54E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              2.56E-01             3.93E-02 300.09                    3.30 Pb212-XR                 0.99            74.82                  10.28 77.11
* 17.10              3.98E-01             1.19E-01 87.35                    3.97                                             [134]

6/12/2019   1:13:27PM         Page 3 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Pb212-XR                 0.99            89.78                1.46 Bi-214                   0.99         609.32
* 45.49  2.82E-01             3.78E-02 768.36                  4.89 806.18                  1.26 934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00         241.99                  7.25 295.22
* 18.42  3.54E-01             6.64E-02 351.93
* 35.60  3.41E-01             4.54E-02 785.96                  1.06 Pb214-XR                 0.99            74.82                5.80 77.11
* 9.70  7.02E-01             2.12E-01 87.35                2.24 89.78                0.82 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32
* 11.27  3.07E-01             8.88E-02 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  3.73E-01             5.78E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
[135]

6/12/2019 1:13:27PM          Page 4 of 7 Analysis Report for   12-Jun-19-10024 L1-10221C-FSGS-011SS INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.963                     8.44E+00              5.73E-01 Tl-208                              0.990                     8.44E-02              1.54E-02 X       Bi-211                              0.888 Pb-212                              0.997                     2.56E-01              3.93E-02
     ?       Pb212-XR                            0.996                     3.98E-01              1.19E-01 Bi-214                              0.999                     2.82E-01              3.78E-02 Pb-214                              1.000                     3.45E-01              3.75E-02
     ?       Pb214-XR                            0.996                     7.02E-01              2.12E-01 Ac-228                              0.993                     3.53E-01              4.84E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[136]

6/12/2019   1:13:27PM       Page 5 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:13:20PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        9.09E-02          6.58E-02        6.58E-02 BE-7            477.60              10.44       1.83E-01          3.87E-01        3.87E-01
+         K-40          1460.82
* 10.66       8.44E+00          4.01E-01        4.01E-01 Mn-54           834.85              99.98       1.74E-03          5.54E-02        5.54E-02 Co-60         1173.23               99.85       7.42E-02          5.73E-02        7.23E-02 1332.49               99.98       3.70E-02                          5.73E-02 Nb-94           702.65              99.81     -1.11E-03           4.67E-02        4.67E-02 871.09              99.89       3.42E-02                          5.51E-02 Ag-108m          79.13                6.60    -4.21E-01           4.41E-02        1.31E+00 433.94              90.50     -2.76E-03                           4.41E-02 614.28              89.80     -6.12E-02                           5.69E-02 722.94              90.80       2.14E-02                          5.81E-02 Sb-125          176.31                6.84      1.19E-01          1.37E-01        5.00E-01 380.45                1.52      6.09E-01                          2.51E+00 427.87              29.60     -3.13E-02                           1.37E-01 463.36              10.49       2.23E-02                          4.32E-01 600.60              17.65       2.52E-01                          2.71E-01 606.71                4.98      3.11E+00                          1.54E+00 635.95              11.22     -1.90E-01                           3.65E-01          [137]

6/12/2019   1:13:27PM Page 6 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -7.59E-01      1.37E-01        2.18E+00 Ba-133        79.61            2.65   -1.17E+00      7.13E-02        3.18E+00 81.00           32.90   -2.83E-01                      2.02E-01 276.40            7.16    2.22E-02                      5.28E-01 302.85           18.34    5.13E-02                      2.05E-01 356.01           62.05   -1.35E-02                      7.13E-02 383.85            8.94    1.40E-01                      4.32E-01 Cs-134       475.36            1.48   -2.23E-02      5.58E-02        2.66E+00 563.25            8.34   -1.24E-01                      5.88E-01 569.33           15.37   -1.35E-01                      2.54E-01 604.72           97.62   -1.09E-02                      6.97E-02 795.86           85.46    2.09E-02                      5.58E-02 801.95            8.69    1.28E-01                      5.44E-01 1038.61             0.99    1.59E+00                      5.52E+00 1167.97             1.79   -1.99E-03                      3.78E+00 1365.19             3.02   -6.98E-01                      1.62E+00 Cs-137       661.66           85.10    2.30E-02      6.06E-02        6.06E-02 Eu-152       121.78           28.67   -3.65E-02      1.25E-01        1.25E-01 244.70            7.61    1.90E-01                      5.43E-01 295.94            0.45    2.40E+00                      1.12E+01 344.28           26.60   -6.34E-02                      1.37E-01 367.79            0.86    2.61E+00                      3.81E+00 411.12            2.24   -3.82E-01                      1.69E+00 443.96            2.83   -4.34E-01                      1.40E+00 488.68            0.42    4.20E+00                      1.01E+01 563.99            0.49   -1.34E+01                      9.09E+00 586.26            0.46   -2.91E+00                      1.32E+01 678.62            0.47    6.84E+00                      8.95E+00 688.67            0.86    2.64E+00                      5.10E+00 719.35            0.28   -1.25E+01                      1.44E+01 778.90           12.96    5.96E-02                      3.42E-01 810.45            0.32   -1.83E+01                      1.18E+01 867.37            4.26   -5.17E-01                      1.27E+00 919.33            0.43    6.49E+00                      1.12E+01 964.08           14.65    4.38E-01                      5.09E-01 1085.87            10.24   -1.53E-01                      5.16E-01 1089.74             1.73    1.46E+00                      3.26E+00 1112.07            13.69   -1.63E-01                      4.41E-01 1212.95             1.43    7.16E-01                      5.46E+00 1249.94             0.19    6.99E+00                      3.58E+01 1299.14             1.63   -6.26E-03                      3.27E+00 1408.01            21.07    2.14E-02                      2.56E-01 1457.64             0.50    1.72E+02                      4.56E+01 1528.10             0.28   -3.63E+00                      1.48E+01 Eu-154       123.07           40.40   -4.03E-02      9.00E-02        9.00E-02 247.93            6.89   -4.01E-01                      4.84E-01 591.76            4.95    1.03E-01                      8.19E-01 692.42            1.78   -9.17E-02                      2.57E+00 723.30           20.06    1.45E-01                      2.71E-01 756.80            4.52   -3.49E-01                      1.03E+00 873.18           12.08   -1.39E-01                      4.52E-01
[138]

6/12/2019   1:13:27PM Page 7 of 7 Analysis Report for     12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        2.34E-01      9.00E-02        5.83E-01 1004.76                  18.01        9.49E-02                      2.93E-01 1274.43                  34.80        6.51E-02                      2.04E-01 1596.48                   1.80       -1.87E+00                      2.16E+00 Eu-155            45.30                  1.31        5.55E+00      2.28E-01        1.41E+01 60.01                  1.22       -1.41E+00                      1.30E+01 86.55                 30.70        1.44E-01                      2.30E-01 105.31                 21.10       -5.85E-02                      2.28E-01 Ra-226           186.21                  3.64        1.08E+00      1.12E+00        1.12E+00 Pa-231            27.36                 10.30        4.88E-01      1.49E+00        1.49E+00 283.69                  1.70        8.75E-01                      2.16E+00 300.07                  2.47       -1.44E+00                      1.55E+00 302.65                  2.20        4.32E-01                      1.70E+00 330.06                  1.40        1.92E-02                      2.99E+00 U-235            143.76                 10.96        1.37E-01      7.10E-02        3.48E-01 163.33                  5.08        4.42E-01                      7.31E-01 185.71                 57.20        8.13E-02                      7.10E-02 202.11                  1.08        1.77E-01                      3.10E+00 205.31                  5.01       -5.34E-01                      6.42E-01 Am-241            59.54                 35.90       -1.72E-01      4.41E-01        4.41E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[139]

6/13/2019 6:00:00AM Page 1 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10024 Sample Description                           : L1-10221C-FSGS-011SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.687E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:05:00AM Acquisition Started                          : 6/12/2019 12:57:59PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 1800.0 seconds Real Time                                    : 1800.7 seconds Dead Time                                    : 0.04 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/13/2019 Efficiency Calibration Description           :
Sample Number                                : 77305 Fill Height                                  : 1686.99 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/13/2019 5:59:52AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[140]

6/13/2019   6:00:00AM         Page 2 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area    Continuum          FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty       Counts           (keV) 1         77.38              307 -    316          310.04          1.20E+02              23.43     1.85E+02            0.61 2         90.16              359 -    365          361.09          3.45E+01              15.09     1.02E+02            0.32 3       186.33               737 -    752          745.18          1.24E+02              24.65     1.61E+02            0.61 4       238.76               948 -    960          954.63          3.99E+02              29.29     1.73E+02            1.02 5       295.27             1173 -   1188         1180.35           1.47E+02              21.98     1.12E+02            0.65 6       338.32             1346 -   1359         1352.36           6.73E+01              16.66     7.57E+01            0.76 7       351.97             1402 -   1413         1406.87           2.90E+02              20.11     4.57E+01            1.06 8       488.01             1946 -   1955         1950.48           1.57E+01                8.59    2.53E+01            0.30 9       511.03             2032 -   2049         2042.49           8.21E+01              18.44     7.89E+01            1.00 10        558.64             2226 -   2241         2232.77           3.37E+01              12.48     4.03E+01            0.62 11        583.01             2323 -   2338         2330.16           1.27E+02              14.93     3.21E+01            1.24 12        609.21             2428 -   2442         2434.87           1.90E+02              17.36     3.88E+01            0.89 13        910.88             3633 -   3650         3640.97           1.08E+02              12.66     1.62E+01            1.48 14        933.72             3726 -   3738         3732.31           1.50E+01                7.96    1.80E+01            0.56 15        968.81             3863 -   3880         3872.64           4.85E+01              12.33     3.15E+01            0.64 16       1120.39             4471 -   4487         4478.96           4.98E+01              10.79     2.13E+01            0.61 17       1460.32             5826 -   5851         5839.20           8.02E+02              30.22     2.60E+01            1.93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                Energy              Yield(%)                   Activity           Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty
[141]

6/13/2019   6:00:00AM         Page 3 of 7 Analysis Report for  12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide             Id               Energy   Yield(%)      Activity           Activity Name             Confidence           (keV)            (pCi/grams)          Uncertainty An Pk                  1.00         511.00
* 100.00   4.78E-02             1.12E-02 K-40                   0.96       1460.82
* 10.66  8.76E+00             5.04E-01 Tl-208                 0.99         583.19
* 85.00  9.35E-02             1.23E-02 Pb-212                 0.99         115.18        0.60 238.63
* 43.60  3.12E-01             3.40E-02 300.09        3.30 Pb212-XR               0.99          74.82       10.28 77.11
* 17.10  4.18E-01             9.20E-02 87.35        3.97 89.78
* 1.46  1.01E+00             4.54E-01 Bi-214                 0.99         609.32
* 45.49  2.70E-01             2.95E-02 768.36        4.89 806.18        1.26 934.06
* 3.11  4.16E-01             2.21E-01 1120.29
* 14.92  3.24E-01             7.14E-02 1155.21         1.63 1238.12         5.83 1280.98         1.43 1377.67         3.99 1385.31         0.79 1401.52         1.33 1407.99         2.39 1509.21         2.13 1661.27         1.05 1729.59         2.88 1764.49        15.30 1847.43         2.03 2118.51         1.16 Pb-214                 1.00         241.99        7.25 295.22
* 18.42  3.09E-01             5.24E-02 351.93
* 35.60  3.59E-01             3.80E-02 785.96        1.06 Ra-226                 0.99         186.21
* 3.64  1.02E+00             2.19E-01 Ac-228                 0.99         129.07        2.42 209.25        3.89 270.24        3.46 328.00        2.95 338.32
* 11.27  2.55E-01             6.65E-02 409.46        1.92 463.00        4.40 794.95        4.25 911.20
* 25.80  3.54E-01             4.43E-02 964.77        4.99 968.97
* 15.80  2.71E-01             6.99E-02 1588.20         3.22 U-235                  0.95         143.76       10.96 163.33        5.08 185.71
* 57.20  6.50E-02             1.39E-02 202.11        1.08 205.31        5.01
[142]

6/13/2019 6:00:00AM          Page 4 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
An Pk                               1.000                     4.78E-02              1.12E-02 K-40                                0.960                     8.76E+00              5.04E-01 Tl-208                              0.995                     9.35E-02              1.23E-02 X       Bi-211                              0.880 Pb-212                              0.998                     3.12E-01              3.40E-02 Pb212-XR                            0.993                     4.41E-01              9.01E-02 Bi-214                              0.998                     2.80E-01              2.70E-02 Pb-214                              1.000                     3.42E-01              3.07E-02 X       Pb214-XR                            0.993
      ?       Ra-226                              0.998                     1.02E+00              2.19E-01 Ac-228                              0.994                     3.12E-01              3.26E-02 X       Ac228-XR                            0.998 X       Th-231                              0.315
      ?       U-235                               0.958                     6.50E-02              1.39E-02 X       U235-XR                             0.998
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[143]

6/13/2019   6:00:00AM       Page 5 of 7 Analysis Report for    12-Jun-19-10024 L1-10221C-FSGS-011SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/13/2019 5:59:52AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide 8            488.01              8.71951E-03                     54.70          Tol.        Eu-152 10             558.64              1.87275E-02                     37.04 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
+         An Pk           511.00
* 100.00        4.78E-02          3.34E-02        3.34E-02 BE-7            477.60              10.44       1.68E-01          2.84E-01        2.84E-01
+         K-40          1460.82
* 10.66       8.76E+00          4.23E-01        4.23E-01 Mn-54           834.85              99.98       7.31E-03          3.76E-02        3.76E-02 Co-60         1173.23               99.85       5.21E-02          3.77E-02        4.92E-02 1332.49               99.98       2.02E-02                          3.77E-02 Nb-94           702.65              99.81       4.88E-03          3.37E-02        3.37E-02 871.09              99.89       1.71E-02                          3.69E-02 Ag-108m          79.13                6.60      1.60E-01          2.99E-02        9.24E-01 433.94              90.50     -1.33E-02                           2.99E-02 614.28              89.80     -2.57E-02                           4.25E-02 722.94              90.80     -1.09E-02                           3.94E-02 Sb-125          176.31                6.84      4.27E-02          9.52E-02        3.54E-01 380.45                1.52    -5.90E-02                           1.74E+00 427.87              29.60       2.74E-02                          9.52E-02 463.36              10.49       9.70E-02                          2.88E-01 600.60              17.65       3.22E-02                          1.73E-01          [144]

6/13/2019   6:00:00AM Page 6 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       606.71            4.98    3.09E+00      9.52E-02        1.08E+00 635.95           11.22   -3.01E-02                      2.46E-01 671.44            1.79   -9.10E-02                      1.71E+00 Ba-133        79.61            2.65    5.26E-01      5.27E-02        2.26E+00 81.00           32.90   -1.18E-01                      1.42E-01 276.40            7.16    2.50E-01                      3.77E-01 302.85           18.34    1.64E-02                      1.43E-01 356.01           62.05   -5.15E-02                      5.27E-02 383.85            8.94   -1.20E-01                      3.05E-01 Cs-134       475.36            1.48   -7.96E-01      4.02E-02        1.86E+00 563.25            8.34   -4.23E-02                      4.01E-01 569.33           15.37   -7.81E-02                      1.76E-01 604.72           97.62   -2.07E-02                      4.76E-02 795.86           85.46    3.65E-02                      4.02E-02 801.95            8.69    3.33E-01                      3.79E-01 1038.61             0.99    6.51E-01                      3.53E+00 1167.97             1.79   -1.62E+00                      2.40E+00 1365.19             3.02   -4.52E-01                      9.86E-01 Cs-137       661.66           85.10    4.53E-03      4.04E-02        4.04E-02 Eu-152       121.78           28.67   -4.88E-02      8.89E-02        8.89E-02 244.70            7.61    2.47E-02                      3.90E-01 295.94            0.45    1.04E+01                      7.84E+00 344.28           26.60   -8.02E-02                      9.47E-02 367.79            0.86    1.01E+00                      2.74E+00 411.12            2.24    2.95E-01                      1.28E+00 443.96            2.83    9.63E-02                      9.59E-01 488.68            0.42    2.48E-02                      6.73E+00 563.99            0.49    9.85E-01                      6.28E+00 586.26            0.46   -2.56E+00                      9.40E+00 678.62            0.47    4.14E+00                      6.57E+00 688.67            0.86   -4.32E-01                      3.44E+00 719.35            0.28   -6.91E+00                      1.07E+01 778.90           12.96   -5.26E-02                      2.46E-01 810.45            0.32   -9.64E+00                      9.52E+00 867.37            4.26   -2.55E-01                      8.58E-01 919.33            0.43    7.17E+00                      8.21E+00 964.08           14.65    1.36E-01                      3.51E-01 1085.87            10.24    3.83E-02                      4.02E-01 1089.74             1.73    5.14E-01                      2.43E+00 1112.07            13.69   -1.49E-01                      3.25E-01 1212.95             1.43    1.09E+00                      3.73E+00 1249.94             0.19    1.31E+01                      2.54E+01 1299.14             1.63   -6.58E-02                      2.42E+00 1408.01            21.07    4.57E-02                      1.61E-01 1457.64             0.50    1.85E+02                      3.29E+01 1528.10             0.28   -1.53E+00                      9.44E+00 Eu-154       123.07           40.40   -3.14E-02      6.36E-02        6.36E-02 247.93            6.89   -3.49E-01                      3.60E-01 591.76            4.95   -1.26E-01                      5.46E-01 692.42            1.78   -4.22E-01                      1.73E+00 723.30           20.06   -4.78E-02                      1.82E-01
[145]

6/13/2019   6:00:00AM Page 7 of 7 Analysis Report for     12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           756.80                  4.52       -5.31E-01      6.36E-02        6.81E-01 873.18                 12.08        8.50E-03                      3.11E-01 996.29                 10.48        3.24E-01                      3.86E-01 1004.76                  18.01       -7.96E-03                      2.02E-01 1274.43                  34.80       -9.17E-02                      1.20E-01 1596.48                   1.80       -8.58E-01                      1.40E+00 Eu-155            45.30                  1.31        4.23E+00      1.56E-01        9.56E+00 60.01                  1.22       -4.68E+00                      9.48E+00 86.55                 30.70        1.47E-01                      1.56E-01 105.31                 21.10       -1.00E-02                      1.57E-01
+         Ra-226           186.21
* 3.64        1.02E+00      6.37E-01        6.37E-01 Pa-231            27.36                 10.30        7.95E-01      1.04E+00        1.04E+00 283.69                  1.70        1.43E-01                      1.44E+00 300.07                  2.47        2.05E-01                      1.10E+00 302.65                  2.20        1.82E-01                      1.19E+00 330.06                  1.40        1.58E+00                      2.09E+00
+         U-235            143.76                 10.96       -2.01E-02      4.05E-02        2.41E-01 163.33                  5.08        4.48E-01                      5.24E-01 185.71
* 57.20        6.50E-02                      4.05E-02 202.11                  1.08       -1.25E+00                      2.20E+00 205.31                  5.01       -2.61E-01                      4.78E-01 Am-241            59.54                 35.90       -7.93E-02      3.31E-01        3.31E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[146]

6/12/2019 1:13:21PM Page 1 of 7 Analysis Report for    12-Jun-19-10025 L1-10221C-FSGS-012SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10025 Sample Description                           : L1-10221C-FSGS-012SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.409E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:10:00AM Acquisition Started                          : 6/12/2019 12:58:06PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.04 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77306 Fill Height                                  : 1408.71 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:13:12PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[147]

6/12/2019   1:13:21PM         Page 2 of 7 Analysis Report for    12-Jun-19-10025 L1-10221C-FSGS-012SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       186.12               739 -    749          745.22          4.23E+01              14.01      6.47E+01           0.50 M      2       238.64               949 -    975          955.02          1.94E+02              14.73      5.28E+01           1.06 m      3       241.80               949 -    975          967.67          4.67E+01                8.62     5.74E+01           1.06 4       295.17             1174 -   1188         1180.88           7.50E+01              13.18      3.40E+01           1.36 5       351.75             1401 -   1413         1407.00           1.25E+02              14.90      3.70E+01           1.20 6       583.15             2326 -   2339         2331.93           7.13E+01              12.28      2.87E+01           1.22 7       609.21             2427 -   2443         2436.09           1.18E+02              13.10      1.71E+01           0.55 8       661.56             2636 -   2655         2645.43           2.01E+02              16.47      2.00E+01           1.47 9       910.96             3633 -   3650         3642.87           6.40E+01                9.67     8.99E+00           0.36 10       1460.37             5828 -   5857         5841.86           4.41E+02              22.07      1.04E+01           2.01 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.96          1460.82
* 10.66              9.45E+00             6.26E-01 Cs-137                   0.99           661.66
* 85.10              3.18E-01             3.23E-02 Tl-208                   1.00           583.19
* 85.00              1.04E-01             1.90E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              3.09E-01             3.43E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              3.31E-01             4.18E-02[148]

6/12/2019   1:13:21PM         Page 3 of 7 Analysis Report for    12-Jun-19-10025 L1-10221C-FSGS-012SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99         768.36                  4.89 806.18                  1.26 934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99
* 7.25  4.50E-01             9.05E-02 295.22
* 18.42  3.17E-01             6.13E-02 351.93
* 35.60  3.09E-01             4.44E-02 785.96                  1.06 Ra-226                   0.99         186.21
* 3.64  7.20E-01             2.46E-01 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  4.14E-01             6.49E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22 U-235                    0.98         143.76                 10.96 163.33                  5.08 185.71
* 57.20  4.58E-02             1.56E-02 202.11                  1.08 205.31                  5.01
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
[149]

6/12/2019 1:13:21PM          Page 4 of 7 Analysis Report for   12-Jun-19-10025 L1-10221C-FSGS-012SS INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.968                     9.45E+00              6.26E-01 Cs-137                              0.999                     3.18E-01              3.23E-02 Tl-208                              1.000                     1.04E-01              1.90E-02 X       Bi-211                              0.928 Pb-212                              1.000                     3.09E-01              3.43E-02 Bi-214                              0.999                     3.31E-01              4.18E-02 Pb-214                              0.996                     3.31E-01              3.34E-02
     ?       Ra-226                              0.999                     7.20E-01              2.46E-01 Ac-228                              0.997                     4.14E-01              6.49E-02
     ?       U-235                               0.981                     4.58E-02              1.56E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[150]

6/12/2019   1:13:21PM       Page 5 of 7 Analysis Report for    12-Jun-19-10025 L1-10221C-FSGS-012SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:13:12PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.41E-02          6.18E-02        6.18E-02 BE-7            477.60              10.44     -1.77E-01           4.06E-01        4.06E-01
+         K-40          1460.82
* 10.66       9.45E+00          5.57E-01        5.57E-01 Mn-54           834.85              99.98     -1.36E-02           5.35E-02        5.35E-02 Co-60         1173.23               99.85       2.59E-02          7.33E-02        8.00E-02 1332.49               99.98     -3.18E-03                           7.33E-02 Nb-94           702.65              99.81       1.69E-02          4.71E-02        5.08E-02 871.09              99.89     -4.22E-02                           4.71E-02 Ag-108m          79.13                6.60    -4.47E-01           4.87E-02        1.81E+00 433.94              90.50     -1.36E-02                           4.87E-02 614.28              89.80     -2.11E-02                           8.29E-02 722.94              90.80     -1.19E-02                           5.95E-02 Sb-125          176.31                6.84      2.98E-01          1.42E-01        5.95E-01 380.45                1.52      1.10E+00                          2.69E+00 427.87              29.60     -4.51E-02                           1.42E-01 463.36              10.49       2.20E-01                          4.25E-01 600.60              17.65       4.12E-02                          2.80E-01 606.71                4.98      2.70E+00                          1.66E+00 635.95              11.22     -1.26E-01                           3.94E-01          [151]

6/12/2019   1:13:21PM Page 6 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    3.35E-01      1.42E-01        2.28E+00 Ba-133        79.61            2.65    9.30E-01      9.13E-02        4.39E+00 81.00           32.90   -7.55E-01                      2.89E-01 276.40            7.16   -5.89E-02                      6.07E-01 302.85           18.34    1.75E-01                      2.43E-01 356.01           62.05   -6.35E-02                      9.13E-02 383.85            8.94    3.67E-02                      4.60E-01 Cs-134       475.36            1.48   -1.10E+00      6.38E-02        2.87E+00 563.25            8.34    3.35E-01                      5.30E-01 569.33           15.37   -1.37E-01                      3.18E-01 604.72           97.62   -3.05E-02                      8.10E-02 795.86           85.46    5.26E-02                      6.38E-02 801.95            8.69   -6.84E-01                      5.72E-01 1038.61             0.99   -3.19E-01                      5.81E+00 1167.97             1.79    4.69E-01                      4.55E+00 1365.19             3.02    1.01E+00                      1.83E+00
+         Cs-137       661.66
* 85.10    3.18E-01      4.96E-02        4.96E-02 Eu-152       121.78           28.67   -3.61E-02      1.58E-01        1.62E-01 244.70            7.61   -2.14E-02                      6.03E-01 295.94            0.45    1.40E+01                      1.15E+01 344.28           26.60   -6.86E-02                      1.58E-01 367.79            0.86    7.91E-02                      4.94E+00 411.12            2.24    4.31E-02                      1.90E+00 443.96            2.83    3.19E-01                      1.64E+00 488.68            0.42   -5.78E+00                      1.06E+01 563.99            0.49   -3.75E+00                      8.75E+00 586.26            0.46    1.35E+01                      1.56E+01 678.62            0.47   -1.46E+00                      8.60E+00 688.67            0.86    5.56E-01                      5.53E+00 719.35            0.28    2.55E-01                      1.68E+01 778.90           12.96   -6.66E-01                      3.71E-01 810.45            0.32   -6.95E+00                      1.59E+01 867.37            4.26   -1.02E+00                      1.13E+00 919.33            0.43   -1.37E+01                      1.07E+01 964.08           14.65    4.45E-01                      4.76E-01 1085.87            10.24    1.96E-01                      6.65E-01 1089.74             1.73    1.52E-01                      4.16E+00 1112.07            13.69   -2.99E-03                      4.81E-01 1212.95             1.43    2.47E+00                      5.55E+00 1249.94             0.19   -9.42E+00                      3.56E+01 1299.14             1.63   -6.04E+00                      3.71E+00 1408.01            21.07   -1.76E-01                      2.51E-01 1457.64             0.50    2.08E+02                      4.79E+01 1528.10             0.28    1.17E+01                      1.75E+01 Eu-154       123.07           40.40    6.97E-02      1.16E-01        1.16E-01 247.93            6.89   -3.47E-01                      5.70E-01 591.76            4.95   -1.86E-01                      9.14E-01 692.42            1.78   -4.11E-01                      2.77E+00 723.30           20.06    2.44E-02                      2.69E-01 756.80            4.52   -6.04E-01                      1.01E+00 873.18           12.08    3.73E-02                      4.08E-01
[152]

6/12/2019   1:13:21PM Page 7 of 7 Analysis Report for     12-Jun-19-10025 L1-10221C-FSGS-012SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        2.52E-01      1.16E-01        6.03E-01 1004.76                  18.01        2.20E-01                      3.24E-01 1274.43                  34.80        2.05E-01                      2.00E-01 1596.48                   1.80        1.00E+00                      2.75E+00 Eu-155            45.30                  1.31        7.93E+00      2.55E-01        2.40E+01 60.01                  1.22        2.16E+01                      2.64E+01 86.55                 30.70       -8.63E-02                      2.58E-01 105.31                 21.10        1.54E-02                      2.55E-01
+         Ra-226           186.21
* 3.64        7.20E-01      7.66E-01        7.66E-01 Pa-231            27.36                 10.30        2.77E+00      1.87E+00        2.69E+00 283.69                  1.70       -2.35E-01                      2.55E+00 300.07                  2.47        1.18E+00                      1.87E+00 302.65                  2.20        1.38E+00                      2.01E+00 330.06                  1.40       -1.37E+00                      2.91E+00
+         U-235            143.76                 10.96       -1.87E-01      4.88E-02        3.98E-01 163.33                  5.08       -4.49E-01                      7.84E-01 185.71
* 57.20        4.58E-02                      4.88E-02 202.11                  1.08       -2.32E+00                      3.86E+00 205.31                  5.01       -2.85E-01                      8.74E-01 Am-241            59.54                 35.90       -5.22E-01      8.95E-01        8.95E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[153]

6/12/2019 1:33:25PM Page 1 of 7 Analysis Report for    12-Jun-19-10026 L1-10221C-FQGS-012SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10026 Sample Description                           : L1-10221C-FQGS-012SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.593E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:10:00AM Acquisition Started                          : 6/12/2019 1:18:13PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.4 seconds Dead Time                                    : 0.04 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77307 Fill Height                                  : 1592.65 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:33:16PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[154]

6/12/2019   1:33:25PM         Page 2 of 7 Analysis Report for    12-Jun-19-10026 L1-10221C-FQGS-012SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1         77.06              305 -    317          309.56          4.50E+01              16.40      7.50E+01           0.80 2       185.86               740 -    752          744.15          6.12E+01              15.70      6.88E+01           0.86 3       238.61               946 -    960          954.92          1.85E+02              21.99      1.04E+02           0.74 4       295.12             1173 -   1188         1180.72           7.57E+01              15.09      5.03E+01           0.76 5       351.79             1398 -   1413         1407.17           1.27E+02              16.39      4.75E+01           0.96 6       583.14             2325 -   2341         2331.88           9.89E+01              11.23      9.11E+00           1.65 7       609.27             2428 -   2443         2436.33           1.21E+02              13.68      2.19E+01           0.86 8       661.50             2637 -   2651         2645.16           9.87E+01              11.19      9.26E+00           1.55 9       910.96             3636 -   3650         3642.88           5.24E+01                9.11     1.06E+01           1.47 10       1120.18             4474 -   4486         4479.99           2.61E+01                7.93     1.39E+01           0.53 11       1460.47             5828 -   5854         5842.26           4.78E+02              22.21      3.47E+00           2.15 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.98          1460.82
* 10.66              9.89E+00             6.29E-01 Cs-137                   0.99           661.66
* 85.10              1.52E-01             1.95E-02 Tl-208                   1.00           583.19
* 85.00              1.40E-01             1.80E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              2.87E-01             4.13E-02 300.09                    3.30                                             [155]

6/12/2019   1:33:25PM         Page 3 of 7 Analysis Report for  12-Jun-19-10026 L1-10221C-FQGS-012SS Nuclide             Id               Energy   Yield(%)      Activity           Activity Name             Confidence           (keV)            (pCi/grams)          Uncertainty Pb212-XR               1.00          74.82       10.28 77.11
* 17.10  4.19E-01             1.59E-01 87.35        3.97 89.78        1.46 Bi-214                 1.00         609.32
* 45.49  3.30E-01             4.22E-02 768.36        4.89 806.18        1.26 934.06        3.11 1120.29
* 14.92  3.23E-01             9.90E-02 1155.21         1.63 1238.12         5.83 1280.98         1.43 1377.67         3.99 1385.31         0.79 1401.52         1.33 1407.99         2.39 1509.21         2.13 1661.27         1.05 1729.59         2.88 1764.49        15.30 1847.43         2.03 2118.51         1.16 Pb-214                 0.99         241.99        7.25 295.22
* 18.42  3.13E-01             6.71E-02 351.93
* 35.60  3.05E-01             4.65E-02 785.96        1.06 Pb214-XR               1.00          74.82        5.80 77.11
* 9.70  7.38E-01             2.82E-01 87.35        2.24 89.78        0.82 Ra-226                 0.98         186.21
* 3.64  1.02E+00             2.74E-01 Ac-228                 0.99         129.07        2.42 209.25        3.89 270.24        3.46 328.00        2.95 338.32       11.27 409.46        1.92 463.00        4.40 794.95        4.25 911.20
* 25.80  3.28E-01             5.87E-02 964.77        4.99 968.97       15.80 1588.20         3.22 U-235                  0.99         143.76       10.96 163.33        5.08 185.71
* 57.20  6.49E-02             1.75E-02 202.11        1.08 205.31        5.01
[156]

6/12/2019 1:33:25PM          Page 4 of 7 Analysis Report for    12-Jun-19-10026 L1-10221C-FQGS-012SS
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.981                     9.89E+00              6.29E-01 Cs-137                              0.996                     1.52E-01              1.95E-02 Tl-208                              1.000                     1.40E-01              1.80E-02 X       Bi-211                              0.920 Pb-212                              1.000                     2.87E-01              4.13E-02
      ?       Pb212-XR                            1.000                     4.19E-01              1.59E-01 Bi-214                              1.000                     3.29E-01              3.88E-02 Pb-214                              0.998                     3.08E-01              3.82E-02
      ?       Pb214-XR                            1.000                     7.38E-01              2.82E-01
      ?       Ra-226                              0.980                     1.02E+00              2.74E-01 Ac-228                              0.997                     3.28E-01              5.87E-02
      ?       U-235                               0.998                     6.49E-02              1.75E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[157]

6/12/2019   1:33:25PM       Page 5 of 7 Analysis Report for    12-Jun-19-10026 L1-10221C-FQGS-012SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:33:16PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        8.67E-02          6.06E-02        6.06E-02 BE-7            477.60              10.44       4.43E-02          4.45E-01        4.45E-01
+         K-40          1460.82
* 10.66       9.89E+00          3.37E-01        3.37E-01 Mn-54           834.85              99.98       2.10E-02          5.57E-02        5.57E-02 Co-60         1173.23               99.85       1.35E-04          5.83E-02        7.19E-02 1332.49               99.98     -1.52E-02                           5.83E-02 Nb-94           702.65              99.81       3.48E-02          5.32E-02        5.46E-02 871.09              99.89     -4.66E-04                           5.32E-02 Ag-108m          79.13                6.60      6.30E-01          4.58E-02        1.54E+00 433.94              90.50     -2.63E-02                           4.58E-02 614.28              89.80     -4.83E-02                           9.03E-02 722.94              90.80       6.09E-03                          5.97E-02 Sb-125          176.31                6.84    -7.96E-01           1.52E-01        5.48E-01 380.45                1.52      8.59E-01                          2.87E+00 427.87              29.60       5.32E-02                          1.52E-01 463.36              10.49       3.55E-01                          4.25E-01 600.60              17.65     -2.99E-02                           2.68E-01 606.71                4.98      2.75E+00                          1.72E+00 635.95              11.22       1.01E-01                          4.34E-01          [158]

6/12/2019   1:33:25PM Page 6 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    8.54E-01      1.52E-01        2.74E+00 Ba-133        79.61            2.65    1.63E-01      9.32E-02        3.67E+00 81.00           32.90    6.09E-02                      2.52E-01 276.40            7.16   -6.45E-02                      5.75E-01 302.85           18.34    1.33E-02                      2.27E-01 356.01           62.05   -3.21E-02                      9.32E-02 383.85            8.94    9.28E-02                      4.94E-01 Cs-134       475.36            1.48   -1.11E+00      6.48E-02        3.03E+00 563.25            8.34   -8.40E-01                      5.44E-01 569.33           15.37    5.26E-02                      3.23E-01 604.72           97.62    8.84E-03                      8.30E-02 795.86           85.46    6.96E-02                      6.48E-02 801.95            8.69   -5.10E-01                      5.13E-01 1038.61             0.99    3.79E-01                      5.48E+00 1167.97             1.79    3.76E+00                      4.00E+00 1365.19             3.02   -3.35E-01                      1.66E+00
+         Cs-137       661.66
* 85.10    1.52E-01      3.13E-02        3.13E-02 Eu-152       121.78           28.67   -1.19E-01      1.60E-01        1.60E-01 244.70            7.61    1.48E-01                      6.17E-01 295.94            0.45    9.63E+00                      1.18E+01 344.28           26.60    9.00E-02                      1.69E-01 367.79            0.86   -1.29E+00                      4.45E+00 411.12            2.24   -4.44E-01                      1.98E+00 443.96            2.83    1.59E-01                      1.52E+00 488.68            0.42    9.26E-02                      9.48E+00 563.99            0.49   -1.33E+00                      9.90E+00 586.26            0.46    1.48E+01                      1.54E+01 678.62            0.47   -1.48E+00                      9.99E+00 688.67            0.86    2.40E+00                      6.12E+00 719.35            0.28   -3.44E+00                      1.74E+01 778.90           12.96   -3.30E-01                      3.94E-01 810.45            0.32    6.28E+00                      1.49E+01 867.37            4.26   -4.40E-01                      1.17E+00 919.33            0.43   -8.62E+00                      1.25E+01 964.08           14.65    3.81E-01                      4.85E-01 1085.87            10.24    2.78E-01                      6.26E-01 1089.74             1.73   -1.08E+00                      3.60E+00 1112.07            13.69   -2.74E-01                      4.85E-01 1212.95             1.43    3.05E+00                      5.28E+00 1249.94             0.19   -5.51E+00                      3.82E+01 1299.14             1.63   -1.87E+00                      4.24E+00 1408.01            21.07   -2.29E-01                      2.59E-01 1457.64             0.50    2.09E+02                      4.79E+01 1528.10             0.28   -3.51E+00                      9.06E+00 Eu-154       123.07           40.40    9.03E-02      1.15E-01        1.15E-01 247.93            6.89    1.41E-01                      5.70E-01 591.76            4.95    1.03E+00                      9.29E-01 692.42            1.78   -2.41E-01                      2.79E+00 723.30           20.06   -6.46E-03                      2.77E-01 756.80            4.52    6.11E-02                      1.15E+00 873.18           12.08    2.56E-01                      4.60E-01
[159]

6/12/2019   1:33:25PM Page 7 of 7 Analysis Report for     12-Jun-19-10026 L1-10221C-FQGS-012SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        4.57E-01      1.15E-01        5.55E-01 1004.76                  18.01        1.49E-01                      3.42E-01 1274.43                  34.80       -1.43E-01                      2.00E-01 1596.48                   1.80       -1.83E+00                      2.65E+00 Eu-155            45.30                  1.31        6.42E+00      2.54E-01        2.41E+01 60.01                  1.22       -1.94E+01                      2.51E+01 86.55                 30.70        3.27E-01                      2.81E-01 105.31                 21.10       -2.79E-01                      2.54E-01
+         Ra-226           186.21
* 3.64        1.02E+00      8.18E-01        8.18E-01 Pa-231            27.36                 10.30        2.30E+00      1.78E+00        2.69E+00 283.69                  1.70       -4.56E-01                      2.22E+00 300.07                  2.47        7.19E-02                      1.78E+00 302.65                  2.20       -4.36E-03                      1.90E+00 330.06                  1.40        3.37E+00                      3.07E+00
+         U-235            143.76                 10.96        9.94E-02      5.21E-02        4.45E-01 163.33                  5.08       -3.27E-02                      7.92E-01 185.71
* 57.20        6.49E-02                      5.21E-02 202.11                  1.08        1.18E+00                      3.89E+00 205.31                  5.01       -1.16E+00                      8.33E-01 Am-241            59.54                 35.90       -3.72E-01      8.85E-01        8.85E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[160]

6/12/2019 1:35:24PM Page 1 of 7 Analysis Report for    12-Jun-19-10027 L1-10221C-FSGS-013SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10027 Sample Description                           : L1-10221C-FSGS-013SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.419E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:15:00AM Acquisition Started                          : 6/12/2019 1:20:14PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.4 seconds Dead Time                                    : 0.04 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77308 Fill Height                                  : 1419.47 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:35:16PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[161]

6/12/2019   1:35:24PM         Page 2 of 7 Analysis Report for    12-Jun-19-10027 L1-10221C-FSGS-013SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       238.63               472 -    481          477.45          2.03E+02              24.20      1.67E+02           1.05 2       295.06               587 -    594          590.18          7.72E+01              13.95      5.78E+01           1.67 3       351.87               700 -    708          703.68          1.35E+02              17.15      7.33E+01           1.41 4       583.20             1162 -   1171         1166.01           6.66E+01              11.53      2.94E+01           0.86 5       609.40             1212 -   1224         1218.37           1.30E+02              15.50      4.21E+01           1.64 6       661.74             1317 -   1328         1323.01           9.93E+01              12.83      2.57E+01           1.78 7       911.53             1818 -   1828         1822.52           4.38E+01                9.49     1.93E+01           1.11 8      1120.71             2236 -   2247         2240.96           4.33E+01                9.65     1.97E+01           1.62 9      1173.39             2342 -   2352         2346.38           4.90E+01              10.26      2.20E+01           1.63 10       1332.79             2660 -   2672         2665.39           5.53E+01                9.12     1.07E+01           1.38 11       1460.92             2915 -   2929         2921.90           4.39E+02              21.31      5.48E+00           2.26 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              8.43E+00             5.49E-01 Co-60                    0.99          1173.23
* 99.85              8.66E-02             1.85E-02 1332.49
* 99.98              1.06E-01             1.80E-02 Cs-137                   0.99           661.66
* 85.10              1.41E-01             2.02E-02 Tl-208                   1.00           583.19
* 85.00              8.74E-02             1.60E-02 Pb-212                   1.00           115.18                    0.60                                             [162]

6/12/2019   1:35:24PM         Page 3 of 7 Analysis Report for    12-Jun-19-10027 L1-10221C-FSGS-013SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Pb-212                   1.00         238.63
* 43.60  2.89E-01             4.16E-02 300.09                  3.30 Bi-214                   0.99         609.32
* 45.49  3.28E-01             4.38E-02 768.36                  4.89 806.18                  1.26 934.06                  3.11 1120.29
* 14.92  4.97E-01             1.13E-01 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42  2.93E-01             5.80E-02 351.93
* 35.60  3.00E-01             4.51E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  2.54E-01             5.62E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
[163]

6/12/2019 1:35:24PM          Page 4 of 7 Analysis Report for   12-Jun-19-10027 L1-10221C-FSGS-013SS INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.998                     8.43E+00              5.49E-01 Co-60                               0.991                     9.66E-02              1.29E-02 Cs-137                              0.999                     1.41E-01              2.02E-02 Tl-208                              1.000                     8.74E-02              1.60E-02 X       Bi-211                              0.904 Pb-212                              1.000                     2.89E-01              4.16E-02 Bi-214                              0.996                     3.50E-01              4.09E-02 Pb-214                              0.998                     2.97E-01              3.56E-02 Ac-228                              0.995                     2.54E-01              5.62E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[164]

6/12/2019   1:35:24PM       Page 5 of 7 Analysis Report for    12-Jun-19-10027 L1-10221C-FSGS-013SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:35:16PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        9.29E-02          6.06E-02        6.06E-02 BE-7            477.60              10.44       4.81E-02          3.71E-01        3.71E-01
+         K-40          1460.82
* 10.66       8.43E+00          3.12E-01        3.12E-01 Mn-54           834.85              99.98     -2.12E-03           5.01E-02        5.01E-02
+         Co-60         1173.23
* 99.85       8.66E-02          3.98E-02        5.00E-02 1332.49
* 99.98       1.06E-01                          3.98E-02 Nb-94           702.65              99.81     -4.16E-02           3.95E-02        3.95E-02 871.09              99.89     -2.80E-02                           4.42E-02 Ag-108m          79.13                6.60      9.10E-01          3.92E-02        1.32E+00 433.94              90.50     -5.35E-03                           3.92E-02 614.28              89.80     -1.01E-02                           6.99E-02 722.94              90.80     -1.15E-02                           5.40E-02 Sb-125          176.31                6.84      5.72E-02          1.27E-01        5.63E-01 380.45                1.52    -1.15E+00                           2.21E+00 427.87              29.60       2.89E-02                          1.27E-01 463.36              10.49       1.22E-01                          3.65E-01 600.60              17.65     -2.42E-02                           2.37E-01 606.71                4.98    -4.43E-04                           1.58E+00 635.95              11.22     -1.90E-01                           3.46E-01          [165]

6/12/2019   1:35:24PM Page 6 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -7.93E-01      1.27E-01        2.14E+00 Ba-133        79.61            2.65    1.06E+00      8.89E-02        3.04E+00 81.00           32.90   -3.77E-01                      2.01E-01 276.40            7.16    1.61E-01                      5.40E-01 302.85           18.34    1.10E-01                      2.10E-01 356.01           62.05   -8.97E-03                      8.89E-02 383.85            8.94   -5.05E-02                      4.08E-01 Cs-134       475.36            1.48    1.34E+00      5.95E-02        2.76E+00 563.25            8.34   -5.84E-02                      4.40E-01 569.33           15.37    6.67E-02                      2.38E-01 604.72           97.62    7.29E-03                      6.77E-02 795.86           85.46    2.34E-02                      5.95E-02 801.95            8.69   -4.40E-01                      4.33E-01 1038.61             0.99    1.04E+00                      5.22E+00 1167.97             1.79   -5.08E+00                      3.81E+00 1365.19             3.02   -6.90E-02                      1.39E+00
+         Cs-137       661.66
* 85.10    1.41E-01      4.32E-02        4.32E-02 Eu-152       121.78           28.67    3.27E-02      1.36E-01        1.36E-01 244.70            7.61   -2.23E-01                      5.42E-01 295.94            0.45    6.21E+00                      1.03E+01 344.28           26.60   -7.97E-02                      1.54E-01 367.79            0.86   -2.41E+00                      3.83E+00 411.12            2.24    7.07E-01                      1.79E+00 443.96            2.83   -1.59E-01                      1.35E+00 488.68            0.42    4.99E+00                      9.67E+00 563.99            0.49    6.88E-01                      7.38E+00 586.26            0.46   -2.75E+00                      1.35E+01 678.62            0.47    3.62E+00                      8.38E+00 688.67            0.86    6.54E-01                      4.53E+00 719.35            0.28    5.07E-01                      1.66E+01 778.90           12.96   -2.62E-01                      3.04E-01 810.45            0.32   -2.05E+00                      1.33E+01 867.37            4.26    3.45E-02                      1.05E+00 919.33            0.43   -3.52E-01                      1.17E+01 964.08           14.65    1.09E-01                      4.41E-01 1085.87            10.24   -2.99E-02                      5.86E-01 1089.74             1.73    2.36E+00                      3.68E+00 1112.07            13.69   -1.53E-01                      4.75E-01 1212.95             1.43   -8.42E-01                      4.47E+00 1249.94             0.19    5.53E+00                      3.23E+01 1299.14             1.63   -2.99E-01                      3.67E+00 1408.01            21.07    1.41E-02                      2.14E-01 1457.64             0.50   -2.51E+00                      4.27E+01 1528.10             0.28   -4.13E+00                      1.17E+01 Eu-154       123.07           40.40    1.17E-02      9.45E-02        9.45E-02 247.93            6.89    1.61E-01                      5.35E-01 591.76            4.95   -3.41E-01                      8.06E-01 692.42            1.78    5.60E-01                      2.54E+00 723.30           20.06    7.21E-02                      2.51E-01 756.80            4.52    4.37E-01                      9.95E-01 873.18           12.08    3.11E-02                      4.09E-01
[166]

6/12/2019   1:35:24PM Page 7 of 7 Analysis Report for     12-Jun-19-10027 L1-10221C-FSGS-013SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        9.31E-02      9.45E-02        5.47E-01 1004.76                  18.01        2.15E-01                      3.35E-01 1274.43                  34.80       -6.35E-02                      1.67E-01 1596.48                   1.80       -1.76E+00                      1.90E+00 Eu-155            45.30                  1.31       -1.62E+00      2.07E-01        1.28E+01 60.01                  1.22       -4.27E-01                      1.41E+01 86.55                 30.70        2.01E-01                      2.21E-01 105.31                 21.10       -1.07E-02                      2.07E-01 Ra-226           186.21                  3.64        9.36E-01      1.17E+00        1.17E+00 Pa-231            27.36                 10.30        6.32E-01      1.28E+00        1.28E+00 283.69                  1.70       -8.58E-01                      2.00E+00 300.07                  2.47       -4.14E-01                      1.56E+00 302.65                  2.20        9.15E-01                      1.75E+00 330.06                  1.40        4.36E-01                      2.80E+00 U-235            143.76                 10.96       -6.11E-02      7.54E-02        3.09E-01 163.33                  5.08       -2.15E-01                      7.95E-01 185.71                 57.20        6.46E-02                      7.54E-02 202.11                  1.08        9.18E-01                      3.54E+00 205.31                  5.01       -4.76E-01                      7.57E-01 Am-241            59.54                 35.90        2.17E-02      4.99E-01        4.99E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[167]

6/12/2019 1:35:35PM Page 1 of 7 Analysis Report for    12-Jun-19-10028 L1-10221C-FSGS-014SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10028 Sample Description                           : L1-10221C-FSGS-014SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.696E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:20:00AM Acquisition Started                          : 6/12/2019 1:20:22PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.8 seconds Dead Time                                    : 0.20 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77309 Fill Height                                  : 1696.06 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:35:26PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[168]

6/12/2019   1:35:35PM         Page 2 of 7 Analysis Report for    12-Jun-19-10028 L1-10221C-FSGS-014SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1         77.29              307 -    316          309.90          5.80E+01              15.91      8.60E+01           0.75 2       238.72               947 -    961          954.97          1.43E+02              21.32      1.08E+02           0.89 3       295.26             1174 -   1189         1180.93           7.61E+01              14.98      4.89E+01           0.51 4       352.08             1402 -   1416         1408.04           1.35E+02              15.42      3.58E+01           1.30 5       583.19             2324 -   2342         2331.97           7.98E+01              12.01      1.92E+01           1.15 6       609.54             2431 -   2445         2437.32           6.18E+01              11.74      2.63E+01           1.58 7       661.76             2638 -   2654         2646.15           2.43E+02              17.37      1.88E+01           1.39 8      1173.36             4685 -   4699         4692.63           4.63E+01              10.01      1.87E+01           0.85 9      1332.70             5323 -   5338         5330.27           4.45E+01                8.87     1.15E+01           0.52 10       1460.99             5832 -   5855         5843.79           4.00E+02              20.00      0.00E+00           1.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              9.70E+00             6.42E-01 Co-60                    0.99          1173.23
* 99.85              1.03E-01             2.26E-02 1332.49
* 99.98              1.07E-01             2.18E-02 Cs-137                   0.99           661.66
* 85.10              4.32E-01             4.03E-02 Tl-208                   1.00           583.19
* 85.00              1.30E-01             2.11E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              2.51E-01             4.26E-02[169]

6/12/2019   1:35:35PM         Page 3 of 7 Analysis Report for    12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Pb-212                   0.99         300.09                  3.30 Pb212-XR                 0.99            74.82               10.28 77.11
* 17.10  6.98E-01             2.04E-01 87.35                3.97 89.78                1.46 Bi-214                   0.99         609.32
* 45.49  1.94E-01             3.87E-02 768.36                  4.89 806.18                  1.26 934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42  3.56E-01             7.57E-02 351.93
* 35.60  3.71E-01             5.17E-02 785.96                  1.06 Pb214-XR                 0.99            74.82                5.80 77.11
* 9.70  1.23E+00             3.65E-01 87.35                2.24 89.78                0.82
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[170]

6/12/2019 1:35:35PM          Page 4 of 7 Analysis Report for   12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.995                     9.70E+00              6.42E-01 Co-60                               0.995                     1.05E-01              1.57E-02 Cs-137                              0.998                     4.32E-01              4.03E-02 Tl-208                              1.000                     1.30E-01              2.11E-02 Pb-212                              0.999                     2.51E-01              4.26E-02
     ?       Pb212-XR                            0.997                     6.98E-01              2.04E-01 Bi-214                              0.997                     1.94E-01              3.87E-02 Pb-214                              0.998                     3.66E-01              4.27E-02
     ?       Pb214-XR                            0.997                     1.23E+00              3.65E-01
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[171]

6/12/2019   1:35:35PM       Page 5 of 7 Analysis Report for    12-Jun-19-10028 L1-10221C-FSGS-014SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:35:26PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.72E-02          6.81E-02        6.81E-02 BE-7            477.60              10.44       2.85E-01          5.16E-01        5.16E-01
+         K-40          1460.82
* 10.66       9.70E+00          6.97E-02        6.97E-02 Mn-54           834.85              99.98     -4.60E-03           5.38E-02        5.38E-02
+         Co-60         1173.23
* 99.85       1.03E-01          5.48E-02        6.17E-02 1332.49
* 99.98       1.07E-01                          5.48E-02 Nb-94           702.65              99.81     -1.07E-02           5.80E-02        5.80E-02 871.09              99.89       3.71E-02                          5.82E-02 Ag-108m          79.13                6.60    -5.69E-01           5.56E-02        2.20E+00 433.94              90.50       1.59E-02                          5.56E-02 614.28              89.80     -3.59E-02                           7.86E-02 722.94              90.80       5.26E-03                          6.67E-02 Sb-125          176.31                6.84    -5.44E-01           1.67E-01        6.68E-01 380.45                1.52      1.63E+00                          3.23E+00 427.87              29.60     -9.78E-03                           1.67E-01 463.36              10.49       1.77E-01                          5.35E-01 600.60              17.65       1.90E-01                          2.87E-01 606.71                4.98    -6.13E-01                           1.50E+00 635.95              11.22       9.19E-02                          4.65E-01          [172]

6/12/2019   1:35:35PM Page 6 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    2.21E-01      1.67E-01        2.96E+00 Ba-133        79.61            2.65   -5.88E-01      9.91E-02        5.37E+00 81.00           32.90   -2.34E-01                      3.62E-01 276.40            7.16   -1.13E-01                      6.33E-01 302.85           18.34   -5.35E-02                      2.54E-01 356.01           62.05   -2.01E-02                      9.91E-02 383.85            8.94   -2.84E-02                      5.51E-01 Cs-134       475.36            1.48    1.30E+00      6.43E-02        3.58E+00 563.25            8.34   -3.16E-01                      5.15E-01 569.33           15.37    1.44E-01                      3.42E-01 604.72           97.62   -3.38E-02                      6.43E-02 795.86           85.46    4.43E-02                      6.95E-02 801.95            8.69    4.45E-02                      6.02E-01 1038.61             0.99    3.00E+00                      7.03E+00 1167.97             1.79   -1.96E+00                      5.69E+00 1365.19             3.02   -1.43E-01                      1.53E+00
+         Cs-137       661.66
* 85.10    4.32E-01      5.11E-02        5.11E-02 Eu-152       121.78           28.67   -9.69E-02      1.66E-01        1.82E-01 244.70            7.61    1.05E-01                      6.75E-01 295.94            0.45    6.77E+00                      1.29E+01 344.28           26.60    5.03E-02                      1.66E-01 367.79            0.86   -6.46E-01                      5.07E+00 411.12            2.24    9.26E-03                      2.22E+00 443.96            2.83   -4.50E-01                      1.84E+00 488.68            0.42    4.08E+00                      1.14E+01 563.99            0.49   -3.54E+00                      8.96E+00 586.26            0.46   -9.81E-01                      1.69E+01 678.62            0.47    7.53E+00                      1.16E+01 688.67            0.86   -2.07E+00                      6.07E+00 719.35            0.28   -8.32E+00                      1.94E+01 778.90           12.96    3.60E-02                      3.67E-01 810.45            0.32   -1.25E+01                      1.52E+01 867.37            4.26   -1.84E-01                      1.44E+00 919.33            0.43    2.35E+00                      1.34E+01 964.08           14.65    4.02E-01                      5.11E-01 1085.87            10.24   -1.91E-01                      6.91E-01 1089.74             1.73   -3.10E-01                      3.86E+00 1112.07            13.69   -1.26E-01                      4.76E-01 1212.95             1.43    1.97E+00                      5.68E+00 1249.94             0.19    1.28E+01                      4.01E+01 1299.14             1.63   -7.33E-01                      4.06E+00 1408.01            21.07   -8.05E-02                      2.41E-01 1457.64             0.50    1.96E+02                      5.08E+01 1528.10             0.28   -1.09E+01                      1.71E+01 Eu-154       123.07           40.40   -9.02E-02      1.28E-01        1.28E-01 247.93            6.89    5.16E-02                      6.68E-01 591.76            4.95    8.94E-01                      1.14E+00 692.42            1.78    1.23E+00                      2.91E+00 723.30           20.06    1.71E-01                      3.13E-01 756.80            4.52    4.35E-01                      1.24E+00 873.18           12.08   -5.75E-01                      4.12E-01
[173]

6/12/2019   1:35:35PM Page 7 of 7 Analysis Report for     12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -2.32E-01      1.28E-01        5.70E-01 1004.76                  18.01        1.95E-01                      3.69E-01 1274.43                  34.80       -1.13E-01                      1.67E-01 1596.48                   1.80        7.86E-01                      2.78E+00 Eu-155            45.30                  1.31        1.43E+01      3.24E-01        4.00E+01 60.01                  1.22        1.07E-01                      3.88E+01 86.55                 30.70        1.31E-01                      3.39E-01 105.31                 21.10       -1.49E-01                      3.24E-01 Ra-226           186.21                  3.64       -3.59E-01      1.43E+00        1.43E+00 Pa-231            27.36                 10.30        4.10E+00      1.95E+00        4.45E+00 283.69                  1.70        1.33E+00                      2.80E+00 300.07                  2.47       -1.19E-01                      1.95E+00 302.65                  2.20        8.32E-01                      2.13E+00 330.06                  1.40        6.85E-01                      3.62E+00 U-235            143.76                 10.96        2.50E-01      8.98E-02        4.82E-01 163.33                  5.08       -3.22E-01                      9.08E-01 185.71                 57.20        4.55E-03                      8.98E-02 202.11                  1.08        3.68E+00                      4.70E+00 205.31                  5.01       -5.07E-01                      9.19E-01 Am-241            59.54                 35.90       -4.11E-01      1.36E+00        1.36E+00
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[174]

6/12/2019 1:35:55PM Page 1 of 7 Analysis Report for    12-Jun-19-10029 L1-10221C-FSGS-015SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10029 Sample Description                           : L1-10221C-FSGS-015SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.635E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:25:00AM Acquisition Started                          : 6/12/2019 1:20:29PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77310 Fill Height                                  : 1634.99 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:35:48PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[175]

6/12/2019   1:35:55PM         Page 2 of 7 Analysis Report for    12-Jun-19-10029 L1-10221C-FSGS-015SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       186.35               741 -    751          745.27          3.13E+01              11.89      4.57E+01           0.91 2       238.75               948 -    960          954.59          1.47E+02              18.40      7.29E+01           0.84 3       295.36             1171 -   1186         1180.72           6.90E+01              12.13      2.60E+01           0.87 4       351.97             1399 -   1414         1406.89           1.05E+02              12.87      2.01E+01           1.31 5       463.19             1846 -   1855         1851.31           2.01E+01                6.71     1.09E+01           0.67 6       582.92             2323 -   2338         2329.80           5.12E+01                9.62     1.38E+01           1.28 7       609.28             2429 -   2442         2435.16           6.58E+01              10.09      1.32E+01           1.12 8       911.29             3637 -   3649         3642.63           2.20E+01                7.53     1.30E+01           0.34 9      1460.39             5826 -   5852         5839.48           4.17E+02              21.14      6.75E+00           1.82 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.97          1460.82
* 10.66              9.19E+00             6.13E-01 Sb-125                   0.42           176.31                    6.84 380.45                    1.52 427.87                  29.60 463.36
* 10.49              2.06E-01             7.06E-02 600.60                  17.65 606.71                    4.98 635.95                  11.22                                              [176]

6/12/2019   1:35:55PM         Page 3 of 7 Analysis Report for  12-Jun-19-10029 L1-10221C-FSGS-015SS Nuclide             Id               Energy   Yield(%)      Activity           Activity Name             Confidence           (keV)            (pCi/grams)          Uncertainty Sb-125                 0.42         671.44        1.79 Tl-208                 0.98         583.19
* 85.00  7.58E-02             1.50E-02 Pb-212                 0.99         115.18        0.60 238.63
* 43.60  2.31E-01             3.44E-02 300.09        3.30 Bi-214                 1.00         609.32
* 45.49  1.88E-01             3.09E-02 768.36        4.89 806.18        1.26 934.06        3.11 1120.29        14.92 1155.21         1.63 1238.12         5.83 1280.98         1.43 1377.67         3.99 1385.31         0.79 1401.52         1.33 1407.99         2.39 1509.21         2.13 1661.27         1.05 1729.59         2.88 1764.49        15.30 1847.43         2.03 2118.51         1.16 Pb-214                 0.99         241.99        7.25 295.22
* 18.42  2.91E-01             5.63E-02 351.93
* 35.60  2.61E-01             3.82E-02 785.96        1.06 Ra-226                 0.99         186.21
* 3.64  5.17E-01             2.01E-01 Ac-228                 0.48         129.07        2.42 209.25        3.89 270.24        3.46 328.00        2.95 338.32       11.27 409.46        1.92 463.00
* 4.40  4.91E-01             1.68E-01 794.95        4.25 911.20
* 25.80  1.45E-01             5.02E-02 964.77        4.99 968.97       15.80 1588.20         3.22 U-235                  0.95         143.76       10.96 163.33        5.08 185.71
* 57.20  3.29E-02             1.28E-02 202.11        1.08 205.31        5.01
[177]

6/12/2019 1:35:55PM          Page 4 of 7 Analysis Report for    12-Jun-19-10029 L1-10221C-FSGS-015SS
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.970                     9.19E+00              6.13E-01 Sb-125                              0.420                     1.45E-01              7.37E-02 Tl-208                              0.989                     7.58E-02              1.50E-02 X       Bi-211                              0.878 Pb-212                              0.998                     2.31E-01              3.44E-02 Bi-214                              1.000                     1.88E-01              3.09E-02 Pb-214                              0.999                     2.70E-01              3.16E-02
      ?       Ra-226                              0.997                     5.17E-01              2.01E-01 Ac-228                              0.483                     1.45E-01              5.01E-02
      ?       U-235                               0.955                     3.29E-02              1.28E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[178]

6/12/2019   1:35:55PM       Page 5 of 7 Analysis Report for    12-Jun-19-10029 L1-10221C-FSGS-015SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:35:48PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        9.50E-02          5.81E-02        5.81E-02 BE-7            477.60              10.44       2.29E-01          3.67E-01        3.67E-01
+         K-40          1460.82
* 10.66       9.19E+00          4.69E-01        4.69E-01 Mn-54           834.85              99.98     -2.70E-02           4.96E-02        4.96E-02 Co-60         1173.23               99.85       2.33E-02          5.09E-02        6.39E-02 1332.49               99.98     -1.64E-02                           5.09E-02 Nb-94           702.65              99.81     -1.72E-02           4.19E-02        4.65E-02 871.09              99.89     -2.29E-03                           4.19E-02 Ag-108m          79.13                6.60      1.65E+00          4.10E-02        1.35E+00 433.94              90.50       4.63E-03                          4.10E-02 614.28              89.80     -4.01E-03                           5.87E-02 722.94              90.80       2.51E-02                          5.39E-02
+         Sb-125          176.31                6.84      4.17E-01          1.24E-01        4.66E-01 380.45                1.52      1.03E-01                          2.29E+00 427.87              29.60       2.87E-04                          1.24E-01 463.36
* 10.49       2.06E-01                          2.04E-01 600.60              17.65       6.11E-02                          2.19E-01 606.71                4.98      2.00E+00                          1.34E+00 635.95              11.22       1.54E-01                          3.53E-01          [179]

6/12/2019   1:35:55PM Page 6 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    2.90E-01      1.24E-01        2.19E+00 Ba-133        79.61            2.65    3.39E+00      6.89E-02        3.22E+00 81.00           32.90   -3.73E-01                      2.03E-01 276.40            7.16    1.26E-01                      4.81E-01 302.85           18.34    1.80E-01                      2.12E-01 356.01           62.05   -6.34E-03                      6.89E-02 383.85            8.94    6.39E-02                      3.81E-01 Cs-134       475.36            1.48   -9.81E-01      5.54E-02        2.50E+00 563.25            8.34    3.12E-02                      5.39E-01 569.33           15.37    2.60E-02                      2.71E-01 604.72           97.62   -2.90E-02                      5.92E-02 795.86           85.46    2.28E-02                      5.54E-02 801.95            8.69    3.40E-01                      5.63E-01 1038.61             0.99   -1.43E+00                      5.05E+00 1167.97             1.79   -1.25E+00                      3.51E+00 1365.19             3.02    4.91E-01                      1.49E+00 Cs-137       661.66           85.10    4.24E-02      5.72E-02        5.72E-02 Eu-152       121.78           28.67    2.61E-02      1.15E-01        1.15E-01 244.70            7.61    1.20E-01                      5.04E-01 295.94            0.45    5.11E+00                      9.83E+00 344.28           26.60   -8.29E-03                      1.23E-01 367.79            0.86    1.91E-01                      3.97E+00 411.12            2.24   -6.53E-01                      1.52E+00 443.96            2.83   -5.48E-01                      9.92E-01 488.68            0.42    3.22E+00                      8.63E+00 563.99            0.49   -9.93E+00                      8.43E+00 586.26            0.46   -1.37E+00                      1.27E+01 678.62            0.47    2.62E+00                      9.61E+00 688.67            0.86   -1.78E+00                      4.57E+00 719.35            0.28   -4.20E-01                      1.54E+01 778.90           12.96   -2.07E-01                      2.81E-01 810.45            0.32   -1.03E+01                      1.34E+01 867.37            4.26   -1.42E-01                      1.07E+00 919.33            0.43    4.67E+00                      1.11E+01 964.08           14.65    4.16E-01                      4.77E-01 1085.87            10.24   -5.38E-02                      5.61E-01 1089.74             1.73   -2.02E-01                      3.38E+00 1112.07            13.69    2.49E-02                      3.75E-01 1212.95             1.43   -5.77E-01                      5.06E+00 1249.94             0.19   -8.61E-01                      3.24E+01 1299.14             1.63    4.77E+00                      4.20E+00 1408.01            21.07    1.73E-01                      2.39E-01 1457.64             0.50    1.93E+02                      4.75E+01 1528.10             0.28    6.90E+00                      1.42E+01 Eu-154       123.07           40.40    1.79E-02      8.01E-02        8.01E-02 247.93            6.89   -3.52E-01                      4.60E-01 591.76            4.95    4.48E-01                      7.83E-01 692.42            1.78   -3.59E-01                      2.32E+00 723.30           20.06    3.30E-02                      2.44E-01 756.80            4.52   -9.95E-02                      9.25E-01 873.18           12.08   -2.50E-01                      3.48E-01
[180]

6/12/2019   1:35:55PM Page 7 of 7 Analysis Report for     12-Jun-19-10029 L1-10221C-FSGS-015SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        6.48E-03      8.01E-02        4.88E-01 1004.76                  18.01        6.91E-03                      2.95E-01 1274.43                  34.80       -1.14E-01                      1.58E-01 1596.48                   1.80        2.35E-01                      2.91E+00 Eu-155            45.30                  1.31       -5.30E+00      1.94E-01        1.12E+01 60.01                  1.22        7.21E-01                      1.29E+01 86.55                 30.70        1.01E-03                      1.94E-01 105.31                 21.10       -8.78E-02                      2.07E-01
+         Ra-226           186.21
* 3.64        5.17E-01      6.36E-01        6.36E-01 Pa-231            27.36                 10.30        1.06E+00      1.29E+00        1.29E+00 283.69                  1.70       -9.38E-01                      1.87E+00 300.07                  2.47       -5.26E-01                      1.47E+00 302.65                  2.20        1.82E+00                      1.80E+00 330.06                  1.40        3.88E-01                      2.59E+00
+         U-235            143.76                 10.96        9.97E-02      4.05E-02        3.12E-01 163.33                  5.08        2.62E-01                      6.67E-01 185.71
* 57.20        3.29E-02                      4.05E-02 202.11                  1.08        5.77E-01                      3.28E+00 205.31                  5.01       -2.15E-01                      6.66E-01 Am-241            59.54                 35.90       -7.55E-02      4.57E-01        4.57E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[181]

6/12/2019 1:57:52PM Page 1 of 7 Analysis Report for    12-Jun-19-10030 L1-10221C-FSGS-016SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10030 Sample Description                           : L1-10221C-FSGS-016SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.527E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:30:00AM Acquisition Started                          : 6/12/2019 1:42:42PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.04 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77311 Fill Height                                  : 1526.95 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:57:45PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[182]

6/12/2019   1:57:52PM         Page 2 of 7 Analysis Report for    12-Jun-19-10030 L1-10221C-FSGS-016SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       238.64               473 -    481          477.46          1.13E+02              19.92      1.29E+02           1.13 2       338.58               675 -    680          677.12          2.47E+01                9.10     3.23E+01           1.18 3       352.04               699 -    708          704.01          8.63E+01              12.74      3.37E+01           1.63 4       583.33             1160 -   1170         1166.27           4.38E+01              10.75      3.03E+01           1.40 5       609.25             1213 -   1223         1218.07           8.80E+01              12.17      2.50E+01           1.50 6       911.27             1818 -   1828         1821.99           3.98E+01                8.59     1.42E+01           0.87 7       968.72             1934 -   1942         1936.91           2.02E+01                7.93     1.98E+01           1.20 8      1460.91             2914 -   2929         2921.87           3.31E+02              18.36      2.02E+00           2.14 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              6.23E+00             4.39E-01 Tl-208                   0.99           583.19
* 85.00              5.64E-02             1.43E-02 Bi-211                   0.86           351.07
* 13.02              5.17E-01             8.70E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              1.59E-01             3.08E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              2.18E-01             3.29E-02 768.36                    4.89 806.18                    1.26                                             [183]

6/12/2019   1:57:52PM         Page 3 of 7 Analysis Report for    12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00         934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22                 18.42 351.93
* 35.60  1.89E-01             3.18E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32
* 11.27  1.67E-01             6.28E-02 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  2.27E-01             4.99E-02 964.77                  4.99 968.97
* 15.80  1.95E-01             7.72E-02 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[184]

6/12/2019 1:57:52PM          Page 4 of 7 Analysis Report for   12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.999                     6.23E+00              4.39E-01 Tl-208                              0.997                     5.64E-02              1.43E-02
     ?       Bi-211                              0.862                     5.17E-01              8.70E-02 Pb-212                              1.000                     1.59E-01              3.08E-02 Bi-214                              1.000                     2.18E-01              3.29E-02
     ?       Pb-214                              0.999                     1.89E-01              3.18E-02 Ac-228                              0.997                     2.02E-01              3.49E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[185]

6/12/2019   1:57:52PM       Page 5 of 7 Analysis Report for    12-Jun-19-10030 L1-10221C-FSGS-016SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:57:45PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.30E-02          5.18E-02        5.18E-02 BE-7            477.60              10.44       1.92E-01          3.68E-01        3.68E-01
+         K-40          1460.82
* 10.66       6.23E+00          2.12E-01        2.12E-01 Mn-54           834.85              99.98     -2.91E-02           4.29E-02        4.29E-02 Co-60         1173.23               99.85       1.68E-02          5.70E-02        5.81E-02 1332.49               99.98       2.67E-02                          5.70E-02 Nb-94           702.65              99.81     -1.58E-02           3.39E-02        3.62E-02 871.09              99.89     -6.77E-03                           3.39E-02 Ag-108m          79.13                6.60      5.06E-01          3.73E-02        1.19E+00 433.94              90.50     -7.16E-03                           3.73E-02 614.28              89.80     -1.87E-02                           5.32E-02 722.94              90.80     -2.83E-02                           4.17E-02 Sb-125          176.31                6.84      1.96E-01          1.24E-01        5.14E-01 380.45                1.52      1.07E+00                          2.19E+00 427.87              29.60       3.49E-03                          1.24E-01 463.36              10.49     -9.92E-02                           2.98E-01 600.60              17.65       8.69E-02                          2.27E-01 606.71                4.98    -3.39E-01                           1.31E+00 635.95              11.22     -8.33E-02                           3.02E-01          [186]

6/12/2019   1:57:52PM Page 6 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.36E+00      1.24E-01        2.21E+00 Ba-133        79.61            2.65    1.67E-01      6.69E-02        2.73E+00 81.00           32.90   -1.78E-01                      1.88E-01 276.40            7.16   -8.18E-02                      4.41E-01 302.85           18.34    1.23E-01                      1.82E-01 356.01           62.05   -4.88E-02                      6.69E-02 383.85            8.94   -1.23E-02                      3.63E-01 Cs-134       475.36            1.48    1.05E+00      4.72E-02        2.66E+00 563.25            8.34   -1.16E-01                      4.02E-01 569.33           15.37    8.64E-02                      2.39E-01 604.72           97.62   -2.30E-02                      5.85E-02 795.86           85.46    3.22E-02                      4.72E-02 801.95            8.69   -1.24E-01                      4.25E-01 1038.61             0.99    6.23E-02                      5.05E+00 1167.97             1.79   -2.31E+00                      2.97E+00 1365.19             3.02    1.98E-01                      1.23E+00 Cs-137       661.66           85.10    5.17E-02      6.02E-02        6.02E-02 Eu-152       121.78           28.67    4.01E-03      1.06E-01        1.06E-01 244.70            7.61    1.57E-02                      4.90E-01 295.94            0.45    3.36E+00                      8.78E+00 344.28           26.60   -1.03E-01                      1.22E-01 367.79            0.86   -1.25E-01                      3.59E+00 411.12            2.24   -8.80E-01                      1.39E+00 443.96            2.83   -1.82E-01                      1.06E+00 488.68            0.42   -4.06E-01                      8.14E+00 563.99            0.49   -1.90E+00                      6.91E+00 586.26            0.46   -4.11E+00                      1.13E+01 678.62            0.47   -3.89E+00                      7.48E+00 688.67            0.86    1.84E+00                      4.99E+00 719.35            0.28    2.17E+00                      1.33E+01 778.90           12.96   -1.43E-01                      3.15E-01 810.45            0.32   -8.27E-01                      1.18E+01 867.37            4.26   -6.46E-01                      8.11E-01 919.33            0.43   -4.99E+00                      8.02E+00 964.08           14.65   -3.02E-01                      3.79E-01 1085.87            10.24    2.92E-02                      4.54E-01 1089.74             1.73    1.45E+00                      3.05E+00 1112.07            13.69    6.09E-02                      3.44E-01 1212.95             1.43   -9.07E-01                      4.29E+00 1249.94             0.19   -3.01E+00                      2.93E+01 1299.14             1.63    1.79E+00                      3.31E+00 1408.01            21.07    7.18E-02                      1.93E-01 1457.64             0.50    0.00E+00                      3.59E+01 1528.10             0.28    2.42E+00                      1.08E+01 Eu-154       123.07           40.40   -2.81E-02      7.32E-02        7.32E-02 247.93            6.89    2.81E-02                      4.84E-01 591.76            4.95   -1.70E-01                      6.81E-01 692.42            1.78    2.37E-01                      2.19E+00 723.30           20.06   -6.29E-03                      2.02E-01 756.80            4.52    2.53E-01                      8.26E-01 873.18           12.08    1.18E-02                      2.87E-01
[187]

6/12/2019   1:57:52PM Page 7 of 7 Analysis Report for     12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -8.62E-03      7.32E-02        4.20E-01 1004.76                  18.01        3.25E-02                      2.50E-01 1274.43                  34.80       -5.55E-02                      9.83E-02 1596.48                   1.80       -1.37E+00                      1.49E+00 Eu-155            45.30                  1.31       -1.49E+00      1.76E-01        1.22E+01 60.01                  1.22        1.19E-01                      1.27E+01 86.55                 30.70       -3.44E-02                      1.76E-01 105.31                 21.10        3.84E-02                      1.88E-01 Ra-226           186.21                  3.64        1.99E-01      9.75E-01        9.75E-01 Pa-231            27.36                 10.30        5.64E-01      1.10E+00        1.10E+00 283.69                  1.70        4.20E-01                      1.92E+00 300.07                  2.47       -1.43E+00                      1.34E+00 302.65                  2.20        1.02E+00                      1.52E+00 330.06                  1.40        9.90E-01                      2.73E+00 U-235            143.76                 10.96       -1.77E-02      6.32E-02        2.89E-01 163.33                  5.08        3.51E-02                      6.81E-01 185.71                 57.20        2.57E-02                      6.32E-02 202.11                  1.08        7.20E-01                      3.18E+00 205.31                  5.01       -2.37E-01                      6.91E-01 Am-241            59.54                 35.90       -1.26E-01      4.22E-01        4.22E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[188]

6/12/2019 1:58:00PM Page 1 of 7 Analysis Report for    12-Jun-19-10031 L1-10221C-FSGS-017SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 12-Jun-19-10031 Sample Description                           : L1-10221C-FSGS-017SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.558E+03 grams Facility                                     : Default Sample Taken On                              : 6/11/2019 9:35:00AM Acquisition Started                          : 6/12/2019 1:42:49PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.5 seconds Dead Time                                    : 0.16 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/12/2019 Efficiency Calibration Description           :
Sample Number                                : 77312 Fill Height                                  : 1558.30 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/12/2019 1:57:53PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[189]

6/12/2019   1:58:00PM         Page 2 of 7 Analysis Report for    12-Jun-19-10031 L1-10221C-FSGS-017SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1         77.11              306 -    314          309.16          3.15E+01              12.99      6.35E+01           0.67 2       186.03               741 -    749          744.41          4.37E+01              12.75      5.53E+01           0.99 3       238.66               947 -    961          954.72          1.30E+02              20.77      1.05E+02           0.68 4       295.19             1173 -   1188         1180.65           4.64E+01              14.18      5.06E+01           1.04 5       351.87             1402 -   1413         1407.23           1.05E+02              13.49      3.05E+01           1.35 6       510.91             2038 -   2048         2043.00           1.86E+01                9.15     2.74E+01           0.54 7       583.16             2327 -   2339         2331.86           4.52E+01              10.03      2.08E+01           1.05 8       609.20             2430 -   2441         2435.97           6.66E+01              10.01      1.34E+01           1.12 9       911.68             3639 -   3652         3645.67           4.12E+01                7.74     6.78E+00           0.44 10       1460.91             5832 -   5855         5843.46           3.41E+02              19.15      6.27E+00           1.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty An Pk                    0.99           511.00
* 100.00               2.44E-02             1.21E-02 K-40                     0.99          1460.82
* 10.66              8.45E+00             6.00E-01 Tl-208                   1.00           583.19
* 85.00              7.51E-02             1.73E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              2.32E-01             4.15E-02 300.09                    3.30 Pb212-XR                 1.00            74.82                  10.28                                              [190]

6/12/2019   1:58:00PM         Page 3 of 7 Analysis Report for  12-Jun-19-10031 L1-10221C-FSGS-017SS Nuclide             Id               Energy   Yield(%)      Activity           Activity Name             Confidence           (keV)            (pCi/grams)          Uncertainty Pb212-XR               1.00          77.11
* 17.10  3.85E-01             1.64E-01 87.35        3.97 89.78        1.46 Bi-214                 0.99         609.32
* 45.49  2.13E-01             3.45E-02 768.36        4.89 806.18        1.26 934.06        3.11 1120.29        14.92 1155.21         1.63 1238.12         5.83 1280.98         1.43 1377.67         3.99 1385.31         0.79 1401.52         1.33 1407.99         2.39 1509.21         2.13 1661.27         1.05 1729.59         2.88 1764.49        15.30 1847.43         2.03 2118.51         1.16 Pb-214                 1.00         241.99        7.25 295.22
* 18.42  2.20E-01             6.96E-02 351.93
* 35.60  2.91E-01             4.43E-02 785.96        1.06 Pb214-XR               1.00          74.82        5.80 77.11
* 9.70  6.79E-01             2.90E-01 87.35        2.24 89.78        0.82 Ra-226                 0.99         186.21
* 3.64  8.31E-01             2.52E-01 Ac-228                 0.98         129.07        2.42 209.25        3.89 270.24        3.46 328.00        2.95 338.32       11.27 409.46        1.92 463.00        4.40 794.95        4.25 911.20
* 25.80  3.06E-01             5.89E-02 964.77        4.99 968.97       15.80 1588.20         3.22 U-235                  0.98         143.76       10.96 163.33        5.08 185.71
* 57.20  5.29E-02             1.60E-02 202.11        1.08 205.31        5.01
[191]

6/12/2019 1:58:00PM          Page 4 of 7 Analysis Report for    12-Jun-19-10031 L1-10221C-FSGS-017SS
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
An Pk                               0.999                     2.44E-02              1.21E-02 K-40                                0.999                     8.45E+00              6.00E-01 Tl-208                              1.000                     7.51E-02              1.73E-02 X       Bi-211                              0.902 Pb-212                              1.000                     2.32E-01              4.15E-02
      ?       Pb212-XR                            1.000                     3.85E-01              1.64E-01 Bi-214                              0.999                     2.13E-01              3.45E-02 Pb-214                              1.000                     2.71E-01              3.73E-02
      ?       Pb214-XR                            1.000                     6.79E-01              2.90E-01
      ?       Ra-226                              0.995                     8.31E-01              2.52E-01 Ac-228                              0.989                     3.06E-01              5.89E-02
      ?       U-235                               0.989                     5.29E-02              1.60E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[192]

6/12/2019   1:58:00PM       Page 5 of 7 Analysis Report for    12-Jun-19-10031 L1-10221C-FSGS-017SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/12/2019 1:57:53PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
+         An Pk           511.00
* 100.00        2.44E-02          3.97E-02        3.97E-02 BE-7            477.60              10.44     -5.90E-02           4.41E-01        4.41E-01
+         K-40          1460.82
* 10.66       8.45E+00          5.01E-01        5.01E-01 Mn-54           834.85              99.98       1.66E-02          5.64E-02        5.64E-02 Co-60         1173.23               99.85       7.14E-03          6.38E-02        7.09E-02 1332.49               99.98       1.06E-02                          6.38E-02 Nb-94           702.65              99.81       3.76E-02          5.15E-02        5.57E-02 871.09              99.89     -1.06E-02                           5.15E-02 Ag-108m          79.13                6.60      4.93E-01          4.98E-02        1.97E+00 433.94              90.50       5.73E-03                          4.98E-02 614.28              89.80     -8.14E-02                           6.82E-02 722.94              90.80       1.43E-02                          6.31E-02 Sb-125          176.31                6.84    -1.97E-01           1.43E-01        6.11E-01 380.45                1.52      1.30E+00                          2.77E+00 427.87              29.60     -1.07E-01                           1.43E-01 463.36              10.49       1.13E-01                          5.18E-01 600.60              17.65     -6.64E-02                           2.59E-01 606.71                4.98      1.68E+00                          1.52E+00 635.95              11.22     -1.02E-01                           4.01E-01          [193]

6/12/2019   1:58:00PM Page 6 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -8.68E-01      1.43E-01        2.57E+00 Ba-133        79.61            2.65    1.33E+00      8.87E-02        4.72E+00 81.00           32.90    1.16E-01                      3.15E-01 276.40            7.16    3.00E-01                      6.24E-01 302.85           18.34    8.78E-03                      2.33E-01 356.01           62.05   -1.13E-01                      8.87E-02 383.85            8.94    2.37E-01                      4.62E-01 Cs-134       475.36            1.48    2.32E+00      5.68E-02        3.20E+00 563.25            8.34    2.40E-01                      5.04E-01 569.33           15.37   -3.25E-02                      2.60E-01 604.72           97.62   -3.37E-02                      7.29E-02 795.86           85.46    1.20E-02                      5.68E-02 801.95            8.69   -9.67E-02                      5.52E-01 1038.61             0.99   -2.84E-01                      6.07E+00 1167.97             1.79    1.98E+00                      4.10E+00 1365.19             3.02    1.17E+00                      1.73E+00 Cs-137       661.66           85.10    9.70E-04      7.02E-02        7.02E-02 Eu-152       121.78           28.67    1.20E-01      1.58E-01        1.83E-01 244.70            7.61    3.19E-02                      6.21E-01 295.94            0.45    9.62E+00                      1.17E+01 344.28           26.60    4.41E-02                      1.58E-01 367.79            0.86   -1.12E+00                      4.38E+00 411.12            2.24   -6.25E-01                      1.76E+00 443.96            2.83   -3.58E-01                      1.49E+00 488.68            0.42   -5.96E-01                      9.07E+00 563.99            0.49    3.93E+00                      8.56E+00 586.26            0.46    1.13E+01                      1.48E+01 678.62            0.47   -6.33E+00                      1.06E+01 688.67            0.86   -1.90E+00                      5.76E+00 719.35            0.28   -6.60E+00                      1.80E+01 778.90           12.96   -2.20E-01                      3.50E-01 810.45            0.32    7.04E+00                      1.55E+01 867.37            4.26   -1.49E-01                      1.28E+00 919.33            0.43   -8.70E+00                      1.23E+01 964.08           14.65    1.74E-01                      4.40E-01 1085.87            10.24    1.26E-01                      5.54E-01 1089.74             1.73   -1.36E+00                      3.23E+00 1112.07            13.69    1.56E-01                      4.44E-01 1212.95             1.43    4.19E+00                      4.73E+00 1249.94             0.19   -4.37E+00                      3.17E+01 1299.14             1.63   -4.03E+00                      3.93E+00 1408.01            21.07    5.76E-02                      2.11E-01 1457.64             0.50    1.85E+02                      4.90E+01 1528.10             0.28    2.67E+00                      1.60E+01 Eu-154       123.07           40.40   -6.53E-02      1.24E-01        1.24E-01 247.93            6.89    1.62E-02                      5.77E-01 591.76            4.95    5.31E-01                      8.89E-01 692.42            1.78    2.23E-02                      2.64E+00 723.30           20.06    4.89E-02                      2.92E-01 756.80            4.52    1.23E+00                      1.28E+00 873.18           12.08    1.43E-01                      4.27E-01
[194]

6/12/2019   1:58:00PM Page 7 of 7 Analysis Report for     12-Jun-19-10031 L1-10221C-FSGS-017SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.15E-01      1.24E-01        5.48E-01 1004.76                  18.01        1.41E-01                      3.77E-01 1274.43                  34.80       -5.84E-02                      1.56E-01 1596.48                   1.80       -5.91E-02                      2.31E+00 Eu-155            45.30                  1.31        1.00E+01      2.76E-01        3.36E+01 60.01                  1.22        7.31E+00                      3.18E+01 86.55                 30.70       -2.75E-02                      2.76E-01 105.31                 21.10        3.11E-02                      3.11E-01
+         Ra-226           186.21
* 3.64        8.31E-01      7.58E-01        7.58E-01 Pa-231            27.36                 10.30        2.79E+00      1.78E+00        3.55E+00 283.69                  1.70       -8.55E-01                      2.28E+00 300.07                  2.47        9.02E-01                      1.78E+00 302.65                  2.20        2.64E-01                      1.98E+00 330.06                  1.40        1.65E+00                      3.01E+00
+         U-235            143.76                 10.96       -7.92E-02      4.82E-02        4.08E-01 163.33                  5.08        7.73E-02                      8.76E-01 185.71
* 57.20        5.29E-02                      4.82E-02 202.11                  1.08       -1.84E+00                      3.69E+00 205.31                  5.01       -4.90E-01                      8.35E-01 Am-241            59.54                 35.90        1.34E-01      1.12E+00        1.12E+00
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[195]

6/18/2019 11:23:30AM Page 1 of 6 Analysis Report for    18-Jun-19-10030 L1-10221C-FJGS-001SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10030 Sample Description                           : L1-10221C-FJGS-001SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.518E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:12:00AM Acquisition Started                          : 6/18/2019 11:08:20AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77463 Fill Height                                  : 1517.73 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 11:23:23AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[196]

6/18/2019   11:23:30AM         Page 2 of 6 Analysis Report for    18-Jun-19-10030 L1-10221C-FJGS-001SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.60               472 -    481          477.38          1.01E+02               16.45      7.38E+01           1.21 2       351.89               698 -    708          703.72          5.34E+01               11.75      3.56E+01           1.05 3       510.54             1016 -   1026         1020.76           3.64E+01               10.24      2.86E+01           0.74 4       583.20             1163 -   1171         1166.01           4.54E+01                8.38      1.16E+01           1.41 5       911.70             1819 -   1828         1822.84           3.30E+01                7.22      7.96E+00           1.38 6      1461.13             2916 -   2928         2922.31           2.03E+02               14.82      6.50E+00           1.72 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty An Pk                    0.96           511.00
* 100.00               3.72E-02              1.08E-02 K-40                     0.98          1460.82
* 10.66              3.82E+00              3.25E-01 Tl-208                   1.00           583.19
* 85.00              5.86E-02              1.14E-02 Bi-211                   0.89           351.07
* 13.02              3.21E-01              7.51E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              1.42E-01              2.58E-02 300.09                    3.30 Pb-214                   1.00           241.99                    7.25 295.22                  18.42 351.93
* 35.60              1.17E-01              2.74E-02 785.96                    1.06                                              [197]

6/18/2019   11:23:30AM         Page 3 of 6 Analysis Report for    18-Jun-19-10030 L1-10221C-FJGS-001SS Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Ac-228                   0.98          129.07                    2.42 209.25                    3.89 270.24                    3.46 328.00                    2.95 338.32                  11.27 409.46                    1.92 463.00                    4.40 794.95                    4.25 911.20
* 25.80              1.89E-01              4.20E-02 964.77                    4.99 968.97                  15.80 1588.20                     3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
An Pk                               0.966                     3.72E-02                1.08E-02 K-40                                0.985                     3.82E+00                3.25E-01 Tl-208                              1.000                     5.86E-02                1.14E-02
      ?       Bi-211                              0.899                     3.21E-01                7.51E-02 Pb-212                              1.000                     1.42E-01                2.58E-02
      ?       Pb-214                              1.000                     1.17E-01                2.74E-02 Ac-228                              0.988                     1.89E-01                4.20E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[198]

6/18/2019  11:23:30AM       Page 4 of 6 Analysis Report for    18-Jun-19-10030 L1-10221C-FJGS-001SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 11:23:23AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
+         An Pk           511.00
* 100.00        3.72E-02          3.16E-02        3.16E-02 BE-7            477.60              10.44       5.71E-02          3.04E-01        3.04E-01
+         K-40          1460.82
* 10.66       3.82E+00          3.18E-01        3.18E-01 Mn-54           834.85              99.98       7.43E-03          3.53E-02        3.53E-02 Co-60         1173.23               99.85       8.17E-04          2.92E-02        4.81E-02 1332.49               99.98     -4.36E-03                           2.92E-02 Nb-94           702.65              99.81     -1.23E-03           2.78E-02        2.96E-02 871.09              99.89     -6.31E-03                           2.78E-02 Ag-108m          79.13                6.60      5.34E-01          2.37E-02        1.01E+00 433.94              90.50     -2.24E-02                           2.37E-02 614.28              89.80     -2.97E-02                           4.61E-02 722.94              90.80       5.74E-03                          3.23E-02 Sb-125          176.31                6.84    -7.81E-02           9.07E-02        4.39E-01 380.45                1.52      5.26E-01                          1.68E+00 427.87              29.60       3.08E-02                          9.07E-02 463.36              10.49       4.58E-02                          3.06E-01 600.60              17.65       8.55E-02                          1.76E-01 606.71                4.98      1.05E+00                          9.68E-01 635.95              11.22       6.82E-02                          2.93E-01          [199]

6/18/2019  11:23:30AM Page 5 of 6 Analysis Report for 18-Jun-19-10030 L1-10221C-FJGS-001SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -2.84E-01      9.07E-02        1.96E+00 Ba-133        79.61            2.65    1.32E+00      5.57E-02        2.43E+00 81.00           32.90   -9.73E-02                      1.57E-01 276.40            7.16   -1.85E-02                      3.54E-01 302.85           18.34    5.76E-02                      1.53E-01 356.01           62.05   -2.52E-03                      5.57E-02 383.85            8.94   -4.21E-02                      2.75E-01 Cs-134       475.36            1.48    7.87E-01      4.08E-02        2.11E+00 563.25            8.34    1.00E-01                      3.58E-01 569.33           15.37   -1.92E-02                      2.08E-01 604.72           97.62   -1.52E-02                      4.08E-02 795.86           85.46    1.74E-02                      4.59E-02 801.95            8.69   -7.99E-02                      3.70E-01 1038.61             0.99   -1.31E+00                      3.15E+00 1167.97             1.79   -1.68E+00                      2.34E+00 1365.19             3.02    2.90E-01                      9.87E-01 Cs-137       661.66           85.10    1.28E-02      4.66E-02        4.66E-02 Eu-152       121.78           28.67   -2.12E-02      9.29E-02        9.72E-02 244.70            7.61   -7.31E-02                      3.76E-01 295.94            0.45    4.98E+00                      8.03E+00 344.28           26.60   -1.06E-01                      9.29E-02 367.79            0.86   -1.17E+00                      3.11E+00 411.12            2.24    8.23E-03                      1.28E+00 443.96            2.83   -4.92E-01                      9.44E-01 488.68            0.42   -1.35E+00                      6.99E+00 563.99            0.49    1.87E+00                      6.18E+00 586.26            0.46   -3.79E+00                      1.03E+01 678.62            0.47    1.50E+00                      7.38E+00 688.67            0.86   -4.01E-01                      3.39E+00 719.35            0.28    2.43E-01                      9.11E+00 778.90           12.96    5.25E-02                      2.70E-01 810.45            0.32   -1.94E+00                      8.27E+00 867.37            4.26   -5.47E-01                      5.49E-01 919.33            0.43   -4.27E+00                      6.74E+00 964.08           14.65   -1.05E-01                      2.70E-01 1085.87            10.24   -1.79E-01                      4.00E-01 1089.74             1.73    1.15E+00                      2.32E+00 1112.07            13.69   -3.74E-02                      2.29E-01 1212.95             1.43    5.47E-01                      2.95E+00 1249.94             0.19    7.66E+00                      2.27E+01 1299.14             1.63    7.67E-01                      2.29E+00 1408.01            21.07    1.04E-02                      1.67E-01 1457.64             0.50   -6.68E+00                      2.92E+01 1528.10             0.28    1.38E-01                      9.19E+00 Eu-154       123.07           40.40   -3.35E-02      6.54E-02        6.54E-02 247.93            6.89   -3.24E-02                      3.76E-01 591.76            4.95   -9.52E-02                      6.43E-01 692.42            1.78    1.05E+00                      1.76E+00 723.30           20.06    2.63E-02                      1.46E-01 756.80            4.52   -3.58E-01                      7.31E-01 873.18           12.08    8.87E-03                      2.54E-01
[200]

6/18/2019  11:23:30AM Page 6 of 6 Analysis Report for     18-Jun-19-10030 L1-10221C-FJGS-001SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -8.37E-02      6.54E-02        3.46E-01 1004.76                  18.01        1.22E-01                      2.16E-01 1274.43                  34.80       -1.83E-02                      9.05E-02 1596.48                   1.80        4.48E-02                      1.49E+00 Eu-155            45.30                  1.31       -5.38E+00      1.42E-01        8.77E+00 60.01                  1.22        2.86E+00                      1.15E+01 86.55                 30.70       -5.25E-03                      1.42E-01 105.31                 21.10        3.53E-02                      1.62E-01 Ra-226           186.21                  3.64        3.32E-01      8.93E-01        8.93E-01 Pa-231            27.36                 10.30        4.28E-01      9.97E-01        9.97E-01 283.69                  1.70        9.28E-01                      1.67E+00 300.07                  2.47       -1.09E+00                      1.11E+00 302.65                  2.20        4.80E-01                      1.27E+00 330.06                  1.40       -3.19E-01                      2.01E+00 U-235            143.76                 10.96        4.57E-02      5.62E-02        2.61E-01 163.33                  5.08       -3.31E-01                      5.96E-01 185.71                 57.20        1.83E-02                      5.62E-02 202.11                  1.08       -2.86E-01                      2.76E+00 205.31                  5.01       -3.30E-01                      5.50E-01 Am-241            59.54                 35.90        8.21E-02      4.02E-01        4.02E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[201]

6/18/2019 12:55:04PM Page 1 of 7 Analysis Report for    18-Jun-19-10031 L1-10221C-QJGS-001SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10031 Sample Description                           : L1-10221C-QJGS-001SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.613E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:12:00AM Acquisition Started                          : 6/18/2019 12:39:54PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77473 Fill Height                                  : 1612.68 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 12:54:57PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[202]

6/18/2019   12:55:04PM         Page 2 of 7 Analysis Report for    18-Jun-19-10031 L1-10221C-QJGS-001SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.72               474 -    482          477.61          1.06E+02               16.41      7.58E+01           1.15 2       351.98               700 -    708          703.91          5.65E+01               10.43      2.45E+01           1.52 3       583.46             1160 -   1170         1166.52           2.67E+01                8.09      1.63E+01           1.02 4       609.28             1215 -   1223         1218.14           3.68E+01                8.35      1.52E+01           0.84 5       911.52             1819 -   1826         1822.50           2.21E+01                6.32      8.87E+00           1.69 6      1461.14             2915 -   2929         2922.34           1.62E+02               13.15      3.75E+00           2.16 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.98          1460.82
* 10.66              3.01E+00              2.77E-01 Tl-208                   0.98           583.19
* 85.00              3.40E-02              1.05E-02 Bi-211                   0.87           351.07
* 13.02              3.35E-01              6.75E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.48E-01              2.57E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              9.01E-02              2.12E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92                                               [203]

6/18/2019   12:55:04PM        Page 3 of 7 Analysis Report for    18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00        1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00         241.99                  7.25 295.22                 18.42 351.93
* 35.60  1.23E-01              2.47E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.24E-01              3.59E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[204]

6/18/2019 12:55:04PM         Page 4 of 7 Analysis Report for   18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.984                     3.01E+00              2.77E-01 Tl-208                              0.988                     3.40E-02              1.05E-02
     ?       Bi-211                              0.876                     3.35E-01              6.75E-02 Pb-212                              0.999                     1.48E-01              2.57E-02 Bi-214                              1.000                     9.01E-02              2.12E-02
     ?       Pb-214                              1.000                     1.23E-01              2.47E-02 Ac-228                              0.995                     1.24E-01              3.59E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[205]

6/18/2019  12:55:04PM       Page 5 of 7 Analysis Report for    18-Jun-19-10031 L1-10221C-QJGS-001SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 12:54:57PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        7.27E-02          4.80E-02        4.80E-02 BE-7            477.60              10.44       1.60E-01          2.73E-01        2.73E-01
+         K-40          1460.82
* 10.66       3.01E+00          2.60E-01        2.60E-01 Mn-54           834.85              99.98     -7.94E-03           2.67E-02        2.67E-02 Co-60         1173.23               99.85     -1.75E-02           4.08E-02        4.15E-02 1332.49               99.98       1.80E-02                          4.08E-02 Nb-94           702.65              99.81     -8.97E-03           2.74E-02        3.63E-02 871.09              99.89     -8.80E-05                           2.74E-02 Ag-108m          79.13                6.60    -5.17E-02           2.83E-02        9.51E-01 433.94              90.50       3.33E-03                          2.83E-02 614.28              89.80     -1.53E-02                           3.90E-02 722.94              90.80     -8.37E-03                           3.94E-02 Sb-125          176.31                6.84    -1.26E-01           8.95E-02        4.37E-01 380.45                1.52    -4.00E-01                           1.70E+00 427.87              29.60     -1.79E-02                           8.95E-02 463.36              10.49       1.30E-01                          2.55E-01 600.60              17.65     -5.09E-03                           1.88E-01 606.71                4.98    -7.35E-01                           9.74E-01 635.95              11.22     -1.79E-02                           1.99E-01          [206]

6/18/2019  12:55:04PM Page 6 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    2.66E-01      8.95E-02        1.75E+00 Ba-133        79.61            2.65   -2.19E-01      5.58E-02        2.27E+00 81.00           32.90   -7.82E-02                      1.63E-01 276.40            7.16    1.85E-01                      4.04E-01 302.85           18.34    3.45E-02                      1.47E-01 356.01           62.05   -3.62E-02                      5.58E-02 383.85            8.94   -4.35E-03                      3.01E-01 Cs-134       475.36            1.48   -7.47E-01      3.94E-02        1.63E+00 563.25            8.34   -3.10E-02                      3.41E-01 569.33           15.37    6.73E-03                      1.83E-01 604.72           97.62   -5.32E-02                      4.55E-02 795.86           85.46   -2.54E-03                      3.94E-02 801.95            8.69   -6.65E-02                      3.90E-01 1038.61             0.99   -6.38E-01                      3.79E+00 1167.97             1.79   -1.70E+00                      2.59E+00 1365.19             3.02    4.37E-01                      9.71E-01 Cs-137       661.66           85.10    1.26E-02      4.09E-02        4.09E-02 Eu-152       121.78           28.67   -1.87E-02      9.50E-02        9.50E-02 244.70            7.61   -2.06E-01                      3.91E-01 295.94            0.45    1.50E+00                      6.92E+00 344.28           26.60    1.34E-02                      1.14E-01 367.79            0.86    3.06E-01                      3.10E+00 411.12            2.24   -2.86E-02                      1.30E+00 443.96            2.83    1.29E-01                      8.58E-01 488.68            0.42    3.04E+00                      7.88E+00 563.99            0.49   -8.59E-01                      5.69E+00 586.26            0.46   -4.07E+00                      8.86E+00 678.62            0.47    1.39E-01                      6.17E+00 688.67            0.86   -5.36E-01                      3.10E+00 719.35            0.28   -2.28E+00                      1.11E+01 778.90           12.96   -1.69E-02                      2.46E-01 810.45            0.32    2.81E+00                      1.02E+01 867.37            4.26   -2.93E-01                      6.42E-01 919.33            0.43   -2.30E+00                      7.72E+00 964.08           14.65   -1.97E-01                      3.08E-01 1085.87            10.24   -4.06E-02                      3.09E-01 1089.74             1.73    6.14E-01                      2.23E+00 1112.07            13.69   -1.86E-01                      3.34E-01 1212.95             1.43    2.74E-01                      2.62E+00 1249.94             0.19    1.05E+01                      2.12E+01 1299.14             1.63   -1.87E+00                      2.10E+00 1408.01            21.07   -1.52E-01                      1.14E-01 1457.64             0.50   -4.71E+00                      2.55E+01 1528.10             0.28   -4.65E+00                      8.11E+00 Eu-154       123.07           40.40    5.05E-03      6.84E-02        6.84E-02 247.93            6.89   -5.15E-02                      3.82E-01 591.76            4.95   -1.93E-01                      5.83E-01 692.42            1.78   -1.65E-01                      1.62E+00 723.30           20.06   -2.02E-02                      1.81E-01 756.80            4.52   -2.98E-01                      7.35E-01 873.18           12.08    9.62E-02                      2.35E-01
[207]

6/18/2019  12:55:04PM Page 7 of 7 Analysis Report for     18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        7.10E-02      6.84E-02        4.01E-01 1004.76                  18.01       -2.63E-02                      2.18E-01 1274.43                  34.80       -2.72E-02                      1.04E-01 1596.48                   1.80       -1.12E+00                      1.31E+00 Eu-155            45.30                  1.31       -1.66E+00      1.41E-01        8.98E+00 60.01                  1.22       -6.99E-01                      9.87E+00 86.55                 30.70       -3.39E-02                      1.41E-01 105.31                 21.10        1.46E-01                      1.77E-01 Ra-226           186.21                  3.64        3.60E-01      8.90E-01        8.90E-01 Pa-231            27.36                 10.30        7.41E-01      1.06E+00        1.08E+00 283.69                  1.70       -7.74E-01                      1.46E+00 300.07                  2.47       -1.02E+00                      1.06E+00 302.65                  2.20        2.87E-01                      1.23E+00 330.06                  1.40        2.75E-01                      2.15E+00 U-235            143.76                 10.96       -1.36E-02      5.66E-02        2.36E-01 163.33                  5.08        2.43E-01                      6.12E-01 185.71                 57.20        1.67E-02                      5.66E-02 202.11                  1.08        1.47E+00                      2.77E+00 205.31                  5.01       -2.32E-01                      5.67E-01 Am-241            59.54                 35.90       -4.59E-02      3.43E-01        3.43E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[208]

6/18/2019 11:24:20AM Page 1 of 7 Analysis Report for    18-Jun-19-10032 L1-10221C-FJGS-002SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10032 Sample Description                           : L1-10221C-FJGS-002SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.739E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:14:00AM Acquisition Started                          : 6/18/2019 11:09:05AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.0 seconds Dead Time                                    : 0.11 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77464 Fill Height                                  : 1738.60 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 11:24:09AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[209]

6/18/2019   11:24:20AM         Page 2 of 7 Analysis Report for    18-Jun-19-10032 L1-10221C-FJGS-002SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.55               947 -    960          954.28          1.04E+02               14.57      3.86E+01           0.78 2       295.06             1175 -   1186         1180.14           1.70E+01                8.34      2.10E+01           0.46 3       351.70             1401 -   1410         1406.53           2.70E+01                7.99      1.60E+01           0.53 4       582.81             2324 -   2336         2330.43           2.75E+01                7.25      9.50E+00           0.31 5       608.82             2429 -   2440         2434.45           2.74E+01                6.26      4.60E+00           0.71 6      1459.83             5829 -   5849         5839.16           1.41E+02               12.22      2.50E+00           1.38 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.85          1460.82
* 10.66              3.38E+00              3.29E-01 Tl-208                   0.97           583.19
* 85.00              4.47E-02              1.21E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.83E-01              2.95E-02 300.09                    3.30 Bi-214                   0.98           609.32
* 45.49              8.56E-02              2.02E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63                                              [210]

6/18/2019   11:24:20AM         Page 3 of 7 Analysis Report for    18-Jun-19-10032 L1-10221C-FJGS-002SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   0.98        1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42       7.92E-02              3.94E-02 351.93
* 35.60       7.37E-02              2.26E-02 785.96                  1.06
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean                Wt mean     Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
K-40                              0.855               3.38E+00               3.29E-01 Tl-208                            0.977               4.47E-02               1.21E-02 X       Bi-211                            0.938 Pb-212                            0.999               1.83E-01               2.95E-02 Bi-214                            0.984               8.56E-02               2.02E-02 Pb-214                            0.994               7.51E-02               1.96E-02
[211]

6/18/2019 11:24:20AM Page 4 of 7 Analysis Report for   18-Jun-19-10032 L1-10221C-FJGS-002SS
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[212]

6/18/2019  11:24:20AM       Page 5 of 7 Analysis Report for    18-Jun-19-10032 L1-10221C-FJGS-002SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 11:24:09AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        7.07E-02          5.43E-02        5.43E-02 BE-7            477.60              10.44       1.35E-01          3.36E-01        3.36E-01
+         K-40          1460.82
* 10.66       3.38E+00          3.11E-01        3.11E-01 Mn-54           834.85              99.98     -2.49E-02           3.78E-02        3.78E-02 Co-60         1173.23               99.85     -1.66E-02           5.00E-02        5.00E-02 1332.49               99.98       4.26E-02                          6.20E-02 Nb-94           702.65              99.81       7.84E-04          3.88E-02        3.90E-02 871.09              99.89       1.62E-02                          3.88E-02 Ag-108m          79.13                6.60      4.73E-01          3.87E-02        1.64E+00 433.94              90.50       1.47E-02                          4.04E-02 614.28              89.80     -2.29E-02                           3.87E-02 722.94              90.80       3.46E-03                          4.72E-02 Sb-125          176.31                6.84    -2.36E-02           1.18E-01        4.68E-01 380.45                1.52    -7.82E-01                           2.09E+00 427.87              29.60     -1.82E-02                           1.18E-01 463.36              10.49       3.77E-01                          3.98E-01 600.60              17.65     -5.02E-02                           2.11E-01 606.71                4.98      9.79E-01                          1.03E+00 635.95              11.22     -7.26E-02                           2.63E-01          [213]

6/18/2019  11:24:20AM Page 6 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.79E+00      1.18E-01        2.32E+00 Ba-133        79.61            2.65   -1.55E+00      5.93E-02        3.82E+00 81.00           32.90   -1.40E-01                      2.76E-01 276.40            7.16   -1.88E-01                      4.22E-01 302.85           18.34   -9.37E-03                      1.62E-01 356.01           62.05   -4.50E-02                      5.93E-02 383.85            8.94   -1.12E-01                      3.67E-01 Cs-134       475.36            1.48   -3.56E-01      4.02E-02        2.41E+00 563.25            8.34    1.12E-01                      3.67E-01 569.33           15.37    9.51E-02                      2.15E-01 604.72           97.62   -1.40E-02                      5.29E-02 795.86           85.46   -2.76E-02                      4.02E-02 801.95            8.69   -2.90E-01                      3.55E-01 1038.61             0.99    1.09E+00                      4.54E+00 1167.97             1.79    2.70E+00                      3.12E+00 1365.19             3.02   -9.78E-01                      1.18E+00 Cs-137       661.66           85.10    7.32E-02      6.32E-02        6.32E-02 Eu-152       121.78           28.67   -6.97E-02      1.20E-01        1.22E-01 244.70            7.61    3.92E-02                      4.32E-01 295.94            0.45    1.47E+00                      8.42E+00 344.28           26.60    6.36E-02                      1.20E-01 367.79            0.86   -1.41E+00                      3.64E+00 411.12            2.24    8.07E-01                      1.46E+00 443.96            2.83    8.19E-01                      1.23E+00 488.68            0.42    3.36E+00                      7.82E+00 563.99            0.49    3.77E+00                      6.39E+00 586.26            0.46   -3.33E+00                      1.13E+01 678.62            0.47   -7.92E+00                      6.32E+00 688.67            0.86    4.50E-01                      4.56E+00 719.35            0.28   -6.08E+00                      1.19E+01 778.90           12.96   -1.55E-02                      3.01E-01 810.45            0.32   -5.61E+00                      1.18E+01 867.37            4.26   -6.54E-02                      9.33E-01 919.33            0.43    6.69E+00                      1.09E+01 964.08           14.65    3.04E-01                      3.42E-01 1085.87            10.24    4.27E-02                      4.64E-01 1089.74             1.73    9.32E-01                      2.53E+00 1112.07            13.69   -1.30E-01                      2.68E-01 1212.95             1.43   -4.99E-01                      3.49E+00 1249.94             0.19    1.52E+00                      2.53E+01 1299.14             1.63    5.17E-01                      2.72E+00 1408.01            21.07   -1.43E-01                      1.85E-01 1457.64             0.50    7.45E+01                      3.10E+01 1528.10             0.28    4.72E+00                      1.28E+01 Eu-154       123.07           40.40    1.63E-02      9.24E-02        9.24E-02 247.93            6.89    1.40E-01                      4.43E-01 591.76            4.95    5.26E-02                      7.70E-01 692.42            1.78   -1.75E-01                      2.30E+00 723.30           20.06   -1.44E-02                      2.14E-01 756.80            4.52    1.79E-01                      8.86E-01 873.18           12.08    2.18E-02                      2.92E-01
[214]

6/18/2019  11:24:20AM Page 7 of 7 Analysis Report for     18-Jun-19-10032 L1-10221C-FJGS-002SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        2.22E-01      9.24E-02        4.28E-01 1004.76                  18.01       -1.37E-02                      2.51E-01 1274.43                  34.80        1.79E-02                      1.21E-01 1596.48                   1.80        9.19E-01                      2.24E+00 Eu-155            45.30                  1.31        1.53E+00      2.42E-01        2.83E+01 60.01                  1.22        7.98E-01                      2.70E+01 86.55                 30.70       -3.63E-02                      2.42E-01 105.31                 21.10        4.02E-02                      2.50E-01 Ra-226           186.21                  3.64       -3.11E-01      1.00E+00        1.00E+00 Pa-231            27.36                 10.30        1.67E+00      1.27E+00        3.09E+00 283.69                  1.70        2.86E-01                      1.99E+00 300.07                  2.47       -1.91E-02                      1.27E+00 302.65                  2.20        1.82E-01                      1.35E+00 330.06                  1.40        1.60E-02                      2.49E+00 U-235            143.76                 10.96       -4.28E-02      6.61E-02        3.65E-01 163.33                  5.08       -2.26E-01                      6.96E-01 185.71                 57.20        2.30E-03                      6.61E-02 202.11                  1.08       -3.35E+00                      2.88E+00 205.31                  5.01        1.73E-01                      6.56E-01 Am-241            59.54                 35.90        1.76E-01      9.87E-01        9.87E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[215]

6/18/2019 11:24:25AM Page 1 of 6 Analysis Report for    18-Jun-19-10033 L1-10221C-FJGS-003SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10033 Sample Description                           : L1-10221C-FJGS-003SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.635E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:16:00AM Acquisition Started                          : 6/18/2019 11:09:14AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77465 Fill Height                                  : 1635.46 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 11:24:16AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[216]

6/18/2019   11:24:25AM         Page 2 of 6 Analysis Report for    18-Jun-19-10033 L1-10221C-FJGS-003SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.88               946 -    960          955.08          7.34E+01               12.89      3.26E+01           0.91 2       295.06             1174 -   1183         1179.52           2.45E+01                8.00      1.75E+01           0.86 3       351.94             1400 -   1415         1406.76           7.77E+01                9.23      2.25E+00           1.04 4       609.23             2430 -   2441         2434.98           3.90E+01                7.36      6.00E+00           0.76 5      1460.38             5830 -   5850         5839.46           1.62E+02               12.73      0.00E+00           1.51 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.96          1460.82
* 10.66              3.57E+00              3.20E-01 Bi-211                   0.88           351.07
* 13.02              5.28E-01              7.58E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.15E-01              2.23E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.11E-01              2.21E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83                                              [217]

6/18/2019   11:24:25AM         Page 3 of 6 Analysis Report for    18-Jun-19-10033 L1-10221C-FJGS-003SS Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Bi-214                   1.00        1280.98                     1.43 1377.67                     3.99 1385.31                     0.79 1401.52                     1.33 1407.99                     2.39 1509.21                     2.13 1661.27                     1.05 1729.59                     2.88 1764.49                   15.30 1847.43                     2.03 2118.51                     1.16 Pb-214                   0.99          241.99                    7.25 295.22
* 18.42              1.03E-01              3.48E-02 351.93
* 35.60              1.93E-01              2.77E-02 785.96                    1.06
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
K-40                                0.969                     3.57E+00                3.20E-01 Bi-211                              0.887                     2.46E-01                1.21E-01 Pb-212                              0.991                     1.15E-01                2.23E-02 Bi-214                              1.000                     1.11E-01                2.21E-02 Pb-214                              0.999                     1.03E-01                3.48E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[218]

6/18/2019  11:24:25AM       Page 4 of 6 Analysis Report for    18-Jun-19-10033 L1-10221C-FJGS-003SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 11:24:16AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        4.06E-02          4.52E-02        4.52E-02 BE-7            477.60              10.44       1.05E-01          3.06E-01        3.06E-01
+         K-40          1460.82
* 10.66       3.57E+00          6.33E-02        6.33E-02 Mn-54           834.85              99.98       1.64E-02          3.83E-02        3.83E-02 Co-60         1173.23               99.85       1.50E-02          3.20E-02        5.42E-02 1332.49               99.98     -5.48E-04                           3.20E-02 Nb-94           702.65              99.81       1.85E-02          3.74E-02        4.24E-02 871.09              99.89       6.88E-03                          3.74E-02 Ag-108m          79.13                6.60      9.99E-01          2.94E-02        1.04E+00 433.94              90.50     -1.82E-02                           2.94E-02 614.28              89.80     -2.21E-02                           4.60E-02 722.94              90.80       2.05E-02                          4.15E-02 Sb-125          176.31                6.84      1.16E-01          7.79E-02        3.32E-01 380.45                1.52    -9.51E-01                           1.54E+00 427.87              29.60     -4.13E-02                           7.79E-02 463.36              10.49       2.66E-01                          3.37E-01 600.60              17.65     -1.68E-01                           1.73E-01 606.71                4.98      1.16E+00                          1.07E+00 635.95              11.22     -1.79E-02                           2.77E-01          [219]

6/18/2019  11:24:25AM Page 5 of 6 Analysis Report for 18-Jun-19-10033 L1-10221C-FJGS-003SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    6.23E-01      7.79E-02        2.01E+00 Ba-133        79.61            2.65    1.37E+00      5.80E-02        2.46E+00 81.00           32.90   -1.90E-01                      1.50E-01 276.40            7.16    4.96E-02                      3.66E-01 302.85           18.34   -2.95E-02                      1.45E-01 356.01           62.05    1.07E-02                      5.80E-02 383.85            8.94    1.23E-02                      2.68E-01 Cs-134       475.36            1.48    2.04E+00      3.79E-02        2.19E+00 563.25            8.34   -1.66E-01                      3.75E-01 569.33           15.37    7.06E-02                      1.87E-01 604.72           97.62   -3.34E-02                      4.69E-02 795.86           85.46   -1.53E-02                      3.79E-02 801.95            8.69   -2.93E-01                      4.08E-01 1038.61             0.99    3.29E-01                      3.79E+00 1167.97             1.79    1.07E+00                      3.12E+00 1365.19             3.02    5.33E-01                      1.39E+00 Cs-137       661.66           85.10   -3.74E-03      4.10E-02        4.10E-02 Eu-152       121.78           28.67    3.15E-02      1.04E-01        1.04E-01 244.70            7.61   -4.89E-03                      3.95E-01 295.94            0.45    6.39E+00                      7.82E+00 344.28           26.60   -2.79E-02                      1.06E-01 367.79            0.86   -3.18E-01                      2.99E+00 411.12            2.24    9.56E-01                      1.35E+00 443.96            2.83   -4.66E-01                      9.54E-01 488.68            0.42   -5.24E-01                      6.46E+00 563.99            0.49   -1.14E+00                      6.10E+00 586.26            0.46    8.48E+00                      1.03E+01 678.62            0.47    1.85E-02                      7.81E+00 688.67            0.86    2.71E-01                      3.72E+00 719.35            0.28   -5.60E+00                      1.05E+01 778.90           12.96   -3.00E-02                      2.46E-01 810.45            0.32    3.80E+00                      1.14E+01 867.37            4.26   -2.06E-02                      8.29E-01 919.33            0.43    4.34E+00                      8.85E+00 964.08           14.65   -8.12E-02                      3.63E-01 1085.87            10.24    2.19E-01                      4.24E-01 1089.74             1.73   -1.98E-01                      2.45E+00 1112.07            13.69   -2.28E-01                      3.05E-01 1212.95             1.43    2.33E+00                      3.74E+00 1249.94             0.19    1.89E+01                      2.52E+01 1299.14             1.63   -2.32E+00                      2.18E+00 1408.01            21.07    1.03E-01                      2.33E-01 1457.64             0.50    7.60E+01                      2.99E+01 1528.10             0.28    1.23E-01                      1.34E+01 Eu-154       123.07           40.40    4.29E-02      7.42E-02        7.42E-02 247.93            6.89   -3.45E-02                      3.84E-01 591.76            4.95    1.97E-01                      6.53E-01 692.42            1.78    1.52E+00                      2.22E+00 723.30           20.06    8.59E-02                      1.88E-01 756.80            4.52    2.48E-01                      6.48E-01 873.18           12.08    2.77E-01                      3.68E-01
[220]

6/18/2019  11:24:25AM Page 6 of 6 Analysis Report for     18-Jun-19-10033 L1-10221C-FJGS-003SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        8.21E-02      7.42E-02        3.81E-01 1004.76                  18.01        1.23E-01                      2.35E-01 1274.43                  34.80        4.37E-02                      1.49E-01 1596.48                   1.80       -9.80E-02                      2.53E+00 Eu-155            45.30                  1.31        3.36E+00      1.50E-01        9.86E+00 60.01                  1.22        2.76E+00                      1.01E+01 86.55                 30.70        9.26E-03                      1.51E-01 105.31                 21.10       -8.31E-02                      1.50E-01 Ra-226           186.21                  3.64        6.71E-01      8.44E-01        8.44E-01 Pa-231            27.36                 10.30        9.58E-01      1.12E+00        1.13E+00 283.69                  1.70       -3.91E-01                      1.52E+00 300.07                  2.47       -7.16E-01                      1.12E+00 302.65                  2.20       -4.66E-01                      1.22E+00 330.06                  1.40       -3.27E-01                      2.05E+00 U-235            143.76                 10.96        4.86E-02      5.21E-02        2.29E-01 163.33                  5.08       -1.68E-01                      4.47E-01 185.71                 57.20        1.72E-02                      5.21E-02 202.11                  1.08        2.37E-01                      2.45E+00 205.31                  5.01       -2.50E-01                      4.94E-01 Am-241            59.54                 35.90        4.18E-02      3.64E-01        3.64E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[221]

6/18/2019 12:25:12PM Page 1 of 6 Analysis Report for    18-Jun-19-10034 L1-10221C-FJGS-004SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10034 Sample Description                           : L1-10221C-FJGS-004SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.701E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:18:00AM Acquisition Started                          : 6/18/2019 12:09:59PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.9 seconds Dead Time                                    : 0.10 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77467 Fill Height                                  : 1700.89 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 12:25:03PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[222]

6/18/2019   12:25:12PM         Page 2 of 6 Analysis Report for    18-Jun-19-10034 L1-10221C-FJGS-004SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.38               948 - 959             953.62          5.79E+01               12.51      3.81E+01           0.66 2       351.77             1402 - 1414           1406.80           3.45E+01                9.03      1.75E+01           0.66 3       609.08             2431 - 2441           2435.48           2.50E+01                6.37      5.99E+00           0.54 4      1459.87             5830 - 5849           5839.32           1.02E+02               10.86      4.61E+00           1.65 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.86          1460.82
* 10.66              2.48E+00              2.84E-01 Bi-211                   0.92           351.07
* 13.02              2.59E-01              7.09E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.02E-01              2.34E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              7.85E-02              2.05E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83 1280.98                    1.43                                              [223]

6/18/2019   12:25:12PM         Page 3 of 6 Analysis Report for    18-Jun-19-10034 L1-10221C-FJGS-004SS Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Bi-214                   0.99        1377.67                     3.99 1385.31                     0.79 1401.52                     1.33 1407.99                     2.39 1509.21                     2.13 1661.27                     1.05 1729.59                     2.88 1764.49                   15.30 1847.43                     2.03 2118.51                     1.16 Pb-214                   0.99          241.99                    7.25 295.22                  18.42 351.93
* 35.60              9.46E-02              2.59E-02 785.96                    1.06
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
K-40                                0.865                     2.48E+00                2.84E-01
      ?       Bi-211                              0.925                     2.59E-01                7.09E-02 Pb-212                              0.991                     1.02E-01                2.34E-02 Bi-214                              0.996                     7.85E-02                2.05E-02
      ?       Pb-214                              0.997                     9.46E-02                2.59E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[224]

6/18/2019  12:25:12PM       Page 4 of 6 Analysis Report for    18-Jun-19-10034 L1-10221C-FJGS-004SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 12:25:03PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        4.92E-02          5.30E-02        5.30E-02 BE-7            477.60              10.44       1.73E-01          3.95E-01        3.95E-01
+         K-40          1460.82
* 10.66       2.48E+00          3.93E-01        3.93E-01 Mn-54           834.85              99.98     -2.13E-02           3.90E-02        3.90E-02 Co-60         1173.23               99.85       1.97E-02          4.70E-02        5.85E-02 1332.49               99.98       1.42E-02                          4.70E-02 Nb-94           702.65              99.81       3.03E-05          3.78E-02        4.31E-02 871.09              99.89     -3.63E-03                           3.78E-02 Ag-108m          79.13                6.60      3.13E-01          3.42E-02        1.57E+00 433.94              90.50       1.06E-02                          3.42E-02 614.28              89.80       3.22E-03                          4.59E-02 722.94              90.80     -2.51E-03                           4.57E-02 Sb-125          176.31                6.84      2.33E-01          9.01E-02        5.00E-01 380.45                1.52      1.14E+00                          2.18E+00 427.87              29.60     -9.38E-02                           9.01E-02 463.36              10.49       2.09E-01                          3.66E-01 600.60              17.65       3.17E-04                          1.91E-01 606.71                4.98      4.51E-01                          9.72E-01 635.95              11.22       7.21E-02                          3.52E-01          [225]

6/18/2019  12:25:12PM Page 5 of 6 Analysis Report for 18-Jun-19-10034 L1-10221C-FJGS-004SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -2.01E+00      9.01E-02        2.07E+00 Ba-133        79.61            2.65   -2.68E+00      5.45E-02        3.59E+00 81.00           32.90   -2.65E-01                      2.59E-01 276.40            7.16    2.40E-01                      4.84E-01 302.85           18.34    5.20E-02                      1.88E-01 356.01           62.05   -2.20E-02                      5.45E-02 383.85            8.94    2.62E-01                      3.82E-01 Cs-134       475.36            1.48    1.63E-01      3.90E-02        2.62E+00 563.25            8.34    2.36E-01                      4.59E-01 569.33           15.37   -1.69E-01                      2.06E-01 604.72           97.62   -3.91E-02                      4.67E-02 795.86           85.46    1.13E-02                      3.90E-02 801.95            8.69   -1.25E-01                      3.25E-01 1038.61             0.99    4.65E-01                      4.31E+00 1167.97             1.79    5.61E-01                      3.26E+00 1365.19             3.02   -1.63E-01                      1.01E+00 Cs-137       661.66           85.10    5.00E-02      6.10E-02        6.10E-02 Eu-152       121.78           28.67    9.51E-03      1.20E-01        1.29E-01 244.70            7.61   -8.73E-02                      4.49E-01 295.94            0.45    5.02E+00                      9.01E+00 344.28           26.60    4.43E-02                      1.20E-01 367.79            0.86   -6.31E-02                      3.80E+00 411.12            2.24    9.08E-01                      1.44E+00 443.96            2.83    2.91E-01                      1.44E+00 488.68            0.42    2.06E-01                      7.42E+00 563.99            0.49    3.89E+00                      7.80E+00 586.26            0.46    1.23E+01                      1.10E+01 678.62            0.47    1.92E-01                      7.38E+00 688.67            0.86   -8.08E-01                      3.26E+00 719.35            0.28    2.72E+00                      1.23E+01 778.90           12.96    1.04E-01                      2.62E-01 810.45            0.32    2.41E+00                      1.01E+01 867.37            4.26    5.38E-01                      1.01E+00 919.33            0.43   -1.71E+00                      8.59E+00 964.08           14.65    1.83E-01                      3.57E-01 1085.87            10.24   -2.13E-02                      5.00E-01 1089.74             1.73    8.13E-01                      2.83E+00 1112.07            13.69   -7.09E-02                      3.25E-01 1212.95             1.43   -3.77E-01                      3.50E+00 1249.94             0.19    2.20E+01                      2.84E+01 1299.14             1.63   -1.77E+00                      1.82E+00 1408.01            21.07    1.07E-01                      2.06E-01 1457.64             0.50    4.96E+01                      2.73E+01 1528.10             0.28    6.64E+00                      1.48E+01 Eu-154       123.07           40.40    4.03E-02      9.54E-02        9.54E-02 247.93            6.89   -8.26E-02                      4.49E-01 591.76            4.95   -1.46E-01                      6.73E-01 692.42            1.78    5.12E-01                      1.93E+00 723.30           20.06    1.67E-01                      2.15E-01 756.80            4.52    9.52E-02                      8.28E-01 873.18           12.08    5.64E-02                      3.23E-01
[226]

6/18/2019  12:25:12PM Page 6 of 6 Analysis Report for     18-Jun-19-10034 L1-10221C-FJGS-004SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.42E-01      9.54E-02        4.07E-01 1004.76                  18.01        1.67E-01                      2.38E-01 1274.43                  34.80        6.32E-03                      1.67E-01 1596.48                   1.80        1.08E+00                      2.40E+00 Eu-155            45.30                  1.31       -5.97E+00      1.97E-01        2.30E+01 60.01                  1.22        1.55E+00                      2.40E+01 86.55                 30.70       -1.67E-01                      2.12E-01 105.31                 21.10       -9.18E-02                      1.97E-01 Ra-226           186.21                  3.64        8.39E-01      9.01E-01        9.01E-01 Pa-231            27.36                 10.30        2.32E+00      1.50E+00        2.83E+00 283.69                  1.70       -1.17E+00                      1.76E+00 300.07                  2.47        3.49E-01                      1.50E+00 302.65                  2.20        3.94E-01                      1.57E+00 330.06                  1.40       -6.98E-01                      2.07E+00 U-235            143.76                 10.96       -2.60E-03      5.60E-02        3.32E-01 163.33                  5.08        3.51E-02                      6.48E-01 185.71                 57.20        2.35E-02                      5.60E-02 202.11                  1.08       -1.42E+00                      3.12E+00 205.31                  5.01       -2.89E-01                      6.31E-01 Am-241            59.54                 35.90       -5.28E-02      8.59E-01        8.59E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[227]

6/18/2019 12:25:17PM Page 1 of 7 Analysis Report for    18-Jun-19-10035 L1-10221C-FJGS-005SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10035 Sample Description                           : L1-10221C-FJGS-005SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.718E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:20:00AM Acquisition Started                          : 6/18/2019 12:10:06PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77468 Fill Height                                  : 1717.57 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 12:25:08PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[228]

6/18/2019   12:25:17PM         Page 2 of 7 Analysis Report for    18-Jun-19-10035 L1-10221C-FJGS-005SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.70               948 -    961          954.38          7.95E+01               13.62      3.85E+01           1.04 2       352.13             1400 -   1413         1407.52           5.51E+01                8.64      6.85E+00           0.64 3       583.19             2326 -   2335         2330.88           1.73E+01                6.08      8.72E+00           0.30 4       609.19             2429 -   2441         2434.80           3.60E+01                7.18      5.99E+00           0.79 5       911.11             3637 -   3646         3641.91           2.00E+01                4.47      0.00E+00           0.83 6      1460.58             5830 -   5850         5840.27           1.29E+02               12.12      5.01E+00           1.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              2.81E+00              2.90E-01 Tl-208                   1.00           583.19
* 85.00              2.54E-02              9.05E-03 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.24E-01              2.35E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              1.02E-01              2.12E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63                                              [229]

6/18/2019   12:25:17PM        Page 3 of 7 Analysis Report for    18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99        1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22                 18.42 351.93
* 35.60  1.36E-01              2.39E-02 785.96                  1.06 Ac-228                   1.00         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.31E-01              2.98E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[230]

6/18/2019 12:25:17PM         Page 4 of 7 Analysis Report for   18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.991                     2.81E+00              2.90E-01 Tl-208                              1.000                     2.54E-02              9.05E-03 Pb-212                              0.999                     1.24E-01              2.35E-02 Bi-214                              0.999                     1.02E-01              2.12E-02 Pb-214                              0.997                     1.36E-01              2.39E-02 Ac-228                              1.000                     1.31E-01              2.98E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[231]

6/18/2019  12:25:17PM       Page 5 of 7 Analysis Report for    18-Jun-19-10035 L1-10221C-FJGS-005SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 12:25:08PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.27E-02          4.74E-02        4.74E-02 BE-7            477.60              10.44       7.52E-02          3.47E-01        3.47E-01
+         K-40          1460.82
* 10.66       2.81E+00          3.74E-01        3.74E-01 Mn-54           834.85              99.98       5.97E-03          3.32E-02        3.32E-02 Co-60         1173.23               99.85       4.25E-03          4.07E-02        4.96E-02 1332.49               99.98     -3.79E-03                           4.07E-02 Nb-94           702.65              99.81     -3.55E-03           2.82E-02        3.21E-02 871.09              99.89       1.47E-02                          2.82E-02 Ag-108m          79.13                6.60      6.53E-01          3.02E-02        9.36E-01 433.94              90.50     -6.88E-03                           3.02E-02 614.28              89.80       4.73E-03                          3.94E-02 722.94              90.80       1.73E-02                          3.78E-02 Sb-125          176.31                6.84      9.95E-02          1.04E-01        3.60E-01 380.45                1.52    -8.61E-01                           1.58E+00 427.87              29.60       5.03E-03                          1.04E-01 463.36              10.49     -1.02E-02                           2.58E-01 600.60              17.65     -1.45E-01                           1.76E-01 606.71                4.98      1.14E+00                          1.04E+00 635.95              11.22     -8.85E-02                           2.30E-01          [232]

6/18/2019  12:25:17PM Page 6 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -2.80E-01      1.04E-01        1.60E+00 Ba-133        79.61            2.65    2.21E+00      5.10E-02        2.33E+00 81.00           32.90   -1.26E-01                      1.55E-01 276.40            7.16    2.48E-01                      3.81E-01 302.85           18.34    1.73E-02                      1.44E-01 356.01           62.05   -2.09E-02                      5.10E-02 383.85            8.94    1.94E-01                      3.09E-01 Cs-134       475.36            1.48    8.13E-01      4.08E-02        2.30E+00 563.25            8.34   -4.05E-01                      3.79E-01 569.33           15.37    2.62E-02                      2.22E-01 604.72           97.62   -3.04E-02                      4.83E-02 795.86           85.46    3.06E-02                      4.08E-02 801.95            8.69   -5.03E-02                      3.71E-01 1038.61             0.99   -2.32E+00                      3.36E+00 1167.97             1.79   -1.84E-01                      2.76E+00 1365.19             3.02   -2.74E-01                      1.26E+00 Cs-137       661.66           85.10   -1.14E-02      3.62E-02        3.62E-02 Eu-152       121.78           28.67    3.90E-02      9.25E-02        9.25E-02 244.70            7.61    3.23E-02                      3.74E-01 295.94            0.45    3.24E+00                      6.77E+00 344.28           26.60    4.40E-02                      1.00E-01 367.79            0.86   -4.81E-01                      2.87E+00 411.12            2.24   -5.23E-01                      1.22E+00 443.96            2.83    5.34E-01                      1.05E+00 488.68            0.42    1.45E+00                      6.68E+00 563.99            0.49   -1.24E+01                      5.77E+00 586.26            0.46    9.46E+00                      9.45E+00 678.62            0.47    7.66E-01                      5.91E+00 688.67            0.86   -5.23E-01                      3.49E+00 719.35            0.28    1.21E+00                      9.30E+00 778.90           12.96    1.14E-02                      2.85E-01 810.45            0.32    4.64E+00                      1.01E+01 867.37            4.26   -1.56E-01                      6.90E-01 919.33            0.43    5.55E+00                      8.26E+00 964.08           14.65    8.97E-02                      3.49E-01 1085.87            10.24   -2.23E-01                      4.19E-01 1089.74             1.73    1.86E+00                      2.49E+00 1112.07            13.69    3.18E-02                      3.34E-01 1212.95             1.43   -7.92E-01                      2.57E+00 1249.94             0.19   -5.98E+00                      1.98E+01 1299.14             1.63    5.18E-01                      2.46E+00 1408.01            21.07   -1.13E-01                      1.76E-01 1457.64             0.50    6.31E+01                      2.72E+01 1528.10             0.28    5.96E+00                      1.33E+01 Eu-154       123.07           40.40    8.18E-03      6.31E-02        6.31E-02 247.93            6.89   -1.26E-01                      3.43E-01 591.76            4.95    3.88E-01                      6.20E-01 692.42            1.78    5.13E-02                      1.92E+00 723.30           20.06   -5.82E-02                      1.67E-01 756.80            4.52   -2.70E-01                      6.64E-01 873.18           12.08   -2.11E-02                      2.34E-01
[233]

6/18/2019  12:25:17PM Page 7 of 7 Analysis Report for     18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        2.22E-01      6.31E-02        3.45E-01 1004.76                  18.01       -1.62E-01                      1.88E-01 1274.43                  34.80       -1.23E-01                      1.22E-01 1596.48                   1.80       -5.99E-01                      1.55E+00 Eu-155            45.30                  1.31       -5.92E-01      1.36E-01        7.73E+00 60.01                  1.22        3.28E-01                      9.48E+00 86.55                 30.70        1.46E-02                      1.47E-01 105.31                 21.10       -4.93E-02                      1.36E-01 Ra-226           186.21                  3.64        1.14E-01      6.57E-01        6.57E-01 Pa-231            27.36                 10.30        6.58E-01      9.83E-01        9.83E-01 283.69                  1.70       -9.72E-01                      1.44E+00 300.07                  2.47       -9.73E-01                      1.03E+00 302.65                  2.20        2.65E-01                      1.20E+00 330.06                  1.40        1.17E+00                      2.02E+00 U-235            143.76                 10.96       -1.61E-01      4.24E-02        2.25E-01 163.33                  5.08        9.18E-02                      5.23E-01 185.71                 57.20        1.58E-02                      4.24E-02 202.11                  1.08       -1.31E+00                      1.85E+00 205.31                  5.01        2.23E-01                      4.78E-01 Am-241            59.54                 35.90       -4.44E-02      3.12E-01        3.12E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[234]

6/18/2019 12:25:34PM Page 1 of 6 Analysis Report for    18-Jun-19-10036 L1-10221C-FJGS-006SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10036 Sample Description                           : L1-10221C-FJGS-006SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.618E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:22:00AM Acquisition Started                          : 6/18/2019 12:10:14PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77469 Fill Height                                  : 1618.20 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 12:25:26PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[235]

6/18/2019   12:25:34PM         Page 2 of 6 Analysis Report for    18-Jun-19-10036 L1-10221C-FJGS-006SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.53               948 -    959          954.59          6.05E+01               11.45      2.75E+01           1.37 2       295.29             1177 -   1186         1181.36           2.35E+01                7.25      1.16E+01           0.69 3       351.75             1402 -   1413         1407.01           3.50E+01                7.08      6.00E+00           0.70 4       609.00             2428 -   2441         2435.26           2.73E+01                8.40      1.57E+01           0.49 5      1460.57             5832 -   5852         5842.64           1.42E+02               13.37      1.03E+01           0.58 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              2.92E+00              3.03E-01 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              9.39E-02              1.93E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              7.41E-02              2.32E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83 1280.98                    1.43                                              [236]

6/18/2019   12:25:34PM         Page 3 of 6 Analysis Report for    18-Jun-19-10036 L1-10221C-FJGS-006SS Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Bi-214                   0.99        1377.67                     3.99 1385.31                     0.79 1401.52                     1.33 1407.99                     2.39 1509.21                     2.13 1661.27                     1.05 1729.59                     2.88 1764.49                   15.30 1847.43                     2.03 2118.51                     1.16 Pb-214                   0.99          241.99                    7.25 295.22
* 18.42              9.66E-02              3.09E-02 351.93
* 35.60              8.43E-02              1.83E-02 785.96                    1.06
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
K-40                                0.990                     2.92E+00                3.03E-01 X       Bi-211                              0.928 Pb-212                              0.998                     9.39E-02                1.93E-02 Bi-214                              0.993                     7.41E-02                2.32E-02 Pb-214                              0.997                     8.75E-02                1.58E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[237]

6/18/2019  12:25:34PM       Page 4 of 6 Analysis Report for    18-Jun-19-10036 L1-10221C-FJGS-006SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 12:25:25PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        2.36E-02          4.37E-02        4.37E-02 BE-7            477.60              10.44     -2.22E-02           3.36E-01        3.36E-01
+         K-40          1460.82
* 10.66       2.92E+00          4.84E-01        4.84E-01 Mn-54           834.85              99.98       0.00E+00          3.62E-02        3.62E-02 Co-60         1173.23               99.85     -4.46E-02           4.28E-02        4.51E-02 1332.49               99.98     -5.14E-04                           4.28E-02 Nb-94           702.65              99.81     -1.71E-02           3.15E-02        3.23E-02 871.09              99.89       1.05E-02                          3.15E-02 Ag-108m          79.13                6.60    -2.83E-01           2.54E-02        1.14E+00 433.94              90.50     -1.64E-03                           2.54E-02 614.28              89.80     -2.74E-02                           5.71E-02 722.94              90.80       5.15E-04                          3.45E-02 Sb-125          176.31                6.84      1.51E-01          9.79E-02        3.95E-01 380.45                1.52    -6.93E-01                           1.96E+00 427.87              29.60       5.80E-02                          9.79E-02 463.36              10.49     -9.56E-02                           2.87E-01 600.60              17.65     -9.00E-02                           1.83E-01 606.71                4.98      6.48E-01                          1.02E+00 635.95              11.22     -7.37E-02                           2.50E-01          [238]

6/18/2019  12:25:34PM Page 5 of 6 Analysis Report for 18-Jun-19-10036 L1-10221C-FJGS-006SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -7.36E-01      9.79E-02        1.91E+00 Ba-133        79.61            2.65   -9.27E-01      5.13E-02        2.69E+00 81.00           32.90    1.53E-03                      2.06E-01 276.40            7.16   -2.37E-01                      4.00E-01 302.85           18.34   -2.38E-02                      1.43E-01 356.01           62.05   -1.26E-02                      5.13E-02 383.85            8.94   -8.14E-03                      3.42E-01 Cs-134       475.36            1.48   -2.21E-01      4.00E-02        2.16E+00 563.25            8.34   -1.54E-01                      2.84E-01 569.33           15.37    3.04E-02                      1.91E-01 604.72           97.62   -1.10E-02                      4.89E-02 795.86           85.46   -1.84E-02                      4.00E-02 801.95            8.69    1.05E-01                      3.76E-01 1038.61             0.99    2.30E+00                      3.57E+00 1167.97             1.79    1.61E+00                      2.62E+00 1365.19             3.02    2.32E-01                      1.25E+00 Cs-137       661.66           85.10    4.68E-02      5.54E-02        5.54E-02 Eu-152       121.78           28.67    9.57E-03      9.39E-02        1.12E-01 244.70            7.61    2.28E-01                      3.32E-01 295.94            0.45    4.65E+00                      7.15E+00 344.28           26.60   -1.56E-02                      9.39E-02 367.79            0.86    8.15E-01                      3.25E+00 411.12            2.24   -1.98E-01                      1.30E+00 443.96            2.83    9.99E-02                      9.00E-01 488.68            0.42   -3.57E+00                      6.33E+00 563.99            0.49   -1.80E+00                      4.83E+00 586.26            0.46    5.29E+00                      8.81E+00 678.62            0.47   -1.37E-01                      6.53E+00 688.67            0.86    5.85E-01                      3.35E+00 719.35            0.28   -3.86E+00                      1.03E+01 778.90           12.96    5.96E-02                      2.54E-01 810.45            0.32    3.27E+00                      9.04E+00 867.37            4.26   -1.21E+00                      7.83E-01 919.33            0.43   -4.39E+00                      7.88E+00 964.08           14.65    1.82E-01                      2.89E-01 1085.87            10.24    1.85E-01                      3.99E-01 1089.74             1.73   -3.17E-01                      2.42E+00 1112.07            13.69   -1.13E-01                      3.03E-01 1212.95             1.43   -7.50E-01                      3.37E+00 1249.94             0.19    1.35E+01                      2.54E+01 1299.14             1.63    5.31E-01                      2.42E+00 1408.01            21.07    1.22E-01                      1.98E-01 1457.64             0.50    6.03E+01                      2.76E+01 1528.10             0.28   -2.12E+00                      1.01E+01 Eu-154       123.07           40.40    2.75E-02      8.04E-02        8.04E-02 247.93            6.89    1.04E-01                      3.58E-01 591.76            4.95   -2.62E-01                      6.46E-01 692.42            1.78    4.35E-01                      1.71E+00 723.30           20.06    7.95E-03                      1.60E-01 756.80            4.52   -4.87E-02                      7.99E-01 873.18           12.08    6.79E-02                      2.52E-01
[239]

6/18/2019  12:25:34PM Page 6 of 6 Analysis Report for     18-Jun-19-10036 L1-10221C-FJGS-006SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -5.15E-02      8.04E-02        3.69E-01 1004.76                  18.01        2.00E-01                      2.37E-01 1274.43                  34.80        4.51E-02                      1.23E-01 1596.48                   1.80       -1.85E-01                      1.91E+00 Eu-155            45.30                  1.31        1.06E+00      1.52E-01        1.45E+01 60.01                  1.22       -5.56E+00                      1.83E+01 86.55                 30.70       -1.70E-01                      1.52E-01 105.31                 21.10        4.52E-02                      1.77E-01 Ra-226           186.21                  3.64        9.53E-01      8.14E-01        8.14E-01 Pa-231            27.36                 10.30        7.21E-01      1.22E+00        1.76E+00 283.69                  1.70       -1.44E+00                      1.47E+00 300.07                  2.47       -8.16E-01                      1.22E+00 302.65                  2.20       -1.02E-01                      1.22E+00 330.06                  1.40        5.43E-02                      2.17E+00 U-235            143.76                 10.96       -1.11E-01      5.04E-02        2.66E-01 163.33                  5.08       -1.94E-01                      4.73E-01 185.71                 57.20        4.28E-02                      5.04E-02 202.11                  1.08       -2.48E-02                      2.69E+00 205.31                  5.01        3.52E-01                      5.47E-01 Am-241            59.54                 35.90       -2.31E-01      6.50E-01        6.50E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[240]

6/18/2019 1:03:45PM Page 1 of 7 Analysis Report for    18-Jun-19-10037 L1-10221C-FJGS-007SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10037 Sample Description                           : L1-10221C-FJGS-007SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.549E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:24:00AM Acquisition Started                          : 6/18/2019 12:30:05PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 1800.0 seconds Real Time                                    : 1801.7 seconds Dead Time                                    : 0.09 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77470 Fill Height                                  : 1549.03 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 1:03:17PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[241]

6/18/2019   1:03:45PM         Page 2 of 7 Analysis Report for    18-Jun-19-10037 L1-10221C-FJGS-007SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       238.46               949 -    960          953.92          9.03E+01              15.94      6.47E+01           0.86 2       294.88             1175 -   1183         1179.41           2.12E+01                8.72     2.58E+01           0.79 3       351.64             1401 -   1412         1406.28           5.31E+01              11.57      3.19E+01           0.95 4       477.22             1904 -   1912         1908.30           3.08E+01                7.40     1.13E+01           0.65 5       582.72             2324 -   2336         2330.10           4.17E+01                8.45     1.13E+01           0.75 6       609.05             2429 -   2440         2435.36           3.17E+01                8.07     1.33E+01           0.45 7       661.25             2638 -   2650         2644.09           3.61E+01                7.92     9.92E+00           1.03 8       910.63             3634 -   3649         3641.47           3.62E+01                7.31     5.82E+00           0.98 9      1172.26             4681 -   4696         4688.23           3.71E+01                7.40     5.90E+00           1.42 10       1331.69             5321 -   5332         5326.23           2.50E+01                5.71     3.00E+00           1.05 11       1459.89             5829 -   5849         5839.38           1.45E+02              12.04      0.00E+00           1.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty BE-7                     0.97           477.60
* 10.44              1.85E-01             4.63E-02 K-40                     0.87          1460.82
* 10.66              1.80E+00             1.69E-01 Co-60                    0.88          1173.23
* 99.85              4.22E-02             8.58E-03 1332.49
* 99.98              3.08E-02             7.15E-03 Cs-137                   0.97           661.66
* 85.10              3.26E-02             7.43E-03 Tl-208                   0.96           583.19
* 85.00              3.47E-02             7.33E-03[242]

6/18/2019   1:03:45PM         Page 3 of 7 Analysis Report for    18-Jun-19-10037 L1-10221C-FJGS-007SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Pb-212                   0.99         115.18                  0.60 238.63
* 43.60  8.05E-02             1.56E-02 300.09                  3.30 Bi-214                   0.99         609.32
* 45.49  5.08E-02             1.33E-02 768.36                  4.89 806.18                  1.26 934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.98         241.99                  7.25 295.22
* 18.42  5.04E-02             2.11E-02 351.93
* 35.60  7.42E-02             1.72E-02 785.96                  1.06 Ac-228                   0.98         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.34E-01             2.78E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
[243]

6/18/2019 1:03:45PM          Page 4 of 7 Analysis Report for   18-Jun-19-10037 L1-10221C-FJGS-007SS INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
BE-7                                0.977                     1.85E-01              4.63E-02 K-40                                0.870                     1.80E+00              1.69E-01 Co-60                               0.882                     3.55E-02              5.49E-03 Cs-137                              0.973                     3.26E-02              7.43E-03 Tl-208                              0.966                     3.47E-02              7.33E-03 X       Bi-211                              0.950 Pb-212                              0.995                     8.05E-02              1.56E-02 Bi-214                              0.995                     5.08E-02              1.33E-02 Pb-214                              0.986                     6.47E-02              1.33E-02 Ac-228                              0.984                     1.34E-01              2.78E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[244]

6/18/2019   1:03:45PM       Page 5 of 7 Analysis Report for    18-Jun-19-10037 L1-10221C-FJGS-007SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 1:03:17PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.02E-02          3.61E-02        3.61E-02
+         BE-7            477.60
* 10.44       1.85E-01          1.17E-01        1.17E-01
+         K-40          1460.82
* 10.66       1.80E+00          3.57E-02        3.57E-02 Mn-54           834.85              99.98       1.36E-02          2.63E-02        2.63E-02
+         Co-60         1173.23
* 99.85       4.22E-02          1.51E-02        1.95E-02 1332.49
* 99.98       3.08E-02                          1.51E-02 Nb-94           702.65              99.81     -5.61E-03           2.26E-02        2.45E-02 871.09              99.89     -1.84E-02                           2.26E-02 Ag-108m          79.13                6.60      5.09E-01          2.57E-02        9.66E-01 433.94              90.50       5.53E-03                          2.57E-02 614.28              89.80     -2.48E-02                           2.77E-02 722.94              90.80       9.24E-03                          3.03E-02 Sb-125          176.31                6.84      2.34E-03          7.61E-02        3.17E-01 380.45                1.52    -9.36E-01                           1.40E+00 427.87              29.60     -3.09E-02                           7.61E-02 463.36              10.49       9.95E-02                          2.33E-01 600.60              17.65       4.81E-02                          1.23E-01 606.71                4.98      4.23E-01                          6.15E-01 635.95              11.22       1.91E-01                          2.30E-01          [245]

6/18/2019   1:03:45PM Page 6 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.52E-01      7.61E-02        1.13E+00 Ba-133        79.61            2.65    1.19E+00      3.83E-02        2.31E+00 81.00           32.90   -4.24E-02                      1.70E-01 276.40            7.16   -1.93E-01                      2.85E-01 302.85           18.34    1.89E-02                      1.25E-01 356.01           62.05   -1.06E-02                      3.83E-02 383.85            8.94    1.10E-01                      2.51E-01 Cs-134       475.36            1.48    1.84E+00      2.70E-02        1.90E+00 563.25            8.34    2.01E-01                      2.72E-01 569.33           15.37   -1.31E-01                      1.26E-01 604.72           97.62   -1.52E-03                      3.07E-02 795.86           85.46    1.03E-02                      2.70E-02 801.95            8.69    5.54E-02                      2.67E-01 1038.61             0.99    1.26E+00                      2.46E+00 1167.97             1.79   -3.18E-01                      2.53E+00 1365.19             3.02   -3.65E-01                      5.20E-01
+         Cs-137       661.66
* 85.10    3.26E-02      1.84E-02        1.84E-02 Eu-152       121.78           28.67    2.10E-02      8.07E-02        8.42E-02 244.70            7.61    1.71E-01                      3.15E-01 295.94            0.45   -1.04E-02                      5.00E+00 344.28           26.60   -4.49E-02                      8.07E-02 367.79            0.86   -8.05E-02                      2.49E+00 411.12            2.24    1.82E-01                      8.88E-01 443.96            2.83   -2.10E-01                      7.77E-01 488.68            0.42    3.93E+00                      5.79E+00 563.99            0.49    2.89E+00                      4.62E+00 586.26            0.46   -5.56E+00                      6.68E+00 678.62            0.47   -3.47E+00                      3.95E+00 688.67            0.86    1.43E+00                      2.88E+00 719.35            0.28   -1.18E+00                      8.78E+00 778.90           12.96   -1.13E-01                      1.58E-01 810.45            0.32   -3.22E+00                      7.78E+00 867.37            4.26   -2.55E-01                      5.51E-01 919.33            0.43    4.48E+00                      6.16E+00 964.08           14.65   -2.94E-02                      2.10E-01 1085.87            10.24    1.51E-02                      2.50E-01 1089.74             1.73    4.53E-01                      1.49E+00 1112.07            13.69    1.22E-01                      2.43E-01 1212.95             1.43   -2.03E-01                      2.06E+00 1249.94             0.19    7.56E+00                      1.49E+01 1299.14             1.63   -4.54E-01                      1.55E+00 1408.01            21.07   -4.07E-02                      1.23E-01 1457.64             0.50    4.00E+01                      1.63E+01 1528.10             0.28    1.92E+00                      9.48E+00 Eu-154       123.07           40.40    1.81E-02      6.13E-02        6.13E-02 247.93            6.89    6.89E-02                      3.43E-01 591.76            4.95    2.42E-01                      4.27E-01 692.42            1.78   -4.85E-01                      1.40E+00 723.30           20.06    2.50E-02                      1.37E-01 756.80            4.52   -2.25E-01                      5.28E-01 873.18           12.08    1.85E-01                      2.03E-01
[246]

6/18/2019   1:03:45PM Page 7 of 7 Analysis Report for     18-Jun-19-10037 L1-10221C-FJGS-007SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        1.03E-01      6.13E-02        2.83E-01 1004.76                  18.01       -1.98E-01                      1.47E-01 1274.43                  34.80       -6.33E-03                      7.80E-02 1596.48                   1.80       -1.12E-01                      1.15E+00 Eu-155            45.30                  1.31        5.21E-01      1.31E-01        1.72E+01 60.01                  1.22       -1.37E+01                      1.56E+01 86.55                 30.70       -8.66E-02                      1.31E-01 105.31                 21.10       -8.78E-02                      1.42E-01 Ra-226           186.21                  3.64        3.18E-01      6.22E-01        6.22E-01 Pa-231            27.36                 10.30        1.74E+00      8.95E-01        2.00E+00 283.69                  1.70        8.31E-01                      1.23E+00 300.07                  2.47        3.05E-01                      8.95E-01 302.65                  2.20        4.54E-01                      1.06E+00 330.06                  1.40        3.57E-01                      1.56E+00 U-235            143.76                 10.96        2.30E-01      3.98E-02        2.28E-01 163.33                  5.08       -2.92E-01                      4.14E-01 185.71                 57.20        1.52E-02                      3.98E-02 202.11                  1.08       -2.36E+00                      1.93E+00 205.31                  5.01       -1.76E-01                      4.35E-01 Am-241            59.54                 35.90       -1.98E-01      5.75E-01        5.75E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[247]

6/18/2019 12:45:27PM Page 1 of 6 Analysis Report for    18-Jun-19-10038 L1-10221C-FJGS-008SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 18-Jun-19-10038 Sample Description                           : L1-10221C-FJGS-008SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.644E+03 grams Facility                                     : Default Sample Taken On                              : 6/17/2019 8:26:00AM Acquisition Started                          : 6/18/2019 12:30:13PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 6/18/2019 Efficiency Calibration Description           :
Sample Number                                : 77471 Fill Height                                  : 1644.14 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/18/2019 12:45:17PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[248]

6/18/2019   12:45:27PM         Page 2 of 6 Analysis Report for    18-Jun-19-10038 L1-10221C-FJGS-008SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1         77.15              305 - 314             309.13          2.45E+01                9.92      3.25E+01           0.89 2       238.71               948 - 962             954.42          6.91E+01               12.70      3.09E+01           0.94 3       352.04             1401 - 1414           1407.18           4.35E+01                7.70      5.48E+00           0.37 4       582.89             2325 - 2334           2329.67           2.00E+01                5.59      5.00E+00           0.30 5      1460.66             5829 - 5849           5840.58           1.14E+02               11.15      2.69E+00           1.91 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              2.51E+00              2.68E-01 Tl-208                   0.98           583.19
* 85.00              2.96E-02              8.47E-03 Bi-211                   0.86           351.07
* 13.02              2.95E-01              5.74E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.08E-01              2.18E-02 300.09                    3.30 Pb212-XR                 1.00            74.82                  10.28 77.11
* 17.10              1.72E-01              7.17E-02 87.35                    3.97 89.78                    1.46 Pb-214                   0.99           241.99                    7.25 295.22                  18.42                                               [249]

6/18/2019   12:45:27PM         Page 3 of 6 Analysis Report for    18-Jun-19-10038 L1-10221C-FJGS-008SS Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Pb-214                   0.99          351.93
* 35.60              1.08E-01              2.10E-02 785.96                    1.06 Pb214-XR                 1.00            74.82                   5.80 77.11
* 9.70             3.03E-01              1.27E-01 87.35                   2.24 89.78                   0.82
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
K-40                                0.996                     2.51E+00                2.68E-01 Tl-208                              0.986                     2.96E-02                8.47E-03
      ?       Bi-211                              0.860                     2.95E-01                5.74E-02 Pb-212                              0.999                     1.08E-01                2.18E-02
      ?       Pb212-XR                            1.000                     1.72E-01                7.17E-02
      ?       Pb-214                              0.999                     1.08E-01                2.10E-02
      ?       Pb214-XR                            1.000                     3.03E-01                1.27E-01
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[250]

6/18/2019  12:45:27PM       Page 4 of 6 Analysis Report for    18-Jun-19-10038 L1-10221C-FJGS-008SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/18/2019 12:45:17PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        4.49E-02          4.52E-02        4.52E-02 BE-7            477.60              10.44       8.44E-03          2.81E-01        2.81E-01
+         K-40          1460.82
* 10.66       2.51E+00          2.99E-01        2.99E-01 Mn-54           834.85              99.98     -1.37E-02           3.13E-02        3.13E-02 Co-60         1173.23               99.85       2.25E-03          4.69E-02        4.79E-02 1332.49               99.98       3.28E-02                          4.69E-02 Nb-94           702.65              99.81       2.15E-03          3.22E-02        3.56E-02 871.09              99.89       2.89E-03                          3.22E-02 Ag-108m          79.13                6.60    -1.85E-01           2.29E-02        8.44E-01 433.94              90.50     -3.88E-02                           2.29E-02 614.28              89.80     -3.50E-02                           4.17E-02 722.94              90.80       9.22E-03                          3.54E-02 Sb-125          176.31                6.84    -3.82E-02           8.35E-02        3.35E-01 380.45                1.52    -1.12E+00                           1.72E+00 427.87              29.60     -2.02E-02                           8.35E-02 463.36              10.49       2.12E-01                          3.16E-01 600.60              17.65     -1.47E-01                           1.42E-01 606.71                4.98      6.84E-01                          8.53E-01 635.95              11.22       2.93E-02                          2.77E-01          [251]

6/18/2019  12:45:27PM Page 5 of 6 Analysis Report for 18-Jun-19-10038 L1-10221C-FJGS-008SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.09E-01      8.35E-02        1.61E+00 Ba-133        79.61            2.65   -6.53E-01      4.98E-02        2.03E+00 81.00           32.90   -5.57E-02                      1.35E-01 276.40            7.16   -4.90E-02                      3.57E-01 302.85           18.34   -4.47E-02                      1.19E-01 356.01           62.05    4.31E-03                      4.98E-02 383.85            8.94    1.05E-02                      2.67E-01 Cs-134       475.36            1.48    1.24E+00      3.42E-02        2.02E+00 563.25            8.34   -3.59E-01                      4.03E-01 569.33           15.37   -1.21E-02                      1.83E-01 604.72           97.62   -3.22E-02                      3.80E-02 795.86           85.46    1.36E-03                      3.42E-02 801.95            8.69   -4.49E-03                      3.24E-01 1038.61             0.99    1.06E+00                      3.53E+00 1167.97             1.79   -3.47E+00                      2.41E+00 1365.19             3.02    5.17E-01                      1.15E+00 Cs-137       661.66           85.10    1.34E-02      4.17E-02        4.17E-02 Eu-152       121.78           28.67    5.18E-02      7.25E-02        7.25E-02 244.70            7.61    5.72E-02                      3.48E-01 295.94            0.45    2.23E+00                      6.17E+00 344.28           26.60    2.21E-02                      9.55E-02 367.79            0.86   -2.18E+00                      2.52E+00 411.12            2.24    5.96E-01                      1.29E+00 443.96            2.83   -9.32E-01                      1.04E+00 488.68            0.42   -5.07E+00                      5.35E+00 563.99            0.49   -1.21E+01                      5.68E+00 586.26            0.46   -7.97E+00                      8.70E+00 678.62            0.47   -6.44E+00                      6.87E+00 688.67            0.86    8.73E-01                      4.08E+00 719.35            0.28   -3.15E+00                      1.05E+01 778.90           12.96    8.49E-02                      2.38E-01 810.45            0.32    1.99E+00                      8.45E+00 867.37            4.26    1.82E-01                      6.67E-01 919.33            0.43   -2.78E+00                      9.07E+00 964.08           14.65   -2.60E-02                      3.00E-01 1085.87            10.24    7.43E-02                      3.64E-01 1089.74             1.73    8.86E-01                      1.82E+00 1112.07            13.69    6.26E-03                      3.21E-01 1212.95             1.43    1.44E+00                      2.60E+00 1249.94             0.19   -1.72E+01                      1.92E+01 1299.14             1.63   -6.29E-01                      2.18E+00 1408.01            21.07   -3.04E-02                      1.35E-01 1457.64             0.50    5.50E+01                      2.60E+01 1528.10             0.28   -3.01E+00                      9.63E+00 Eu-154       123.07           40.40   -3.10E-02      4.89E-02        4.89E-02 247.93            6.89   -3.60E-02                      3.46E-01 591.76            4.95    1.57E-01                      5.67E-01 692.42            1.78    7.48E-01                      1.89E+00 723.30           20.06   -1.26E-02                      1.56E-01 756.80            4.52    1.38E-02                      6.47E-01 873.18           12.08   -1.49E-01                      2.57E-01
[252]

6/18/2019  12:45:27PM Page 6 of 6 Analysis Report for     18-Jun-19-10038 L1-10221C-FJGS-008SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.60E-02      4.89E-02        2.69E-01 1004.76                  18.01       -1.33E-01                      1.74E-01 1274.43                  34.80        9.66E-03                      1.05E-01 1596.48                   1.80       -2.53E+00                      1.74E+00 Eu-155            45.30                  1.31        5.07E-01      1.34E-01        7.66E+00 60.01                  1.22        1.47E+00                      9.25E+00 86.55                 30.70        6.29E-02                      1.34E-01 105.31                 21.10       -1.04E-02                      1.45E-01 Ra-226           186.21                  3.64        5.36E-01      6.96E-01        6.96E-01 Pa-231            27.36                 10.30        5.44E-01      9.24E-01        1.07E+00 283.69                  1.70        6.57E-01                      1.50E+00 300.07                  2.47       -6.02E-01                      9.24E-01 302.65                  2.20       -3.36E-01                      1.01E+00 330.06                  1.40        1.38E-01                      1.82E+00 U-235            143.76                 10.96        4.21E-03      4.36E-02        2.00E-01 163.33                  5.08        2.29E-01                      4.54E-01 185.71                 57.20        1.56E-02                      4.36E-02 202.11                  1.08       -3.24E-01                      1.97E+00 205.31                  5.01       -1.64E-01                      4.04E-01 Am-241            59.54                 35.90        1.25E-01      3.29E-01        3.29E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[253]

6/24/2019 8:18:14AM Page 1 of 7 Analysis Report for    24-Jun-19-10009 L1-10221C-FIGS-100SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 24-Jun-19-10009 Sample Description                           : L1-10221C-FIGS-100SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.375E+03 grams Facility                                     : Default Sample Taken On                              : 6/20/2019 9:50:00AM Acquisition Started                          : 6/24/2019 8:03:01AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/24/2019 Efficiency Calibration Description           :
Sample Number                                : 77579 Fill Height                                  : 1374.75 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/24/2019 8:18:05AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[254]

6/24/2019   8:18:14AM         Page 2 of 7 Analysis Report for    24-Jun-19-10009 L1-10221C-FIGS-100SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       238.62               948 -    961          954.93          6.04E+01              12.41      3.36E+01           0.89 2       295.45             1177 -   1187         1182.03           2.10E+01                7.42     1.40E+01           1.11 3       351.92             1402 -   1413         1407.67           3.23E+01                8.31     1.47E+01           0.60 4       510.74             2037 -   2047         2042.46           2.91E+01                7.94     1.39E+01           0.34 5       582.99             2325 -   2336         2331.28           3.20E+01                6.88     6.03E+00           0.43 6       609.08             2427 -   2443         2435.57           4.79E+01                7.38     2.08E+00           0.57 7       911.00             3638 -   3649         3643.02           1.75E+01                5.99     6.46E+00           0.77 8      1460.41             5833 -   5853         5842.03           1.15E+02              11.47      4.77E+00           1.33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty An Pk                    0.99           511.00
* 100.00               3.51E-02             9.86E-03 K-40                     0.97          1460.82
* 10.66              2.49E+00             2.71E-01 Tl-208                   0.99           583.19
* 85.00              4.70E-02             1.05E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              9.66E-02             2.13E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              1.35E-01             2.24E-02 768.36                    4.89 806.18                    1.26                                             [255]

6/24/2019   8:18:14AM         Page 3 of 7 Analysis Report for    24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99         934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42  8.94E-02             3.24E-02 351.93
* 35.60  8.05E-02             2.17E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.14E-01             3.93E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[256]

6/24/2019 8:18:14AM          Page 4 of 7 Analysis Report for   24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
An Pk                               0.990                     3.51E-02              9.86E-03 K-40                                0.974                     2.49E+00              2.71E-01 Tl-208                              0.994                     4.70E-02              1.05E-02 X       Bi-211                              0.891 Pb-212                              1.000                     9.66E-02              2.13E-02 Bi-214                              0.996                     1.35E-01              2.24E-02 Pb-214                              0.998                     8.33E-02              1.80E-02 Ac-228                              0.998                     1.14E-01              3.93E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[257]

6/24/2019   8:18:14AM       Page 5 of 7 Analysis Report for    24-Jun-19-10009 L1-10221C-FIGS-100SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/24/2019 8:18:05AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
+         An Pk           511.00
* 100.00        3.51E-02          2.73E-02        2.73E-02 BE-7            477.60              10.44       5.67E-02          3.26E-01        3.26E-01
+         K-40          1460.82
* 10.66       2.49E+00          3.59E-01        3.59E-01 Mn-54           834.85              99.98       3.19E-02          3.88E-02        3.88E-02 Co-60         1173.23               99.85       4.22E-03          3.89E-02        4.38E-02 1332.49               99.98     -9.16E-03                           3.89E-02 Nb-94           702.65              99.81       1.58E-02          3.21E-02        3.21E-02 871.09              99.89       8.14E-04                          4.37E-02 Ag-108m          79.13                6.60      1.34E+00          3.35E-02        1.30E+00 433.94              90.50       7.95E-03                          3.35E-02 614.28              89.80     -3.53E-02                           5.34E-02 722.94              90.80       2.24E-02                          3.86E-02 Sb-125          176.31                6.84      2.80E-01          9.07E-02        3.76E-01 380.45                1.52      8.82E-01                          2.10E+00 427.87              29.60       1.55E-02                          9.07E-02 463.36              10.49     -3.61E-02                           3.24E-01 600.60              17.65     -9.38E-02                           1.87E-01 606.71                4.98      5.52E-01                          1.07E+00 635.95              11.22       4.99E-02                          2.61E-01          [258]

6/24/2019   8:18:14AM Page 6 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    8.25E-01      9.07E-02        1.95E+00 Ba-133        79.61            2.65    2.75E+00      5.40E-02        3.14E+00 81.00           32.90   -2.74E-01                      2.14E-01 276.40            7.16    1.45E-01                      3.74E-01 302.85           18.34   -3.59E-02                      1.40E-01 356.01           62.05   -1.67E-02                      5.40E-02 383.85            8.94   -2.48E-01                      3.17E-01 Cs-134       475.36            1.48   -6.74E-03      4.28E-02        2.26E+00 563.25            8.34   -2.39E-01                      3.65E-01 569.33           15.37    1.84E-01                      2.30E-01 604.72           97.62    5.24E-03                      5.22E-02 795.86           85.46   -4.59E-03                      4.28E-02 801.95            8.69    3.62E-02                      3.71E-01 1038.61             0.99   -2.03E+00                      3.48E+00 1167.97             1.79   -1.49E+00                      2.30E+00 1365.19             3.02    5.83E-01                      1.20E+00 Cs-137       661.66           85.10    1.97E-02      3.71E-02        3.71E-02 Eu-152       121.78           28.67    1.08E-02      1.08E-01        1.08E-01 244.70            7.61    1.14E-01                      3.86E-01 295.94            0.45    2.89E+00                      7.28E+00 344.28           26.60    4.29E-02                      1.08E-01 367.79            0.86   -8.23E-01                      3.09E+00 411.12            2.24    1.99E-01                      1.17E+00 443.96            2.83   -1.28E-01                      1.07E+00 488.68            0.42    7.35E+00                      8.59E+00 563.99            0.49   -4.12E-01                      6.57E+00 586.26            0.46    1.08E+01                      1.03E+01 678.62            0.47   -1.14E+01                      6.46E+00 688.67            0.86   -2.86E+00                      4.04E+00 719.35            0.28   -6.94E+00                      1.10E+01 778.90           12.96   -3.56E-01                      2.19E-01 810.45            0.32   -7.18E+00                      8.72E+00 867.37            4.26    5.38E-02                      9.27E-01 919.33            0.43   -3.17E-01                      9.39E+00 964.08           14.65    1.58E-01                      3.25E-01 1085.87            10.24   -2.22E-01                      3.18E-01 1089.74             1.73    1.09E+00                      1.97E+00 1112.07            13.69   -2.47E-01                      2.91E-01 1212.95             1.43   -1.42E+00                      2.56E+00 1249.94             0.19    2.18E+01                      2.66E+01 1299.14             1.63    9.27E-01                      2.80E+00 1408.01            21.07    9.58E-02                      1.84E-01 1457.64             0.50    5.81E+01                      2.61E+01 1528.10             0.28   -6.98E+00                      1.32E+01 Eu-154       123.07           40.40    1.57E-02      7.62E-02        7.62E-02 247.93            6.89   -3.73E-01                      3.84E-01 591.76            4.95    2.24E-01                      6.20E-01 692.42            1.78    7.68E-01                      1.96E+00 723.30           20.06   -3.23E-02                      1.67E-01 756.80            4.52    4.02E-01                      8.66E-01 873.18           12.08    1.21E-01                      3.42E-01
[259]

6/24/2019   8:18:14AM Page 7 of 7 Analysis Report for     24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        1.56E-01      7.62E-02        3.65E-01 1004.76                  18.01        1.79E-01                      2.31E-01 1274.43                  34.80        3.77E-02                      1.21E-01 1596.48                   1.80       -3.78E+00                      1.33E+00 Eu-155            45.30                  1.31        1.85E+00      1.63E-01        1.60E+01 60.01                  1.22       -2.54E+01                      1.57E+01 86.55                 30.70        7.20E-02                      1.78E-01 105.31                 21.10       -2.44E-02                      1.63E-01 Ra-226           186.21                  3.64        3.64E-01      8.02E-01        8.02E-01 Pa-231            27.36                 10.30        1.27E+00      1.15E+00        1.95E+00 283.69                  1.70        7.92E-01                      1.55E+00 300.07                  2.47       -4.60E-01                      1.21E+00 302.65                  2.20       -7.79E-01                      1.15E+00 330.06                  1.40        6.24E-01                      1.96E+00 U-235            143.76                 10.96       -8.15E-02      5.07E-02        2.54E-01 163.33                  5.08        6.71E-03                      5.37E-01 185.71                 57.20        1.77E-02                      5.07E-02 202.11                  1.08       -8.33E-01                      2.52E+00 205.31                  5.01       -4.91E-02                      5.44E-01 Am-241            59.54                 35.90       -5.85E-01      5.80E-01        5.80E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[260]

6/25/2019 8:44:44AM Page 1 of 7 Analysis Report for    25-Jun-19-10013 L1-10221C-FIGS-101SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 25-Jun-19-10013 Sample Description                           : L1-10221C-FIGS-101SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.518E+03 grams Facility                                     : Default Sample Taken On                              : 6/24/2019 9:00:00AM Acquisition Started                          : 6/25/2019 8:29:13AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 6/25/2019 Efficiency Calibration Description           :
Sample Number                                : 77600 Fill Height                                  : 1517.55 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 6/25/2019 8:44:35AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[261]

6/25/2019   8:44:44AM         Page 2 of 7 Analysis Report for    25-Jun-19-10013 L1-10221C-FIGS-101SS Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty        Counts          (keV) 1       238.62               950 -    961          954.94          6.91E+01              15.89      6.99E+01           0.85 2       295.15             1176 -   1186         1180.84           2.28E+01              10.21      3.42E+01           0.93 3       351.80             1402 -   1412         1407.20           3.67E+01                9.99     2.63E+01           1.06 4       609.13             2430 -   2442         2435.79           2.77E+01                8.56     1.73E+01           0.73 5       661.48             2636 -   2654         2645.10           3.66E+02              21.46      2.82E+01           1.36 6       911.16             3638 -   3650         3643.69           2.88E+01                6.32     4.18E+00           0.87 7      1173.18             4683 -   4700         4692.10           6.83E+01                9.81     8.70E+00           1.66 8      1460.45             5830 -   5851         5842.16           1.71E+02              14.17      8.08E+00           0.74 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.97          1460.82
* 10.66              3.59E+00             3.36E-01 Cs-137                   0.99           661.66
* 85.10              5.69E-01             4.78E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              1.08E-01             2.64E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              7.64E-02             2.40E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11                                             [262]

6/25/2019   8:44:44AM         Page 3 of 7 Analysis Report for    25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99        1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42  9.49E-02             4.32E-02 351.93
* 35.60  8.94E-02             2.54E-02 785.96                  1.06 Ac-228                   1.00         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.83E-01             4.08E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[263]

6/25/2019 8:44:44AM          Page 4 of 7 Analysis Report for   25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.978                     3.59E+00              3.36E-01 Cs-137                              0.995                     5.69E-01              4.78E-02 X       Bi-211                              0.918 Pb-212                              1.000                     1.08E-01              2.64E-02 Bi-214                              0.998                     7.64E-02              2.40E-02 Pb-214                              0.998                     9.08E-02              2.19E-02 Ac-228                              1.000                     1.83E-01              4.08E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[264]

6/25/2019   8:44:44AM       Page 5 of 7 Analysis Report for    25-Jun-19-10013 L1-10221C-FIGS-101SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 6/25/2019 8:44:35AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide 7           1173.18              7.58874E-02                     14.37          Tol.        Co-60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                           (pCi/grams)        (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        4.58E-02          5.66E-02        5.66E-02 BE-7            477.60              10.44       3.40E-01          4.71E-01        4.71E-01
+         K-40          1460.82
* 10.66       3.59E+00          4.50E-01        4.50E-01 Mn-54           834.85              99.98       3.44E-02          4.76E-02        4.76E-02 Co-60         1173.23               99.85       1.09E-01          8.69E-02        9.70E-02 1332.49               99.98       8.80E-02                          8.69E-02 Nb-94           702.65              99.81       1.10E-02          4.55E-02        4.68E-02 871.09              99.89     -1.14E-02                           4.55E-02 Ag-108m          79.13                6.60    -3.82E-01           4.72E-02        1.40E+00 433.94              90.50       1.12E-03                          4.72E-02 614.28              89.80       1.10E-02                          5.66E-02 722.94              90.80       1.84E-03                          5.13E-02 Sb-125          176.31                6.84      3.61E-02          1.37E-01        4.48E-01 380.45                1.52      5.04E-01                          2.22E+00 427.87              29.60       3.07E-02                          1.37E-01 463.36              10.49       2.97E-01                          4.48E-01 600.60              17.65       2.58E-01                          2.39E-01 606.71                4.98      1.25E+00                          1.14E+00          [265]

6/25/2019   8:44:44AM Page 6 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       635.95           11.22   -2.54E-01      1.37E-01        3.25E-01 671.44            1.79   -3.18E-02                      2.08E+00 Ba-133        79.61            2.65    4.81E-01      6.96E-02        3.42E+00 81.00           32.90   -2.47E-01                      2.40E-01 276.40            7.16    1.49E-01                      5.48E-01 302.85           18.34    8.63E-02                      2.16E-01 356.01           62.05   -4.48E-02                      6.96E-02 383.85            8.94   -1.27E-01                      3.72E-01 Cs-134       475.36            1.48    2.35E-01      5.25E-02        3.32E+00 563.25            8.34   -3.90E-02                      4.35E-01 569.33           15.37    1.03E-01                      2.41E-01 604.72           97.62   -3.43E-02                      5.54E-02 795.86           85.46    3.79E-02                      5.25E-02 801.95            8.69   -2.44E-01                      4.39E-01 1038.61             0.99   -4.06E+00                      4.28E+00 1167.97             1.79   -1.49E-01                      5.45E+00 1365.19             3.02    3.53E-01                      9.60E-01
+         Cs-137       661.66
* 85.10    5.69E-01      5.58E-02        5.58E-02 Eu-152       121.78           28.67    2.29E-02      1.31E-01        1.31E-01 244.70            7.61    8.43E-02                      5.30E-01 295.94            0.45    2.28E+00                      9.70E+00 344.28           26.60   -5.11E-03                      1.33E-01 367.79            0.86   -2.43E+00                      4.19E+00 411.12            2.24   -4.44E-01                      1.88E+00 443.96            2.83    7.81E-01                      1.74E+00 488.68            0.42    2.64E+00                      8.66E+00 563.99            0.49   -3.87E+00                      7.18E+00 586.26            0.46    8.04E+00                      1.10E+01 678.62            0.47   -2.64E+00                      8.31E+00 688.67            0.86   -1.63E+00                      4.54E+00 719.35            0.28   -1.84E+00                      1.53E+01 778.90           12.96   -1.64E-01                      2.88E-01 810.45            0.32   -5.77E+00                      1.22E+01 867.37            4.26   -7.14E-01                      1.10E+00 919.33            0.43   -8.81E+00                      9.55E+00 964.08           14.65    3.11E-01                      4.14E-01 1085.87            10.24    3.26E-01                      5.29E-01 1089.74             1.73    9.35E-01                      3.14E+00 1112.07            13.69   -2.78E-01                      3.65E-01 1212.95             1.43   -4.93E+00                      3.77E+00 1249.94             0.19    1.77E+01                      2.74E+01 1299.14             1.63    1.86E+00                      3.08E+00 1408.01            21.07    1.24E-01                      2.01E-01 1457.64             0.50    8.15E+01                      3.05E+01 1528.10             0.28   -6.24E+00                      1.42E+01 Eu-154       123.07           40.40   -3.30E-02      9.19E-02        9.19E-02 247.93            6.89    1.34E-01                      5.25E-01 591.76            4.95   -8.94E-01                      7.56E-01 692.42            1.78   -1.56E+00                      2.20E+00 723.30           20.06   -8.69E-02                      2.30E-01 756.80            4.52   -2.64E-01                      8.89E-01
[266]

6/25/2019   8:44:44AM Page 7 of 7 Analysis Report for     25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           873.18                 12.08        2.46E-01      9.19E-02        3.88E-01 996.29                 10.48        1.68E-01                      4.11E-01 1004.76                  18.01       -1.05E-01                      2.73E-01 1274.43                  34.80       -5.67E-02                      1.42E-01 1596.48                   1.80       -3.26E+00                      1.95E+00 Eu-155            45.30                  1.31       -1.16E+01      2.00E-01        1.98E+01 60.01                  1.22       -1.86E+01                      1.84E+01 86.55                 30.70       -4.30E-02                      2.10E-01 105.31                 21.10        5.31E-02                      2.00E-01 Ra-226           186.21                  3.64        1.12E+00      1.04E+00        1.04E+00 Pa-231            27.36                 10.30        1.66E+00      1.64E+00        2.33E+00 283.69                  1.70       -1.81E+00                      2.18E+00 300.07                  2.47       -8.68E-01                      1.64E+00 302.65                  2.20        7.41E-01                      1.80E+00 330.06                  1.40        1.12E-01                      2.57E+00 U-235            143.76                 10.96       -1.42E-01      6.56E-02        3.16E-01 163.33                  5.08       -1.69E-01                      6.54E-01 185.71                 57.20        5.18E-02                      6.56E-02 202.11                  1.08        8.95E-03                      3.36E+00 205.31                  5.01       -8.29E-01                      6.82E-01 Am-241            59.54                 35.90       -9.99E-02      6.90E-01        6.90E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[267]

7/9/2019 10:24:30AM Page 1 of 7 Analysis Report for    09-Jul-19-10026 L1-10221C-FIGS-102SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10026 Sample Description                           : L1-10221C-FIGS-102SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.647E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:45:00PM Acquisition Started                          : 7/9/2019 10:09:18AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77834 Fill Height                                  : 1646.93 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:24:21AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[268]

7/9/2019   10:24:30AM         Page 2 of 7 Analysis Report for    09-Jul-19-10026 L1-10221C-FIGS-102SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       238.66               469 -    481          477.51          1.26E+02              22.18      1.39E+02           1.21 2       295.33               586 -    595          590.72          3.99E+01              12.48      5.11E+01           1.02 3       351.88               700 -    708          703.71          6.24E+01              11.66      3.46E+01           1.03 4       583.21             1161 -   1171         1166.03           5.53E+01               9.91      1.77E+01           0.94 5       609.44             1215 -   1223         1218.46           3.82E+01               8.99      1.98E+01           1.18 6       661.88             1318 -   1328         1323.29           6.66E+01              10.73      2.04E+01           1.34 7       911.31             1817 -   1826         1822.07           4.38E+01               8.30      1.12E+01           1.19 8      1460.91             2915 -   2929         2921.88           2.35E+02              16.01      7.50E+00           1.84 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     0.99          1460.82
* 10.66             4.32E+00              3.50E-01 Cs-137                   0.99           661.66
* 85.10             9.16E-02              1.57E-02 Tl-208                   1.00           583.19
* 85.00             7.02E-02              1.33E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60             1.74E-01              3.38E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49             9.33E-02              2.27E-02 768.36                    4.89 806.18                    1.26                                             [269]

7/9/2019   10:24:30AM        Page 3 of 7 Analysis Report for    09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99          934.06                 3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99          241.99                 7.25 295.22
* 18.42  1.48E-01              4.76E-02 351.93
* 35.60  1.35E-01              2.74E-02 785.96                 1.06 Ac-228                   0.99          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32                11.27 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20
* 25.80  2.45E-01              4.76E-02 964.77                 4.99 968.97                15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[270]

7/9/2019 10:24:30AM         Page 4 of 7 Analysis Report for   09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.999                     4.32E+00              3.50E-01 Cs-137                              0.992                     9.16E-02              1.57E-02 Tl-208                              1.000                     7.02E-02              1.33E-02 X       Bi-211                              0.900 Pb-212                              1.000                     1.74E-01              3.38E-02 Bi-214                              0.999                     9.33E-02              2.27E-02 Pb-214                              0.999                     1.38E-01              2.38E-02 Ac-228                              0.999                     2.45E-01              4.76E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[271]

7/9/2019  10:24:30AM       Page 5 of 7 Analysis Report for    09-Jul-19-10026 L1-10221C-FIGS-102SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:24:21AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        5.28E-02          5.01E-02         5.01E-02 BE-7            477.60              10.44       2.42E-01          3.78E-01         3.78E-01
+         K-40          1460.82
* 10.66       4.32E+00          3.44E-01         3.44E-01 Mn-54           834.85              99.98       8.97E-05          3.24E-02         3.24E-02 Co-60         1173.23               99.85       1.55E-02          5.11E-02         5.57E-02 1332.49               99.98       2.60E-02                           5.11E-02 Nb-94           702.65              99.81       1.85E-02          3.33E-02         3.39E-02 871.09              99.89     -2.60E-02                            3.33E-02 Ag-108m          79.13                6.60      6.64E-01          3.26E-02         1.12E+00 433.94              90.50     -6.76E-03                            3.26E-02 614.28              89.80     -2.05E-02                            4.57E-02 722.94              90.80     -2.31E-02                            4.04E-02 Sb-125          176.31                6.84    -9.61E-02           9.29E-02         4.53E-01 380.45                1.52      1.79E-01                           1.97E+00 427.87              29.60     -6.27E-02                            9.29E-02 463.36              10.49       8.41E-02                           3.40E-01 600.60              17.65     -4.03E-02                            1.87E-01 606.71                4.98    -5.67E-01                            1.02E+00 635.95              11.22     -9.57E-03                            2.73E-01          [272]

7/9/2019  10:24:30AM Page 6 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.65E-01      9.29E-02         1.80E+00 Ba-133        79.61            2.65    5.50E-01      6.42E-02         2.59E+00 81.00           32.90   -1.98E-01                       1.74E-01 276.40            7.16    1.08E-01                       4.46E-01 302.85           18.34    2.08E-01                       1.87E-01 356.01           62.05   -1.46E-02                       6.42E-02 383.85            8.94   -3.50E-03                       3.21E-01 Cs-134       475.36            1.48    1.76E+00      4.39E-02         2.67E+00 563.25            8.34    7.23E-02                       3.85E-01 569.33           15.37   -7.64E-03                       1.89E-01 604.72           97.62   -4.63E-02                       4.39E-02 795.86           85.46    1.53E-02                       4.64E-02 801.95            8.69   -3.41E-01                       3.63E-01 1038.61             0.99   -1.39E+00                       4.18E+00 1167.97             1.79    4.37E-01                       3.13E+00 1365.19             3.02   -4.73E-01                       1.02E+00
+         Cs-137       661.66
* 85.10    9.16E-02      3.64E-02         3.64E-02 Eu-152       121.78           28.67    1.26E-02      1.06E-01         1.06E-01 244.70            7.61    4.45E-03                       4.44E-01 295.94            0.45    1.17E+00                       7.81E+00 344.28           26.60   -1.05E-01                       1.09E-01 367.79            0.86   -4.47E-01                       3.57E+00 411.12            2.24    4.30E-01                       1.38E+00 443.96            2.83    2.64E-01                       1.06E+00 488.68            0.42    3.48E+00                       7.68E+00 563.99            0.49    2.53E+00                       6.54E+00 586.26            0.46   -1.44E-01                       1.12E+01 678.62            0.47    7.21E-01                       6.77E+00 688.67            0.86   -1.54E+00                       3.55E+00 719.35            0.28    4.32E+00                       1.17E+01 778.90           12.96   -8.68E-02                       2.27E-01 810.45            0.32    4.48E+00                       1.12E+01 867.37            4.26   -3.11E-01                       7.97E-01 919.33            0.43    6.78E-01                       8.78E+00 964.08           14.65   -1.11E-02                       3.69E-01 1085.87            10.24    1.17E-01                       4.00E-01 1089.74             1.73   -1.05E+00                       2.27E+00 1112.07            13.69    4.01E-02                       3.74E-01 1212.95             1.43   -2.65E+00                       3.26E+00 1249.94             0.19    6.43E+00                       2.59E+01 1299.14             1.63   -3.92E-01                       2.17E+00 1408.01            21.07   -3.98E-02                       1.71E-01 1457.64             0.50   -2.60E+00                       3.04E+01 1528.10             0.28   -3.33E+00                       8.99E+00 Eu-154       123.07           40.40   -4.43E-02      6.99E-02         6.99E-02 247.93            6.89   -2.92E-02                       4.12E-01 591.76            4.95    9.25E-02                       6.70E-01 692.42            1.78    5.43E-01                       1.82E+00 723.30           20.06   -6.40E-02                       1.96E-01 756.80            4.52    5.03E-02                       7.45E-01 873.18           12.08    1.36E-01                       3.17E-01
[273]

7/9/2019  10:24:30AM Page 7 of 7 Analysis Report for     09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -8.33E-03      6.99E-02         3.04E-01 1004.76                  18.01        1.45E-01                       2.49E-01 1274.43                  34.80        4.53E-02                       1.35E-01 1596.48                   1.80        1.14E-01                       2.02E+00 Eu-155            45.30                  1.31        2.26E+00      1.70E-01         1.12E+01 60.01                  1.22       -4.41E+00                       1.08E+01 86.55                 30.70        9.49E-02                       1.70E-01 105.31                 21.10       -6.96E-03                       1.80E-01 Ra-226           186.21                  3.64        2.39E-02      8.54E-01         8.54E-01 Pa-231            27.36                 10.30        8.34E-01      1.14E+00         1.14E+00 283.69                  1.70        9.46E-02                       1.76E+00 300.07                  2.47        3.09E-01                       1.26E+00 302.65                  2.20        1.73E+00                       1.55E+00 330.06                  1.40        2.97E-01                       2.17E+00 U-235            143.76                 10.96       -1.38E-02      5.60E-02         2.68E-01 163.33                  5.08       -1.34E-01                       6.32E-01 185.71                 57.20        2.66E-02                       5.60E-02 202.11                  1.08       -1.43E+00                       2.81E+00 205.31                  5.01       -2.01E-01                       6.36E-01 Am-241            59.54                 35.90       -7.79E-02      3.91E-01         3.91E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[274]

7/9/2019 10:24:40AM Page 1 of 7 Analysis Report for    09-Jul-19-10027 L1-10221C-FIGS-103SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10027 Sample Description                           : L1-10221C-FIGS-103SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.543E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:47:00PM Acquisition Started                          : 7/9/2019 10:09:29AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.2 seconds Dead Time                                    : 0.13 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77835 Fill Height                                  : 1542.77 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:24:33AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[275]

7/9/2019   10:24:40AM         Page 2 of 7 Analysis Report for    09-Jul-19-10027 L1-10221C-FIGS-103SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       238.52               945 -    961          954.16          1.22E+02              17.32      5.60E+01           0.85 2       351.77             1402 -   1414         1406.80           5.22E+01               9.68      1.58E+01           0.99 3       477.16             1903 -   1913         1908.06           3.00E+01               9.08      2.20E+01           0.62 4       510.79             2038 -   2047         2042.49           1.41E+01               8.20      2.29E+01           0.41 5       582.61             2325 -   2335         2329.64           3.19E+01               7.01      7.05E+00           0.40 6       608.83             2429 -   2443         2434.50           4.54E+01               7.79      5.57E+00           0.80 7       661.39             2637 -   2651         2644.65           8.73E+01              10.19      5.67E+00           0.55 8       910.57             3636 -   3646         3641.25           1.81E+01               5.87      5.92E+00           0.71 9      1459.91             5829 -   5849         5839.47           1.76E+02              13.96      5.25E+00           1.53 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty An Pk                    0.99           511.00
* 100.00              1.84E-02              1.08E-02 BE-7                     0.96           477.60
* 10.44             3.59E-01              1.12E-01 K-40                     0.87          1460.82
* 10.66             4.37E+00              3.95E-01 Cs-137                   0.98           661.66
* 85.10             1.58E-01              2.08E-02 Tl-208                   0.94           583.19
* 85.00             5.32E-02              1.21E-02 Bi-211                   0.92           351.07
* 13.02             3.99E-01              8.06E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60             2.18E-01              3.56E-02[276]

7/9/2019   10:24:40AM        Page 3 of 7 Analysis Report for    09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Pb-212                   0.99          300.09                 3.30 Bi-214                   0.98          609.32
* 45.49  1.46E-01              2.65E-02 768.36                 4.89 806.18                 1.26 934.06                 3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99          241.99                 7.25 295.22                18.42 351.93
* 35.60  1.46E-01              2.95E-02 785.96                 1.06 Ac-228                   0.98          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32                11.27 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20
* 25.80  1.34E-01              4.40E-02 964.77                 4.99 968.97                15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[277]

7/9/2019 10:24:40AM         Page 4 of 7 Analysis Report for   09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
An Pk                               0.993                     1.84E-02              1.08E-02 BE-7                                0.969                     3.59E-01              1.12E-01 K-40                                0.876                     4.37E+00              3.95E-01 Cs-137                              0.988                     1.58E-01              2.08E-02 Tl-208                              0.948                     5.32E-02              1.21E-02
     ?       Bi-211                              0.925                     3.99E-01              8.06E-02 Pb-212                              0.998                     2.18E-01              3.56E-02 Bi-214                              0.985                     1.46E-01              2.65E-02
     ?       Pb-214                              0.998                     1.46E-01              2.95E-02 Ac-228                              0.981                     1.34E-01              4.40E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[278]

7/9/2019  10:24:40AM       Page 5 of 7 Analysis Report for    09-Jul-19-10027 L1-10221C-FIGS-103SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:24:33AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
+         An Pk           511.00
* 100.00        1.84E-02          3.62E-02         3.62E-02
+         BE-7            477.60
* 10.44       3.59E-01          3.29E-01         3.29E-01
+         K-40          1460.82
* 10.66       4.37E+00          4.39E-01         4.39E-01 Mn-54           834.85              99.98       4.52E-02          4.86E-02         4.86E-02 Co-60         1173.23               99.85       5.84E-02          6.40E-02         6.83E-02 1332.49               99.98       5.69E-02                           6.40E-02 Nb-94           702.65              99.81     -1.25E-02           4.10E-02         4.25E-02 871.09              99.89     -2.80E-02                            4.10E-02 Ag-108m          79.13                6.60      8.99E-01          3.83E-02         1.73E+00 433.94              90.50     -5.88E-02                            3.83E-02 614.28              89.80     -1.01E-02                            4.69E-02 722.94              90.80     -9.04E-03                            5.78E-02 Sb-125          176.31                6.84      1.70E-01          1.31E-01         5.76E-01 380.45                1.52      1.34E+00                           2.74E+00 427.87              29.60       4.40E-02                           1.31E-01 463.36              10.49     -6.43E-02                            4.29E-01 600.60              17.65     -9.04E-02                            2.12E-01 606.71                4.98      1.58E+00                           1.22E+00 635.95              11.22       1.10E-01                           4.02E-01          [279]

7/9/2019  10:24:40AM Page 6 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79    8.69E-01      1.31E-01         2.07E+00 Ba-133        79.61            2.65    1.75E+00      7.00E-02         4.13E+00 81.00           32.90   -2.49E-01                       2.84E-01 276.40            7.16    2.60E-01                       5.17E-01 302.85           18.34    1.32E-01                       2.07E-01 356.01           62.05   -7.81E-03                       7.00E-02 383.85            8.94    1.64E-02                       4.44E-01 Cs-134       475.36            1.48    3.17E+00      6.05E-02         3.98E+00 563.25            8.34    8.48E-03                       4.30E-01 569.33           15.37   -3.99E-02                       2.39E-01 604.72           97.62   -3.56E-02                       6.05E-02 795.86           85.46    5.71E-03                       6.23E-02 801.95            8.69    1.94E-01                       6.24E-01 1038.61             0.99   -3.16E+00                       5.27E+00 1167.97             1.79   -1.42E+00                       3.40E+00 1365.19             3.02   -4.55E-01                       1.44E+00
+         Cs-137       661.66
* 85.10    1.58E-01      3.02E-02         3.02E-02 Eu-152       121.78           28.67   -9.37E-03      1.55E-01         1.55E-01 244.70            7.61   -3.78E-01                       4.90E-01 295.94            0.45   -2.73E+00                       8.84E+00 344.28           26.60    7.58E-02                       1.65E-01 367.79            0.86    1.76E+00                       3.87E+00 411.12            2.24    7.73E-01                       1.74E+00 443.96            2.83   -1.35E-01                       1.35E+00 488.68            0.42   -4.51E+00                       8.98E+00 563.99            0.49    4.16E+00                       7.44E+00 586.26            0.46   -6.95E+00                       1.21E+01 678.62            0.47    3.59E-01                       7.34E+00 688.67            0.86   -1.58E-01                       4.87E+00 719.35            0.28    2.05E+00                       1.54E+01 778.90           12.96    2.46E-02                       3.88E-01 810.45            0.32   -1.33E+01                       1.04E+01 867.37            4.26   -3.32E-01                       8.17E-01 919.33            0.43    3.32E-01                       1.05E+01 964.08           14.65    3.02E-01                       4.82E-01 1085.87            10.24   -1.22E-01                       4.11E-01 1089.74             1.73    4.51E-01                       2.60E+00 1112.07            13.69   -4.41E-01                       3.81E-01 1212.95             1.43    1.65E+00                       3.69E+00 1249.94             0.19   -1.94E+00                       3.37E+01 1299.14             1.63   -3.07E+00                       2.03E+00 1408.01            21.07   -5.81E-02                       2.55E-01 1457.64             0.50    9.61E+01                       3.60E+01 1528.10             0.28    2.78E-01                       1.52E+01 Eu-154       123.07           40.40    2.47E-02      1.07E-01         1.07E-01 247.93            6.89   -2.54E-02                       5.33E-01 591.76            4.95    4.75E-01                       8.55E-01 692.42            1.78    1.03E+00                       2.49E+00 723.30           20.06   -1.17E-01                       2.55E-01 756.80            4.52   -2.83E-01                       1.17E+00 873.18           12.08    3.08E-01                       3.75E-01
[280]

7/9/2019  10:24:40AM Page 7 of 7 Analysis Report for     09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48        1.18E-02      1.07E-01         4.05E-01 1004.76                  18.01        5.41E-02                       2.51E-01 1274.43                  34.80        7.58E-02                       1.30E-01 1596.48                   1.80        1.26E+00                       2.60E+00 Eu-155            45.30                  1.31       -7.78E+00      2.40E-01         2.99E+01 60.01                  1.22        1.35E+01                       3.00E+01 86.55                 30.70       -9.35E-02                       2.40E-01 105.31                 21.10        4.94E-03                       2.63E-01 Ra-226           186.21                  3.64        1.01E+00      1.17E+00         1.17E+00 Pa-231            27.36                 10.30        1.28E+00      1.47E+00         3.16E+00 283.69                  1.70       -9.07E-01                       2.08E+00 300.07                  2.47       -1.09E+00                       1.47E+00 302.65                  2.20        5.65E-01                       1.68E+00 330.06                  1.40        4.57E-01                       2.65E+00 U-235            143.76                 10.96       -1.61E-01      7.46E-02         3.70E-01 163.33                  5.08        5.63E-02                       7.61E-01 185.71                 57.20        6.29E-02                       7.46E-02 202.11                  1.08       -8.90E-01                       3.33E+00 205.31                  5.01       -4.62E-02                       7.65E-01 Am-241            59.54                 35.90       -1.50E-01      1.03E+00         1.03E+00
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[281]

7/9/2019 10:24:59AM Page 1 of 7 Analysis Report for    09-Jul-19-10028 L1-10221C-FIGS-104SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10028 Sample Description                           : L1-10221C-FIGS-104SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.648E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:49:00PM Acquisition Started                          : 7/9/2019 10:09:37AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77836 Fill Height                                  : 1648.34 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:24:52AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[282]

7/9/2019   10:24:59AM         Page 2 of 7 Analysis Report for    09-Jul-19-10028 L1-10221C-FIGS-104SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1         77.42              307 -    316          310.21          2.05E+01              10.68      4.05E+01           0.73 2       238.68               949 -    962          954.30          7.55E+01              12.77      3.15E+01           0.86 3       351.97             1401 -   1413         1406.90           4.55E+01               9.47      1.65E+01           1.08 4       477.59             1902 -   1916         1908.83           4.08E+01               8.55      1.13E+01           1.02 5       911.25             3638 -   3648         3642.46           2.21E+01               6.11      5.93E+00           0.45 6      1460.33             5830 -   5850         5839.28           1.46E+02              13.26      8.07E+00           0.46 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty BE-7                     1.00           477.60
* 10.44             4.34E-01              9.62E-02 K-40                     0.96          1460.82
* 10.66             3.21E+00              3.23E-01 Bi-211                   0.87           351.07
* 13.02             3.09E-01              6.89E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60             1.18E-01              2.22E-02 300.09                    3.30 Pb212-XR                 0.99            74.82                  10.28 77.11
* 17.10             1.42E-01              7.55E-02 87.35                    3.97 89.78                    1.46 Pb-214                   1.00           241.99                    7.25                                             [283]

7/9/2019   10:24:59AM         Page 3 of 7 Analysis Report for    09-Jul-19-10028 L1-10221C-FIGS-104SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Pb-214                   1.00          295.22                18.42 351.93
* 35.60       1.13E-01              2.52E-02 785.96                 1.06 Pb214-XR                 0.99            74.82                5.80 77.11
* 9.70       2.51E-01              1.34E-01 87.35                2.24 89.78                0.82 Ac-228                   1.00          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32                11.27 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20
* 25.80       1.46E-01              4.08E-02 964.77                 4.99 968.97                15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean                Wt mean     Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
BE-7                              1.000               4.34E-01               9.62E-02 K-40                              0.963               3.21E+00               3.23E-01
      ?       Bi-211                            0.878               3.09E-01               6.89E-02 Pb-212                            1.000               1.18E-01               2.22E-02
      ?       Pb212-XR                          0.992               1.42E-01               7.55E-02
      ?       Pb-214                            1.000               1.13E-01               2.52E-02
      ?       Pb214-XR                          0.992               2.51E-01               1.34E-01 Ac-228                            1.000               1.46E-01               4.08E-02      [284]

7/9/2019 10:24:59AM Page 4 of 7 Analysis Report for   09-Jul-19-10028 L1-10221C-FIGS-104SS
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[285]

7/9/2019  10:24:59AM       Page 5 of 7 Analysis Report for    09-Jul-19-10028 L1-10221C-FIGS-104SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:24:52AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        5.53E-02          4.84E-02         4.84E-02
+         BE-7            477.60
* 10.44       4.34E-01          2.36E-01         2.36E-01
+         K-40          1460.82
* 10.66       3.21E+00          4.71E-01         4.71E-01 Mn-54           834.85              99.98       1.24E-02          3.73E-02         3.73E-02 Co-60         1173.23               99.85       2.70E-02          3.77E-02         4.90E-02 1332.49               99.98       1.97E-02                           3.77E-02 Nb-94           702.65              99.81       2.89E-03          3.44E-02         3.63E-02 871.09              99.89       6.19E-03                           3.44E-02 Ag-108m          79.13                6.60      1.55E-01          3.36E-02         8.46E-01 433.94              90.50       2.04E-02                           3.36E-02 614.28              89.80     -2.79E-02                            4.60E-02 722.94              90.80     -4.32E-02                            3.90E-02 Sb-125          176.31                6.84    -2.42E-01           9.55E-02         3.35E-01 380.45                1.52      1.75E-01                           1.63E+00 427.87              29.60     -1.25E-02                            9.55E-02 463.36              10.49       1.03E-01                           3.16E-01 600.60              17.65     -7.28E-03                            1.52E-01 606.71                4.98      1.30E+00                           9.56E-01 635.95              11.22     -2.11E-01                            2.55E-01          [286]

7/9/2019  10:24:59AM Page 6 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79    9.33E-01      9.55E-02         1.71E+00 Ba-133        79.61            2.65    4.51E-01      5.57E-02         2.08E+00 81.00           32.90   -1.12E-01                       1.26E-01 276.40            7.16    4.41E-03                       4.08E-01 302.85           18.34   -2.43E-02                       1.47E-01 356.01           62.05   -1.68E-02                       5.57E-02 383.85            8.94   -1.17E-01                       2.62E-01 Cs-134       475.36            1.48   -2.73E-01      3.85E-02         3.11E+00 563.25            8.34   -3.18E-01                       3.74E-01 569.33           15.37    1.03E-01                       2.05E-01 604.72           97.62   -2.42E-02                       3.85E-02 795.86           85.46    6.48E-03                       4.32E-02 801.95            8.69    3.51E-02                       4.07E-01 1038.61             0.99   -4.18E+00                       3.39E+00 1167.97             1.79   -1.38E+00                       2.60E+00 1365.19             3.02   -1.82E+00                       1.21E+00 Cs-137       661.66           85.10    7.55E-03      4.25E-02         4.25E-02 Eu-152       121.78           28.67    4.45E-02      9.46E-02         9.46E-02 244.70            7.61    2.76E-01                       3.93E-01 295.94            0.45    1.91E+00                       7.91E+00 344.28           26.60    3.52E-02                       1.01E-01 367.79            0.86    6.28E-01                       3.22E+00 411.12            2.24    9.53E-01                       1.36E+00 443.96            2.83    2.20E-01                       8.77E-01 488.68            0.42    2.68E+00                       7.14E+00 563.99            0.49   -4.27E+00                       5.96E+00 586.26            0.46    8.65E+00                       1.01E+01 678.62            0.47    6.21E+00                       7.35E+00 688.67            0.86   -2.34E+00                       3.52E+00 719.35            0.28   -3.25E+00                       1.37E+01 778.90           12.96    1.39E-01                       2.99E-01 810.45            0.32    3.74E+00                       9.87E+00 867.37            4.26    2.29E-01                       8.51E-01 919.33            0.43   -6.79E+00                       6.23E+00 964.08           14.65    5.76E-02                       3.24E-01 1085.87            10.24    1.26E-01                       3.89E-01 1089.74             1.73    6.76E-01                       2.75E+00 1112.07            13.69   -2.87E-01                       3.04E-01 1212.95             1.43    4.65E-01                       3.58E+00 1249.94             0.19    1.33E+01                       2.16E+01 1299.14             1.63    3.37E-01                       2.48E+00 1408.01            21.07   -5.14E-02                       1.78E-01 1457.64             0.50    6.94E+01                       2.97E+01 1528.10             0.28    5.16E+00                       1.26E+01 Eu-154       123.07           40.40    2.38E-02      6.73E-02         6.73E-02 247.93            6.89   -3.53E-01                       3.57E-01 591.76            4.95    1.09E-01                       7.14E-01 692.42            1.78   -2.15E-01                       1.71E+00 723.30           20.06   -1.08E-01                       1.84E-01 756.80            4.52    4.23E-01                       8.59E-01 873.18           12.08   -4.12E-01                       2.57E-01
[287]

7/9/2019  10:24:59AM Page 7 of 7 Analysis Report for     09-Jul-19-10028 L1-10221C-FIGS-104SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48        6.47E-02      6.73E-02         3.70E-01 1004.76                  18.01       -2.49E-02                       2.10E-01 1274.43                  34.80        9.15E-02                       1.31E-01 1596.48                   1.80        6.98E-01                       1.90E+00 Eu-155            45.30                  1.31        1.52E+00      1.54E-01         8.61E+00 60.01                  1.22        4.66E+00                       1.05E+01 86.55                 30.70        1.17E-01                       1.64E-01 105.31                 21.10        4.06E-02                       1.54E-01 Ra-226           186.21                  3.64        1.42E-01      7.51E-01         7.51E-01 Pa-231            27.36                 10.30        9.28E-01      1.09E+00         1.09E+00 283.69                  1.70       -5.86E-02                       1.50E+00 300.07                  2.47       -9.36E-01                       1.24E+00 302.65                  2.20        4.30E-01                       1.23E+00 330.06                  1.40        8.08E-01                       2.12E+00 U-235            143.76                 10.96        2.46E-02      4.91E-02         2.69E-01 163.33                  5.08        3.32E-02                       5.22E-01 185.71                 57.20        1.90E-02                       4.91E-02 202.11                  1.08        5.93E-01                       2.32E+00 205.31                  5.01       -5.99E-02                       5.20E-01 Am-241            59.54                 35.90        1.40E-01      3.72E-01         3.72E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[288]

7/9/2019 10:25:05AM Page 1 of 7 Analysis Report for    09-Jul-19-10029 L1-10221C-FIGS-105SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10029 Sample Description                           : L1-10221C-FIGS-105SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.613E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:51:00PM Acquisition Started                          : 7/9/2019 10:09:45AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77837 Fill Height                                  : 1612.90 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:24:55AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[289]

7/9/2019   10:25:05AM         Page 2 of 7 Analysis Report for    09-Jul-19-10029 L1-10221C-FIGS-105SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       238.61               950 -    962          954.90          9.43E+01              13.38      2.97E+01           1.15 2       351.97             1403 -   1413         1407.87           3.71E+01               9.06      1.89E+01           0.40 3       477.71             1905 -   1917         1910.41           2.72E+01               7.73      1.18E+01           0.60 4       583.19             2326 -   2337         2332.07           2.17E+01               7.44      1.33E+01           0.44 5       609.44             2431 -   2444         2437.04           2.77E+01               7.44      9.28E+00           0.64 6       661.79             2642 -   2651         2646.35           1.84E+01               5.37      4.61E+00           0.50 7       969.04             3870 -   3881         3875.23           2.60E+01               5.10      0.00E+00           0.58 8      1460.72             5831 -   5853         5843.24           1.50E+02              13.12      5.65E+00           1.41 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty BE-7                     0.99           477.60
* 10.44             2.79E-01              8.15E-02 K-40                     0.99          1460.82
* 10.66             3.10E+00              3.02E-01 Cs-137                   0.99           661.66
* 85.10             2.82E-02              8.41E-03 Tl-208                   1.00           583.19
* 85.00             3.07E-02              1.07E-02 Bi-211                   0.87           351.07
* 13.02             2.44E-01              6.29E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60             1.46E-01              2.39E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49             7.54E-02              2.07E-02[290]

7/9/2019   10:25:05AM        Page 3 of 7 Analysis Report for    09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99          768.36                 4.89 806.18                 1.26 934.06                 3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00          241.99                 7.25 295.22                18.42 351.93
* 35.60  8.94E-02              2.30E-02 785.96                 1.06 Ac-228                   0.57          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32                11.27 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20                25.80 964.77                 4.99 968.97
* 15.80  2.76E-01              5.54E-02 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[291]

7/9/2019 10:25:05AM         Page 4 of 7 Analysis Report for   09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
BE-7                                0.998                     2.79E-01              8.15E-02 K-40                                0.998                     3.10E+00              3.02E-01 Cs-137                              0.997                     2.82E-02              8.41E-03 Tl-208                              1.000                     3.07E-02              1.07E-02
     ?       Bi-211                              0.879                     2.44E-01              6.29E-02 Pb-212                              1.000                     1.46E-01              2.39E-02 Bi-214                              0.999                     7.54E-02              2.07E-02
     ?       Pb-214                              1.000                     8.94E-02              2.30E-02 Ac-228                              0.571                     2.76E-01              5.54E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[292]

7/9/2019  10:25:05AM       Page 5 of 7 Analysis Report for    09-Jul-19-10029 L1-10221C-FIGS-105SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:24:55AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        7.68E-02          5.08E-02         5.08E-02
+         BE-7            477.60
* 10.44       2.79E-01          2.27E-01         2.27E-01
+         K-40          1460.82
* 10.66       3.10E+00          3.86E-01         3.86E-01 Mn-54           834.85              99.98       2.58E-02          3.94E-02         3.94E-02 Co-60         1173.23               99.85       4.93E-02          4.15E-02         5.18E-02 1332.49               99.98       2.67E-02                           4.15E-02 Nb-94           702.65              99.81       1.34E-02          3.72E-02         4.02E-02 871.09              99.89     -8.59E-03                            3.72E-02 Ag-108m          79.13                6.60    -3.56E-01           3.19E-02         1.24E+00 433.94              90.50       3.66E-03                           3.19E-02 614.28              89.80     -1.56E-02                            5.14E-02 722.94              90.80     -6.71E-03                            4.09E-02 Sb-125          176.31                6.84    -2.00E-01           9.81E-02         3.75E-01 380.45                1.52    -1.14E+00                            1.77E+00 427.87              29.60     -2.51E-02                            9.81E-02 463.36              10.49       1.43E-01                           2.83E-01 600.60              17.65       1.95E-01                           1.96E-01 606.71                4.98      5.67E-01                           9.03E-01 635.95              11.22     -1.80E-01                            2.70E-01          [293]

7/9/2019  10:25:05AM Page 6 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.40E-01      9.81E-02         1.48E+00 Ba-133        79.61            2.65    5.34E-01      6.03E-02         2.96E+00 81.00           32.90   -2.45E-01                       2.03E-01 276.40            7.16    1.44E-01                       4.51E-01 302.85           18.34   -6.13E-03                       1.68E-01 356.01           62.05   -2.46E-02                       6.03E-02 383.85            8.94    1.51E-01                       3.31E-01 Cs-134       475.36            1.48    1.73E+00      3.90E-02         2.79E+00 563.25            8.34   -3.43E-01                       3.20E-01 569.33           15.37   -3.62E-02                       1.92E-01 604.72           97.62   -4.09E-02                       4.09E-02 795.86           85.46   -1.98E-02                       3.90E-02 801.95            8.69   -1.84E-01                       4.05E-01 1038.61             0.99   -2.04E+00                       3.69E+00 1167.97             1.79   -1.40E+00                       2.68E+00 1365.19             3.02   -7.44E-02                       1.08E+00
+         Cs-137       661.66
* 85.10    2.82E-02      2.12E-02         2.12E-02 Eu-152       121.78           28.67    2.63E-02      8.99E-02         1.14E-01 244.70            7.61    1.13E-01                       3.81E-01 295.94            0.45    1.74E+00                       7.41E+00 344.28           26.60   -8.43E-02                       8.99E-02 367.79            0.86    1.75E-01                       3.52E+00 411.12            2.24    1.01E-01                       1.32E+00 443.96            2.83   -2.68E-01                       1.14E+00 488.68            0.42    6.38E-02                       7.55E+00 563.99            0.49   -2.05E+00                       5.43E+00 586.26            0.46    7.58E+00                       1.00E+01 678.62            0.47    2.80E+00                       6.03E+00 688.67            0.86   -1.48E+00                       3.15E+00 719.35            0.28    1.41E+00                       1.23E+01 778.90           12.96   -8.64E-02                       2.40E-01 810.45            0.32    7.21E+00                       1.31E+01 867.37            4.26    2.83E-01                       9.45E-01 919.33            0.43   -2.25E+00                       9.00E+00 964.08           14.65   -2.21E-01                       4.16E-01 1085.87            10.24   -1.56E-01                       3.18E-01 1089.74             1.73   -3.34E-01                       2.48E+00 1112.07            13.69   -1.00E-01                       3.18E-01 1212.95             1.43   -7.21E-01                       3.44E+00 1249.94             0.19    7.17E+00                       2.03E+01 1299.14             1.63   -1.90E+00                       2.82E+00 1408.01            21.07    2.94E-02                       1.75E-01 1457.64             0.50    6.55E+01                       2.78E+01 1528.10             0.28   -3.03E+00                       1.10E+01 Eu-154       123.07           40.40   -2.55E-02      7.79E-02         7.79E-02 247.93            6.89   -2.16E-01                       3.41E-01 591.76            4.95    2.24E-01                       6.59E-01 692.42            1.78    3.45E-02                       1.71E+00 723.30           20.06    5.64E-02                       1.88E-01 756.80            4.52   -8.29E-03                       7.50E-01 873.18           12.08   -2.78E-01                       3.22E-01
[294]

7/9/2019  10:25:05AM Page 7 of 7 Analysis Report for     09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -6.16E-02      7.79E-02         3.59E-01 1004.76                  18.01        1.33E-01                       1.98E-01 1274.43                  34.80       -8.32E-02                       1.16E-01 1596.48                   1.80       -9.49E-01                       1.63E+00 Eu-155            45.30                  1.31       -7.25E+00      1.82E-01         1.54E+01 60.01                  1.22       -7.21E+00                       1.86E+01 86.55                 30.70       -1.51E-03                       1.83E-01 105.31                 21.10       -7.81E-02                       1.82E-01 Ra-226           186.21                  3.64        8.41E-02      8.51E-01         8.51E-01 Pa-231            27.36                 10.30        1.30E+00      1.36E+00         1.76E+00 283.69                  1.70       -2.98E-01                       1.88E+00 300.07                  2.47       -5.02E-01                       1.36E+00 302.65                  2.20       -2.12E-01                       1.41E+00 330.06                  1.40       -1.23E+00                       2.39E+00 U-235            143.76                 10.96       -1.27E-01      5.43E-02         2.82E-01 163.33                  5.08       -2.34E-01                       5.86E-01 185.71                 57.20        1.43E-02                       5.43E-02 202.11                  1.08        3.08E-01                       2.57E+00 205.31                  5.01       -4.31E-01                       5.65E-01 Am-241            59.54                 35.90       -7.23E-03      6.67E-01         6.67E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[295]

7/9/2019 10:42:53AM Page 1 of 7 Analysis Report for    09-Jul-19-10030 L1-10221C-FIGS-106SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10030 Sample Description                           : L1-10221C-FIGS-106SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.676E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:53:00PM Acquisition Started                          : 7/9/2019 10:27:41AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77838 Fill Height                                  : 1675.50 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:42:44AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[296]

7/9/2019   10:42:53AM         Page 2 of 7 Analysis Report for    09-Jul-19-10030 L1-10221C-FIGS-106SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       238.81               474 -    481          477.81          1.04E+02              15.63      6.75E+01           1.55 2       352.00               700 -    708          703.94          6.90E+01              11.44      2.90E+01           1.51 3       583.32             1161 -   1169         1166.24           3.66E+01               8.34      1.54E+01           1.14 4       609.09             1212 -   1223         1217.76           6.79E+01               9.13      6.07E+00           1.24 5       661.79             1319 -   1328         1323.11           3.35E+01               7.86      1.25E+01           0.85 6      1460.85             2916 -   2928         2921.76           1.65E+02              13.55      6.80E+00           1.64 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     1.00          1460.82
* 10.66             3.03E+00              2.82E-01 Cs-137                   0.99           661.66
* 85.10             4.60E-02              1.11E-02 Tl-208                   0.99           583.19
* 85.00             4.63E-02              1.09E-02 Bi-211                   0.87           351.07
* 13.02             4.07E-01              7.50E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60             1.44E-01              2.46E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49             1.65E-01              2.43E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11                                             [297]

7/9/2019   10:42:53AM         Page 3 of 7 Analysis Report for    09-Jul-19-10030 L1-10221C-FIGS-106SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   0.99        1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00          241.99                 7.25 295.22                18.42 351.93
* 35.60       1.49E-01              2.74E-02 785.96                 1.06
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean                Wt mean     Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
K-40                              1.000               3.03E+00               2.82E-01 Cs-137                            0.997               4.60E-02               1.11E-02 Tl-208                            0.997               4.63E-02               1.09E-02
      ?       Bi-211                            0.872               4.07E-01               7.50E-02 Pb-212                            0.995               1.44E-01               2.46E-02 Bi-214                            0.997               1.65E-01               2.43E-02
      ?       Pb-214                            1.000               1.49E-01               2.74E-02
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7/9/2019 10:42:53AM Page 4 of 7 Analysis Report for   09-Jul-19-10030 L1-10221C-FIGS-106SS
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[299]

7/9/2019  10:42:53AM       Page 5 of 7 Analysis Report for    09-Jul-19-10030 L1-10221C-FIGS-106SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:42:44AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        6.26E-02          4.62E-02         4.62E-02 BE-7            477.60              10.44       2.33E-01          3.39E-01         3.39E-01
+         K-40          1460.82
* 10.66       3.03E+00          3.21E-01         3.21E-01 Mn-54           834.85              99.98       3.11E-03          2.83E-02         2.83E-02 Co-60         1173.23               99.85       2.97E-02          3.69E-02         4.62E-02 1332.49               99.98       1.24E-02                           3.69E-02 Nb-94           702.65              99.81       1.23E-02          3.47E-02         3.49E-02 871.09              99.89       1.85E-02                           3.47E-02 Ag-108m          79.13                6.60      1.37E-01          3.05E-02         9.77E-01 433.94              90.50     -2.18E-03                            3.05E-02 614.28              89.80     -4.17E-02                            4.34E-02 722.94              90.80       7.90E-03                           3.85E-02 Sb-125          176.31                6.84      7.07E-03          9.95E-02         4.43E-01 380.45                1.52    -1.07E-01                            1.95E+00 427.87              29.60     -1.02E-02                            9.95E-02 463.36              10.49       5.29E-02                           3.02E-01 600.60              17.65       1.06E-02                           1.89E-01 606.71                4.98    -1.85E-01                            1.02E+00 635.95              11.22       6.58E-02                           2.63E-01          [300]

7/9/2019  10:42:53AM Page 6 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79    6.32E-02      9.95E-02         1.57E+00 Ba-133        79.61            2.65    1.88E-01      6.03E-02         2.32E+00 81.00           32.90   -1.14E-01                       1.64E-01 276.40            7.16   -2.25E-01                       3.91E-01 302.85           18.34    9.78E-02                       1.56E-01 356.01           62.05   -3.08E-02                       6.03E-02 383.85            8.94   -1.15E-01                       2.85E-01 Cs-134       475.36            1.48    1.18E+00      3.49E-02         2.45E+00 563.25            8.34   -4.32E-02                       3.51E-01 569.33           15.37   -5.93E-03                       1.92E-01 604.72           97.62   -7.83E-03                       4.55E-02 795.86           85.46   -2.09E-02                       3.49E-02 801.95            8.69   -6.80E-02                       3.86E-01 1038.61             0.99    4.98E-01                       3.67E+00 1167.97             1.79   -2.25E+00                       2.07E+00 1365.19             3.02   -4.63E-01                       8.40E-01
+         Cs-137       661.66
* 85.10    4.60E-02      2.87E-02         2.87E-02 Eu-152       121.78           28.67   -5.86E-03      1.00E-01         1.00E-01 244.70            7.61   -3.30E-01                       3.81E-01 295.94            0.45    6.27E+00                       7.40E+00 344.28           26.60   -5.27E-02                       1.16E-01 367.79            0.86   -7.09E-01                       3.01E+00 411.12            2.24    7.15E-01                       1.53E+00 443.96            2.83   -5.13E-03                       9.79E-01 488.68            0.42   -3.33E+00                       6.12E+00 563.99            0.49   -5.40E-01                       5.96E+00 586.26            0.46   -7.87E+00                       1.02E+01 678.62            0.47   -5.03E-01                       5.39E+00 688.67            0.86   -1.54E-01                       3.47E+00 719.35            0.28    5.13E+00                       1.10E+01 778.90           12.96   -2.98E-02                       2.54E-01 810.45            0.32    2.07E+00                       1.09E+01 867.37            4.26    1.10E-01                       8.61E-01 919.33            0.43    7.27E-01                       8.22E+00 964.08           14.65   -9.45E-02                       3.05E-01 1085.87            10.24   -1.98E-01                       3.16E-01 1089.74             1.73    6.05E-01                       2.16E+00 1112.07            13.69   -4.76E-02                       2.83E-01 1212.95             1.43    1.94E+00                       3.30E+00 1249.94             0.19   -7.14E+00                       1.81E+01 1299.14             1.63   -5.81E-01                       1.62E+00 1408.01            21.07    1.03E-01                       1.94E-01 1457.64             0.50   -7.71E+00                       2.59E+01 1528.10             0.28    3.38E+00                       1.12E+01 Eu-154       123.07           40.40   -1.45E-03      6.95E-02         6.95E-02 247.93            6.89   -9.90E-02                       4.03E-01 591.76            4.95    2.38E-02                       7.20E-01 692.42            1.78   -2.05E-01                       1.75E+00 723.30           20.06    7.32E-02                       1.82E-01 756.80            4.52    2.26E-01                       7.29E-01 873.18           12.08   -8.34E-02                       2.41E-01
[301]

7/9/2019  10:42:53AM Page 7 of 7 Analysis Report for     09-Jul-19-10030 L1-10221C-FIGS-106SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.99E-01      6.95E-02         2.93E-01 1004.76                  18.01        3.20E-02                       1.93E-01 1274.43                  34.80        1.45E-02                       9.96E-02 1596.48                   1.80        4.65E-01                       1.45E+00 Eu-155            45.30                  1.31        5.57E+00      1.47E-01         1.06E+01 60.01                  1.22        8.65E+00                       1.23E+01 86.55                 30.70        3.98E-02                       1.48E-01 105.31                 21.10       -6.52E-02                       1.47E-01 Ra-226           186.21                  3.64        3.37E-01      8.89E-01         8.89E-01 Pa-231            27.36                 10.30        6.17E-01      1.01E+00         1.01E+00 283.69                  1.70        5.71E-01                       1.75E+00 300.07                  2.47       -1.49E+00                       1.07E+00 302.65                  2.20        8.15E-01                       1.30E+00 330.06                  1.40       -1.92E-01                       2.12E+00 U-235            143.76                 10.96        7.07E-02      5.70E-02         2.66E-01 163.33                  5.08        1.26E-01                       6.35E-01 185.71                 57.20        3.62E-02                       5.70E-02 202.11                  1.08        9.69E-03                       2.87E+00 205.31                  5.01       -2.76E-01                       5.88E-01 Am-241            59.54                 35.90        3.21E-01      4.36E-01         4.36E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[302]

7/9/2019 10:43:04AM Page 1 of 7 Analysis Report for    09-Jul-19-10031 L1-10221C-FIGS-107SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10031 Sample Description                           : L1-10221C-FIGS-107SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.657E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:55:00PM Acquisition Started                          : 7/9/2019 10:27:51AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.0 seconds Dead Time                                    : 0.11 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77839 Fill Height                                  : 1657.29 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:42:55AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[303]

7/9/2019   10:43:04AM         Page 2 of 7 Analysis Report for    09-Jul-19-10031 L1-10221C-FIGS-107SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       238.58               948 -    959          954.43          6.53E+01              13.62      4.77E+01           0.67 2       351.69             1400 -   1415         1406.48           5.77E+01              10.46      1.74E+01           1.18 3       582.78             2325 -   2337         2330.32           2.83E+01               7.35      9.75E+00           1.22 4       609.04             2429 -   2442         2435.34           4.25E+01               7.76      6.51E+00           1.20 5       910.76             3638 -   3647         3642.01           1.65E+01               5.99      8.46E+00           0.74 6      1460.04             5830 -   5849         5839.98           1.42E+02              12.94      7.41E+00           1.50 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     0.90          1460.82
* 10.66             3.45E+00              3.49E-01 Tl-208                   0.97           583.19
* 85.00             4.63E-02              1.24E-02 Bi-211                   0.94           351.07
* 13.02             4.34E-01              8.62E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60             1.15E-01              2.58E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49             1.34E-01              2.58E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92                                              [304]

7/9/2019   10:43:04AM        Page 3 of 7 Analysis Report for    09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99        1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99          241.99                 7.25 295.22                18.42 351.93
* 35.60  1.59E-01              3.15E-02 785.96                 1.06 Ac-228                   0.99          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32                11.27 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20
* 25.80  1.21E-01              4.41E-02 964.77                 4.99 968.97                15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[305]

7/9/2019 10:43:04AM         Page 4 of 7 Analysis Report for   09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.906                     3.45E+00              3.49E-01 Tl-208                              0.974                     4.63E-02              1.24E-02
     ?       Bi-211                              0.941                     4.34E-01              8.62E-02 Pb-212                              1.000                     1.15E-01              2.58E-02 Bi-214                              0.995                     1.34E-01              2.58E-02
     ?       Pb-214                              0.995                     1.59E-01              3.15E-02 Ac-228                              0.990                     1.21E-01              4.41E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[306]

7/9/2019  10:43:04AM       Page 5 of 7 Analysis Report for    09-Jul-19-10031 L1-10221C-FIGS-107SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:42:55AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        6.37E-02          5.27E-02         5.27E-02 BE-7            477.60              10.44       8.24E-02          4.00E-01         4.00E-01
+         K-40          1460.82
* 10.66       3.45E+00          4.90E-01         4.90E-01 Mn-54           834.85              99.98       0.00E+00          4.32E-02         4.32E-02 Co-60         1173.23               99.85       8.24E-03          3.77E-02         5.66E-02 1332.49               99.98       3.20E-03                           3.77E-02 Nb-94           702.65              99.81     -7.92E-04           3.85E-02         3.85E-02 871.09              99.89       6.85E-03                           3.92E-02 Ag-108m          79.13                6.60      7.43E-01          3.77E-02         1.61E+00 433.94              90.50     -3.97E-03                            3.77E-02 614.28              89.80     -1.03E-02                            4.61E-02 722.94              90.80       3.62E-02                           4.68E-02 Sb-125          176.31                6.84      2.48E-02          1.08E-01         4.79E-01 380.45                1.52    -9.56E-01                            2.25E+00 427.87              29.60     -4.21E-02                            1.08E-01 463.36              10.49       1.29E-02                           3.41E-01 600.60              17.65     -1.13E-01                            2.16E-01 606.71                4.98      1.27E+00                           1.18E+00 635.95              11.22       2.09E-01                           4.01E-01          [307]

7/9/2019  10:43:04AM Page 6 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.35E+00      1.08E-01         2.50E+00 Ba-133        79.61            2.65    7.58E-01      6.34E-02         3.83E+00 81.00           32.90   -1.11E-01                       2.72E-01 276.40            7.16    6.58E-02                       4.60E-01 302.85           18.34    1.00E-01                       1.96E-01 356.01           62.05   -5.63E-03                       6.34E-02 383.85            8.94    5.84E-02                       3.79E-01 Cs-134       475.36            1.48    1.36E+00      5.40E-02         2.82E+00 563.25            8.34    7.19E-02                       3.79E-01 569.33           15.37    5.94E-02                       2.22E-01 604.72           97.62   -1.55E-02                       5.77E-02 795.86           85.46    5.03E-02                       5.40E-02 801.95            8.69    2.36E-01                       4.51E-01 1038.61             0.99    0.00E+00                       4.83E+00 1167.97             1.79   -8.98E-01                       3.15E+00 1365.19             3.02   -1.80E+00                       9.16E-01 Cs-137       661.66           85.10    1.39E-02      5.04E-02         5.04E-02 Eu-152       121.78           28.67   -4.63E-02      1.30E-01         1.44E-01 244.70            7.61   -2.14E-01                       4.97E-01 295.94            0.45    7.37E-01                       8.45E+00 344.28           26.60    1.36E-02                       1.30E-01 367.79            0.86    1.81E+00                       4.03E+00 411.12            2.24    7.47E-01                       1.63E+00 443.96            2.83    6.11E-01                       1.29E+00 488.68            0.42   -3.65E+00                       8.03E+00 563.99            0.49   -7.01E-01                       6.60E+00 586.26            0.46   -1.71E+00                       1.12E+01 678.62            0.47   -2.08E+00                       8.31E+00 688.67            0.86    2.41E+00                       4.70E+00 719.35            0.28   -1.23E+01                       1.16E+01 778.90           12.96   -5.13E-01                       2.96E-01 810.45            0.32    1.08E+01                       1.32E+01 867.37            4.26    7.47E-02                       8.62E-01 919.33            0.43   -5.76E+00                       7.29E+00 964.08           14.65    8.69E-02                       3.84E-01 1085.87            10.24   -2.90E-02                       4.44E-01 1089.74             1.73    2.09E+00                       2.78E+00 1112.07            13.69    8.55E-02                       3.56E-01 1212.95             1.43    2.21E-01                       3.97E+00 1249.94             0.19    6.15E+00                       1.67E+01 1299.14             1.63   -3.41E+00                       2.41E+00 1408.01            21.07    4.07E-02                       2.07E-01 1457.64             0.50    8.00E+01                       3.23E+01 1528.10             0.28   -2.43E+00                       1.30E+01 Eu-154       123.07           40.40   -6.72E-03      9.93E-02         9.93E-02 247.93            6.89    1.19E-01                       4.78E-01 591.76            4.95   -7.67E-02                       8.04E-01 692.42            1.78   -1.32E-01                       2.10E+00 723.30           20.06    2.01E-01                       2.16E-01 756.80            4.52    6.27E-02                       8.33E-01 873.18           12.08    1.56E-02                       3.43E-01
[308]

7/9/2019  10:43:04AM Page 7 of 7 Analysis Report for     09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -6.21E-02      9.93E-02         3.14E-01 1004.76                  18.01        6.44E-02                       2.53E-01 1274.43                  34.80       -1.54E-01                       1.57E-01 1596.48                   1.80       -2.37E+00                       2.11E+00 Eu-155            45.30                  1.31        1.08E+01      2.35E-01         2.70E+01 60.01                  1.22       -4.57E+00                       2.64E+01 86.55                 30.70        2.27E-01                       2.67E-01 105.31                 21.10        1.24E-02                       2.35E-01 Ra-226           186.21                  3.64        1.90E-01      9.28E-01         9.28E-01 Pa-231            27.36                 10.30        1.50E+00      1.41E+00         2.92E+00 283.69                  1.70       -6.87E-01                       1.82E+00 300.07                  2.47       -2.90E-01                       1.41E+00 302.65                  2.20        1.09E+00                       1.62E+00 330.06                  1.40        8.05E-01                       2.67E+00 U-235            143.76                 10.96        9.47E-02      5.78E-02         3.68E-01 163.33                  5.08        3.60E-01                       7.35E-01 185.71                 57.20       -1.62E-03                       5.78E-02 202.11                  1.08       -1.02E+00                       3.02E+00 205.31                  5.01       -1.61E-01                       6.57E-01 Am-241            59.54                 35.90       -6.30E-01      8.83E-01         8.83E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[309]

7/9/2019 10:43:17AM Page 1 of 7 Analysis Report for    09-Jul-19-10032 L1-10221C-FIGS-108SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10032 Sample Description                           : L1-10221C-FIGS-108SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.641E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:57:00PM Acquisition Started                          : 7/9/2019 10:28:01AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77840 Fill Height                                  : 1640.53 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:43:10AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[310]

7/9/2019   10:43:17AM         Page 2 of 7 Analysis Report for    09-Jul-19-10032 L1-10221C-FIGS-108SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       238.81               946 - 961             954.80          6.68E+01              13.86      4.12E+01           0.42 2       609.57             2431 - 2441           2436.31           3.16E+01               6.84      6.36E+00           0.52 3       911.18             3635 - 3648           3642.19           2.92E+01               5.85      1.77E+00           0.68 4      1460.41             5830 - 5849           5839.57           1.30E+02              12.80      9.71E+00           1.11 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     0.97          1460.82
* 10.66             2.87E+00              3.08E-01 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60             1.05E-01              2.33E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49             9.03E-02              2.03E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83 1280.98                    1.43 1377.67                    3.99                                             [311]

7/9/2019   10:43:17AM         Page 3 of 7 Analysis Report for    09-Jul-19-10032 L1-10221C-FIGS-108SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   0.99        1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Ac-228                   1.00          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32                11.27 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20
* 25.80       1.93E-01              3.95E-02 964.77                 4.99 968.97                15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean                Wt mean     Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
K-40                              0.973               2.87E+00               3.08E-01 Pb-212                            0.996               1.05E-01               2.33E-02 Bi-214                            0.996               9.03E-02               2.03E-02 Ac-228                            1.000               1.93E-01               3.95E-02
[312]

7/9/2019 10:43:17AM Page 4 of 7 Analysis Report for   09-Jul-19-10032 L1-10221C-FIGS-108SS
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[313]

7/9/2019  10:43:17AM       Page 5 of 7 Analysis Report for    09-Jul-19-10032 L1-10221C-FIGS-108SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:43:10AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        5.18E-02          4.69E-02         4.69E-02 BE-7            477.60              10.44       1.90E-01          3.69E-01         3.69E-01
+         K-40          1460.82
* 10.66       2.87E+00          4.96E-01         4.96E-01 Mn-54           834.85              99.98       2.18E-02          3.73E-02         3.73E-02 Co-60         1173.23               99.85     -3.02E-03           4.11E-02         4.45E-02 1332.49               99.98       2.41E-02                           4.11E-02 Nb-94           702.65              99.81       1.64E-02          3.16E-02         3.16E-02 871.09              99.89       1.80E-02                           4.02E-02 Ag-108m          79.13                6.60      1.36E-01          3.05E-02         9.78E-01 433.94              90.50     -2.87E-02                            3.05E-02 614.28              89.80     -6.67E-02                            4.48E-02 722.94              90.80       9.10E-03                           3.90E-02 Sb-125          176.31                6.84    -2.14E-02           1.02E-01         3.41E-01 380.45                1.52    -5.70E-01                            1.60E+00 427.87              29.60       4.40E-02                           1.02E-01 463.36              10.49     -9.38E-02                            2.80E-01 600.60              17.65     -1.32E-01                            1.52E-01 606.71                4.98      7.16E-01                           9.65E-01 635.95              11.22       1.72E-01                           3.42E-01          [314]

7/9/2019  10:43:17AM Page 6 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79   -2.20E-01      1.02E-01         1.97E+00 Ba-133        79.61            2.65    2.55E-01      4.83E-02         2.35E+00 81.00           32.90   -1.24E-01                       1.60E-01 276.40            7.16    1.99E-01                       4.15E-01 302.85           18.34    7.60E-02                       1.42E-01 356.01           62.05   -5.29E-02                       4.83E-02 383.85            8.94    5.09E-02                       2.93E-01 Cs-134       475.36            1.48    1.73E+00      4.12E-02         2.62E+00 563.25            8.34   -1.01E+00                       3.59E-01 569.33           15.37   -1.40E-01                       1.73E-01 604.72           97.62   -5.37E-02                       4.19E-02 795.86           85.46    6.42E-04                       4.12E-02 801.95            8.69    1.21E-01                       4.07E-01 1038.61             0.99    1.83E+00                       4.67E+00 1167.97             1.79   -3.22E-01                       2.34E+00 1365.19             3.02   -6.76E-01                       1.33E+00 Cs-137       661.66           85.10    1.17E-02      4.01E-02         4.01E-02 Eu-152       121.78           28.67    4.69E-02      9.16E-02         9.16E-02 244.70            7.61   -3.99E-02                       3.85E-01 295.94            0.45    6.62E+00                       7.87E+00 344.28           26.60   -4.16E-02                       9.97E-02 367.79            0.86   -4.41E-01                       3.13E+00 411.12            2.24    2.64E-01                       1.23E+00 443.96            2.83   -7.53E-02                       1.14E+00 488.68            0.42    1.54E-01                       6.73E+00 563.99            0.49   -7.74E+00                       6.10E+00 586.26            0.46    1.11E+01                       9.63E+00 678.62            0.47   -1.92E+00                       5.97E+00 688.67            0.86   -1.63E+00                       3.20E+00 719.35            0.28    5.07E+00                       1.27E+01 778.90           12.96   -1.88E-01                       2.22E-01 810.45            0.32   -2.13E+00                       8.84E+00 867.37            4.26   -2.99E-01                       8.97E-01 919.33            0.43    2.39E+00                       8.08E+00 964.08           14.65    1.34E-01                       3.00E-01 1085.87            10.24    2.80E-01                       4.01E-01 1089.74             1.73    1.34E-01                       2.16E+00 1112.07            13.69    2.13E-02                       2.86E-01 1212.95             1.43   -2.97E-01                       4.08E+00 1249.94             0.19    8.60E+00                       2.70E+01 1299.14             1.63   -1.06E+00                       2.06E+00 1408.01            21.07    1.02E-02                       1.78E-01 1457.64             0.50    6.21E+01                       2.83E+01 1528.10             0.28   -4.52E+00                       1.07E+01 Eu-154       123.07           40.40   -2.08E-02      6.47E-02         6.47E-02 247.93            6.89    4.53E-02                       3.88E-01 591.76            4.95    1.22E-01                       5.35E-01 692.42            1.78    1.19E+00                       1.71E+00 723.30           20.06    3.45E-02                       1.73E-01 756.80            4.52   -2.18E-01                       7.13E-01 873.18           12.08    9.71E-02                       3.02E-01
[315]

7/9/2019  10:43:17AM Page 7 of 7 Analysis Report for     09-Jul-19-10032 L1-10221C-FIGS-108SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48        8.20E-02      6.47E-02         3.81E-01 1004.76                  18.01        1.68E-02                       1.97E-01 1274.43                  34.80        2.28E-02                       1.23E-01 1596.48                   1.80       -1.08E+00                       2.05E+00 Eu-155            45.30                  1.31       -1.15E+00      1.44E-01         8.43E+00 60.01                  1.22       -7.39E+00                       9.16E+00 86.55                 30.70        2.88E-02                       1.44E-01 105.31                 21.10        3.03E-02                       1.65E-01 Ra-226           186.21                  3.64        1.03E-01      7.47E-01         7.47E-01 Pa-231            27.36                 10.30        8.71E-01      1.11E+00         1.11E+00 283.69                  1.70       -6.96E-01                       1.46E+00 300.07                  2.47       -8.40E-01                       1.16E+00 302.65                  2.20        8.05E-01                       1.19E+00 330.06                  1.40       -5.33E-01                       1.87E+00 U-235            143.76                 10.96       -5.16E-02      4.89E-02         2.09E-01 163.33                  5.08        1.77E-01                       5.44E-01 185.71                 57.20        3.77E-02                       4.89E-02 202.11                  1.08       -9.17E-01                       2.16E+00 205.31                  5.01       -1.63E-01                       4.89E-01 Am-241            59.54                 35.90       -2.03E-01      3.20E-01         3.20E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[316]

7/9/2019 10:43:24AM Page 1 of 7 Analysis Report for    09-Jul-19-10033 L1-10221C-FIGS-109SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 09-Jul-19-10033 Sample Description                           : L1-10221C-FIGS-109SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.658E+03 grams Facility                                     : Default Sample Taken On                              : 7/8/2019 12:59:00PM Acquisition Started                          : 7/9/2019 10:28:11AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 7/9/2019 Efficiency Calibration Description           :
Sample Number                                : 77841 Fill Height                                  : 1657.61 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/9/2019 10:43:16AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[317]

7/9/2019   10:43:24AM         Page 2 of 7 Analysis Report for    09-Jul-19-10033 L1-10221C-FIGS-109SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       185.77               740 - 751             743.79          3.38E+01              10.36      2.92E+01           0.50 2       238.54               948 - 961             954.65          9.44E+01              12.74      2.46E+01           1.03 3       351.95             1401 - 1415           1407.78           5.00E+01               9.68      1.50E+01           1.06 4       609.30             2431 - 2442           2436.47           3.49E+01               7.10      6.06E+00           0.67 5      1460.98             5833 - 5854           5844.30           1.30E+02              11.83      2.64E+00           0.93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     0.99          1460.82
* 10.66             2.67E+00              2.69E-01 Bi-211                   0.88           351.07
* 13.02             3.28E-01              6.87E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60             1.46E-01              2.30E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49             9.45E-02              2.00E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83                                             [318]

7/9/2019   10:43:24AM         Page 3 of 7 Analysis Report for    09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   1.00        1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00          241.99                 7.25 295.22                18.42 351.93
* 35.60       1.20E-01              2.51E-02 785.96                 1.06 Ra-226                   0.96          186.21
* 3.64       5.61E-01              1.78E-01 U-235                    1.00          143.76                10.96 163.33                 5.08 185.71
* 57.20       3.57E-02              1.13E-02 202.11                 1.08 205.31                 5.01
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean                Wt mean     Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
K-40                              0.996               2.67E+00               2.69E-01
      ?       Bi-211                            0.884               3.28E-01               6.87E-02 Pb-212                            0.999               1.46E-01               2.30E-02 Bi-214                            1.000               9.45E-02               2.00E-02
      ?       Pb-214                            1.000               1.20E-01               2.51E-02
      ?       Ra-226                            0.969               5.61E-01               1.78E-01      [319]

7/9/2019 10:43:24AM         Page 4 of 7 Analysis Report for   09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
     ?       U-235                               1.000                     3.57E-02              1.13E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[320]

7/9/2019  10:43:24AM       Page 5 of 7 Analysis Report for    09-Jul-19-10033 L1-10221C-FIGS-109SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/9/2019 10:43:16AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        3.67E-02          4.74E-02         4.74E-02 BE-7            477.60              10.44       4.11E-01          3.94E-01         3.94E-01
+         K-40          1460.82
* 10.66       2.67E+00          2.75E-01         2.75E-01 Mn-54           834.85              99.98       3.44E-04          2.84E-02         2.84E-02 Co-60         1173.23               99.85     -4.12E-02           2.55E-02         3.10E-02 1332.49               99.98       8.17E-03                           2.55E-02 Nb-94           702.65              99.81     -6.35E-03           2.80E-02         3.57E-02 871.09              99.89     -1.89E-02                            2.80E-02 Ag-108m          79.13                6.60    -2.07E-01           3.35E-02         1.17E+00 433.94              90.50     -2.48E-04                            3.35E-02 614.28              89.80     -2.55E-02                            5.60E-02 722.94              90.80     -2.05E-03                            3.43E-02 Sb-125          176.31                6.84    -5.42E-02           9.31E-02         4.46E-01 380.45                1.52      7.97E-01                           1.65E+00 427.87              29.60     -6.95E-02                            9.31E-02 463.36              10.49       7.76E-02                           2.94E-01 600.60              17.65     -1.14E-02                            1.82E-01 606.71                4.98      1.15E+00                           1.00E+00 635.95              11.22       2.32E-01                           3.14E-01          [321]

7/9/2019  10:43:24AM Page 6 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.73E-01      9.31E-02         1.70E+00 Ba-133        79.61            2.65   -7.20E-01      5.89E-02         2.86E+00 81.00           32.90   -2.29E-01                       2.04E-01 276.40            7.16   -1.12E-01                       3.96E-01 302.85           18.34    4.31E-02                       1.73E-01 356.01           62.05   -4.86E-03                       5.89E-02 383.85            8.94   -1.01E-01                       2.82E-01 Cs-134       475.36            1.48   -1.51E-01      3.68E-02         2.58E+00 563.25            8.34    1.93E-01                       4.03E-01 569.33           15.37   -1.27E-01                       2.27E-01 604.72           97.62   -1.43E-02                       4.66E-02 795.86           85.46   -2.29E-02                       3.68E-02 801.95            8.69    1.69E-01                       3.74E-01 1038.61             0.99    2.29E+00                       3.55E+00 1167.97             1.79    9.74E-01                       2.12E+00 1365.19             3.02    6.21E-01                       1.19E+00 Cs-137       661.66           85.10    5.13E-02      4.95E-02         4.95E-02 Eu-152       121.78           28.67   -4.45E-02      1.04E-01         1.08E-01 244.70            7.61    2.07E-01                       4.00E-01 295.94            0.45    1.46E+00                       7.62E+00 344.28           26.60   -5.14E-02                       1.04E-01 367.79            0.86    1.47E+00                       3.31E+00 411.12            2.24    9.16E-01                       1.49E+00 443.96            2.83   -1.16E+00                       8.96E-01 488.68            0.42   -8.26E-01                       6.56E+00 563.99            0.49   -4.17E-01                       6.84E+00 586.26            0.46    6.65E+00                       9.24E+00 678.62            0.47    2.54E+00                       6.65E+00 688.67            0.86    3.41E+00                       3.94E+00 719.35            0.28    1.84E+00                       1.05E+01 778.90           12.96   -1.61E-01                       1.92E-01 810.45            0.32    8.39E-02                       8.67E+00 867.37            4.26   -8.82E-02                       7.56E-01 919.33            0.43   -1.09E+01                       8.07E+00 964.08           14.65    2.44E-01                       3.25E-01 1085.87            10.24    9.74E-02                       3.29E-01 1089.74             1.73   -2.46E+00                       1.87E+00 1112.07            13.69   -2.18E-01                       2.68E-01 1212.95             1.43    2.38E+00                       3.55E+00 1249.94             0.19   -7.60E+00                       2.22E+01 1299.14             1.63   -3.09E-02                       2.57E+00 1408.01            21.07   -7.32E-02                       1.57E-01 1457.64             0.50    5.77E+01                       2.56E+01 1528.10             0.28    2.40E+00                       8.96E+00 Eu-154       123.07           40.40   -1.06E-01      7.28E-02         7.28E-02 247.93            6.89   -1.60E-01                       3.58E-01 591.76            4.95    3.40E-01                       7.11E-01 692.42            1.78    1.72E+00                       2.16E+00 723.30           20.06    1.69E-02                       1.55E-01 756.80            4.52    2.19E-01                       6.11E-01 873.18           12.08   -3.28E-01                       2.22E-01
[322]

7/9/2019  10:43:24AM Page 7 of 7 Analysis Report for     09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48        1.29E-01      7.28E-02         3.57E-01 1004.76                  18.01       -1.21E-01                       1.71E-01 1274.43                  34.80        4.13E-02                       1.42E-01 1596.48                   1.80       -8.77E-01                       1.90E+00 Eu-155            45.30                  1.31        9.14E-01      1.66E-01         1.56E+01 60.01                  1.22        1.95E+00                       1.77E+01 86.55                 30.70       -4.13E-02                       1.79E-01 105.31                 21.10       -2.92E-02                       1.66E-01
+         Ra-226           186.21
* 3.64        5.61E-01      5.30E-01         5.30E-01 Pa-231            27.36                 10.30        9.34E-01      1.30E+00         1.84E+00 283.69                  1.70       -5.07E-01                       1.67E+00 300.07                  2.47       -1.79E+00                       1.30E+00 302.65                  2.20       -1.54E-01                       1.43E+00 330.06                  1.40        4.11E-01                       1.99E+00
+         U-235            143.76                 10.96        1.01E-01      3.37E-02         2.73E-01 163.33                  5.08       -2.52E-01                       5.21E-01 185.71
* 57.20        3.57E-02                       3.37E-02 202.11                  1.08       -2.09E-01                       2.51E+00 205.31                  5.01       -7.65E-02                       5.20E-01 Am-241            59.54                 35.90       -2.34E-01      6.12E-01         6.12E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[323]

8/1/2019 7:44:46AM Page 1 of 7 Analysis Report for    01-Aug-19-10008 L1-10221C-FIGS-110SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 01-Aug-19-10008 Sample Description                           : L1-10221C-FIGS-110SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.535E+03 grams Facility                                     : Default Sample Taken On                              : 7/31/2019 9:30:00AM Acquisition Started                          : 8/1/2019 7:29:33AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 8/1/2019 Efficiency Calibration Description           :
Sample Number                                : 78402 Fill Height                                  : 1534.89 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 8/1/2019 7:44:36AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[324]

8/1/2019   7:44:46AM         Page 2 of 7 Analysis Report for    01-Aug-19-10008 L1-10221C-FIGS-110SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty        Counts          (keV) 1         92.68              367 -    379          371.95          3.93E+01             11.22      3.27E+01           0.30 2       185.95               741 -    749          744.53          2.30E+01               9.54     3.10E+01           0.76 3       238.64               949 -    961          955.03          7.26E+01             13.12      3.64E+01           0.92 4       351.90             1400 -   1413         1407.61           6.43E+01             10.37      1.57E+01           0.82 5       583.14             2325 -   2339         2331.89           3.88E+01               7.71     7.18E+00           0.72 6       609.30             2429 -   2444         2436.45           4.66E+01               8.91     1.04E+01           0.83 7      1460.76             5833 -   5854         5843.40           1.69E+02             14.36      1.03E+01           1.31 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     0.99          1460.82
* 10.66             3.53E+00             3.37E-01 Tl-208                   1.00           583.19
* 85.00             5.55E-02             1.15E-02 Bi-211                   0.89           351.07
* 13.02             4.27E-01             7.71E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60             1.14E-01             2.25E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49             1.28E-01             2.57E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11                                            [325]

8/1/2019   7:44:46AM         Page 3 of 7 Analysis Report for    01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00        1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00         241.99                  7.25 295.22                 18.42 351.93
* 35.60  1.56E-01             2.82E-02 785.96                  1.06 Ra-226                   0.98         186.21
* 3.64  3.85E-01             1.63E-01 Ac228-XR                 0.95            89.96                1.90 93.35
* 3.10  1.24E+00             4.08E-01 Th-234                   0.99            92.38                2.13 92.80
* 2.10  1.88E+00             5.96E-01 112.81                  0.21 U-235                    0.99         143.76                 10.96 163.33                  5.08 185.71
* 57.20  2.45E-02             1.04E-02 202.11                  1.08 205.31                  5.01 U235-XR                  0.96            89.96                3.47 93.35
* 5.60  6.86E-01             2.08E-01 105.60                  1.32
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[326]

8/1/2019 7:44:46AM          Page 4 of 7 Analysis Report for   01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.999                     3.53E+00              3.37E-01 Tl-208                              1.000                     5.55E-02              1.15E-02
     ?       Bi-211                              0.895                     4.27E-01              7.71E-02 Pb-212                              1.000                     1.14E-01              2.25E-02 Bi-214                              1.000                     1.28E-01              2.57E-02
     ?       Pb-214                              1.000                     1.56E-01              2.82E-02
     ?       Ra-226                              0.989                     3.85E-01              1.63E-01
     ?       Ac228-XR                            0.957                     1.24E+00              4.08E-01
     ?       Th-234                              0.999                     1.88E+00              5.96E-01
     ?       U-235                               0.994                     2.45E-02              1.04E-02
     ?       U235-XR                             0.962                     6.86E-01              2.08E-01
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[327]

8/1/2019   7:44:46AM       Page 5 of 7 Analysis Report for    01-Aug-19-10008 L1-10221C-FIGS-110SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 8/1/2019 7:44:36AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                           (pCi/grams)        (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        3.71E-02          4.61E-02         4.61E-02 BE-7            477.60              10.44     -1.01E-01           2.56E-01         2.56E-01
+         K-40          1460.82
* 10.66       3.53E+00          4.94E-01         4.94E-01 Mn-54           834.85              99.98       3.67E-02          4.42E-02         4.42E-02 Co-60         1173.23               99.85       1.75E-02          3.05E-02         4.97E-02 1332.49               99.98     -3.07E-02                            3.05E-02 Nb-94           702.65              99.81     -1.32E-02           3.20E-02         3.20E-02 871.09              99.89     -1.08E-02                            3.39E-02 Ag-108m          79.13                6.60      7.83E-01          3.62E-02         1.30E+00 433.94              90.50       1.08E-02                           3.62E-02 614.28              89.80       1.64E-02                           6.02E-02 722.94              90.80       1.93E-03                           5.06E-02 Sb-125          176.31                6.84      1.92E-01          1.15E-01         4.34E-01 380.45                1.52      1.28E+00                           1.88E+00 427.87              29.60     -1.70E-02                            1.15E-01 463.36              10.49       1.88E-01                           3.03E-01 600.60              17.65     -1.21E-01                            2.08E-01 606.71                4.98      9.04E-01                           1.12E+00 635.95              11.22     -3.21E-01                            2.60E-01          [328]

8/1/2019   7:44:46AM Page 6 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79   -6.62E-01      1.15E-01         1.77E+00 Ba-133        79.61            2.65    9.33E-01      6.77E-02         3.02E+00 81.00           32.90   -2.77E-01                       1.96E-01 276.40            7.16   -1.63E-02                       4.69E-01 302.85           18.34    4.04E-02                       1.61E-01 356.01           62.05   -2.47E-02                       6.77E-02 383.85            8.94    2.56E-01                       3.38E-01 Cs-134       475.36            1.48   -9.61E-02      4.24E-02         1.75E+00 563.25            8.34    9.90E-02                       4.34E-01 569.33           15.37    6.72E-02                       2.16E-01 604.72           97.62   -6.03E-02                       5.45E-02 795.86           85.46    3.92E-03                       4.24E-02 801.95            8.69   -2.63E-01                       3.70E-01 1038.61             0.99    5.51E-01                       4.46E+00 1167.97             1.79    1.10E+00                       2.82E+00 1365.19             3.02   -1.58E-01                       1.37E+00 Cs-137       661.66           85.10    2.51E-02      4.72E-02         4.72E-02 Eu-152       121.78           28.67   -1.10E-02      1.14E-01         1.18E-01 244.70            7.61    4.17E-02                       4.29E-01 295.94            0.45    1.74E+00                       7.96E+00 344.28           26.60    5.39E-03                       1.14E-01 367.79            0.86   -1.27E+00                       3.02E+00 411.12            2.24    5.07E-01                       1.26E+00 443.96            2.83   -5.96E-01                       9.09E-01 488.68            0.42   -2.16E+00                       7.15E+00 563.99            0.49    4.33E+00                       7.47E+00 586.26            0.46    1.15E+01                       1.01E+01 678.62            0.47   -4.80E+00                       7.22E+00 688.67            0.86    2.56E+00                       3.84E+00 719.35            0.28    7.87E+00                       1.39E+01 778.90           12.96    1.14E-01                       2.36E-01 810.45            0.32    2.11E+00                       1.04E+01 867.37            4.26    3.34E-01                       9.38E-01 919.33            0.43    2.81E+00                       7.47E+00 964.08           14.65    4.04E-02                       3.31E-01 1085.87            10.24    9.99E-02                       4.24E-01 1089.74             1.73    3.90E-02                       2.51E+00 1112.07            13.69    1.05E-01                       3.36E-01 1212.95             1.43   -2.21E+00                       2.58E+00 1249.94             0.19    2.05E+01                       2.84E+01 1299.14             1.63   -1.48E+00                       2.18E+00 1408.01            21.07   -1.40E-01                       1.78E-01 1457.64             0.50    8.32E+01                       3.04E+01 1528.10             0.28   -7.84E-01                       1.20E+01 Eu-154       123.07           40.40   -1.48E-02      8.13E-02         8.13E-02 247.93            6.89   -6.54E-02                       4.00E-01 591.76            4.95    2.51E-02                       6.29E-01 692.42            1.78    3.44E-01                       1.64E+00 723.30           20.06    1.78E-01                       2.37E-01 756.80            4.52    2.35E-01                       6.43E-01 873.18           12.08   -6.72E-02                       2.81E-01
[329]

8/1/2019   7:44:46AM Page 7 of 7 Analysis Report for     01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -3.79E-02      8.13E-02         3.64E-01 1004.76                  18.01        5.96E-03                       2.19E-01 1274.43                  34.80       -7.27E-02                       1.25E-01 1596.48                   1.80       -8.29E-01                       2.29E+00 Eu-155            45.30                  1.31       -3.00E-01      1.76E-01         1.55E+01 60.01                  1.22       -8.26E+00                       1.66E+01 86.55                 30.70        8.83E-02                       1.76E-01 105.31                 21.10        4.90E-02                       1.83E-01
+         Ra-226           186.21
* 3.64        3.85E-01      5.16E-01         5.16E-01 Pa-231            27.36                 10.30        1.73E+00      1.30E+00         1.88E+00 283.69                  1.70       -3.12E-01                       1.85E+00 300.07                  2.47       -2.42E+00                       1.30E+00 302.65                  2.20        6.66E-01                       1.36E+00 330.06                  1.40        8.03E-01                       2.00E+00
+         U-235            143.76                 10.96       -1.58E-01      3.29E-02         2.59E-01 163.33                  5.08        5.59E-02                       5.72E-01 185.71
* 57.20        2.45E-02                       3.29E-02 202.11                  1.08        1.85E+00                       3.04E+00 205.31                  5.01       -3.68E-01                       6.44E-01 Am-241            59.54                 35.90       -4.39E-02      6.05E-01         6.05E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[330]

8/1/2019 8:46:11AM Page 1 of 7 Analysis Report for    01-Aug-19-10009 L1-10221C-QIGS-110SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 01-Aug-19-10009 Sample Description                           : L1-10221C-QIGS-110SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.529E+03 grams Facility                                     : Default Sample Taken On                              : 7/31/2019 9:30:00AM Acquisition Started                          : 8/1/2019 8:30:59AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 8/1/2019 Efficiency Calibration Description           :
Sample Number                                : 78403 Fill Height                                  : 1528.92 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 8/1/2019 8:46:02AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[331]

8/1/2019   8:46:11AM         Page 2 of 7 Analysis Report for    01-Aug-19-10009 L1-10221C-QIGS-110SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty        Counts          (keV) 1       186.21               740 -    750          745.55          3.16E+01             10.44      3.24E+01           0.77 2       238.63               949 -    960          954.99          7.05E+01             13.13      4.05E+01           1.07 3       295.28             1173 -   1185         1181.35           4.10E+01               9.76     2.00E+01           1.14 4       338.38             1348 -   1359         1353.58           3.84E+01               7.74     8.62E+00           0.91 5       351.70             1401 -   1413         1406.81           6.15E+01             10.36      1.75E+01           0.65 6       511.13             2040 -   2051         2044.00           2.86E+01               8.40     1.64E+01           0.65 7       583.24             2326 -   2338         2332.30           4.20E+01               7.44     4.97E+00           0.98 8      1460.55             5834 -   5852         5842.57           1.40E+02             13.30      1.13E+01           2.00 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty An Pk                    0.99           511.00
* 100.00              3.23E-02             9.75E-03 K-40                     0.98          1460.82
* 10.66             2.93E+00             3.06E-01 Tl-208                   0.99           583.19
* 85.00             6.01E-02             1.12E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60             1.10E-01             2.24E-02 300.09                    3.30 Pb-214                   0.99           241.99                    7.25 295.22
* 18.42             1.71E-01             4.28E-02 351.93
* 35.60             1.50E-01             2.79E-02[332]

8/1/2019   8:46:11AM          Page 3 of 7 Analysis Report for    01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Pb-214                   0.99         785.96                  1.06 Ra-226                   1.00         186.21
* 3.64       5.30E-01             1.80E-01 Ac-228                   0.57         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32
* 11.27       2.87E-01             6.24E-02 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20                 25.80 964.77                  4.99 968.97                 15.80 1588.20                  3.22 U-235                    0.97         143.76                 10.96 163.33                  5.08 185.71
* 57.20       3.37E-02             1.15E-02 202.11                  1.08 205.31                  5.01
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean               Wt mean      Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
An Pk                             0.997               3.23E-02               9.75E-03 K-40                              0.988               2.93E+00               3.06E-01 Tl-208                            0.999               6.01E-02               1.12E-02 X       Bi-211                            0.938 Pb-212                            1.000               1.10E-01               2.24E-02 Pb-214                            0.995               1.56E-01               2.34E-02
      ?       Ra-226                            1.000               5.30E-01               1.80E-01 Ac-228                            0.571               2.87E-01               6.24E-02      [333]

8/1/2019 8:46:11AM          Page 4 of 7 Analysis Report for   01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
     ?       U-235                               0.972                     3.37E-02              1.15E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[334]

8/1/2019   8:46:11AM       Page 5 of 7 Analysis Report for    01-Aug-19-10009 L1-10221C-QIGS-110SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 8/1/2019 8:46:02AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                           (pCi/grams)        (pCi/grams)    (pCi/grams)
(keV)
+         An Pk           511.00
* 100.00        3.23E-02          2.81E-02         2.81E-02 BE-7            477.60              10.44       3.62E-01          3.70E-01         3.70E-01
+         K-40          1460.82
* 10.66       2.93E+00          4.93E-01         4.93E-01 Mn-54           834.85              99.98     -2.73E-02           4.06E-02         4.06E-02 Co-60         1173.23               99.85       2.09E-05          4.48E-02         4.98E-02 1332.49               99.98       2.05E-02                           4.48E-02 Nb-94           702.65              99.81       6.88E-04          3.56E-02         3.56E-02 871.09              99.89     -1.95E-02                            4.40E-02 Ag-108m          79.13                6.60      2.49E-01          3.22E-02         1.32E+00 433.94              90.50     -8.97E-03                            3.22E-02 614.28              89.80     -1.50E-02                            5.70E-02 722.94              90.80     -2.70E-03                            4.63E-02 Sb-125          176.31                6.84      5.82E-03          1.07E-01         4.43E-01 380.45                1.52    -1.86E-02                            2.07E+00 427.87              29.60       8.19E-03                           1.07E-01 463.36              10.49     -1.33E-01                            3.12E-01 600.60              17.65       1.35E-01                           2.20E-01 606.71                4.98      1.38E+00                           1.15E+00 635.95              11.22     -8.44E-02                            2.85E-01          [335]

8/1/2019   8:46:11AM Page 6 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79    5.92E-01      1.07E-01         1.97E+00 Ba-133        79.61            2.65    1.10E+00      6.18E-02         3.19E+00 81.00           32.90   -1.74E-01                       2.12E-01 276.40            7.16    3.59E-02                       4.50E-01 302.85           18.34    9.82E-02                       1.82E-01 356.01           62.05   -3.78E-02                       6.18E-02 383.85            8.94   -1.61E-01                       3.13E-01 Cs-134       475.36            1.48   -5.87E-02      4.85E-02         2.47E+00 563.25            8.34   -1.11E-01                       3.70E-01 569.33           15.37   -6.86E-02                       2.24E-01 604.72           97.62    6.66E-03                       5.31E-02 795.86           85.46    3.01E-02                       4.85E-02 801.95            8.69   -3.66E-01                       3.81E-01 1038.61             0.99    2.69E-01                       4.46E+00 1167.97             1.79    1.72E+00                       2.71E+00 1365.19             3.02    5.63E-01                       1.16E+00 Cs-137       661.66           85.10    5.65E-02      5.28E-02         5.28E-02 Eu-152       121.78           28.67    2.00E-02      1.10E-01         1.14E-01 244.70            7.61    3.85E-01                       4.49E-01 295.94            0.45    7.34E+00                       8.72E+00 344.28           26.60   -3.05E-02                       1.10E-01 367.79            0.86    1.45E+00                       3.32E+00 411.12            2.24   -1.86E-01                       1.50E+00 443.96            2.83    1.37E-01                       1.16E+00 488.68            0.42    2.08E+00                       6.81E+00 563.99            0.49   -3.36E+00                       6.15E+00 586.26            0.46    1.11E+01                       1.09E+01 678.62            0.47    4.20E+00                       7.78E+00 688.67            0.86    9.20E-01                       4.09E+00 719.35            0.28    1.25E+00                       1.34E+01 778.90           12.96   -1.82E-01                       2.76E-01 810.45            0.32    4.03E+00                       1.28E+01 867.37            4.26   -7.75E-01                       1.13E+00 919.33            0.43   -1.58E+01                       7.98E+00 964.08           14.65    2.05E-01                       3.52E-01 1085.87            10.24   -1.91E-01                       3.22E-01 1089.74             1.73   -8.30E-01                       2.14E+00 1112.07            13.69   -2.34E-01                       2.82E-01 1212.95             1.43   -5.49E+00                       3.49E+00 1249.94             0.19   -4.26E+01                       2.20E+01 1299.14             1.63    1.36E+00                       2.93E+00 1408.01            21.07   -4.12E-03                       1.40E-01 1457.64             0.50    7.18E+01                       2.83E+01 1528.10             0.28    5.73E+00                       1.27E+01 Eu-154       123.07           40.40   -2.36E-02      7.89E-02         7.89E-02 247.93            6.89    1.46E-01                       4.18E-01 591.76            4.95    8.69E-02                       6.55E-01 692.42            1.78    6.29E-01                       2.09E+00 723.30           20.06    3.13E-02                       2.13E-01 756.80            4.52    3.50E-01                       7.23E-01 873.18           12.08   -1.09E-01                       3.46E-01
[336]

8/1/2019   8:46:11AM Page 7 of 7 Analysis Report for     01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.24E-02      7.89E-02         3.22E-01 1004.76                  18.01        8.19E-02                       2.13E-01 1274.43                  34.80        7.63E-02                       1.42E-01 1596.48                   1.80        4.98E-02                       1.94E+00 Eu-155            45.30                  1.31        3.73E+00      1.79E-01         1.60E+01 60.01                  1.22       -2.23E+01                       1.60E+01 86.55                 30.70        5.36E-02                       1.86E-01 105.31                 21.10       -1.28E-01                       1.79E-01
+         Ra-226           186.21
* 3.64        5.30E-01      5.49E-01         5.49E-01 Pa-231            27.36                 10.30        6.74E-01      1.44E+00         1.88E+00 283.69                  1.70        8.45E-01                       1.87E+00 300.07                  2.47       -1.95E+00                       1.44E+00 302.65                  2.20        1.01E+00                       1.53E+00 330.06                  1.40        3.44E-01                       2.39E+00
+         U-235            143.76                 10.96       -4.62E-02      3.50E-02         3.10E-01 163.33                  5.08        9.55E-02                       6.39E-01 185.71
* 57.20        3.37E-02                       3.50E-02 202.11                  1.08       -2.32E-01                       2.93E+00 205.31                  5.01       -1.22E-01                       6.36E-01 Am-241            59.54                 35.90       -3.43E-01      5.90E-01         5.90E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[337]

8/1/2019 9:07:17AM Page 1 of 7 Analysis Report for    01-Aug-19-10010 L1-10221C-FIGS-111SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 01-Aug-19-10010 Sample Description                           : L1-10221C-FIGS-111SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.728E+03 grams Facility                                     : Default Sample Taken On                              : 7/31/2019 9:32:00AM Acquisition Started                          : 8/1/2019 8:51:59AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.02 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 8/1/2019 Efficiency Calibration Description           :
Sample Number                                : 78407 Fill Height                                  : 1728.28 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 8/1/2019 9:07:08AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[338]

8/1/2019   9:07:17AM         Page 2 of 7 Analysis Report for    01-Aug-19-10010 L1-10221C-FIGS-111SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty        Counts          (keV) 1       238.73               950 -    961          955.39          7.68E+01             11.72      2.43E+01           0.40 2       351.62             1401 -   1414         1406.47           5.55E+01             10.31      1.85E+01           0.92 3       583.29             2325 -   2338         2332.48           3.60E+01               7.43     7.00E+00           0.54 4       609.11             2428 -   2443         2435.69           5.51E+01               9.21     9.95E+00           0.42 5       910.96             3636 -   3649         3642.88           2.73E+01               5.66     1.72E+00           0.32 6      1460.66             5832 -   5854         5843.01           1.61E+02             13.40      5.17E+00           2.13 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     0.99          1460.82
* 10.66             3.26E+00             3.07E-01 Tl-208                   0.99           583.19
* 85.00             5.03E-02             1.08E-02 Bi-211                   0.95           351.07
* 13.02             3.61E-01             7.32E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60             1.18E-01             2.04E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49             1.48E-01             2.63E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92                                             [339]

8/1/2019   9:07:17AM         Page 3 of 7 Analysis Report for    01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide               Id                Energy            Yield(%)      Activity           Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   0.99        1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22                 18.42 351.93
* 35.60  1.32E-01             2.67E-02 785.96                  1.06 Ac-228                   0.99         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.68E-01             3.56E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[340]

8/1/2019 9:07:17AM          Page 4 of 7 Analysis Report for   01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.996                     3.26E+00              3.07E-01 Tl-208                              0.998                     5.03E-02              1.08E-02
     ?       Bi-211                              0.953                     3.61E-01              7.32E-02 Pb-212                              0.999                     1.18E-01              2.04E-02 Bi-214                              0.997                     1.48E-01              2.63E-02
     ?       Pb-214                              0.991                     1.32E-01              2.67E-02 Ac-228                              0.997                     1.68E-01              3.56E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[341]

8/1/2019   9:07:17AM       Page 5 of 7 Analysis Report for    01-Aug-19-10010 L1-10221C-FIGS-111SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 8/1/2019 9:07:08AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                           (pCi/grams)        (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        2.86E-02          4.13E-02         4.13E-02 BE-7            477.60              10.44       2.63E-01          3.78E-01         3.78E-01
+         K-40          1460.82
* 10.66       3.26E+00          3.57E-01         3.57E-01 Mn-54           834.85              99.98       2.26E-02          3.73E-02         3.73E-02 Co-60         1173.23               99.85     -1.86E-02           4.21E-02         4.92E-02 1332.49               99.98     -1.27E-02                            4.21E-02 Nb-94           702.65              99.81       1.07E-02          3.73E-02         3.73E-02 871.09              99.89       5.39E-03                           4.35E-02 Ag-108m          79.13                6.60    -3.67E-01           3.42E-02         1.23E+00 433.94              90.50       9.10E-03                           3.42E-02 614.28              89.80     -1.93E-02                            5.96E-02 722.94              90.80     -2.43E-02                            3.49E-02 Sb-125          176.31                6.84      9.75E-02          1.05E-01         4.09E-01 380.45                1.52    -8.56E-01                            1.98E+00 427.87              29.60     -7.04E-02                            1.05E-01 463.36              10.49       1.21E-01                           3.45E-01 600.60              17.65       3.13E-02                           1.67E-01 606.71                4.98      9.33E-01                           1.12E+00 635.95              11.22       6.62E-02                           2.84E-01          [342]

8/1/2019   9:07:17AM Page 6 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79   -5.48E-01      1.05E-01         1.77E+00 Ba-133        79.61            2.65    1.29E+00      5.81E-02         3.04E+00 81.00           32.90   -2.40E-01                       2.08E-01 276.40            7.16    7.80E-02                       4.22E-01 302.85           18.34   -7.20E-03                       1.70E-01 356.01           62.05   -3.42E-02                       5.81E-02 383.85            8.94    1.90E-02                       3.39E-01 Cs-134       475.36            1.48    5.39E-01      3.85E-02         2.49E+00 563.25            8.34   -2.19E-01                       3.67E-01 569.33           15.37    1.20E-01                       2.08E-01 604.72           97.62   -7.61E-03                       5.43E-02 795.86           85.46   -5.50E-04                       3.85E-02 801.95            8.69   -1.39E-01                       4.00E-01 1038.61             0.99   -3.64E+00                       4.05E+00 1167.97             1.79   -4.72E-01                       2.41E+00 1365.19             3.02   -1.20E-01                       9.29E-01 Cs-137       661.66           85.10    3.55E-02      5.03E-02         5.03E-02 Eu-152       121.78           28.67   -6.89E-02      1.09E-01         1.09E-01 244.70            7.61    2.71E-01                       4.28E-01 295.94            0.45    4.81E-02                       8.42E+00 344.28           26.60    5.01E-02                       1.13E-01 367.79            0.86    4.01E-01                       3.45E+00 411.12            2.24    6.22E-01                       1.46E+00 443.96            2.83   -2.15E-01                       1.01E+00 488.68            0.42    8.18E-01                       7.76E+00 563.99            0.49    3.63E+00                       6.58E+00 586.26            0.46    9.42E+00                       9.87E+00 678.62            0.47    4.21E+00                       7.04E+00 688.67            0.86    7.31E-01                       3.40E+00 719.35            0.28   -9.41E+00                       1.13E+01 778.90           12.96   -1.24E-01                       2.91E-01 810.45            0.32   -9.03E-02                       1.09E+01 867.37            4.26   -1.03E-01                       1.02E+00 919.33            0.43   -5.55E+00                       8.00E+00 964.08           14.65    2.67E-01                       3.37E-01 1085.87            10.24    2.58E-02                       4.22E-01 1089.74             1.73    2.37E+00                       2.66E+00 1112.07            13.69    2.21E-01                       3.41E-01 1212.95             1.43    1.96E+00                       3.71E+00 1249.94             0.19   -4.24E+00                       2.27E+01 1299.14             1.63   -1.53E-01                       2.47E+00 1408.01            21.07    1.20E-01                       1.95E-01 1457.64             0.50    7.09E+01                       2.84E+01 1528.10             0.28   -3.37E+00                       7.67E+00 Eu-154       123.07           40.40   -2.48E-02      7.86E-02         7.86E-02 247.93            6.89    1.89E-01                       4.37E-01 591.76            4.95    1.35E-01                       5.49E-01 692.42            1.78   -4.63E-01                       1.82E+00 723.30           20.06   -2.38E-02                       1.62E-01 756.80            4.52   -1.19E-01                       6.86E-01 873.18           12.08   -2.15E-01                       3.55E-01
[343]

8/1/2019   9:07:17AM Page 7 of 7 Analysis Report for     01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -4.26E-02      7.86E-02         3.54E-01 1004.76                  18.01        1.88E-01                       2.28E-01 1274.43                  34.80        3.31E-02                       1.18E-01 1596.48                   1.80        7.72E-01                       1.88E+00 Eu-155            45.30                  1.31       -1.01E+01      1.71E-01         1.52E+01 60.01                  1.22        8.54E-01                       1.73E+01 86.55                 30.70        1.10E-02                       1.88E-01 105.31                 21.10        9.72E-02                       1.71E-01 Ra-226           186.21                  3.64        7.78E-01      9.30E-01         9.30E-01 Pa-231            27.36                 10.30        1.52E+00      1.40E+00         2.02E+00 283.69                  1.70       -4.88E-01                       1.68E+00 300.07                  2.47       -1.61E+00                       1.40E+00 302.65                  2.20        4.05E-01                       1.45E+00 330.06                  1.40        1.34E+00                       2.18E+00 U-235            143.76                 10.96        2.98E-02      5.95E-02         2.84E-01 163.33                  5.08       -2.64E-02                       5.75E-01 185.71                 57.20        7.09E-02                       5.95E-02 202.11                  1.08        6.01E-01                       2.66E+00 205.31                  5.01       -2.58E-01                       5.67E-01 Am-241            59.54                 35.90        1.41E-01      6.16E-01         6.16E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[344]

8/1/2019 9:24:35AM Page 1 of 7 Analysis Report for    01-Aug-19-10011 L1-10221C-FIGS-112SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 01-Aug-19-10011 Sample Description                           : L1-10221C-FIGS-112SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.531E+03 grams Facility                                     : Default Sample Taken On                              : 7/31/2019 9:34:00AM Acquisition Started                          : 8/1/2019 9:09:24AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 8/1/2019 Efficiency Calibration Description           :
Sample Number                                : 78408 Fill Height                                  : 1530.94 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 8/1/2019 9:24:26AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[345]

8/1/2019   9:24:35AM         Page 2 of 7 Analysis Report for    01-Aug-19-10011 L1-10221C-FIGS-112SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty        Counts          (keV) 1       185.92               740 -    748          744.41          2.91E+01               9.18     2.59E+01           1.17 2       238.84               948 -    960          955.82          7.33E+01             13.74      4.37E+01           1.09 3       295.09             1173 -   1185         1180.58           2.79E+01               8.35     1.51E+01           0.58 4       351.87             1399 -   1416         1407.47           6.20E+01               9.56     9.00E+00           1.08 5       583.07             2327 -   2336         2331.58           2.27E+01               6.95     1.13E+01           0.30 6       609.11             2430 -   2444         2435.71           6.10E+01               8.90     5.97E+00           0.61 7      1460.66             5832 -   5853         5843.00           1.64E+02             13.22      2.80E+00           2.03 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     0.99          1460.82
* 10.66             3.44E+00             3.14E-01 Tl-208                   0.99           583.19
* 85.00             3.25E-02             1.01E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60             1.15E-01             2.34E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49             1.68E-01             2.65E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92                                             [346]

8/1/2019   9:24:35AM          Page 3 of 7 Analysis Report for    01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   0.99        1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22
* 18.42       1.16E-01             3.59E-02 351.93
* 35.60       1.51E-01             2.62E-02 785.96                  1.06 Ra-226                   0.98         186.21
* 3.64       4.88E-01             1.59E-01 U-235                    0.99         143.76                 10.96 163.33                  5.08 185.71
* 57.20       3.11E-02             1.01E-02 202.11                  1.08 205.31                  5.01
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean               Wt mean      Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
K-40                              0.996               3.44E+00               3.14E-01 Tl-208                            0.998               3.25E-02               1.01E-02 X       Bi-211                            0.903 Pb-212                            0.994               1.15E-01               2.34E-02      [347]

8/1/2019 9:24:35AM          Page 4 of 7 Analysis Report for   01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
Bi-214                              0.997                     1.68E-01              2.65E-02 Pb-214                              0.999                     1.39E-01              2.12E-02
     ?       Ra-226                              0.987                     4.88E-01              1.59E-01
     ?       U-235                               0.995                     3.11E-02              1.01E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[348]

8/1/2019   9:24:35AM       Page 5 of 7 Analysis Report for    01-Aug-19-10011 L1-10221C-FIGS-112SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 8/1/2019 9:24:26AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                           (pCi/grams)        (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        5.21E-02          4.92E-02         4.92E-02 BE-7            477.60              10.44       1.40E-01          3.55E-01         3.55E-01
+         K-40          1460.82
* 10.66       3.44E+00          2.92E-01         2.92E-01 Mn-54           834.85              99.98       2.63E-02          3.83E-02         3.83E-02 Co-60         1173.23               99.85       1.37E-02          4.84E-02         4.97E-02 1332.49               99.98       3.13E-03                           4.84E-02 Nb-94           702.65              99.81     -5.06E-02           3.95E-02         3.95E-02 871.09              99.89       5.38E-03                           4.09E-02 Ag-108m          79.13                6.60      8.95E-02          3.31E-02         1.29E+00 433.94              90.50       1.26E-02                           3.31E-02 614.28              89.80     -1.19E-02                            6.38E-02 722.94              90.80       1.41E-02                           5.51E-02 Sb-125          176.31                6.84      2.89E-02          9.46E-02         4.40E-01 380.45                1.52      1.41E+00                           1.96E+00 427.87              29.60     -5.41E-02                            9.46E-02 463.36              10.49       2.55E-01                           3.15E-01 600.60              17.65       1.82E-04                           2.02E-01 606.71                4.98      1.91E+00                           1.17E+00 635.95              11.22       3.24E-02                           2.85E-01          [349]

8/1/2019   9:24:35AM Page 6 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79    1.70E-01      9.46E-02         1.55E+00 Ba-133        79.61            2.65    1.71E+00      6.29E-02         3.20E+00 81.00           32.90   -2.43E-01                       2.07E-01 276.40            7.16    1.17E-01                       4.53E-01 302.85           18.34    5.65E-02                       1.48E-01 356.01           62.05    2.01E-02                       6.29E-02 383.85            8.94    8.31E-02                       3.00E-01 Cs-134       475.36            1.48    2.25E+00      4.25E-02         2.42E+00 563.25            8.34    2.07E-01                       4.46E-01 569.33           15.37    7.35E-02                       2.37E-01 604.72           97.62   -3.09E-02                       5.42E-02 795.86           85.46    4.34E-03                       4.25E-02 801.95            8.69   -7.76E-02                       4.10E-01 1038.61             0.99    2.86E+00                       4.73E+00 1167.97             1.79   -5.35E-02                       2.97E+00 1365.19             3.02   -8.18E-01                       1.32E+00 Cs-137       661.66           85.10    8.17E-03      3.94E-02         3.94E-02 Eu-152       121.78           28.67   -2.04E-02      1.04E-01         1.07E-01 244.70            7.61    5.72E-02                       4.67E-01 295.94            0.45    3.00E+00                       7.17E+00 344.28           26.60   -9.43E-03                       1.04E-01 367.79            0.86    1.16E+00                       3.78E+00 411.12            2.24    4.20E-01                       1.50E+00 443.96            2.83   -3.47E-01                       1.04E+00 488.68            0.42   -3.09E+00                       7.94E+00 563.99            0.49    7.20E-01                       7.47E+00 586.26            0.46    7.53E+00                       9.94E+00 678.62            0.47    1.58E+00                       7.08E+00 688.67            0.86    1.89E+00                       3.58E+00 719.35            0.28    1.02E+00                       1.48E+01 778.90           12.96    7.12E-02                       2.88E-01 810.45            0.32    2.00E+00                       1.04E+01 867.37            4.26   -4.43E-01                       9.94E-01 919.33            0.43   -8.67E+00                       9.73E+00 964.08           14.65    2.12E-01                       3.61E-01 1085.87            10.24   -2.20E-02                       4.14E-01 1089.74             1.73    5.03E-01                       2.46E+00 1112.07            13.69   -1.68E-01                       3.30E-01 1212.95             1.43   -3.52E+00                       3.42E+00 1249.94             0.19    6.61E+00                       2.57E+01 1299.14             1.63   -6.48E-01                       2.86E+00 1408.01            21.07   -2.65E-01                       2.08E-01 1457.64             0.50    7.88E+01                       2.96E+01 1528.10             0.28    2.46E+00                       9.15E+00 Eu-154       123.07           40.40    2.38E-02      7.71E-02         7.71E-02 247.93            6.89    6.89E-02                       4.44E-01 591.76            4.95   -4.19E-01                       6.54E-01 692.42            1.78    3.57E-01                       2.02E+00 723.30           20.06   -4.62E-02                       2.47E-01 756.80            4.52    2.63E-01                       7.76E-01 873.18           12.08    7.63E-02                       3.46E-01
[350]

8/1/2019   9:24:35AM Page 7 of 7 Analysis Report for     01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48        1.86E-01      7.71E-02         4.35E-01 1004.76                  18.01       -1.40E-01                       2.24E-01 1274.43                  34.80        4.82E-02                       1.25E-01 1596.48                   1.80       -2.27E+00                       2.18E+00 Eu-155            45.30                  1.31        4.53E+00      1.83E-01         1.64E+01 60.01                  1.22       -3.84E+00                       1.71E+01 86.55                 30.70       -1.12E-02                       1.89E-01 105.31                 21.10        3.61E-02                       1.83E-01
+         Ra-226           186.21
* 3.64        4.88E-01      4.71E-01         4.71E-01 Pa-231            27.36                 10.30        2.63E+00      1.11E+00         2.15E+00 283.69                  1.70       -1.43E-01                       1.75E+00 300.07                  2.47       -9.34E-01                       1.11E+00 302.65                  2.20        3.90E-01                       1.26E+00 330.06                  1.40       -1.38E-01                       2.26E+00
+         U-235            143.76                 10.96        5.32E-02      3.00E-02         2.90E-01 163.33                  5.08       -3.01E-01                       5.60E-01 185.71
* 57.20        3.11E-02                       3.00E-02 202.11                  1.08        8.96E-01                       2.87E+00 205.31                  5.01       -4.98E-02                       6.04E-01 Am-241            59.54                 35.90       -1.46E-01      6.10E-01         6.10E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[351]

8/1/2019 9:41:10AM Page 1 of 7 Analysis Report for    01-Aug-19-10012 L1-10221C-FIGS-113SS GAMMA SPECTRUM ANALYSIS Sample Identification                        : 01-Aug-19-10012 Sample Description                           : L1-10221C-FIGS-113SS Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.769E+03 grams Facility                                     : Default Sample Taken On                              : 7/31/2019 9:36:00AM Acquisition Started                          : 8/1/2019 9:25:58AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.2 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 8/1/2019 Efficiency Calibration Description           :
Sample Number                                : 78409 Fill Height                                  : 1768.92 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 8/1/2019 9:41:01AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[352]

8/1/2019   9:41:10AM         Page 2 of 7 Analysis Report for    01-Aug-19-10012 L1-10221C-FIGS-113SS Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area     Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty        Counts          (keV) 1       238.57               948 -    962          954.76          1.06E+02             14.59      3.72E+01           1.29 2       351.74             1401 -   1414         1406.95           6.01E+01             10.32      1.69E+01           0.93 3       609.28             2429 -   2445         2436.37           6.19E+01               8.98     6.07E+00           0.68 4       911.30             3639 -   3650         3644.26           2.16E+01               5.71     4.38E+00           0.70 5      1460.80             5833 -   5853         5843.56           1.69E+02             14.05      7.84E+00           1.10 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity            Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty K-40                     1.00          1460.82
* 10.66             3.42E+00             3.20E-01 Bi-211                   0.93           351.07
* 13.02             3.91E-01             7.40E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60             1.62E-01             2.59E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49             1.66E-01             2.60E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83                                            [353]

8/1/2019   9:41:10AM          Page 3 of 7 Analysis Report for    01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide               Id                Energy            Yield(%)           Activity            Activity Name             Confidence               (keV)                         (pCi/grams)          Uncertainty Bi-214                   1.00        1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99         241.99                  7.25 295.22                 18.42 351.93
* 35.60       1.43E-01             2.70E-02 785.96                  1.06 Ac-228                   1.00         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32                 11.27 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80       1.32E-01             3.54E-02 964.77                  4.99 968.97                 15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                           Nuclide                Wt mean               Wt mean      Comments Name                                Id                    Activity               Activity Confidence                                     Uncertainty (pCi/grams)
[354]

8/1/2019 9:41:10AM          Page 4 of 7 Analysis Report for   01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide                            Nuclide                       Wt mean             Wt mean      Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                1.000                     3.42E+00              3.20E-01
     ?       Bi-211                              0.931                     3.91E-01              7.40E-02 Pb-212                              0.999                     1.62E-01              2.59E-02 Bi-214                              1.000                     1.66E-01              2.60E-02
     ?       Pb-214                              0.997                     1.43E-01              2.70E-02 Ac-228                              1.000                     1.32E-01              3.54E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[355]

8/1/2019   9:41:10AM       Page 5 of 7 Analysis Report for    01-Aug-19-10012 L1-10221C-FIGS-113SS UNIDENTIFIED PEAKS Peak Locate Performed on        : 8/1/2019 9:41:01AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                           (pCi/grams)        (pCi/grams)    (pCi/grams)
(keV)
An Pk           511.00            100.00        3.69E-02          5.03E-02         5.03E-02 BE-7            477.60              10.44     -2.55E-02           3.30E-01         3.30E-01
+         K-40          1460.82
* 10.66       3.42E+00          4.23E-01         4.23E-01 Mn-54           834.85              99.98       3.09E-02          4.08E-02         4.08E-02 Co-60         1173.23               99.85       2.35E-02          4.19E-02         4.52E-02 1332.49               99.98       2.82E-02                           4.19E-02 Nb-94           702.65              99.81     -1.55E-02           3.39E-02         3.39E-02 871.09              99.89       2.26E-02                           3.81E-02 Ag-108m          79.13                6.60    -1.63E-01           3.32E-02         1.25E+00 433.94              90.50     -5.38E-03                            3.32E-02 614.28              89.80     -8.00E-04                            6.09E-02 722.94              90.80       9.90E-03                           4.68E-02 Sb-125          176.31                6.84    -3.17E-01           1.03E-01         3.98E-01 380.45                1.52    -8.45E-01                            2.19E+00 427.87              29.60       6.93E-03                           1.03E-01 463.36              10.49     -1.18E-01                            2.83E-01 600.60              17.65     -4.41E-04                            2.02E-01 606.71                4.98      1.86E+00                           1.19E+00 635.95              11.22       1.67E-02                           2.94E-01          [356]

8/1/2019   9:41:10AM Page 6 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.35E+00      1.03E-01         1.80E+00 Ba-133        79.61            2.65    4.89E-01      6.51E-02         3.00E+00 81.00           32.90   -2.32E-01                       2.02E-01 276.40            7.16    1.11E-01                       4.51E-01 302.85           18.34    9.74E-02                       1.71E-01 356.01           62.05   -2.54E-02                       6.51E-02 383.85            8.94   -1.48E-01                       3.70E-01 Cs-134       475.36            1.48    6.58E-01      4.38E-02         2.25E+00 563.25            8.34   -7.98E-02                       3.73E-01 569.33           15.37    7.73E-02                       2.07E-01 604.72           97.62   -2.39E-02                       5.51E-02 795.86           85.46   -8.46E-04                       4.38E-02 801.95            8.69   -2.72E-01                       3.98E-01 1038.61             0.99   -1.50E+00                       3.94E+00 1167.97             1.79    3.32E-01                       2.34E+00 1365.19             3.02    2.79E-01                       1.32E+00 Cs-137       661.66           85.10   -9.24E-03      3.83E-02         3.83E-02 Eu-152       121.78           28.67   -6.21E-02      1.12E-01         1.19E-01 244.70            7.61   -4.01E-02                       4.04E-01 295.94            0.45    1.74E+00                       8.27E+00 344.28           26.60   -6.17E-02                       1.12E-01 367.79            0.86    4.89E-01                       3.32E+00 411.12            2.24   -2.34E-01                       1.28E+00 443.96            2.83   -1.49E-01                       1.02E+00 488.68            0.42    6.74E-01                       7.08E+00 563.99            0.49    2.46E+00                       6.44E+00 586.26            0.46    7.25E+00                       1.00E+01 678.62            0.47    3.19E+00                       7.81E+00 688.67            0.86    1.29E-01                       4.33E+00 719.35            0.28    2.70E+00                       1.48E+01 778.90           12.96   -3.65E-01                       2.79E-01 810.45            0.32    5.37E+00                       1.22E+01 867.37            4.26   -1.78E+00                       8.53E-01 919.33            0.43   -1.17E+01                       9.23E+00 964.08           14.65    1.77E-01                       3.40E-01 1085.87            10.24    5.66E-02                       3.81E-01 1089.74             1.73    6.94E-01                       2.49E+00 1112.07            13.69    5.20E-02                       3.32E-01 1212.95             1.43    1.66E-01                       3.87E+00 1249.94             0.19    9.29E+00                       2.65E+01 1299.14             1.63   -4.34E-01                       2.46E+00 1408.01            21.07    9.95E-02                       1.79E-01 1457.64             0.50    7.90E+01                       2.94E+01 1528.10             0.28   -7.76E+00                       1.69E+01 Eu-154       123.07           40.40    1.75E-02      8.74E-02         8.74E-02 247.93            6.89   -6.45E-02                       4.21E-01 591.76            4.95    3.18E-02                       6.59E-01 692.42            1.78    1.12E+00                       2.07E+00 723.30           20.06    8.47E-02                       2.12E-01 756.80            4.52    2.80E-01                       7.86E-01 873.18           12.08    1.78E-01                       3.22E-01
[357]

8/1/2019   9:41:10AM Page 7 of 7 Analysis Report for     01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -1.15E-01      8.74E-02         3.97E-01 1004.76                  18.01       -3.23E-02                       2.06E-01 1274.43                  34.80       -3.65E-02                       1.40E-01 1596.48                   1.80       -1.75E+00                       1.99E+00 Eu-155            45.30                  1.31       -4.42E+00      1.81E-01         1.64E+01 60.01                  1.22        2.93E+00                       2.08E+01 86.55                 30.70        5.57E-02                       1.90E-01 105.31                 21.10       -4.69E-02                       1.81E-01 Ra-226           186.21                  3.64        4.79E-01      9.38E-01         9.38E-01 Pa-231            27.36                 10.30        8.39E-01      1.43E+00         1.75E+00 283.69                  1.70        2.72E-01                       1.79E+00 300.07                  2.47       -1.10E+00                       1.45E+00 302.65                  2.20        3.87E-01                       1.43E+00 330.06                  1.40       -9.08E-01                       2.02E+00 U-235            143.76                 10.96       -5.42E-02      6.01E-02         2.82E-01 163.33                  5.08        2.21E-02                       5.80E-01 185.71                 57.20       -2.04E-03                       6.01E-02 202.11                  1.08        1.28E+00                       2.84E+00 205.31                  5.01       -3.22E-01                       5.79E-01 Am-241            59.54                 35.90       -6.27E-02      7.11E-01         7.11E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[358]

7/31/2019 10:38:10AM Page 1 of 7 Analysis Report for    31-Jul-19-10018 L1-10221C-FSGS-005SB GAMMA SPECTRUM ANALYSIS Sample Identification                        : 31-Jul-19-10018 Sample Description                           : L1-10221C-FSGS-005SB Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.519E+03 grams Facility                                     : Default Sample Taken On                              : 7/30/2019 3:09:00PM Acquisition Started                          : 7/31/2019 10:22:58AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P40818B Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 901.1 seconds Dead Time                                    : 0.12 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/29/2019 Efficiency Calibration Used Done On          : 7/31/2019 Efficiency Calibration Description           :
Sample Number                                : 78348 Fill Height                                  : 1519.21 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/31/2019 10:38:03AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[359]

7/31/2019   10:38:10AM         Page 2 of 7 Analysis Report for    31-Jul-19-10018 L1-10221C-FSGS-005SB Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.64               948 -    962          954.65          9.22E+01               17.17      6.98E+01           0.78 2       338.10             1348 -   1356         1352.17           2.68E+01                7.27      1.22E+01           0.88 3       351.96             1401 -   1415         1407.57           6.52E+01               12.46      3.08E+01           0.98 4       583.14             2325 -   2338         2331.76           3.17E+01                7.81      1.03E+01           0.37 5       609.26             2431 -   2443         2436.19           4.47E+01                8.19      8.26E+00           0.52 6       911.10             3638 -   3649         3643.35           3.06E+01                5.83      1.38E+00           0.70 7      1460.54             5831 -   5852         5841.98           2.11E+02               14.87      2.66E+00           1.97 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.98          1460.82
* 10.66              5.28E+00              4.36E-01 Tl-208                   1.00           583.19
* 85.00              5.31E-02              1.34E-02 Bi-211                   0.88           351.07
* 13.02              5.00E-01              1.04E-01 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              1.65E-01              3.35E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.44E-01              2.77E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11                                              [360]

7/31/2019   10:38:10AM        Page 3 of 7 Analysis Report for    31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00        1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00          241.99                 7.25 295.22                18.42 351.93
* 35.60  1.83E-01              3.79E-02 785.96                 1.06 Ac-228                   0.99          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32
* 11.27  2.30E-01              6.53E-02 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20
* 25.80  2.29E-01              4.46E-02 964.77                 4.99 968.97                15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[361]

7/31/2019 10:38:10AM         Page 4 of 7 Analysis Report for   31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.987                     5.28E+00              4.36E-01 Tl-208                              1.000                     5.31E-02              1.34E-02
     ?       Bi-211                              0.881                     5.00E-01              1.04E-01 Pb-212                              1.000                     1.65E-01              3.35E-02 Bi-214                              1.000                     1.44E-01              2.77E-02
     ?       Pb-214                              1.000                     1.83E-01              3.79E-02 Ac-228                              0.998                     2.29E-01              3.68E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[362]

7/31/2019  10:38:10AM       Page 5 of 7 Analysis Report for    31-Jul-19-10018 L1-10221C-FSGS-005SB UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/31/2019 10:38:03AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        9.47E-02          6.03E-02        6.03E-02 BE-7            477.60              10.44       1.36E-01          4.24E-01        4.24E-01
+         K-40          1460.82
* 10.66       5.28E+00          3.37E-01        3.37E-01 Mn-54           834.85              99.98     -2.22E-02           4.88E-02        4.88E-02 Co-60         1173.23               99.85       5.21E-02          5.77E-02        7.14E-02 1332.49               99.98       2.17E-02                          5.77E-02 Nb-94           702.65              99.81     -9.30E-03           3.89E-02        4.34E-02 871.09              99.89     -1.05E-02                           3.89E-02 Ag-108m          79.13                6.60      3.45E-01          4.44E-02        1.71E+00 433.94              90.50     -1.09E-02                           4.44E-02 614.28              89.80     -2.72E-02                           5.57E-02 722.94              90.80       2.90E-02                          5.28E-02 Sb-125          176.31                6.84      2.14E-01          1.45E-01        5.13E-01 380.45                1.52      1.27E-01                          2.29E+00 427.87              29.60       3.25E-02                          1.45E-01 463.36              10.49       2.48E-01                          4.37E-01 600.60              17.65       6.18E-02                          2.21E-01 606.71                4.98      1.71E+00                          1.24E+00 635.95              11.22       9.30E-02                          3.34E-01          [363]

7/31/2019  10:38:10AM Page 6 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79    5.85E-01      1.45E-01        2.22E+00 Ba-133        79.61            2.65    2.12E+00      7.16E-02        4.19E+00 81.00           32.90   -1.17E-01                      2.86E-01 276.40            7.16    8.88E-02                      4.96E-01 302.85           18.34   -1.73E-02                      1.95E-01 356.01           62.05   -1.23E-02                      7.16E-02 383.85            8.94    2.91E-01                      4.17E-01 Cs-134       475.36            1.48    1.43E+00      5.74E-02        2.99E+00 563.25            8.34   -5.49E-02                      4.47E-01 569.33           15.37   -3.41E-02                      2.40E-01 604.72           97.62   -2.29E-02                      5.74E-02 795.86           85.46    2.71E-03                      5.81E-02 801.95            8.69    1.70E-01                      5.36E-01 1038.61             0.99   -1.09E-01                      4.94E+00 1167.97             1.79   -2.17E-01                      3.59E+00 1365.19             3.02   -4.19E-02                      1.63E+00 Cs-137       661.66           85.10    2.73E-03      4.53E-02        4.53E-02 Eu-152       121.78           28.67   -9.45E-02      1.27E-01        1.44E-01 244.70            7.61   -1.81E-01                      5.09E-01 295.94            0.45    5.97E+00                      9.94E+00 344.28           26.60    3.21E-02                      1.27E-01 367.79            0.86    5.94E-01                      3.97E+00 411.12            2.24    1.44E+00                      1.67E+00 443.96            2.83   -5.55E-01                      1.14E+00 488.68            0.42   -6.34E+00                      7.75E+00 563.99            0.49   -4.94E+00                      7.60E+00 586.26            0.46   -2.87E+00                      1.20E+01 678.62            0.47    8.35E-01                      8.48E+00 688.67            0.86   -5.69E-01                      4.61E+00 719.35            0.28   -4.88E+00                      1.40E+01 778.90           12.96    9.02E-02                      3.39E-01 810.45            0.32   -7.61E+00                      1.25E+01 867.37            4.26   -1.53E+00                      7.88E-01 919.33            0.43    6.79E+00                      9.72E+00 964.08           14.65    1.74E-01                      3.60E-01 1085.87            10.24    4.00E-01                      5.58E-01 1089.74             1.73    1.79E+00                      3.43E+00 1112.07            13.69   -3.12E-02                      3.64E-01 1212.95             1.43   -2.83E-01                      4.39E+00 1249.94             0.19   -1.26E+01                      3.13E+01 1299.14             1.63    6.61E-01                      3.65E+00 1408.01            21.07    1.80E-02                      2.48E-01 1457.64             0.50    1.11E+02                      3.90E+01 1528.10             0.28   -2.08E+00                      1.43E+01 Eu-154       123.07           40.40   -1.83E-02      1.06E-01        1.06E-01 247.93            6.89   -1.94E-01                      5.12E-01 591.76            4.95    6.74E-01                      8.83E-01 692.42            1.78   -7.78E-01                      2.19E+00 723.30           20.06    7.79E-02                      2.39E-01 756.80            4.52   -9.18E-02                      9.71E-01 873.18           12.08    9.47E-02                      3.76E-01
[364]

7/31/2019  10:38:10AM Page 7 of 7 Analysis Report for     31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -7.57E-02      1.06E-01        3.81E-01 1004.76                  18.01       -1.01E-01                      1.67E-01 1274.43                  34.80       -4.53E-02                      1.44E-01 1596.48                   1.80       -2.74E-01                      2.74E+00 Eu-155            45.30                  1.31       -1.18E+01      2.33E-01        2.74E+01 60.01                  1.22       -8.08E+00                      3.11E+01 86.55                 30.70        1.95E-01                      2.54E-01 105.31                 21.10       -1.24E-01                      2.33E-01 Ra-226           186.21                  3.64        6.48E-01      1.12E+00        1.12E+00 Pa-231            27.36                 10.30        2.41E+00      1.48E+00        3.45E+00 283.69                  1.70        1.69E-01                      2.12E+00 300.07                  2.47       -1.62E-01                      1.48E+00 302.65                  2.20        8.23E-02                      1.65E+00 330.06                  1.40        8.25E-01                      2.62E+00 U-235            143.76                 10.96        5.26E-03      6.82E-02        3.68E-01 163.33                  5.08       -2.53E-01                      6.96E-01 185.71                 57.20       -1.03E-02                      6.82E-02 202.11                  1.08       -8.00E-01                      3.34E+00 205.31                  5.01       -3.43E-01                      6.81E-01 Am-241            59.54                 35.90       -4.79E-01      1.11E+00        1.11E+00
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[365]

8/1/2019 12:38:31PM Page 1 of 7 Analysis Report for    01-Aug-19-10033 L1-10221C-FSGS-005SB GAMMA SPECTRUM ANALYSIS Sample Identification                        : 01-Aug-19-10033 Sample Description                           : L1-10221C-FSGS-005SB Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.519E+03 grams Facility                                     : Default Sample Taken On                              : 7/30/2019 1:09:00PM Acquisition Started                          : 8/1/2019 12:08:17PM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 1800.0 seconds Real Time                                    : 1800.6 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 8/1/2019 Efficiency Calibration Description           :
Sample Number                                : 78430 Fill Height                                  : 1519.21 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 8/1/2019 12:38:21PM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[366]

8/1/2019   12:38:31PM         Page 2 of 7 Analysis Report for    01-Aug-19-10033 L1-10221C-FSGS-005SB Peak          Energy            ROI       ROI              Peak          Net Peak         Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area     Uncertainty         Counts          (keV) 1       185.76               367 -    376          371.84          8.64E+01              22.34      1.81E+02           0.84 2       238.62               473 -    481          477.42          2.37E+02              26.68      2.15E+02           1.04 3       295.27               585 -    595          590.59          7.84E+01              19.62      1.25E+02           1.32 4       338.25               671 -    681          676.47          1.01E+02              16.44      7.13E+01           1.43 5       351.92               698 -    707          703.77          1.88E+02              18.82      7.36E+01           1.19 6       511.03             1016 -   1027         1021.75           1.22E+02              14.74      3.83E+01           1.65 7       583.20             1162 -   1170         1166.00           7.68E+01              12.60      3.83E+01           1.40 8       609.27             1213 -   1223         1218.13           9.75E+01              14.35      4.55E+01           1.53 9       911.25             1817 -   1827         1821.96           5.90E+01              10.91      2.50E+01           1.36 10        969.02             1933 -   1944         1937.49           4.36E+01              10.37      2.34E+01           1.45 11       1460.67             2913 -   2928         2921.40           5.60E+02              23.92      4.00E+00           2.04 12       1764.04             3525 -   3532         3528.92           1.91E+01               5.38      4.94E+00           0.73 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                  Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)          Uncertainty An Pk                    1.00           511.00
* 100.00              6.29E-02              8.74E-03 K-40                     0.99          1460.82
* 10.66             5.27E+00              3.21E-01 Tl-208                   1.00           583.19
* 85.00             4.96E-02              8.66E-03 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60             1.66E-01              2.31E-02[367]

8/1/2019   12:38:31PM        Page 3 of 7 Analysis Report for    01-Aug-19-10033 L1-10221C-FSGS-005SB Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Pb-212                   1.00         300.09                  3.30 Bi-214                   0.99         609.32
* 45.49  1.21E-01              1.92E-02 768.36                  4.89 806.18                  1.26 934.06                  3.11 1120.29                 14.92 1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49
* 15.30  1.44E-01              4.11E-02 1847.43                  2.03 2118.51                  1.16 Pb-214                   1.00         241.99                  7.25 295.22
* 18.42  1.47E-01              3.86E-02 351.93
* 35.60  2.07E-01              2.65E-02 785.96                  1.06 Ra-226                   0.96         186.21
* 3.64  6.45E-01              1.75E-01 Ac-228                   1.00         129.07                  2.42 209.25                  3.89 270.24                  3.46 328.00                  2.95 338.32
* 11.27  3.39E-01              6.20E-02 409.46                  1.92 463.00                  4.40 794.95                  4.25 911.20
* 25.80  1.68E-01              3.19E-02 964.77                  4.99 968.97
* 15.80  2.11E-01              5.11E-02 1588.20                  3.22 U-235                    1.00         143.76                 10.96 163.33                  5.08 185.71
* 57.20  4.10E-02              1.11E-02 202.11                  1.08 205.31                  5.01
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
[368]

8/1/2019 12:38:31PM         Page 4 of 7 Analysis Report for   01-Aug-19-10033 L1-10221C-FSGS-005SB INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
An Pk                               1.000                     6.29E-02              8.74E-03 K-40                                0.996                     5.27E+00              3.21E-01 Tl-208                              1.000                     4.96E-02              8.66E-03 X       Bi-211                              0.892 Pb-212                              1.000                     1.66E-01              2.31E-02 Bi-214                              0.995                     1.25E-01              1.74E-02 Pb-214                              1.000                     1.88E-01              2.18E-02
     ?       Ra-226                              0.969                     6.45E-01              1.75E-01 Ac-228                              1.000                     2.06E-01              2.48E-02
     ?       U-235                               1.000                     4.10E-02              1.11E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[369]

8/1/2019  12:38:31PM       Page 5 of 7 Analysis Report for    01-Aug-19-10033 L1-10221C-FSGS-005SB UNIDENTIFIED PEAKS Peak Locate Performed on        : 8/1/2019 12:38:21PM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)          Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty          Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA        Line MDA Name                                            (pCi/grams)       (pCi/grams)    (pCi/grams)
(keV)
+         An Pk           511.00
* 100.00        6.29E-02          1.86E-02         1.86E-02 BE-7            477.60              10.44       5.12E-02          2.22E-01         2.22E-01
+         K-40          1460.82
* 10.66       5.27E+00          1.38E-01         1.38E-01 Mn-54           834.85              99.98     -7.32E-03           2.54E-02         2.54E-02 Co-60         1173.23               99.85       1.25E-02          2.48E-02         3.52E-02 1332.49               99.98     -9.72E-03                            2.48E-02 Nb-94           702.65              99.81     -3.30E-03           2.33E-02         2.33E-02 871.09              99.89       2.65E-04                           2.40E-02 Ag-108m          79.13                6.60      4.15E-01          2.35E-02         7.46E-01 433.94              90.50       6.66E-03                           2.35E-02 614.28              89.80     -2.12E-03                            3.45E-02 722.94              90.80       1.11E-02                           2.89E-02 Sb-125          176.31                6.84      7.78E-02          6.63E-02         3.21E-01 380.45                1.52    -2.21E-01                            1.32E+00 427.87              29.60     -8.62E-03                            6.63E-02 463.36              10.49       1.29E-01                           2.22E-01 600.60              17.65       2.35E-02                           1.34E-01 606.71                4.98      4.28E-02                           7.49E-01 635.95              11.22     -1.20E-01                            2.20E-01          [370]

8/1/2019  12:38:31PM Page 6 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB Nuclide        Energy        Yield(%)      Activity Nuclide MDA       Line MDA Name                                   (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.16E-01      6.63E-02         1.24E+00 Ba-133        79.61            2.65    5.62E-01      4.69E-02         1.75E+00 81.00           32.90   -1.46E-01                       1.17E-01 276.40            7.16   -2.03E-02                       2.92E-01 302.85           18.34    6.83E-02                       1.17E-01 356.01           62.05   -7.66E-02                       4.69E-02 383.85            8.94   -1.35E-02                       2.21E-01 Cs-134       475.36            1.48   -8.44E-02      3.01E-02         1.49E+00 563.25            8.34   -2.17E-01                       2.31E-01 569.33           15.37    2.32E-02                       1.45E-01 604.72           97.62   -3.68E-03                       3.28E-02 795.86           85.46    3.85E-03                       3.01E-02 801.95            8.69   -5.12E-02                       2.76E-01 1038.61             0.99   -2.09E+00                       2.63E+00 1167.97             1.79    1.08E+00                       2.05E+00 1365.19             3.02   -4.07E-02                       6.80E-01 Cs-137       661.66           85.10    4.63E-03      2.91E-02         2.91E-02 Eu-152       121.78           28.67    1.27E-02      7.48E-02         7.48E-02 244.70            7.61    2.32E-02                       3.15E-01 295.94            0.45   -7.37E-01                       5.77E+00 344.28           26.60   -3.10E-02                       7.73E-02 367.79            0.86    3.86E-01                       2.27E+00 411.12            2.24    4.72E-01                       9.56E-01 443.96            2.83   -1.37E-01                       7.50E-01 488.68            0.42    9.72E-01                       5.33E+00 563.99            0.49   -3.59E+00                       3.87E+00 586.26            0.46   -3.90E+00                       7.36E+00 678.62            0.47   -1.87E+00                       4.27E+00 688.67            0.86   -6.94E-01                       3.02E+00 719.35            0.28   -3.50E+00                       8.23E+00 778.90           12.96   -6.63E-03                       1.87E-01 810.45            0.32   -3.64E+00                       6.88E+00 867.37            4.26   -7.61E-01                       5.22E-01 919.33            0.43    6.57E-02                       6.36E+00 964.08           14.65   -7.33E-02                       2.45E-01 1085.87            10.24   -7.84E-02                       2.73E-01 1089.74             1.73   -4.58E-01                       1.74E+00 1112.07            13.69    8.96E-02                       2.61E-01 1212.95             1.43   -1.03E+00                       2.21E+00 1249.94             0.19   -4.47E+00                       1.55E+01 1299.14             1.63   -1.08E+00                       1.75E+00 1408.01            21.07   -3.44E-02                       1.29E-01 1457.64             0.50   -4.39E-01                       2.34E+01 1528.10             0.28    3.96E+00                       8.34E+00 Eu-154       123.07           40.40    1.27E-02      5.30E-02         5.30E-02 247.93            6.89   -5.63E-02                       2.99E-01 591.76            4.95   -4.92E-02                       4.55E-01 692.42            1.78   -4.67E-01                       1.45E+00 723.30           20.06    5.22E-02                       1.32E-01 756.80            4.52    2.09E-02                       5.54E-01 873.18           12.08    1.54E-01                       2.07E-01
[371]

8/1/2019  12:38:31PM Page 7 of 7 Analysis Report for     01-Aug-19-10033 L1-10221C-FSGS-005SB Nuclide            Energy             Yield(%)           Activity Nuclide MDA       Line MDA Name                                                 (pCi/grams)   (pCi/grams)    (pCi/grams)
(keV)
Eu-154           996.29                 10.48        9.85E-02      5.30E-02         2.66E-01 1004.76                  18.01        6.77E-02                       1.56E-01 1274.43                  34.80       -2.02E-02                       8.60E-02 1596.48                   1.80       -1.28E+00                       1.32E+00 Eu-155            45.30                  1.31       -6.60E-02      1.11E-01         6.95E+00 60.01                  1.22        1.46E+00                       8.19E+00 86.55                 30.70        2.98E-02                       1.11E-01 105.31                 21.10       -1.42E-02                       1.15E-01
+         Ra-226           186.21
* 3.64        6.45E-01      5.35E-01         5.35E-01 Pa-231            27.36                 10.30        3.42E-01      6.83E-01         6.83E-01 283.69                  1.70       -8.58E-01                       1.08E+00 300.07                  2.47        2.70E-01                       8.74E-01 302.65                  2.20        5.69E-01                       9.78E-01 330.06                  1.40        1.18E+00                       1.64E+00
+         U-235            143.76                 10.96        5.13E-02      3.41E-02         1.86E-01 163.33                  5.08        2.47E-01                       4.56E-01 185.71
* 57.20        4.10E-02                       3.41E-02 202.11                  1.08       -1.49E-02                       2.08E+00 205.31                  5.01       -1.44E-01                       4.59E-01 Am-241            59.54                 35.90        3.26E-03      2.83E-01         2.83E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[372]

7/31/2019 10:19:05AM Page 1 of 7 Analysis Report for    31-Jul-19-10016 L1-10221C-FSGS-013SB GAMMA SPECTRUM ANALYSIS Sample Identification                        : 31-Jul-19-10016 Sample Description                           : L1-10221C-FSGS-013SB Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.409E+03 grams Facility                                     : Default Sample Taken On                              : 7/29/2019 3:20:00PM Acquisition Started                          : 7/31/2019 10:03:51AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 352 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 7/31/2019 Efficiency Calibration Description           :
Sample Number                                : 78346 Fill Height                                  : 1408.64 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/31/2019 10:18:53AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[373]

7/31/2019   10:19:05AM         Page 2 of 7 Analysis Report for    31-Jul-19-10016 L1-10221C-FSGS-013SB Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1         77.33              305 -    315          310.65          2.50E+01               15.23      8.20E+01           0.57 2       185.82               739 -    751          743.99          5.41E+01               16.29      7.99E+01           1.26 3       238.71               946 -    962          955.32          1.79E+02               22.29      1.02E+02           1.05 4       295.22             1176 -   1190         1181.09           9.12E+01               14.47      3.98E+01           1.14 5       338.22             1348 -   1358         1352.92           3.62E+01               11.38      3.88E+01           1.21 6       351.90             1401 -   1414         1407.61           1.02E+02               15.20      4.68E+01           0.97 7       583.20             2325 -   2339         2332.12           7.08E+01               11.34      2.02E+01           0.61 8       609.43             2429 -   2446         2436.99           1.10E+02               13.08      1.91E+01           1.34 9       661.55             2638 -   2654         2645.39           9.42E+01               12.61      1.98E+01           1.11 10        911.42             3639 -   3653         3644.72           4.02E+01                9.30      1.58E+01           0.75 11       1460.68             5830 -   5856         5843.09           4.67E+02               21.61      0.00E+00           2.10 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              1.00E+01              6.36E-01 Cs-137                   0.99           661.66
* 85.10              1.49E-01              2.19E-02 Tl-208                   1.00           583.19
* 85.00              1.03E-01              1.77E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              2.85E-01              4.23E-02 300.09                    3.30                                              [374]

7/31/2019   10:19:05AM        Page 3 of 7 Analysis Report for  31-Jul-19-10016 L1-10221C-FSGS-013SB Nuclide             Id                Energy   Yield(%)      Activity            Activity Name             Confidence            (keV)            (pCi/grams)          Uncertainty Pb212-XR               0.99           74.82       10.28 77.11
* 17.10  2.33E-01              1.44E-01 87.35        3.97 89.78        1.46 Bi-214                 0.99          609.32
* 45.49  3.08E-01              4.11E-02 768.36        4.89 806.18        1.26 934.06        3.11 1120.29        14.92 1155.21         1.63 1238.12         5.83 1280.98         1.43 1377.67         3.99 1385.31         0.79 1401.52         1.33 1407.99         2.39 1509.21         2.13 1661.27         1.05 1729.59         2.88 1764.49        15.30 1847.43         2.03 2118.51         1.16 Pb-214                 1.00          241.99        7.25 295.22
* 18.42  3.86E-01              6.86E-02 351.93
* 35.60  2.53E-01              4.27E-02 785.96        1.06 Pb214-XR               0.99           74.82        5.80 77.11
* 9.70  4.11E-01              2.54E-01 87.35        2.24 89.78        0.82 Ra-226                 0.97          186.21
* 3.64  9.22E-01              2.87E-01 Ac-228                 0.99          129.07        2.42 209.25        3.89 270.24        3.46 328.00        2.95 338.32
* 11.27  2.75E-01              8.94E-02 409.46        1.92 463.00        4.40 794.95        4.25 911.20
* 25.80  2.60E-01              6.11E-02 964.77        4.99 968.97       15.80 1588.20         3.22 U-235                  0.99          143.76       10.96 163.33        5.08 185.71
* 57.20  5.87E-02              1.83E-02 202.11        1.08 205.31        5.01
[375]

7/31/2019 10:19:05AM         Page 4 of 7 Analysis Report for    31-Jul-19-10016 L1-10221C-FSGS-013SB
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.997                     1.00E+01              6.36E-01 Cs-137                              0.998                     1.49E-01              2.19E-02 Tl-208                              1.000                     1.03E-01              1.77E-02 X       Bi-211                              0.894 Pb-212                              0.999                     2.85E-01              4.23E-02
      ?       Pb212-XR                            0.996                     2.33E-01              1.44E-01 Bi-214                              0.999                     3.08E-01              4.11E-02 Pb-214                              1.000                     2.90E-01              3.63E-02
      ?       Pb214-XR                            0.996                     4.11E-01              2.54E-01
      ?       Ra-226                              0.975                     9.22E-01              2.87E-01 Ac-228                              0.998                     2.65E-01              5.05E-02
      ?       U-235                               0.999                     5.87E-02              1.83E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[376]

7/31/2019  10:19:05AM       Page 5 of 7 Analysis Report for    31-Jul-19-10016 L1-10221C-FSGS-013SB UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/31/2019 10:18:53AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        8.77E-02          6.49E-02        6.49E-02 BE-7            477.60              10.44       3.99E-01          4.67E-01        4.67E-01
+         K-40          1460.82
* 10.66       1.00E+01          6.17E-02        6.17E-02 Mn-54           834.85              99.98       1.72E-02          4.93E-02        4.93E-02 Co-60         1173.23               99.85       6.59E-02          6.59E-02        7.94E-02 1332.49               99.98       2.82E-02                          6.59E-02 Nb-94           702.65              99.81     -1.36E-02           4.56E-02        4.56E-02 871.09              99.89     -3.38E-03                           4.99E-02 Ag-108m          79.13                6.60    -4.51E-01           4.77E-02        1.49E+00 433.94              90.50     -4.83E-03                           4.77E-02 614.28              89.80       2.74E-03                          8.64E-02 722.94              90.80       4.72E-02                          5.85E-02 Sb-125          176.31                6.84    -3.00E-01           1.55E-01        5.49E-01 380.45                1.52    -3.69E-01                           2.86E+00 427.87              29.60       8.69E-02                          1.55E-01 463.36              10.49     -2.08E-01                           4.16E-01 600.60              17.65       4.00E-02                          2.69E-01 606.71                4.98      3.46E+00                          1.65E+00 635.95              11.22     -8.28E-02                           4.19E-01          [377]

7/31/2019  10:19:05AM Page 6 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -4.41E-02      1.55E-01        2.47E+00 Ba-133        79.61            2.65   -6.60E-01      9.02E-02        3.59E+00 81.00           32.90   -2.04E-01                      2.35E-01 276.40            7.16   -5.08E-01                      5.11E-01 302.85           18.34    6.90E-02                      2.21E-01 356.01           62.05   -5.52E-02                      9.02E-02 383.85            8.94   -9.30E-02                      4.77E-01 Cs-134       475.36            1.48    7.70E-01      6.50E-02        3.13E+00 563.25            8.34    2.53E-01                      5.26E-01 569.33           15.37   -1.11E-01                      2.70E-01 604.72           97.62   -1.47E-02                      7.59E-02 795.86           85.46    3.57E-03                      6.50E-02 801.95            8.69   -4.95E-01                      5.79E-01 1038.61             0.99   -3.78E+00                      4.93E+00 1167.97             1.79    3.38E+00                      4.35E+00 1365.19             3.02    6.34E-01                      1.97E+00
+         Cs-137       661.66
* 85.10    1.49E-01      4.78E-02        4.78E-02 Eu-152       121.78           28.67   -6.25E-02      1.49E-01        1.49E-01 244.70            7.61   -3.75E-01                      6.21E-01 295.94            0.45    2.18E+01                      1.21E+01 344.28           26.60   -1.58E-01                      1.56E-01 367.79            0.86    2.78E+00                      4.38E+00 411.12            2.24    6.38E-01                      1.96E+00 443.96            2.83   -3.17E-01                      1.40E+00 488.68            0.42    6.89E+00                      1.03E+01 563.99            0.49    4.26E+00                      8.92E+00 586.26            0.46    1.20E+01                      1.48E+01 678.62            0.47   -1.43E+00                      9.76E+00 688.67            0.86    2.70E+00                      4.56E+00 719.35            0.28   -2.47E+00                      1.68E+01 778.90           12.96   -1.05E-02                      3.67E-01 810.45            0.32    1.70E+00                      1.59E+01 867.37            4.26   -3.44E+00                      1.15E+00 919.33            0.43    7.84E+00                      1.19E+01 964.08           14.65    4.87E-01                      5.38E-01 1085.87            10.24   -2.31E-01                      5.85E-01 1089.74             1.73   -2.06E+00                      3.34E+00 1112.07            13.69   -3.52E-01                      4.39E-01 1212.95             1.43    2.31E+00                      5.55E+00 1249.94             0.19    1.68E+01                      3.72E+01 1299.14             1.63    1.29E+00                      4.14E+00 1408.01            21.07   -1.78E-01                      1.91E-01 1457.64             0.50    2.17E+02                      4.89E+01 1528.10             0.28   -1.44E+01                      1.05E+01 Eu-154       123.07           40.40   -2.19E-03      1.08E-01        1.08E-01 247.93            6.89    4.67E-01                      6.28E-01 591.76            4.95    4.84E-01                      9.23E-01 692.42            1.78   -1.55E-01                      2.35E+00 723.30           20.06    1.38E-01                      2.67E-01 756.80            4.52    1.85E-01                      1.17E+00 873.18           12.08    1.83E-01                      3.96E-01
[378]

7/31/2019  10:19:05AM Page 7 of 7 Analysis Report for     31-Jul-19-10016 L1-10221C-FSGS-013SB Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48        4.40E-01      1.08E-01        5.54E-01 1004.76                  18.01        2.05E-02                      3.05E-01 1274.43                  34.80        1.71E-02                      1.89E-01 1596.48                   1.80       -2.25E+00                      2.83E+00 Eu-155            45.30                  1.31       -1.17E+01      2.38E-01        2.14E+01 60.01                  1.22        1.25E+00                      2.45E+01 86.55                 30.70       -2.02E-02                      2.54E-01 105.31                 21.10        3.98E-02                      2.38E-01
+         Ra-226           186.21
* 3.64        9.22E-01      8.89E-01        8.89E-01 Pa-231            27.36                 10.30        2.82E+00      1.86E+00        2.61E+00 283.69                  1.70        1.42E+00                      2.39E+00 300.07                  2.47       -8.71E-02                      1.86E+00 302.65                  2.20        1.01E+00                      1.86E+00 330.06                  1.40        3.08E-01                      2.87E+00
+         U-235            143.76                 10.96       -3.36E-01      5.66E-02        3.98E-01 163.33                  5.08        1.83E-01                      7.99E-01 185.71
* 57.20        5.87E-02                      5.66E-02 202.11                  1.08        2.30E+00                      3.84E+00 205.31                  5.01       -8.12E-01                      7.67E-01 Am-241            59.54                 35.90       -5.20E-02      8.69E-01        8.69E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[379]

7/31/2019 10:37:54AM Page 1 of 7 Analysis Report for    31-Jul-19-10017 L1-10221C-FIGS-100SB GAMMA SPECTRUM ANALYSIS Sample Identification                        : 31-Jul-19-10017 Sample Description                           : L1-10221C-FIGS-100SB Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.257E+03 grams Facility                                     : Default Sample Taken On                              : 7/30/2019 9:54:00AM Acquisition Started                          : 7/31/2019 10:22:45AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : 324 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 4096 Peak Area Range (in channels)                : 120 - 4096 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 9/29/2018 Efficiency Calibration Used Done On          : 7/31/2019 Efficiency Calibration Description           :
Sample Number                                : 78347 Fill Height                                  : 1257.48 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/31/2019 10:37:48AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 4096
[380]

7/31/2019   10:37:54AM         Page 2 of 7 Analysis Report for    31-Jul-19-10017 L1-10221C-FIGS-100SB Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.65               473 -    481          477.49          1.04E+02               16.71      8.13E+01           1.17 2       351.80               700 -    708          703.54          6.92E+01               12.35      3.88E+01           1.20 3       583.18             1162 -   1171         1165.97           4.88E+01                8.34      9.19E+00           1.66 4       609.27             1215 -   1223         1218.13           4.74E+01                8.52      1.16E+01           0.98 5       911.28             1818 -   1828         1822.00           3.26E+01                8.34      1.54E+01           1.01 6      1460.74             2915 -   2928         2921.53           2.37E+02               15.39      0.00E+00           2.11 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.99          1460.82
* 10.66              4.75E+00              3.71E-01 Tl-208                   1.00           583.19
* 85.00              6.64E-02              1.20E-02 Bi-211                   0.91           351.07
* 13.02              4.35E-01              8.51E-02 Pb-212                   1.00           115.18                    0.60 238.63
* 43.60              1.52E-01              2.74E-02 300.09                    3.30 Bi-214                   1.00           609.32
* 45.49              1.24E-01              2.35E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92                                               [381]

7/31/2019   10:37:54AM        Page 3 of 7 Analysis Report for    31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide               Id                Energy            Yield(%)      Activity            Activity Name             Confidence               (keV)                    (pCi/grams)          Uncertainty Bi-214                   1.00        1155.21                  1.63 1238.12                  5.83 1280.98                  1.43 1377.67                  3.99 1385.31                  0.79 1401.52                  1.33 1407.99                  2.39 1509.21                  2.13 1661.27                  1.05 1729.59                  2.88 1764.49                 15.30 1847.43                  2.03 2118.51                  1.16 Pb-214                   0.99          241.99                 7.25 295.22                18.42 351.93
* 35.60  1.59E-01              3.11E-02 785.96                 1.06 Ac-228                   1.00          129.07                 2.42 209.25                 3.89 270.24                 3.46 328.00                 2.95 338.32                11.27 409.46                 1.92 463.00                 4.40 794.95                 4.25 911.20
* 25.80  1.97E-01              5.11E-02 964.77                 4.99 968.97                15.80 1588.20                  3.22
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
[382]

7/31/2019 10:37:54AM         Page 4 of 7 Analysis Report for   31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide                            Nuclide                       Wt mean              Wt mean     Comments Name                                 Id                           Activity             Activity Confidence                                           Uncertainty (pCi/grams)
K-40                                0.999                     4.75E+00              3.71E-01 Tl-208                              1.000                     6.64E-02              1.20E-02
     ?       Bi-211                              0.919                     4.35E-01              8.51E-02 Pb-212                              1.000                     1.52E-01              2.74E-02 Bi-214                              1.000                     1.24E-01              2.35E-02
     ?       Pb-214                              0.998                     1.59E-01              3.11E-02 Ac-228                              1.000                     1.97E-01              5.11E-02
        ?  = nuclide is part of an undetermined solution X  = nuclide rejected by the interference analysis
       @   = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[383]

7/31/2019  10:37:54AM       Page 5 of 7 Analysis Report for    31-Jul-19-10017 L1-10221C-FIGS-100SB UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/31/2019 10:37:48AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 4096 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide All peaks were identified.
M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.69E-02          5.18E-02        5.18E-02 BE-7            477.60              10.44       8.76E-02          3.33E-01        3.33E-01
+         K-40          1460.82
* 10.66       4.75E+00          5.76E-02        5.76E-02 Mn-54           834.85              99.98       1.13E-02          4.15E-02        4.15E-02 Co-60         1173.23               99.85     -1.13E-02           3.60E-02        3.83E-02 1332.49               99.98     -9.97E-04                           3.60E-02 Nb-94           702.65              99.81     -1.61E-02           2.97E-02        2.97E-02 871.09              99.89       6.24E-03                          3.42E-02 Ag-108m          79.13                6.60    -9.08E-02           2.76E-02        1.01E+00 433.94              90.50     -1.21E-02                           2.76E-02 614.28              89.80     -1.00E-03                           4.48E-02 722.94              90.80     -3.67E-03                           4.02E-02 Sb-125          176.31                6.84    -1.67E-01           9.65E-02        4.56E-01 380.45                1.52    -6.56E-01                           1.92E+00 427.87              29.60       2.59E-02                          9.65E-02 463.36              10.49       2.05E-01                          3.47E-01 600.60              17.65       6.39E-02                          2.30E-01 606.71                4.98    -9.74E-01                           1.09E+00 635.95              11.22     -4.70E-02                           2.41E-01          [384]

7/31/2019  10:37:54AM Page 6 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       671.44            1.79   -1.42E+00      9.65E-02        1.80E+00 Ba-133        79.61            2.65    1.21E+00      6.37E-02        2.53E+00 81.00           32.90   -3.99E-02                      1.76E-01 276.40            7.16    6.91E-02                      4.16E-01 302.85           18.34    2.43E-02                      1.60E-01 356.01           62.05   -2.74E-02                      6.37E-02 383.85            8.94   -1.80E-02                      3.34E-01 Cs-134       475.36            1.48    4.51E-01      5.05E-02        2.24E+00 563.25            8.34    9.77E-02                      4.13E-01 569.33           15.37    1.38E-02                      2.40E-01 604.72           97.62   -8.00E-02                      5.05E-02 795.86           85.46    1.00E-02                      5.13E-02 801.95            8.69   -1.41E-02                      4.65E-01 1038.61             0.99    4.75E-01                      4.69E+00 1167.97             1.79   -1.41E+00                      2.19E+00 1365.19             3.02    2.19E-01                      1.36E+00 Cs-137       661.66           85.10    3.56E-02      5.18E-02        5.18E-02 Eu-152       121.78           28.67    2.02E-02      1.05E-01        1.05E-01 244.70            7.61   -2.75E-01                      4.08E-01 295.94            0.45    6.58E+00                      8.24E+00 344.28           26.60   -1.03E-01                      1.13E-01 367.79            0.86    9.59E-01                      3.44E+00 411.12            2.24    4.25E-01                      1.47E+00 443.96            2.83   -4.12E-02                      1.13E+00 488.68            0.42    1.68E+00                      7.33E+00 563.99            0.49    5.18E-01                      6.91E+00 586.26            0.46   -2.04E+00                      1.08E+01 678.62            0.47    5.08E+00                      8.58E+00 688.67            0.86   -1.99E+00                      3.97E+00 719.35            0.28   -2.14E+00                      1.26E+01 778.90           12.96   -1.90E-01                      2.63E-01 810.45            0.32   -6.39E+00                      1.07E+01 867.37            4.26    8.64E-02                      7.35E-01 919.33            0.43   -6.95E+00                      8.29E+00 964.08           14.65    1.60E-01                      3.54E-01 1085.87            10.24   -1.27E-01                      3.76E-01 1089.74             1.73    1.64E+00                      2.86E+00 1112.07            13.69    6.92E-02                      3.35E-01 1212.95             1.43   -1.75E+00                      3.65E+00 1249.94             0.19    1.23E+01                      3.04E+01 1299.14             1.63   -1.41E-01                      2.66E+00 1408.01            21.07    8.61E-02                      1.85E-01 1457.64             0.50   -1.15E+01                      3.26E+01 1528.10             0.28    2.55E+00                      1.15E+01 Eu-154       123.07           40.40    9.48E-03      7.45E-02        7.45E-02 247.93            6.89   -1.92E-01                      4.06E-01 591.76            4.95   -2.64E-01                      6.67E-01 692.42            1.78    8.36E-01                      1.99E+00 723.30           20.06   -2.42E-02                      1.79E-01 756.80            4.52   -1.37E-01                      8.02E-01 873.18           12.08   -1.28E-01                      2.76E-01
[385]

7/31/2019  10:37:54AM Page 7 of 7 Analysis Report for     31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           996.29                 10.48       -2.25E-02      7.45E-02        3.83E-01 1004.76                  18.01        6.24E-02                      2.61E-01 1274.43                  34.80       -5.87E-02                      1.19E-01 1596.48                   1.80       -2.32E-01                      1.98E+00 Eu-155            45.30                  1.31        7.30E-01      1.62E-01        1.00E+01 60.01                  1.22       -3.62E+00                      1.07E+01 86.55                 30.70        9.46E-02                      1.62E-01 105.31                 21.10        6.72E-02                      1.70E-01 Ra-226           186.21                  3.64        3.35E-01      9.32E-01        9.32E-01 Pa-231            27.36                 10.30        1.80E-01      9.77E-01        9.77E-01 283.69                  1.70        4.07E-01                      1.78E+00 300.07                  2.47       -2.09E+00                      1.11E+00 302.65                  2.20        2.03E-01                      1.33E+00 330.06                  1.40        5.72E-02                      2.10E+00 U-235            143.76                 10.96        8.30E-02      5.96E-02        2.63E-01 163.33                  5.08       -6.70E-02                      6.64E-01 185.71                 57.20        2.22E-02                      5.96E-02 202.11                  1.08       -1.31E+00                      2.84E+00 205.31                  5.01       -2.32E-01                      6.48E-01 Am-241            59.54                 35.90       -8.25E-03      3.87E-01        3.87E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[386]

7/31/2019 10:18:43AM Page 1 of 6 Analysis Report for    31-Jul-19-10015 L1-10221C-FIGS-101SB GAMMA SPECTRUM ANALYSIS Sample Identification                        : 31-Jul-19-10015 Sample Description                           : L1-10221C-FIGS-101SB Sample Type                                  : Soil Unit                                         :
Sample Point                                 :
Sample Size                                  : 1.409E+03 grams Facility                                     : Default Sample Taken On                              : 7/29/2019 3:10:00PM Acquisition Started                          : 7/31/2019 10:03:34AM Procedure                                    : 130G_SOIL_1 Operator                                     : Administrator Detector Name                                : P11314 Geometry                                     : 130G_SOIL_1 Live Time                                    : 900.0 seconds Real Time                                    : 900.3 seconds Dead Time                                    : 0.03 %
Peak Locate Threshold                        : 3.00 Peak Locate Range (in channels)              : 120 - 8192 Peak Area Range (in channels)                : 120 - 8192 Identification Energy Tolerance              : 1.000 keV Energy Calibration Used Done On              : 1/24/2019 Efficiency Calibration Used Done On          : 7/31/2019 Efficiency Calibration Description           :
Sample Number                                : 78345 Fill Height                                  : 1409.48 gram Certificate Name                             : Eu155-Na22 Certificate Date                             : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on        : 7/31/2019 10:18:36AM Peak Analysis From Channel        : 120 Peak Analysis To Channel          : 8192
[387]

7/31/2019   10:18:43AM         Page 2 of 6 Analysis Report for    31-Jul-19-10015 L1-10221C-FIGS-101SB Peak          Energy            ROI       ROI              Peak          Net Peak          Net Area      Continuum         FWHM No.             (keV)         start      end          Centroid               Area      Uncertainty         Counts          (keV) 1       238.83               948 -    960          954.91          8.48E+01               15.20      5.52E+01           1.07 2       558.48             2226 -   2238         2232.12           2.78E+01                6.55      5.18E+00           1.17 3       583.03             2325 -   2339         2330.25           5.20E+01                8.96      9.96E+00           1.01 4       609.19             2429 -   2441         2434.81           5.93E+01                9.21      9.75E+00           1.01 5      1460.45             5828 -   5851         5839.74           2.63E+02               17.27      8.87E+00           1.97 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
NUCLIDE IDENTIFICATION REPORT Nuclide Library Used       : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide               Id                 Energy             Yield(%)                   Activity             Activity Name             Confidence                (keV)                                 (pCi/grams)           Uncertainty K-40                     0.97          1460.82
* 10.66              6.06E+00              4.77E-01 Tl-208                   0.99           583.19
* 85.00              8.00E-02              1.46E-02 Pb-212                   0.99           115.18                    0.60 238.63
* 43.60              1.37E-01              2.69E-02 300.09                    3.30 Bi-214                   0.99           609.32
* 45.49              1.75E-01              2.92E-02 768.36                    4.89 806.18                    1.26 934.06                    3.11 1120.29                  14.92 1155.21                    1.63 1238.12                    5.83                                              [388]

7/31/2019   10:18:43AM         Page 3 of 6 Analysis Report for    31-Jul-19-10015 L1-10221C-FIGS-101SB Nuclide               Id                Energy              Yield(%)                  Activity            Activity Name             Confidence                (keV)                                (pCi/grams)           Uncertainty Bi-214                   0.99        1280.98                     1.43 1377.67                     3.99 1385.31                     0.79 1401.52                     1.33 1407.99                     2.39 1509.21                     2.13 1661.27                     1.05 1729.59                     2.88 1764.49                   15.30 1847.43                     2.03 2118.51                     1.16
      * = Energy line found in the spectrum.
      - = Manually added nuclide.
      ? = Manually edited nuclide.
      @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide                            Nuclide                       Wt mean                Wt mean     Comments Name                                 Id                           Activity               Activity Confidence                                             Uncertainty (pCi/grams)
K-40                                0.978                     6.06E+00                4.77E-01 Tl-208                              0.996                     8.00E-02                1.46E-02 Pb-212                              0.994                     1.37E-01                2.69E-02 Bi-214                              0.999                     1.75E-01                2.92E-02
        ?   = nuclide is part of an undetermined solution X   = nuclide rejected by the interference analysis
       @    = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
[389]

7/31/2019  10:18:43AM       Page 4 of 6 Analysis Report for    31-Jul-19-10015 L1-10221C-FIGS-101SB UNIDENTIFIED PEAKS Peak Locate Performed on        : 7/31/2019 10:18:36AM Peak Locate From Channel        : 120 Peak Locate To Channel          : 8192 Peak CPS (%)         Peak       Tolerance Peak No.           Energy (keV)              Peak Size (CPS)         Uncertainty         Type        Nuclide 2            558.48              3.09091E-02                     23.54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used      : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide           Energy           Yield(%)          Activity   Nuclide MDA       Line MDA Name                                            (pCi/grams)       (pCi/grams)   (pCi/grams)
(keV)
An Pk           511.00            100.00        6.57E-02          5.28E-02        5.28E-02 BE-7            477.60              10.44     -1.96E-01           3.25E-01        3.25E-01
+         K-40          1460.82
* 10.66       6.06E+00          5.29E-01        5.29E-01 Mn-54           834.85              99.98     -1.36E-02           4.08E-02        4.08E-02 Co-60         1173.23               99.85     -5.63E-04           4.91E-02        6.04E-02 1332.49               99.98     -7.13E-03                           4.91E-02 Nb-94           702.65              99.81       1.35E-02          3.79E-02        3.85E-02 871.09              99.89     -2.81E-02                           3.79E-02 Ag-108m          79.13                6.60      3.33E-01          3.72E-02        1.16E+00 433.94              90.50       6.65E-03                          3.72E-02 614.28              89.80     -5.49E-02                           5.70E-02 722.94              90.80       1.71E-02                          5.00E-02 Sb-125          176.31                6.84      3.52E-01          1.21E-01        4.57E-01 380.45                1.52      4.43E-01                          2.21E+00 427.87              29.60       5.70E-02                          1.21E-01 463.36              10.49       1.84E-01                          3.65E-01 600.60              17.65       1.67E-02                          2.03E-01 606.71                4.98      1.90E+00                          1.31E+00          [390]

7/31/2019  10:18:43AM Page 5 of 6 Analysis Report for 31-Jul-19-10015 L1-10221C-FIGS-101SB Nuclide        Energy        Yield(%)      Activity Nuclide MDA      Line MDA Name                                   (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Sb-125       635.95           11.22   -9.51E-02      1.21E-01        3.44E-01 671.44            1.79   -3.07E-01                      2.12E+00 Ba-133        79.61            2.65   -2.98E-02      5.71E-02        2.79E+00 81.00           32.90   -1.08E-01                      1.94E-01 276.40            7.16   -1.19E-01                      4.14E-01 302.85           18.34    8.35E-02                      1.96E-01 356.01           62.05   -3.87E-02                      5.71E-02 383.85            8.94    8.43E-02                      3.82E-01 Cs-134       475.36            1.48   -1.48E+00      5.35E-02        2.21E+00 563.25            8.34   -2.68E-01                      4.85E-01 569.33           15.37    1.79E-02                      2.33E-01 604.72           97.62   -7.31E-03                      5.50E-02 795.86           85.46    4.49E-02                      5.35E-02 801.95            8.69   -2.54E-01                      4.35E-01 1038.61             0.99   -1.83E+00                      4.56E+00 1167.97             1.79   -2.56E-01                      2.97E+00 1365.19             3.02    5.98E-02                      1.45E+00 Cs-137       661.66           85.10    2.18E-02      5.69E-02        5.69E-02 Eu-152       121.78           28.67   -6.68E-02      1.06E-01        1.06E-01 244.70            7.61    3.38E-01                      4.81E-01 295.94            0.45   -3.31E+00                      8.83E+00 344.28           26.60    4.74E-02                      1.19E-01 367.79            0.86    1.04E+00                      3.51E+00 411.12            2.24    6.40E-01                      1.64E+00 443.96            2.83   -9.76E-01                      1.15E+00 488.68            0.42    4.73E-01                      8.26E+00 563.99            0.49   -1.12E+00                      7.24E+00 586.26            0.46   -1.76E+00                      1.26E+01 678.62            0.47    4.61E-01                      7.64E+00 688.67            0.86    1.01E+00                      4.33E+00 719.35            0.28   -6.68E+00                      1.32E+01 778.90           12.96    1.68E-02                      2.78E-01 810.45            0.32   -2.70E+00                      1.24E+01 867.37            4.26   -7.24E-01                      8.87E-01 919.33            0.43   -9.65E+00                      9.93E+00 964.08           14.65    9.47E-02                      4.46E-01 1085.87            10.24   -3.19E-01                      4.06E-01 1089.74             1.73   -4.05E-01                      2.81E+00 1112.07            13.69   -1.20E-01                      4.05E-01 1212.95             1.43   -1.59E+00                      4.32E+00 1249.94             0.19   -1.36E+01                      3.11E+01 1299.14             1.63    1.09E+00                      3.05E+00 1408.01            21.07   -1.18E-01                      1.76E-01 1457.64             0.50    1.33E+02                      4.02E+01 1528.10             0.28    1.63E+00                      1.48E+01 Eu-154       123.07           40.40    1.60E-02      8.19E-02        8.19E-02 247.93            6.89   -2.50E-01                      4.20E-01 591.76            4.95   -6.01E-01                      6.35E-01 692.42            1.78   -1.64E+00                      2.01E+00 723.30           20.06    1.18E-01                      2.27E-01 756.80            4.52   -6.67E-01                      7.83E-01
[391]

7/31/2019  10:18:43AM Page 6 of 6 Analysis Report for     31-Jul-19-10015 L1-10221C-FIGS-101SB Nuclide            Energy             Yield(%)           Activity Nuclide MDA      Line MDA Name                                                 (pCi/grams)   (pCi/grams)   (pCi/grams)
(keV)
Eu-154           873.18                 12.08        6.24E-02      8.19E-02        3.23E-01 996.29                 10.48        1.04E-01                      4.08E-01 1004.76                  18.01        8.17E-02                      2.51E-01 1274.43                  34.80       -1.87E-01                      1.10E-01 1596.48                   1.80        6.10E-02                      2.14E+00 Eu-155            45.30                  1.31       -4.78E+00      1.76E-01        9.61E+00 60.01                  1.22       -2.15E+00                      1.06E+01 86.55                 30.70       -3.41E-03                      1.76E-01 105.31                 21.10        1.29E-01                      1.91E-01 Ra-226           186.21                  3.64       -5.67E-01      8.66E-01        8.66E-01 Pa-231            27.36                 10.30        6.64E-01      1.20E+00        1.20E+00 283.69                  1.70        3.73E-01                      1.96E+00 300.07                  2.47       -1.56E+00                      1.48E+00 302.65                  2.20        3.86E-01                      1.62E+00 330.06                  1.40        4.25E-01                      2.46E+00 U-235            143.76                 10.96        1.10E-01      5.63E-02        2.94E-01 163.33                  5.08        6.09E-02                      5.74E-01 185.71                 57.20       -1.38E-02                      5.63E-02 202.11                  1.08        1.28E-01                      2.84E+00 205.31                  5.01       -4.31E-01                      6.14E-01 Am-241            59.54                 35.90       -9.68E-02      3.66E-01        3.66E-01
    +    =  Nuclide identified during the nuclide identification
     *    = Energy line found in the spectrum
    >    =  MDA value not calculated
    @    =  Half-life too short to be able to perform the decay correction
    ?    =  CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
[392]

ATTACHMENT 8 EBERLINE ANALYTICAL REPORTS
[393]

EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TENNESSEE 37830 ANALYTICAL                                                       PHONE (865) 481-0683 FAX (865) 483-4621 EBS-OR-46230 October 22, 2019 Patricia Giza Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099
* CASE NARRATIVE Work Order# 19-09001-0R SAMPLE RECEIPT This work order contains sixteen soil samples received 09/03/2019. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.
CLIENT ID                            LABID              CLIENT ID                       LAB ID Ll-1022 lA-FSGS-004-SS-A              19-09001-04       Ll-10221A-FIGS-003-SS-A         19-09001-12 Ll-1022 lA-FSGS-002-SS-A              19-09001-05       Ll-1022 lA-FIGS-004-SS-A        19-09001-13 Ll-10221 C-FSGS-012-SS-A              19-09001-06       Ll-10220I-FJGS-005-SS-A         19-09001-14 Ll-10221C-FSGS-013-SS-A               19-09001-07       Ll-10220I-QJGS-005-SS-A         19-09001-15 Ll-10221 C-FSGS-014-SS-A              19-09001-08       L 1-1022 lA-FIGS-003-SB-A       19-09001-16 Ll-1022 lA-FIGS-001-SS-A              19-09001-09       Ll-1022 lA-FIGS-001-SB-A        19-09001-1 7 L 1-1022 lA-QIGS-OO 1-SS-A            19-09001-10       L 1-10221 A-FIGS-004-SB-A       19-09001-18 L 1-1022 lA-FIGS-002-SS-A             19-09001-11       L 1-1022 lA-FIGS-002-SB-A       19-09001-19 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.
Gamma Spectroscopy was performed using EPA Method 901.1 Modified; Laboratory qualifiers are as follows:
U - Result is less than the MDA.
ANALYTICAL RESULTS Combined Standard Uncertainty is reported at I-sigma value.
Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.
Page 1 of 3

ANALYTICAL RES UL TS CONTINUED TOTAL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filters were reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.
Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are reported from Total Strontium assuming secular equilibrium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.
TRITIUM A representative aliquot of each sample was equilibrated with tritium free water. Equilibrates were transferred into a round-bottomed distillation flask and attached to a single stage still. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were counted by beta liquid scintillation.
Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.
NICKEL-63 A representative aliquot of each sample was prepared by leaching in acids. Aliquots were placed into an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion.
Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.
Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.
GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.
Page 2 of 3

ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Cobalt-60, Cesium-137 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data c::_**~~'.'.'.'.'.'
contained in this hard copy data package has been authorized by the cognizant project manager or his/her to be accurate as verified by the following signature.
l '\__ ~
M.RcMctlou:>                        .
Laboratory Manager Date: 10/22/2019 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services.
Page 3 of 3

Printed: 101211201911:34AM                                                                                                                                                                                                                                            Page 1 of 21 Report To:                                                                                Work Order Details:
Patricia Giza                                                                                                              19-09001 Eberline Analytical                                                                          Zion Solutions
                                                                                                                   * ,*m**,~*-,  *------**w**
Purchase Order:
SDG:
677118
                                                                                        ***- - - - * - - - - " " - - - - - - - - - - - ~ * - "'""'-''-""'''*-A~ __,,
Final Report of Analysis                                                               2701 Deborah Ave                                                                            Analysis Category: ... ....... E.=_N..Y:~RONflll_E:~TAL:... ________ .
Zion, IL 60099                                                                                  Sample Matrix:             SO Lab                  Sample                           Client                     Sample                          Receipt                Analysis         Batch                                                                                                                           Report ID                    Type                            ID                           Date                             Date                  Date            ID Analyte         Method                Result           cu            CSU              MDA           Qualifier Units 19-09001-01                    LCS        KNOWN                                   09/04/19 00:00                        9/3/2019              9/24/2019        19-09001        Tritium   LANL ER-210 Modified      2.04E+02        7.34E+OO 19-09001-01                    LCS        SPIKE 09/04/19 00:00                        9/3/2019 9/24/2019 19-09001 Tritium   LANL ER-210 Modified      2.03E+02        7.79E+OO      1.38E+01        5-70E+OO 19-09001-02                   MBL         BLANK                                   09/04/19 00:00                        9/3/2019              9/24/2019        19-09001        Tritium   LANL ER-210 Modified      4.61E+OO        3.45E+OO      3.46E+OO        5.69E+OO
.....-------------------------, ---                                                     06/06/1912:20                         9/3/2019              9/24/2019        19-09001        Tritium . LANL ER~--21*orc,~difi~d 19-09001-03                   DUP         L 1-10221A-FSGS-004-SS-A                                                 I                                                    <
* 1.49E+OO        3.25E+OO      3-25E+OO        5.54E+OO 19-09001-04                    DO         L 1-10221A-FSGS-004-SS-A                06/06/19 12:20                        9/3/2019              9/24/2019        19-09001        Tritium   LANL ER-210 Modified      3-14E+OO        3.27E+OO      3.28E+OO         5.48E+OO
                                                                                    *-* -*-*--~,--,,--~-
19-09001-05                   TRG         L1-10221A-FSGS-002-SS-A                 06/06/19 12:10                        9/3/2019              9/24/2019        19-09001        Tritium   LANL ER-210 Modified     -7.35E-01        3-11E+OO      3-11E+OO        5.45E+OO 19-09001-06                   TRG         L 1-10221 C-FSGS-012-SS-A               06/11/19 09:10                                              9/24/2019        19-09001        Tritium   LANL ER-210 Modified      1.46E+OO        3-17E+OO      3.17E+OO        5.41E+OO 19-09001-07                   TRG         L 1-10221C-FSGS-013-SS-A                06/11/19 09:15                                              9/24/2019                        Tritium   LANL ER-210 Modified     -1.14E+OO        3.20E+OO      3.20E+OO        5.62E+OO 19-09001-08                   TRG         L 1-10221C-FSGS-014-SS-A                06/11/19 09:20                                              9/24/2019                        Tritium   LANL ER-210 Modified     -9.46E-01        3.20E+OO      3.20E+OO        5.61E+OO 19-09001-09                   TRG         L 1-10221A-FIGS-001-SS-A                06/11/1912:15                                                                                Tritium   LANL ER-210 Modified      1.09E+OO        3.13E+OO      3.13E+OO        5.37E+OO 19-09001-10 :                 TRG         L1-10221A-QIGS-001-SS-A                 06/11/19 12:15                                                                               Tritium   LANL ER-210 Modified                                    3.29E+OO
                                         -------------------------------+---------------i---------------------'-----"-------------------------------1------------------'-------,------------'----'--.:...:::.=-.__,_;_::..:..;:__:_:_                           ____---'5.49E+OO
                                                                                                                                                                                                                                                                        -___;_:::__:__:_ ___::____.____'.:..:.:.:::._-1 19-09001-11                   TRG         L 1-10221A-FIGS-002-SS-A                06/11/19 12:17                                                                               Tritium   LANL ER-210 Modified                                    3.28E+OO        5.54E+OO
 -*-*-'"-'""*--~-,-~,a_, _____ ,_, __ _. '"'"'"""--,----*---
19-09001-12                   TRG         L1-10221A-FIGS-003-SS-A                 06/11/19 12:19                                                                               Tritium   LANL ER-210 Modified                                    3.05E+OO        5.37E+OO 19-09001-13                   TRG         L1-10221A-FIGS-004-SS-A                 06/11/19 12:21                                                                                                                                                 3.16E+OO        5.50E+OO 07/09/19                                                                                                      -210 Modified                                    3.09E+OO        5.45E+OO 07/09/19 08:30                                                                                                                                                 3.07E+OO        5.30E+OO LANL ER-210 Modified                                    3.16E+OO        5.47E+OO LANL ER-210 Modified                                    3.20E+OO        5.43E+OO Tritium   LANL ER-210 Modified                                    3-19E+OO        5.40E+OO             u          pCi/g 19-09001-19                   TRG                                                                                                                                              Tritium   LANL ER-210 Modified                      3.26E+OO      3.26E+OO        5.53E+OO             u          pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                   865/481-0683               FAX    865/ 483-4621

Printed: 10/21/201911:34AM                                                                                                                                                                                                                                                                      Page 2 of 21 Report To:                                                                                                                                 Work Order Details:
Patricia Giza                                                                                                                                      19-09001 Eberline Analytical                                                                     Zion Solutions                                                                               Purchase Order:
SDG.
677118 Final Report of Analysis                                                            2701 Deborah Ave                                                                    ..... Analysis Category: .                                     ENVIRONMENTAL Zion, IL 60099                                                                                 Sample Matrix:                                      so Lab               Sample                           Client                        Sample             Receipt         Analysis            Batch                                                                                                                                                                  Report Analyte                     Method                                                                                                   MDA   Qualifier ID                 Type                            ID                            Date                Date             Date                 ID                                                                                                                                                                  Units 19-09001-01               LCS             KNOWN                                   09/04/19 00:00         9/3/2019        9/23/2019                                             ASTM 3500-Ni Modified 19-09001-01
 --,-.,.,                        LCS             SPIKE                                   09/04/19 00:00
                                                         ,_,_,_____,__,---*~* ---- -w*--*-------"*--*-----*-    9/3/2019        9/23/2019                                             ASTM 3500-Ni Modified                                                                                            3.45E+OO 19-09001-02               MBL             BLANK                                    09/04/19 00:00        9/3/2019        9/23/2019                            Nickel-63        ASTM 3500-Ni Modified                                                                                            3.53E+OO    u
 ......!~:09-0~.1.:.&deg;-~---     -~~---L_1:.1..~~-2.:_A-_FSG~?_04_-S_S:_I\___.              06/06/19 12:20     , 9/312_0_1_9__9_12_312019           .19-:0_9~?_1 _ --~ckel~---_....__A__    ST_M_3_5_o_o__-_N
____i __M_o___d_ifi_e__d******** ___1_.9_8E
__+o_1___ ,_____2               2.95E+OO
___._7_1E_+_o_o*-*-**--*-**---* * *3.76E+OO 1
19-09001-04                DO             L1-10221A-FSGS-004-SS-A                  06/06/1912:20      : 9/3/2019         9/23/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                         2.69E+OO        2.92E+OO           3.75E+OO
/-** *-----*******-****-----***--*-*-------*-******------*******---***-+**                                                                                       .. ***-------+-*--*-**-*-------*********---**-**---'--------*--*--*-*-
19-09001-05              TRG              L1-10221A-FSGS-002-SS-A                 06/06/1912:10                          9/23/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.73E+OO    u
      **---"-''          "<rn"_ _ _ .......,.__,             *--*--*-----
19-09001-06              TRG              L1-10221C-FSGS-012-SS-A                 06/11/19 09:10                         9/23/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.54E+OO    u 19-09001-07              TRG              L1-10221C-FSGS-013-SS-A                  06/11/19 09:15                        9/23/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.61E+OO    u
 ********-***--***----*----***********--- ***----*---**------***--l-********--------+-*-*--------------******-*******-------*-***-1--**---------******--+-------*--=****------+**-**-*-****------
19-09001-08              TRG              L1-10221C-FSGS-014-SS-A                  06/11/19 09:20                        9/23/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.58E+OO
 -*--*---*-- ****-***-*******-***------------------ t*******-------+-------~----.,.----*-*-****                                                                                ---t-*--------***+******--------;--------,-----*--
19-09001-09              TRG              L1-10221A-FIGS-001-SS-A                  06/11/1912:15                         9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.62E+OO 19-09001-10              TRG              L1-10221A-QIGS-001-SS-A                                                        9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.60E+OO
       -----*-*-**--*--------------*------------J---**************----j---------****-------***'*                                                                               ****-1------*----*-----'-**-*******-----------*-------+---*--*-*-***--
19-09001-11              TRG              L1-10221A-FIGS-002-SS-A                                                        9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.71E+OO    u
                                                      *--*--*-----------*+----*-***---**--**+----~---*-*------******-******-*----,-----*---*-****--+---*--*---------+*****-**---...;-------------***---
19-09001-12              TRG              L1-10221A-FIGS-003-SS-A                                                        9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.54E+OO             pCi/g
                             ***---------                                  -------- -***t*---------*----*---~----**-*---**---***--**r*-------**1--..*-------*--***--*-------;---------,-----***--0-----------
19-09001-13              TRG              L1-10221A-FIGS-004-SS-A                                                        9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.57E+OO             pCi/g 19-09001-14                               L1-102201-FJGS-005-SS-A                                                        9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                            3.81E+OO    u 19-09001-15               TRG             L1-10220I-QJGS-005-SS-A                                                        9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                                        u 19-09001-16               TRG                                                                                            9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                                        u        pCi/g 19-09001-17              TRG                                                                                             9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                                                        u
                                                                                                                ------------'"*=-"-*-----------------1------*---**--+-*---*----f-----*-*------------------------
19-09001-18              TRG                                                       06/26/19 10:                          9/24/2019          19-09001 i        Nickel-63        ASTM 3500-Ni Modified                                                                                            3.60E+OO    u        pCi/g
                                                                                          ------;-----,..--------*---"""r-~---------+---------*---~--------+-------c-------*------------
19-09001-19              TRG                                                       06/26/1910:02         9/3/2019        9/24/2019          19-09001          Nickel-63        ASTM 3500-Ni Modified                                                                         2.11E+OO           3.60E+OO    u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma};MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(   "'M> EBERLINE                                 ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                     865/481-0683                                        FAX       865/ 483-4621

Printed: 10/21/201911:34 AM                                                                                                                                                                                                                  Page 3 of 21 Report To:                                                                                                 Work Order Details:
Patricia Giza                                                                                                           19-09001 Eberline Analytical                                           **-**-*.,***-***-- ...
Zion       Solutions SDG:
                                                              ****A*---*~-*--=--*---          -A- _V,___,,
Final Report of Analysis                                               2701 Deborah Ave Zion, IL 60099                                                                               Sample Matrix:
Lab         Sample                   Client                     Sample               Receipt         Analysis       Batch                                                                                                                                   Report ID                                               Date            Date Analyte                   Method                  Result              cu             CSU        MDA    Qualifier ID          Type                                                  Date                                                ID                                                                                                                                    Units 19-09001-01       LCS                                        09/04/19 00:00              9/3/2019        9/24/2019    19-09001           Strontium-90        EIChroM SRW01 Modified           5.09E+01         2 _ 85E-01
                                                                          -*------****                                  *-**-*--*----~--- ---- --*                                .. ----;----*--------,----------
19-09001-01                                                  09/04119 00:00              9/3/2019        9/24/2019    19-09001           Strontium-90        EIChroM SRW01 Modified           5-D1E+01        U9E+OO           U5E+01     7 _ 94E-01 19-09001-02      MBL       BLANK                             09/04/19 00:00              9/3/2019        9/24/2019    19-09001           Strontium-90        EIChroM SRW01 Modified           -2,75E-02        3.49E-01        3.49E-01   7.48E-01     u 19-09001-03      DUP       L 1-10221A-FSGS-004-SS-A          06/06/1912:20             . 9/3/2019        9/24/2019 09001 -                       ----i-****-*--*                          4.18E-02        3 _ 33E-01      3 _ 33E-01              u         pCi/g 19-09001-04       DO       L 1-10221 A-FSGS-004-SS-A          06/06/19 12:20                                          19-09001                                                                                 3 _ 72E-01      3--73E-01  7 _ 97E-01    u 19-09001-05      TRG       L 1-10221A-FSGS-002-SS-A                                                                                                                                                            3.60E-01        3.62E-01   7.79E-01     u 19-09001-06      TRG       L 1-10221 C-FSGS-012-SS-A                                                                                                                                                           3.71E-01        3.73E-01   7.SOE-01      u 19-09001-07      TRG       L 1-10221C-FSGS-013-SS-A                                                                                                                                                            2.71E-01        2.87E-01   5.48E-01      u 19-09001-08      TRG       L 1-10221 C-FSGS-014-SS-A                                                                                                                                                           3.72E-01        3.73E-01   7.86E-01      u 19-09001-09      TRG       L 1-10221A-FIGS-001-SS-A           06/11/19 12:15                                                                                                                                   3.45E-01        3.SOE-01   7.55E-01      u 19-09001-10      TRG        L1-10221A-QIGS-001-SS-A                                                                                                                                                            3.40E-01        3.51E-01   7.00E-01 19-09001-11      TRG       L 1-10221A-FIGS-002-SS-A                                                                                                                                                            3.18E-01        3.27E-01   6.56E-01     u 19-09001-12      TRG       L 1-10221A-FIGS-003-SS-A           06/11/19 12:19                                                                                                                                   3.34E-01        3.69E-01   6.65E-01     u 19-09001-13      TRG       L 1-10221A-FIGS-004-SS-A           06/11/19 12:21                                                                                                                                   3.33E-01        3.59E-01   6.67E-01      u L1-102201-FJGS-005-SS-A                                                                                                                                                            3.SSE-01        3.96E-01   8.0SE-01      u TRG        L1-10220!-QJGS-005-SS-A                                                                                                                                                            4.36E-01        4.38E-01   9.43E-01      u TRG        L 1-10221A-FIGS-003-SB-A                                                                                                                                                           3.29E-01        3.29E-01   7.13E-01      u L 1-10221A-FIGS-001-SB-A                                                                                                                                                            3.87E-01        4.44E-01   8.SSE-01     u 3.14E-01        3.19E-01   6.52E-01      u 3.57E-01   7.37E-01      u EPA 901.1 Modified EPA 901.1 Modified EPA SPIKE                                                                                                                                  EPA901.1 Modified CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(  '"MJ EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                               865/481-0683                 FAX 865/483-4621

Printed: 10/21/201911:34AM                                                                                                                                                                                                                                  Page 4 of 21 Report To:                                                                            Work Order Details:
Patricia Giza                                                                                       19-09001 Eberline Analytical                                                                                    Zion Solutions SDG:
Purchase Order:             677118
                                                                                                        """"'~-  --- "-------''"'""- *----~--------*-
Final Report of Analysis 2701 Deborah Ave                                                     Analysis Category:             ENVIRONMENTAL Zion, IL 60099                                                            Sample Matrix:            so Lab             Sample                          Client                                       Sample              Receipt       Analysis      Batch                                                                                                                         Report JO                                             Date             Date            Date         JO Analyte              Method                 Result          cu               CSU                  MOA   Qualifier 10               Type                                                                                                                                                                                                                                                      Units 19-09001-02              MBL               BLANK                                            09/04/19 00:00            9/3/2019       9/10/2019    19-09001  Actinium-228      EPA 901.1 Modified        6.98E-02       7.46E-02          7.47E-02 19-09001-02              MBL               BLANK                                            09/04/19 00:00            9/3/2019       9/10/2019    19-09001  Silver-108m       EPA 901.1 Modified         1.64E-03      3.23E-02          3.23E-02                        u        pCi/g
                               """' '" *-*-----&#xa5;-*---- """-----*,.,,-,.-----~ "--------,----*''"
19-09001-02              MBL               BLANK                                                                                                  19-09001 Americium-241      EPA 901.1 Modified         5.81E-03      4.03E-02          4.03E-02            6.08E-02 19-09001-02              MBL               BLANK
                                                            ***--***--******-***-*****--J**--********---****** **<***---*-*-**------~--------*-***-
19-09001   Barium-133
                                                                                                                                                                             +****----***-*****------*-*-**-*-*--- ""*********-****-*--*-*****--
EPA 901.1 Modified        2.87E-02       4.84E-02         4.84E-02             6.11E-02
                                        ----~*----------,,,*--**---------*-*---+**--********** *-*----*******-**--*-------**-****-**-"********* .,,_,,_,__ ---* '"""                                  ***,.*--**---********----
19-09001-02                                                                                                                                       19-09001  Bismuth-214       EPA 901.1 Modified                       7.51E-02          7.51E-02            1.19E-01 19-09001-02                                                                                                                                       19-09001    Cobalt-60       EPA 901.1 Modified                       3.11E-02          3.11E-02            4.87E-02 19-09001-02              MBL               BLANK                                                                                                  19-09001  Cesium-134        EPA901.1Modified                                           4.14E-02            4.95E-02
 *-*--*--------*-"-*---- *-.-*-------------*----*----------+--*----*--*-**-*-+******----,-------***-----*-*-** *******----****+*-***---------*---,...,....,.____..,..... *****--*---+-----*-****-*****-**
19-09001-02              MBL               BLANK                                                                                                  19-09001  Cesium-137                                                 3.33E-02          3.34E-02            5.34E-02 1--------****-****-----*********--*-----**********---*--------+-*--*---*--***--*--------------*******-**-***-****                                                                 **********-*----*-******,***-****------*-***-**---*-***---------******
MBL               BLANK                                                                                                  19-09001                                              7 .08E-02      9.03E-02          9.04E-02            1.04E-01 19-09001-02              MBL               BLANK                                                                                                  19-09001                                              -6.27E-03      9.34E-02          9.34E-02            5.22E-02
                      ---~***---*-*--*---~------~--------*---*----,,,,--t--***************--**"*~--------***----*--*---********-******-----*-****1***-**------**-***-**--*------*-*---**-***--*--~--****----
19-09001-02              MBL               BLANK                                                                                                  19-09001                    EPA 901.1 Modified        -2.87E-02      4.89E-02          4.89E-02            6.67E-02
           -           '        -"""_____,_"________,________ ----+--------***********--------**-------------**--~*******-***---*-*---------------**********-+**----***--***----*-***~,---------
19-09001-02              MBL               BLANK                                                                                                  19-09001 Holmium-166m       EPA901.1                                 6.76E-02          6.76E-02            3.71E-02
   ------,------------------"-------------------------------------*-------------+-*--------*-~-------,.---**---..-----,----*-**--****--+----*-*-*--*---l ***--*-*----e---------------
19-09001-02              MBL               BLANK                                                                                                  19-09001   lodine-129       EPA 901.1                                3.51E-02          3.51E-02            5.03E-02
     ---*~-----*------------------------,---t---*------,.----**-----*---------********-- -------------+---*-*------*--***------------------------
19-09001-02              MBL               BLANK                                                                                                  19-09001                    EPA 901.1 Modified                       3.04E-01          3.04E-01            6.49E-01
                                   -~------------------+-------------------i---------r--*---***-'-**-----l--*-*****-***--**----*****----i------**-------*****-*--------
19-09001-02 ,            MBL               BLANK                                                                                                  19-09001                                                             3.81E-02          3.81E-02            5.57E-02
       ***---------**--*******--******-*----*-**---**---+**---*****-*******-f--****-......O---....;.-------'----:C... -...----1--*--****--*---*-,--*----***.--*-----**------
3.43E-02            4.38E-02 2.94E-02            4.81E-02 3.34E-01            5.65E-01 4.17E-02            6.94E-02 8.81E-02            1.42E-01 7.51E-02          7.51E-02 8.58E-02          8.58E-02 3.76E-01          3.77E-01 EPA 901.1 Modified                       1.01E-01          1.01E-01 EPA901.1 Modified                        1.33E-01          1.33E-01 CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control SampJe;MBL=BJank;OUP=Ouplicate;TRG=Normal Sample;OO=Ouplicate OriginaJ;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601    SCARBORO ROAD OAK RIDGE,                   TN 37830           865/481-0683               FAX    865/483-4621

Printed: 10/21/201911:34AM                                                                                                                                                                                                                                                                                                                           Page 5 of 21 Report To:                                                                                                     Work Order Details:
Patricia Giza                                                                                                                            19-09001 Eberline Analytical                                                                                                                           ____
Zion Solutions                                                                                    Purchase Order:
SDG:
677118
                                                                                                                                                                                                                                                    --,~-----*--
Final Report of Analysis                                                                                                     2701 Deborah Ave
                                                                                                                                                 *--------                                                                            .Analysis.Category: .                      ENVIRONMENTAL Zion, IL 60099                                                                                       Sample Matrix:                       so Lab                 Sample                                       Client                                                Sample                     Receipt           Analysis             Batch                                                                                                                                                                      Report ID                   Type                                          ID                                                    Date                      Date                Date               ID Analyte                Method                          Result      cu                     CSU                          MDA                 Qualifier Units 19*09001-03                  DUP                L1-10221 A-FSGS-004-SS-A                                                06/06/19 12:20                 9/3/2019           9/10/2019          19-09001            Actinium-228      EPA901.1 Modiiied                     5.98E-01   3 05E-01              3.07E-01                     5.39E-01
                                                                                                                                                      "-" ,----~------------                       ----- --- ,,,-,,-                                                                   ---~-****-        " ' - * - - * - * - - - - - - - . - - , , w_rn_,, ___ _,'
19*09001-03                  DUP                L1-10221A-FSGS-004-SS-A                                                 06/06/19 12:20                 9/3/2019           9/10/2019          19-09001            Silver-108m       EPA 901.1 Modiiied                   -4.26E-02   8.25E-02              8.25E-02                     1.05E-01 19-09001-03                  DUP                L1-10221 A-FSGS-004-SS-A                                                ~~!&deg;.~_9_12_:_2-D___ 9/3/2019                     9/1.".0_D..1.?.... 19-090D_1_ ,.*.. Americium-241        EPA 901.1 Modified                    1.06E-01   1.59E-01              1.59E-01                     2.11E-01 19-09001-03                  DUP                L1-10221A-FSGS-004-SS-A                                                 06/06/1912:20                  9/3/2019           9/10/2019          19-09001             Barium-133       EPA901.1 Modiiied                     6.50E-02   7.66E-02              7.67E-02                     1.56E-01
     ---------"*----*--*, *--*-------"-------------~-----*-----                                                     ................... ---*---------------------~-----
19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                06/06/1912:20                  9/3/2019           9/10/2019          19-09001            Bismuth-214       EPA 901.1 Modiiied                    5.50E-01   2.16E-01              2.18E-01                     3.26E-01
                     .................................................... - ..---*-****-------                          **---*-**--*----**'------***------------~---*-- -------***----
19*09001*03                  DUP                 l1*10221A-FSGS-004*SS-A                                                06/06/1912:20                                     9/10/2019          19-09001              Cobalt-60       EPA 901.1 Modified                    2.52E+OO   2.37E-01              2.70E-01                     1.87E-01
  *-*-----*-*"wmw,"',***               ""   "" _ _ _ _ _ ,_, __, , _ , _ , , ~ ~ - - - - * - * " ' " ' " " '_ _ _ ,                                                                                                           *-**-*+**----*-*-*--*-,.,"*****--****-**-*--,**-----**-**-------
19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                06/06/1912:20                                                        19-09001             Cesium-134                                                        4.81E-02              4.81E-02                     9.53E-02
                  ---------*------------*---------*-----------*---t****-*-----** ..----------*+----..C....--...............,_ ------*+****-----------------------------------------*----*---**---,------*
06/06/19 12:20                                                                                                                                                                    1.01E+OO                     1.89E-01 3.05E-01                     2.90E-01 19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                           EPA901.1 Modilied                                                      1.09E-01                     1.49E-01
   -----~                                      '     -'-"" -
19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                           EPA901.1 Modiiied 19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                           EPA 901.1 Modified
                         *------------------------------+-*---------***+------------~'-----r---*--;...-,_*-------1--c-c-~--*--------'-*-***----*--,---*--**c:--..,.-----------------'------.:.........:::.._-f 19-09001-03                                      L1-10221A-FSGS-004-SS-A                                                06/06/1912:20                                                                              lodine-129      EPA901.1 Modified
                                                                                                                                         --*--------+*-----------0----...,--------------------+-------------+*
L1-10221 A-FSGS-004-SS-A                                               06/06/19 12:20                                                                           Potassium-40      EPA 901.1 Modiiied                                                                                  1.04E+OO
                                                                                                                             "----~                                                                              t"----------*+ ... -*-*------***------------;-----*--**--*----,--------------*---*-----......;
*------------*---**-**--------------L_1-__10_2_2_1_A-_F_S_G_s_-0_04-               __s_s_-A     _______-t-_o~o_611~_2:2_0--9_13_12_0_1_9-r-_9_11012019                                                                                                                                                                                     1.28E-01 19-0900_1___ Manganese-54-i--*-*-E_P_____A___9_0__1_.1_M_o_d_ifi_,e_d____-+-----------~-------------------------*------------*------*--*--t L1-10221A-FSGS-004-SS-A                                                06/06/19 12:20 i 9/3/2019                         9/10/2019~ 19-09001 __ Molybdenum-93+---------------+------,-------~-------------------------------i                                                         4.87E-02 DUP                 L1-10221A-FSGS-004-SS-A                                                06/06/19 12:20 ! 9/3/2019                         9/10/2019
* 19-09001                    Niobium-94                                                                                                           9.88E-02 1--------**-+--------*-*------*-------------;--0-6-/06/...                                                                             19_1_2_:2_0___ -l_9_/3_/2_0_1_9......._9_/1-0-/2-0-19-.-19-09001                 Lead-2_1_0-+--::E,-::P*A,*-:9*co:-1.""1-----+----:c-*:---:***-'--:--:*=-:-::--i--*---:--:-:-::=-:c-*~-:-:---*-,--.:...*...:::.._;
DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                                                                                                                               2.87E+OO
                                                                                                                                                                  --+---=---------***---*----*------+----------------!-------*-+*---*-----+--*--*-~----'----*--"-;;;__*------1 DUP                 L1-10221A-FSGS-004-SS-A 1----------,'------*---'***--------------------*------+--06_1_06_119                                                                       12:20 i 9131201_9-+_9_11_0_,2_0_1_9-+-_19-?_9_00_1 ____L..:~~:_21_2__ t------------,**-*---                                                                                                     3.27E-01 DUP                 L1-10221A-FSGS-004-SS-A                                                06106119 12:20 -r-9/3/2019                        9/10/2019          19-09001               Lead-214                                                                                                           3.49E-01                            pCi/g
                                                  *------------+-                                                                                    ----+----,-
DUP                 L1-10221A-FSGS-004-SS-A 1----------'-*-----c-*-----*---------------+--06/06/19                                                                                     12:20        I 9/3/2019            9/10/2019          19-09001                                                                                                                                                             u        pCi/g DUP                 L1-10221A-FSGS-004-SS-A                                                06/06/19 12:20                 9/3/2019           9/10/2019          19-09001             Radium-226                                                                                                           3.26E-01                            pCi/g DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                                                                                                                               3.69E-01                   u 19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                                                                                                  1.40E+OO                     1.78E+OO                   u        pCi/g 19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                                                                                                  1.01E-01                     1.11E-01                            pCi/g 19-09001-03                  DUP                 L1-10221A-FSGS-004-SS-A                                                                                                                                                                                                                                  4.58E-01                     6.15E-01                   u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>               EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                         865/481-0683                          FAX  865/483-4621

Printed: 1012112019 11 :34 AM                                                                                                                                                                                                                     Page 6 of 21 Report To:                                                                       Work Order Details:
Patricia Giza                                                                                             19-09001 Eberline Analytical                                                                Zion Solutions SDG:
Purchase Order:       677118 Final Report of Analysis                                                       2701 Deborah
                                                                                                -"'""'"    _______ ,,._"'Ave                                            Analysis Category:      ENVIRONMENTAL Zion, IL 60099                                                                      Sample Matrix:       so Lab                   Sample                         Client                  Sample                   Receipt         Analysis    Batch                                                                                                                           Report ID                    Type                           ID                      Date                      Date              Date      ID Analyte          Method           Result            cu                         CSU         MDA    Qualifier Units 19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20              9/312019        9/10/2019  19-09001         Actinium-228   EPA 901.1 Modified   5.30E-01     2.49E-01                     2.50E-01     4.55E-01              pCi/g
    *-*---*----------A,__                                                                 " ' " " " " .---'<=~-"''""'m'"'="                                                                             - "   ' " ' " m - - = _ , , _ , , _ , __ ,_
19-09001-04                  DO L 1-10221A-FSGS-004-SS-A              06/06/19 12:20              9/3/2019
                                                                                -*------------""'"<"''---------*-*---~~--- "'
9/10/2019  19-09001         Silver-108m    EPA 901.1 Modified  -1.09E-02     4.03E-02                     4.03E-02     9.41E-02 19-09001-04                  DO         L 1-10221 A-FSGS-004-SS-A             06/06/19 12:20              9/3/2019        9/10/2019
                                                                              ---*-------~-- . .,,,_,,___-<*---------"*--,------
19-09001        Americium-241   EPA901.1 Modified   -1.62E-01      1.69E-01                    1.69E-01     2.04E-01     u        pCi/g 19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20              9/3/2019        9/10/2019  19-09001          Barium-133    EPA 901.1 Modified  -1.66E-02      5.22E-02                    5.22E-02     1.41E-01     u
-*----......;-----*--- ------------***-----*---*------- **-*----------* -----~-----                                                    m,~,-~-*--**-n, 19-09001-04                  DO         L1-10221A-FSGS-004-SS-A               06/06/19 12:20              9/3/2019        9/10/2019  19-09001         Bismuth-214    EPA901.1 Modified    5.07E-01      1.76E-01                    1.78E-01     3.28E-01 19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20              9/3/2019        9/10/2019  19-09001                                            2.52E+OO      2.36E-01                     2.69E-01     1.82E-01
                                                                                  ,~---~------ *---~- ------*--*--------- . ----------*
19-09001-04                  DO         L 1-10221 A-FSGS-004-SS-A             06/06/19 12:20              9/3/2019        9/10/2019  19-09001         Cesium-134     EPA 901.1 Modified  -5.53E-02      6.12E-02                    6.12E-02     8.97E-02     u
 ---*-                  -*--*------,,.*--..- - ~....-*---*--*---*
19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20              9/3/2019        9/10/2019  19-09001         Cesium-137     EPA 901.1 Modified  8.24E+OO       9.40E-01                    1.03E+OO     1.81E-01
                       -----*----.. .~-----&#xa5;*-------------                    -------'"'" ___
19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20              9/3/2019        9/10/2019  19-09001                        EPA 901.1 Modified  -6.65E-02      3.09E-01                    3.09E-01     2.83E-01     u 19-09001-04                  DO L 1-10221A-FSGS-004-SS-A
                                       . -~----*,=*-----..--
06/06/19 12:20 ,__,._,. 9/3/2019         ,  9/10/2019  19-09001 ,_/_, _______ , ______
Europium-154    EPA 901.1 Modified   3.88E-04      1.68E-01                    1.68E-01     1.44E-01     u 19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20
                                                                              ---*------~&#xa5;                   9/3/2019 9/10/2019  19-09001        Europium-155    EPA 901.1 Modified   1.19E-01      1.43E-01                     1.43E-01     1.89E-01    u
--*------              , ....---*--..-------------*-*--*------*                                                                                      "-------~---
19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20                              9/10/2019  19-09001        Holmium-166m    EPA 901.1 Modified                 1.06E-01                    1.06E-01     1.11E-01     u 19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20                              9/10/2019  19-09001          lodine-129    EPA 901.1 Modified                                            2.01E+01      4.16E+OO     u 19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A              06/06/19 12:20                              9/10/2019  19-09001         Potassium-40   EPA 901.1 Modified  1.25E+01      1.86E+OO                     1.97E+OO     8.55E-01 19-09001-04                  DO         L1-10221A-FSGS-004-SS-A               06/06/19 12:20                              9/1012019  19-09001        Manganese-54    EPA901.1 Modified                                              9.08E-02     1.29E-01     u 19-09001-04                  DO                                                                                                                     Molybdenum-93                                                                   5.98E-02     8.88E-02     u 19-09001-04                  DO                                                                                                                        Niobium-94                                                                   7.72E-02     8.53E-02     u 19-09001-04                  DO                                                                                                                         Lead-210                                                                   2.38E+OO      3.93E+OO     u 19-09001-04                  DO                                                                                                                         Lead-212                                                                    1.59E-01     3.61E-01 19-09001-04                  DO                                                                                                                         Lead-214                                        2.12E-01                    2.14E-01     3.77E-01 19-09001-04                  DO                                                                                                                                                                        1.16E+OO 19-09001-04                  DO                                                                                                                                      EPA 901.1 Modified                  1.76E-01                    1.78E-01    3.28E-01 19-09001-04         f        DO    _..______________                                                                                                                 EPA901.1 Modified    1.16E-01      2.23E-01                    2.23E-01     3.75E-01     u 19-09001-04                  DO         L1-10221A-FSGS-004-SS-A                                                                                                      EPA901.1 Modified    5.20E-01     1.44E+OO                                               u 19-09001-04                  DO         L 1-10221A-FSGS-004-SS-A                                                                                      Thallium-208                                      1.05E-01 19-09001-04                  DO         L1-10221A-FSGS-004-SS-A               06/06/19 12:20                                                          Uranium-235                                       5.13E-01                    5.13E-01     6.22E-01     u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(    ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601          SCARBORO ROAD OAK RIDGE,                          TN 37830       865/481-0683          FAX    865/483-4621

Printed: 10/21/2019 11 :34 AM                                                                                                                                                                                                                                                           Page 7 of 21 Report To:                                                                                 Work Order'Details:
Patricia Giza                                                                                                  19-09001 Eberline Analytical                                                                                             Zion Solutions SDG:
Purchase Order:       677118 Final Report of Analysis                                                                                  2701 Deborah Ave                                                               ...... Ana/ysisCategory:       ENVIRONMENTAL Zion, IL 60099                                                                           Sample Matrix:       so Lab               Sample                                     Client                                  Sample                   Receipt          Analysis             Batch                                                                                                                                              Report Type                                     ID                                        Date                    Date              Date               ID Analyte                Method           Result             cu             CSU            MDA                 Qualifier ID                                                                                                                                                                                                                                                                                                                     Units 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                              06/06/19 12:10                9/3/2019         9/10/2019         19-09001   Actinium-228        EPA 901.1 Modified   5.67E-01         2.19E-01        2.21E-01       4.71E-01                                           pCi/g 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                              06/06/19 12:10                9/3/2019         9/10/2019          19-09001  Silver-108m                                               6.34E-02        6.35E-02       1.09E-01                        U                  pCi/g
                                                                                                                                                                                                                                         --- ****-------------------------------------- -*-* *****-----* ,,,._ ,----,~----- ---
19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                              06/06/19 12:10                                 9/10/2019          19-09001 Americium-241                                              8.94E-02        8.95E-02       1.24E-01                        U                  pCi/g
                                                   ,--*-------"-------*--,                           ..j--- * - * * * - * - * - - * - - - - - - - , - - - - - - - - - - - - * - *                                                                                                             ....._. . . . . . . . . , - * - - - v*ce-*----""
19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                                                                              9/10/2019         19-09001    Balium-133         EPA 901.1 Modified                    1.18E-01        1.18E-01       1.32E-01                        U 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                                                                                               19-09001   Bismuth-214         EPA 901.1 Modified   4.88E-01         1.62E-01        1.64E-01       2.50E-01                                           pCi/g
                                      .. *-* -- ---------------------*-****----*---**-* - ---------------------*---t-----------------***---*----*-- -------------0-------------1-----------*----------------------
19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                                                                                                 19-09001    Cobalt-60         EPA901.1 Modified    5.12E-01         1.07E-01        1.10E-01       1.41E-01
 '""""' _ _ _ _,_,v' 19-09001-05
    -------------~---'"'"""'
19-09001-05 TRG TRG L1-10221A-FSGS-002-SS-A L1-10221A-FSGS-002-SS-A 19-09001 19-09001 Cesium-134 Cesium-137 EPA 901.1 Modified EPA901.1 Modified 4.37E-02 2.27E-01 4.37E-02 2.45E-01 1.18E-01 1.50E-01 u
     , __ , _ _ _ "'"'"-""'"<""-  os* , - - - - - - - " ' ' " " " ' _ _ _ _ _ _ , _ , _ _ _ **---***--*****-*-**--***--******--*****---.*--*--***'---*--***
                                                                                                                                                                                                                                 ----------*---~------**------------***---------~---
19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                                                                                                19-09001                       EPA901.1 Modified                     1.29E-01        1.29E-01       2.29E-01                        U 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                              EPA 901.1 Modified                                    2.65E-01       1.10E-01                        U 19-09001-05                    TRG           ,     L 1-10221A-FSGS-002-SS-A                                                                                                                              EPA 901.1 Modified                                    1.01 E-01      1.63E-01                        U
       ----------------------------------------- ------1----------------i--------,-----------****-------------------------11---------------* --,----------------*--------,--------------------------------------1 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                              EPA 901.1 Modified                                    1.07E-01       8.25E-02                        U
   ------------*-*-----****-----                                             ----*-----t-------------~c-----;-----*----*------*--*----*"-------1--*-*--*----**--*-*----********-*--*-------+-------;-----------------------*---------*--*----------1 19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                                                                                                                               EPA 901.1 Modified                                    2.30E-01       3.28E-01                        U 19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                                                                                                                                                                                                                                                       pCi/g
                      -----~---'-'-"
19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                                                                                                                               EPA901.1 Modified                                     7.70E-02       1.18E-01                        U 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                              EPA 901.1 Modified                                    5.42E-02       9.43E-02                        U                  pCi/g 0
                                  ~=--------*-*-----------1-----------*-+-----+-----*-*---*--*---------*---1--**-***--**-----*---*4*--*--*--******----+-------------*--------t 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                              EPA 901.1 Modified                                    6.09E-02       9.36E-02                        U
,__19-09001-05                     TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                                                                                                                                                      pCi/g 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                              EPA 901.1 Modified                                    1.24E-01       2.85E-01 19-09001-05                    TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                              EPA 901.1 Modified                                                   3.29E-01 TRG                 L 1-10221A-FSGS-002-SS-A                                                                                                                                                                                                                                   u                  pCiig 19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                                                                                                                               EPA 901.1 Modified                                                   2.50E-01                                           pCi/g 19-09001-05                    TRG                 L1-10221A-FSGS-002-SS-A                               06/06/19 12:10                                                                                  EPA 901.1 Modified                                                   3.38E-01                        u u
CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601       SCARBORO ROAD OAK RIDGE,                            TN 37830             865/481-0683          FAX     865/483-4621

Printed: 10/21/201911:34AM                                                                                                                                                                                                              Page 8 of 21 Report To:                                                                                        Work Order Details:
Patricia Giza                                                                                             19-09001 Eberline Analytical                                                              Zion    Solutions SDG:
Purchase Order:                   677118 Final Report of Analysis                                                  2701 Deborah Ave
                                                                                   *-,---*----~---                                                         Analysis_ Category: *-              ENVIRONMENTAL Zion, IL 60099                                                           Sample Matrix:                   so Lab                Sample                       Client                  Sample         Receipt   Analysis       Batch                                                                                                                                      Report Date       Date Analyte                     Method                     Result            cu             CSU                MDA      Qualifier ID                 Type                        ID                       Date                                   ID                                                                                                                                         Units 19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A              06/11/19 09:10    9/3/2019  9/10/2019    19-09001                                                                                         2.70E-01           5.24E-01       u 19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A           _ 06/1_1/19 0910 .. 9~2~_9     9/10/2019    19-09001                                                                                         7.64E-02           9.64E-02       u 19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A              06/11119 09:10    9/3/2019  9/10/2019    19-09001                                                                          1.10E-01       1.10E-01           1.58E-01       u 19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A              06/11/19 09:10    9/3/2019  9/10/2019    19-09001   Barium-133              EPA 901.1 Modified                             1.23E-01       1.24E-01           1.86E-01       u TRG        L1-10221 C-FSGS-012-SS-A             06/11/19 09:10    9/3/2019  9/10/2019    19-09001  Bismuth-214              EPA 901.1 Modified                             1.47E-01       1.51E-01           5.11E-01 TRG        L1-10221C-FSGS-012-SS-A           --~~~19 09: 10     : 9/3/20~ _ 9/10/2019 ---~-09001 _                          EPA 901.1 Modified ..__,,*.....*.**.---*----*,*---------*-
J~alt-6_&deg;. _____1____________________                                  1.07E-01    ___1__                1.34E-01       u
                                                                                                                                                                                                                           .0_7_E-_0_1 -------*--------*-**---*-*-----------*--t TRG        L1-10221   ________________
                                               '""""" C-FSGS-012-SS-A
                                                                                               . 9/3/2019
                                                                        -,--*---------*--*--+---**
9/10/2019    19-09001                           EPA 901.1 Modified                             1.38E-01       1.39E-01           1.27E-01
                                                                                                                                                    "'"'" -----,-----~= -+---------------------*-----*--*-------------------,---*--**"------!              u TRG        L1-10221 C-FSGS-012-SS-A                                                                                         EPA 901.1 Modified                             1.04E-01       1.05E-01           1.62E-01 TRG        L1-10221 C-FSGS-012-SS-A                                                                                         EPA 901.1 Modified                             1.55E-01       1.55E-01           2.50E-01       u TRG        L1-10221C-FSGS-012-SS-A                                                                                          EPA 901.1 Modified                             2.57E-01       2.57E-01           1.29E-01       u
  -***---~-----**                                         ***------------**-**+---------+-----'*--*---*--*---*-r-----;-----------t---*--
"""""'19-09001-06              TRG
       """"'"'""""___________,__________  L1-10221C-FSGS-012-SS-A
                                            "_'_"=---------------                                                                                          EPA 901.1 Modified                             9.18E-02       9.19E-02           1.94E-01       u 19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A                                                                                          EPA 901.1 Modified                             1.42E-01       1.42E-01           8.56E-02       u TRG        L1-10221 C-FSGS-012-SS-A                                                                                         EPA 901.1 Modified                                            7.97E-02           1.11E-01       u 19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A                                                                                          EPA 901.1 Modified                                           2.27E+OO            1.45E+OO 19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A                                                                                                                                                        8.72E-02           1.52E-01       u
 *-****---------------------*--**--------------+-~----.;__---':---------,------,--t---=---------jl---=---.-~-:------,---,-----=***-**---:----,-~--:-*-*+*----,-~-----*----
19-09001-06                 TRG        L1-10221C-FSGS-012-SS-A                                                                                                                                                        8.07E-02           9.06E-02       u 19-09001-06                 TRG        L1-10221 C-FSGS-012-SS-A                                                                                                                                                       7.27E-02           9.44E-02        u TRG        L1-10221 C-FSGS-012-SS-A                                                                                                                                                       8.56E-01           1.31E+OO       u 19-09001-06                 TRG                                                                                                                                                                                       1.28E-01           2.20E-01                  pCi/g 3.69E-01                  pCilg 1.38E-01       u 5.11E-01 3.06E-01       u Thorium-234                                                                            1.50E+OO           2.49E+OO       u Thallium-208             EPA901.1 Modified                                             1-73E-01           3.09E-01 L1-10221 C-FSGS-012-SS-A                                                                Uranium-235              EPA901.1 Modified                                             3.51E-01                          u          pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                               865/ 481-0683                    FAX    865/ 483-4621

Printed: 10/21/2019 11 :34 AM                                                                                                                                                                                                                                                              Page 9 of 21 Report To:                                                                                             Work Order Details:
Patricia Giza                                                                                                    19-09001 Eberline Analytical                                                                                                    Zion Solutions SDG:
Purchase Order:                   677118 Final Report of Analysis                                                                                           2701 Deborah Ave                                                             Analysis Category:                  ENVIRONMENTAL Zion, IL 60099                                                                   Sample Matrix:                  so Lab            Sample                                             Client                                       Sample                Receipt    Analysis        Batch                                                                                                                                      Report ID              Type                                                ID                                           Date                 Date        Date           ID Analyte            Method                      Result                cu           CSU             MDA       Qualifier Units 19-09001-07          TRG                  L 1-10221 C-FSGS-013-SS-A                                            06/11/19 09:15            9/3/2019   9/10/2019      19-09001         Actinium-228     EPA 901 _1 Modified             4_84E-01           2.01E-01                      4_07E-01
                                                                                                                                                                                                                                                                                    -----------~-
19-09001-07          TRG                  L 1-10221C-FSGS-013-SS-A                                             06/11/19 09:15            9/3/2019   9/10/2019      19-09001          Silver-108m                                                                                      8.27E-02       u          pCi/g
                                            ''"'"----*-----------------                                                                                                                                                                                                              &deg;'----------,--=-           --*--*-" -*---
19-09001-07          TRG                  L1-10221C-FSGS-013-SS-A                                              06/11/19 09:15            9/3/2019   9/10/2019      19-09001        Americium-241     EPA 901 _1 Modified
                                                  ,-,--------*--*----*-----,,                                                                                                                           __ ,,,---.*-*------,-       __ ,-1.28E-01           9_25E-02      9.27E-02        1.24E-01
__,_,__,__,, ___,_,_,._,,--w----------------*---*--**-           U 19-09001-07 TRG
                         ---,----~----
L1-10221C-FSGS-013-SS-A            ____ _________ --~
                                                                                                ,                  06/11/1909:15
____________ ,        9/3/2019   9/10/2019      19-09001
                                                                                                                                      ""'""'=-------~------*-------,w--,w Barium-133
                                                                                                                                                                                       *A' EPA 901 _1 Modified             2_91E-02           1_17E-01       1_17E-01       1.41E-01        U 19-09001-07           TRG                 L1-10221C-FSGS-013-SS-A                                              06/11/1909:15             9/3/2019   9/10/2019      19-09001          Bismuth-214     EPA901.1 Modified               7.43E-01           1_75E-01       1_79E-01       2_26E-01
_____L_1___1_0___2_2____1___c_____F_S_G_._s_____o._1__
3_-S-S--A-----+---0-6_/_1._1_/_1_9__o*-9*---:15  ' 9/3/2019 . 9/10/2019 ____ - ; 9 ~             Cobalt-60     EPA 901 _1 Mo--d--ifi*-,e-d*---*---------*----------------------
19-09001-07          TRG                                                                                                                                                                                                             1.SOE-02           9.42E-02      9.42E-02        1.55E-01       u 19-09001-0_'.._ __ TRG _____ ----~_1.:1022:~:tSGS-013-SS-A                                         _           06/11/19 09:15            9/3/2019
__,_,,_._ w-------'-"**--- ""' w-,-
9/10/2019      19-09001
                                                                                                                                                                   - - - * - :~*
Cesium-134
__ w, EPA901_1 Modified               9.24E-03           2.70E-02      2.70E-02        1_17E-01        u 19-09001-07           TRG                 L1-10221C-FSGS-013-SS-A                                              06/11/1909:15             9/3/2019   9/10/2019      19-09001          Cesium-137      EPA901_1 Modified               1_76E-01           9_04E-02      9.09E-02        1.39E-01
,-------------------- -------------*------------------------------*-t---                                               --*-***-m**-*-~       --~-,-----=**---____               ,_"\me
                                                                                                                                                                                       -------+-----------------------------r------------------------------>*---------------------*-*------'-------~---1 19-09001-07           TRG                 L 1-10221C-FSGS-013-SS-A                                             06/11/19 09:15            9/3/2019   9/10/2019      19-09001         Europium-152     EPA 901_1 Modified              1_23E-01           1_97E-01      1_97E-01        1.91E-01        u 19-09001-07           TRG                 L 1-10221C-FSGS-013-SS-A                                             06/11/19 09:15            9/3/2019   9/10/2019      19-09001                          EPA 901.1 Modified             -1.42E-02           2_53E-01      2.53E-01        9_92E-02        u 19-09001-07           TRG                 L1-10221C-FSGS-013-SS-A                                              06/11/19 09:15            9/3/2019   9/10/2019      19-09001                          EPA 901.1 Modified                                 1.23E-01       1_23E-01       1.88E-01        u 19-09001-07           TRG            __________________
L1-10221C-FSGS-013-SS-A                        " _____,              06/11/19 09:15            9/3/2019   9/10/2019      19-09001                          EPA 901 _1 Modified            -1_69E-02                         9_63E-02        8_61E-02       u 19-09001-07           TRG                 L1-10221C-FSGS-013-SS-A                                              06/11/19 09:15                       9/10/2019      19-09001                          EPA901_1 Modified               6_07E-02                         2.25E-01        3_32E-01       u 19-09001-07           TRG                 L1-10221C-FSGS-013-SS-A                                              06/11/19 09:15                       9/10/2019      19-09001                          EPA 901.1 Modified             2.05E+01                          4_02E+OO        1_13E+OO
     -----,------------------------------t-------------------~-----+--------------------+---------+-------------------f-----------,----~,--------------------:-----'---=----1 19-09001-07 .         TRG                 L1-10221C-FSGS-013-SS-A                                              06/11/19 09:15                       9/10/2019      19-09001                          EPA901_1 Modified               1_74E-02                         7_27E-02        1.19E-01        u
     -------------------------*--------------------+-----------------i-----c-----------<---------''-------+--------------------+-----------C---------~----------------------------------"---;;:_---1 19-09001-07           TRG                 L1-10221C-FSGS-013-SS-A                                      ___,1------
06/11/19 09:15                                                                        EPA 901.1 Modified        . 9.84E-03               5.20E-02      5_20E-02        8.58E-02        u
_ _ _ _ _ _ _ _ _ 'f""' _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
                                                                                                                                                                                                        ----- *------~--- - - - -
19-09001         TRG                 L 1-10221C-FSGS-013-SS-A                                             06/11/19 09:15                                                                        EPA 901 _1 Modified            -2.00E-02           5_34E-02      5_34E-02        8_30E-02        u TRG                 L 1-10221C-FSGS-013-SS-A                                                                                                                                   EPA 901_1 Modified             1.32E+OO            1_25E+OO      1_25E+OO        2.08E+OO       u TRG                 L 1-10221C-FSGS-013-SS-A                                                                                                                                   EPA901_1 Modified                                                1_16E-01        2_05E-01 19-09001-07           TRG                 L 1-10221C-FSGS-013-SS-A                                                                                                                                   EPA901_1 Modified                                                1.49E-01        2.44E-01 19-09001-07           TRG                 L 1-10221 C-FSGS-013-SS-A                                            06/11/19 09:15                                      19-09001                          EPA 901_1 Modified                                                1.50E-01       2.23E-01        u 19-09001-07           TRG                 L 1-10221C-FSGS-013-SS-A                                             06/11/19 09:15                                      19-09001                          EPA 901.1 Modified                                                1_79E-01       2.26E-01                  pCi/g 19-09001-07          TRG                  L 1-10221C-FSGS-013-SS-A                                             06/11/19 09:15                                      19-09001                          EPA901.1 Modified                                                 1_93E-01       2_53E-01        u         pCi/g 19-09001-07           TRG                 L1-10221C-FSGS-013-SS-A                                              06/11/19 09:15                                      19-09001                          EPA901_1 Modified                                                                               u          pCi/g TRG                 L1-10221 C-FSGS-013-SS-A                                             06/11/19 09:15                                      19-09001                          EPA 901.1 Modified 19-09001-07           TRG                 L 1-10221C-FSGS-013-SS-A                                             06/11/19 09:15                                      19-09001         Uranium-235      EPA 901_1 Modified                                                                              u          pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(  "'M> EBERLINE                                                  ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601      SCARBORO ROAD OAK RIDGE,                       TN 37830          865/481-0683                     FAX      865/483-4621

Printed: 101211201911:34AM                                                                                                                                                                                                                                              Page 10 of 21 Report To:                                                                                                         Work Order Details:
Patricia Giza                                                                                                              19-09001 Eberline Analytical                                                                       Zion Solutions                                                                     Purchase Order:
SDG:
677118 Final Report of Analysis                                                             2701 Deborah Ave                                                               Analysis Category: .                        ENVIRONMENTAL Zion, IL 60099                                                                       Sample Matrix:                        so Lab                 Sample                     Client                             Sample                        Analysis       Batch                                                                                                                                                           Report Analyte                     Method                           Result               cu              CSU          MDA             Qualifier ID                  Type                       ID                                 Date                           Date           ID                                                                                                                                                            Units 19-09001-08                  TRG                                                      06/11/19 09:20                   9/10/2019     19-09001       Actinium-228            EPA 901.1 Modified                     3.24E-01           2.23E-01        2.24E-01      3.84E-01                           pCi/g 19-09001-08                  TRG                                                                                                                    Si1ver-108m
                                                                                                                                                                 ----,f---*
EPA901.1Modified                                          5.45E-02        5.45E-02     7.08E-02                              _____
pCi/g 19-09001-08                  TRG                                                                                                                   Americium-241            EPA901.1 Modified                                         1.10E-01         1.10E-01     1.45E-01
----******-* -------                  - - - - --* ----*--*****                      +*----*--*-**********---~----***--***-*---------*-*********-------*---*****---*****-+-
19-09001-08                  TRG     L1-10221C-FSGS-014-SS-A                          06/11/1909:20       9/3/2019     9/10/2019     19-09001        Barium-133             EPA901.1 Modified                     -1.81E-01           1.07E-01         1.07E-01     9.57E-02 19-09001-08 ~--T-RG*-~""i'1"~10221C-F.sG*s--0           ..SS-A                   06/11/1909:20     I 9/3/2019 ' 9/10/2019       19-osoo1""~w--Bi~-u-th--2-14           EPA901.1 Modified                      3.55E-01           1.08E-01         1.09E-01     1.66E-01
    ***********-*--*****--*-**-*-**-------**********------**--*-***************-******-f--                                                          -*-*-***-------t-**--*-******-******--****-------------~---***
19-09001-08                  TRG     L1-10221C-FSGS-014-SS-A
                                                 ---------~-,_,__                        06/11/19 09:20      9/3/2019     9/10/2019     19-09001         Cobalt-60             EPA 901.1 Modified                     5.93E-01           9.00E-02
_.,,. __ ,_ - - - * *- --,-- --~----- ,.,,, _____________ --------------~-,-
9.50E-02      1.17E-01
                                                                                                                                                                                                                                                                                                . ******- pCi/g 19-09001-08 .                TRG     L1-10221C-FSGS-014-SS-A                          06/11/1909:20       9/3/2019     9/10/2019     19-09001       Cesium-134              EPA901.1 Modified                      7.28E-03           2.90E-02         2.90E-02     5.86E-02             u 9/3/2019     9/10/2019     19-09001       Cesium-137              EPA 901.1 Modified                     2.29E+OO           2.83E-01         3.06E-01     1.47E-01
                                                                                                                                                                                                                 --------------,-----*                             ,--"----~'""
9/3/2019     9/10/2019     19-09001                               EPA 901.1 Modified                     6.00E-02           2.23E-01         2.23E-01     2.00E-01             u 19-09001-08                  TRG     L1-10221C-FSGS-014-SS-A                                              9/3/2019     9/10/2019                                            EPA 901.1 Modified                     7.62E-02           1.36E-01         1.36E-01     9.93E-02             u 19-09001-08 ,                TRG     L1-10221C-FSGS-014-SS-A                                              9/3/2019     9/10/2019                                            EPA901.1 Modified                                         5.02E-02         5.03E-02     1.41E-01             u 19-09001-08                  TRG     L1-10221 C-FSGS-014-SS-A                         06/11/19 09:20      9/3/2019     9/10/2019                                            EPA 901.1 Modified                                        8.25E-02         8.25E-02    7.86E-02              u
                                                                ***--*------~l---------l-----i----------*--c--***----*-----l-----------;*********-**-------*------;,.---*---*-**--------**---***------------.:....::...---1 19-09001-08                  TRG     L1-10221C-FSGS-014-SS-A                                              9/3/2019     9/10/2019                                            EPA901.1 Modified                     -1.54E+OO          7.48E+OO         7.48E+OO     3.13E+OO              u
-'"""'----~----*--~--------------*----..---,--"
19-09001-08                  TRG     L1-10221 C-FSGS-014-SS-A                                             9/3/2019     9/10/2019                                                                                   1.29E+01 19-09001-08                  TRG     L1-10221C-FSGS-014-SS-A                                                                                                                                                      -2.52E-02                                         8.07E-02             u 1 - - - - - - + - .- - * - * - - - - -                         **--*
19-09001-08                  TRG     L1-10221C-FSGS-014-SS-A                                                                                                                                                      -3.90E-03                                         5.93E-02             u 19-09001-08                  TRG     L 1-10221C-FSGS-014-SS-A                                                                                                                                                                         4.46E-02         4.46E-02     6.58E-02             u 19-09001-08                  TRG     L1-10221 C-FSGS-014-SS-A                                                                                                                                                                        1.73E+OO         1.73E+OO                           u 19-09001-08 TRG     L1-10221C-FSGS-014-SS-A                                                                                                                EPA901.1 Modified                      4.83E-01                            1.03E-01     3.30E-01                           pCi/g 19-09001-08                  TRG     L1-10221C-FSGS-014-SS-A                                                                                                                EPA901.1 Modified                      6.07E-01                            1.59E-01     2.75E-01                           pCi/g TRG     L1-10221C-FSGS-014-SS-A                                                                                                                EPA901.1 Modified                      9.65E-01                            8.09E-01     9.80E-01             u
                                                                  -----+*-------+-----+----*---*-------:------*-------;----------****-,*-*-----,
L1-10221C-FSGS-014-SS-A                                                                                                                EPA 901.1 Modified                                                                      1.66E-01 u             pCVg EPA 901.1 Modified                                                                                           u             pCVg Thallium-208            EPA 901.1 Modified                                                                                                         pCi/g Uranium-235             EPA 901.1 Modified                    -2.28E-01                                                              u             pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>               EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                         865/481-0683                            FAX 865/483-4621

Printed: 10/21/201911:34AM                                                                                                                                                                                              Page 11 of 21 Report To:                                                                                Work Order Details:
Patricia Giza                                                                                             19-09001 Eberline Analytical                                                       Zion Solutions SDG:
Purchase Order:           677118 Final Report of Analysis                                               2701 Deborah Ave                                                             Analysis Catefjory           E NVI RON MENTAL Zion, IL 60099                                                                  Sample Matrix:            so Lab        Sample                    Client                       Sample              Receipt         Analysis           Batch                                                                                                          Report ID                                                Date            Date Analyte            Method               Result           cu            CSU      MDA    Qualifier ID         Type                                                     Date                                                 ID                                                                                                             Units 19-09001-09     TRG        L 1-10221A-FIGS-001-SS-A             06/11/19 12:15           9/312019        9/10/2019      19-09001       Actinium-228     EPA901.1 Modified      4-77E-01        5.95E-01       5.96E-01 19-09001-09     TRG        L 1-10221A-FIGS-001-SS-A             06/11/19 12:15           9/3/2019        9/10/2019      19-09001        Silver-108m     EPA 901-1 Modified                      U1E-01        U1E-01
                                                            ""' * - - - * - o w e *                                                    -------
19-09001-09     TRG        L 1-10221A-FIGS-001-SS-A             06/11/1912:15            9/3/2019         9/10/2019     19-09001      Americium-241                                             1.48E-01      1.48E-01
                                  *-                                                ---"'~-------
19-09001-09     TRG        L 1-10221A-FIGS-001-SS-A             06/11/19 12:15           9/312019         9/10/2019     19-09001        Barium-133                                              1.06E-01      1.06E-01              u
                                                            ---*-------*--*-                      '""" - -~---*----------- ---**-------*-*--------------*
19-09001-09     TRG        L1-10221A-FIGS-001-SS-A              06111/19 12:15           9/312019         9/10/2019     19-09001
                                                                                                                        ,w, 0 Bismuth-214
                                                                                                                              ,,-,*=------------~    mm-,
3.07E-01      3.08E-01 4.42E-01     u 19-09001-09     TRG        L 1-10221A-FIGS-001-SS-A             06/11119 12:15           9/312019        9110/2019      19-09001         Cobalt-60                                             4.04E-01       4.74E-01 2.52E-01
--"*-------~--*---*~*------*---~-- '"-------~----
19-09001-09     TRG                                                                                                                                                                             1.76E-01      1.76E-01 2.04E-01    u 1.15E+OO       1.26E+OO 3.24E-01 4.91E-01      4.91E-01 4.15E-01     u 2.48E-01      2.49E-01 2.12E-01     u 1.90E-01      1.90E-01 2.76E-01     u 7.31E-02       7.31E-02 1.48E-01     u 19-09001-09     TRG                                                                                                                                                                                           5.33E-02 2.21E-01     u TRG                                                                                                                                                                                           1.88E+OO 1.66E+OO TRG                                                                                                                                                                                           1.71E-01 2.82E-01     u TRG                                                                                                                                                                                                    1.15E-01     u 1.83E-01     u 06/11/19 12:15                                                                                                                                         1.91E+OO     u 06/11/19 12:15                                                                                                                                         4.74E-01 06/11/19 12:15                                                                                                                                         4.72E-01 TRG        L 1-10221A-FIGS-001-SS-A             06/11/19 12:15                            9/10/2019                                                                                                    2.45E-01     u TRG        L 1-10221A-FIGS-001-SS-A                                                       9/10/2019     19-09001        Radium-226                                                                     4.42E-01     u TRG        L1-10221A-FIGS-001-SS-A                                                        9/10/2019     19-09001      Antimony-125                                                                     7.38E-01     u TRG        L1-10221A-FIGS-001-SS-A                                                        9/10/2019     19-09001       Thorium-234                                                                                  u        pCi/g TRG        L 1-10221A-FIGS-001-SS-A                                                       9/10/2019     19-09001       Thallium-208     EPA901.1                                                                    u        pCi/g TRG        L 1-10221A-FIGS-001-SS-A                                                       9/10/2019     19-09001       Uranium-235                                                                                  u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
( ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                     865/481-0683               FAX 865/483-4621

Printed: 10/21/201911:34AM                                                                                                                                                                                                                                             Page 12 of 21 Report To:                                                                                  Work Order Details:
Patricia Giza                                                                                                        19-09001 Eberline Analytical                                                                     Zion Solutions SDG:
Purchase Order:       677118 Final Report of Analysis                                                          2701 Deborah Ave                                                                           Analysis Category: _      ENVIRONMENTAL Zion, IL 60099                                                                                  Sample Matrix:       so Lab                       Sample                     Client                    Sample                    Receipt         Analysis       Batch                                                                                                                                                        Report ID                       Type                        ID                        Date                     Date              Date          ID Analyte                   Method           Result         cu                   CSU                        MDA        Qualifier Units 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A                                                         9/10/2019     19-09001       Actinium-228             EPA 901.1 Modified   8.03E-01     2.69E-01           2.72E-01                     4.13E-01                             pCilg 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A 9/10/2019     19-09001        Si1ver-108m             EPA 901.1 Modified   5.26E-04          ___
6.72E-02 ___
6.72E-02                     1.03E-01         u 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A                                                         9/10/2019     19-09001      Americium-241             EPA901.1 Modified   -1.26E-01     9.46E-02           9.49E-02                     1.26E-01          u 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/1912:15                                9/10/2019     19-09001        Barium-133              EPA 901.1 Modified   1.24E-01     1.12E-01           1.12E-01                     1.50E-01          u                  pCi/g 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/19 12:15              9/3/2019         9/10/2019     19-09001        Bismuth-214             EPA 901.1 Modified   3.24E-01     1.43E-01           1.44E-01                     2.84E-01
                                                                                             -------- ----*---- --> m-.-'-"-.N"-- >       ------------~*        '
                                                                                                                                                                                 *******+---
19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/19 12:15              9/3/2019         9/10/2019     19-09001          Cobalt-60             EPA 901.1 Modified   4.96E-01     9.43E-02           9.77E-02                     1.25E-01                             pCi/g
                                                                                                                                                                                                                                           , , , , _ mv _ _ _ _ , _ _ _ _ _ _
                                                                                                                                                                                                                                                                                                    ._,,m, ,_,_, * - - - - ' " ' ' -
19-09001-10 :                      TRG      . L1-10221A-QIGS-001-SS-A            06/11/1912:15               9/3/2019         9/10/2019                     Cesium-134              EPA 901.1 Modified   6.42E-03     4.74E-02           4.74E-02                     1.18E-01         u 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/1912:15               9/3/2019         9/10/2019                     Cesium-137              EPA 901.1 Modified  2.14E+OO      2.85E-01           3.06E-01                     1.40E-01 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/1912:15               9/3/2019         9/10/2019                                             EPA901.1 Modified   -1.93E-01     2.53E-01
                                      ----*-***** *-*--*-**********-----**-***--1--*---**----*******-i*---------*-****"""-*******---'----'-----+-*---***-*---'---------****t--*---=**.........../-...::....~:.::.________....::.:.:..::.....:.._
2.53E-01                     2.28E-01         u 19-09001 ~ - - - L1-102}_1_1,:_<?_19'S-001-~~---*                             06/11/19 12:15              9/3/2019         9/10/2019     19-09001                                EPA 901.1 Modified  -7.59E-02     1.64E-01           1.64E-01                     1.18E-01         u 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/19 12:15              9/3/2019         9/10/2019     19-09001                                EPA 901.1 Modified   7.72E-02     1.12E-01           1.12E-01                     1.66E-01          u
                                                                   **-*---*---*+***-*-------********---****-*--***~--------*******--*--'----****-****l*****--****--********-*---*-*-*+*-------C-*-*----**--*-*-*-**---*****-
19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/19 12:15              9/3/2019         9/10/2019     19-09001                                EPA 901.1 Modified  -1.36E-02     1.18E-01           1.18E-01                     8.34E-02         u
  **-*-**-*********-*************-**----------****--***-*--l-***--**-**-- -'***--***--****-*---C---******--********-*****--l,*******----***-**----+*--*-*--'-**---************--*-**-
19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/19 12:15              9/3/2019         9/10/2019     19-09001         lodine-129             EPA 901.1 Modified   3.24E-02
                                                                                                                                                                                                                          '   7.32E-02           7.33E-02                     1.10E-01         u 19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/1912:15                                9/10/2019     19-09001       Potassium-40             EPA 901.1 Modified                1.60E+OO          1.68E+OO                      7.97E-01
                          *--*-**-****-*-***-***-**-------******-**--*-J---*-**---***-**+-------**-***-****-**-------~---******-*-***-1-----*---------++--*'"-**-**------*******<---***----
19-09001-10                        TRG          L1-10221A-QIGS-001-SS-A            06/11/1912:15                                9/10/2019                                                                                                  7.77E-02                     1.32E-01          u
                                                    ****-------------***--!--**-*--*--*---,****-*-------**--*****----r------1---*
L1-10221A-QIGS-001-SS-A            06/11/19 12:15                               9/10/2019                                                                                                  6.78E-02                     8.39E-02          u 6.11E-02                     9.31E-02          u 8.15E-01                     1.36E+OO         u 19-09001                                                                                     1.12E-01                     2.36E-01 19-09001                                                                                     1.29E-01                     3.70E-01 9/10/2019     19-09001                                                                                     9.33E-02                     1.29E-01         u 9/10/2019     19-09001 9/10/2019     19-09001 L1-10221A-QIGS-001-SS-A            06/11/19                                     9/10/2019     19-09001                                                                                                                                   u                   pCi/g L1-10221A-QIGS-001-SS-A            06/11/19                                     9/10/2019     19-09001                                                                                     1.65E-01                     2.42E-01                             pCi/g TRG          L1-10221A-QIGS-001-SS-A                                                         9/10/2019     19-09001                                                                                     3.30E-01                     4.73E-01         u                   pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
(    "'M> EBERLINE                                ANAL YT! CAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                    865/481-0683          FAX 865/483-4621

Printed: 10/21/201911:34AM                                                                                                                                                                                                                             Page 13 of 21 Report To:                                                                                          Work Order Details:
Patricia Giza                                                                                                                 19-09001 Eberline Analytical                                                             Zion Solutions ___                ____  ,                                                        Purchase Order:
SDG.
677118 Final Report of Analysis                                                     2701 Deborah Ave                                                                          _.. Analysis. Category: ..           ENVIRONMENTAL Zion, IL 60099                                                                                      Sample Matrix:             so Lab           Sample                         Client                    Sample                             Receipt     Analysis     Batch                                                                                                                               Report ID             Type                          ID                                                            Date        Date         ID Analyte                     Method                 Result          cu                  CSU    MDA     Qualifier Date                                                                                                                                                                                          Units 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/19 12:17                         9/3/2019   9/10/2019    19-09001         Actinium-228            EPA 901.1 Modified           2.28E-01     3A9E-01             3A9E-01  5.71E-01     u        pCi/g 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/1912:17 w,'---*-*--                            9/3/2019   9/10/2019 " _____
                                                                                                 .... . . ., ____________________       19-09001 . --**--'""*-------
Silver-108m            EPA 901.1 Modified          -3.68E-02     8-57E-02            8-57E-02 1.30E-01    u
                ',-w,**--*--**----*----"''-""'--*---*----
19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/1912:17                          9/3/2019   9/10/2019    19-09001        Americium-241            EPA 901.1 Modified                                            1-01E-01 1A3E-01      u        pCi/g
                                                                          - - * - - * - * - - - - " " "">'- - - -        ,-------m-o~--'"-"-"''-* '""'
19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/1912:17                          9/3/2019   9/10/2019    19-09001          Barium-133
                                                                                                                                                 , _ _, _______                  EPA90U Modified
                                                                                                                                                                    ,,,, -+*---*-----------------------*--*-                                   7.86E-02 1.53E-01     u        pCi/g 19-09001-11          TRG            L 1-10221A-FIGS-002-SS-A           06/11/19 12:17                         9/3/2019   9/10/2019    19-09001         Bismuth-214             EPA901.1 Modified            6.11E-01      1-75E-01           1.78E-01 4.10E-01
                                                                                                             *- *------'--------*------- ,,,*--------------*+--------*------*---*----- ---.-----------------*-:----------------
19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/19 12:17                         9/3/2019   9/10/2019    19-09001            Cobalt-60            EPA 901-1 Modified          3.13E+OO      3.21E-01            3-59E-01 2.31E-01 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A                                                                                             Cesium-134                                                       4A2E-02             4A2E-02  1A9E-01 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A                                                                                             Cesium-137                                                       8-68E-01            9.85E-01 1.88E-01 EPA 901.1 Modified                        3.27E-01            3.27E-01 2.78E-01 EPA 901.1 Modified          -1.39E-02      2.39E-01           2.39E-01 1A5E-01 19-09001-11          TRG            L1-10221 A-FIGS-002-SS-A                                                                                                                                                9A4E-02       U5E-01             U5E-01   1-69E-01 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/19 12:17                                                 19-09001                                               Modified      -3.74E-02      1-31E-01           1-31E-01 1-0SE-01    U         pCi/g
   ------------------------------------*-1-------------------------------------*--------------s----------t-----------------*-----,------*-------*---------------------------------------------<
19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/1912:17                                                  19-09001           lodine-129            EPA 901-1 Modified          -1A2E-02       1A4E-01            1A4E-01  4.33E-01    U         pCi/g
                                                            -----*--**---1-----------------;-------------------------------+--,-----------,-------------------------------*---------------~---------------------------------------<
19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/1912:17                                                                                           EPA 901-1 Modified          1.53E+01                          3.08E+OO U4E+OO 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A                                                                                                                    EPA 901.1 Modified           6.25E-02      1-03E-01                    1.67E-01 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A                                                                                                                    EPA 901-1 Modified           4.54E-02     7.22E-02            7.23E-02 1.0SE-01 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A                                                                                                                    EPA901.1 Modified            1.54E-02     9-34E-02            9.34E-02 1.09E-01 19-09001-11          TRG                                                                                                                                                       EPA901.1 Modified           1.12E+OO
                                - -L1-10221A-FIGS-002-SS-A
                                        - - ----------------1-----:      06/11/19
_____________  12:17 _;______ ,_ ________;,____-+------------l----------*-                                                                                          1.06E+OO 1.75E+OO 19-09001-11   -      TRG            L1-10221A-FIGS-002-SS-A            06/11/1912:17                                                                                           EPA901.1 Modified            4.74E-01                                  4.73E-01
                '----*-*=--*------* -
19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/19 12:17                                                                                          EPA901.1 Modified            4.75E-01                                  3.67E-01 1----------*----*=
19-09001-11          TRG            L1-10221A-FIGS-002-SS-A            06/11/19 12:17                                                                                          EPA901.1 Modified           -6AOE-02                                   2.85E-01     u        pCi/g L1-10221A-FIGS-002-SS-A                                                                                                                    EPA 901.1 Modified           6.11E-01                                  4.10E-01 L1-10221A-FIGS-002-SS-A                                                                                                                    EPA 901.1 Modified          36E-01                                  5.07E-01     u L 1-10221A-FIGS-002-SS-A                                                                                                                   EPA 901-1 Modified           5.66E-01                                  1-32E+OO     u 19-09001-11          TRG            L1-10221A-FIGS-002-SS-A                                                                                            Thallium-208                                         4.76E-01                                  5.15E-01     u 19-09001-11          TRG            L1-10221 A-FIGS-002-SS-A                                                                                           Uranium-235             EPA 901-1 Modified           2.00E-01                                  5.98E-01     u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
( ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601          SCARBORO ROAD OAK RIDGE,                           TN 37830                 865/481-0683                 FAX   865/483-4621

Printed: 10/21/201911:34 AM                                                                                                                                                                                       Page 14 of 21 Report To:                                                                         Work Order Details:
Patricia Giza                                                                                                 19-09001 Eberline Analytical                                               -  ~,v._.,__,_,., * - -
* Zion Solutions SDG:
Purchase Order:          677118 Final Report of Analysis                                         2701 Deborah Ave                                                                  Analysis Category: ..      ENVIRONMENTAL Zion, IL 60099                                                                       Sample Matrix:          so Lab         Sample                    Client                 Sample                        Receipt    Analysis          Batch                                                                                                     Report ID          Type                      ID                      Date                          Date       Date               ID Analyte        Method              Result       cu            CSU      MDA    Qualifier Units 19-09001-12      TRG       L 1-10221 A-Fl GS-003-SS-A         06/11119 12:19                   9/3/2019                                   Actinium-228 EPA901.1 Modified       5.38E-01   2.63E-01 TRG       L 1-10221A-FIGS-003-SS-A           06/11/1912:19                    9/3/2019   9/10/2019                        Si1ver-108m EPA 901.1 Modified      2.SSE-02   6.48E-02 19-09001-12      TRG       L 1-10221A-FIGS-003-SS-A           06/11119 12:19                   9/3/2019   9/10/2019        19-09001                    EPA 901.1 Modified                                        1.20E-01     u 19-09001-12      TRG       L 1-10221A-FIGS-003-SS-A                                            9/3/2019   9/10/2019        19-09001                    EPA 901.1 Modified      1.19E-02   3.82E-02      3.82E-02 1.26E-01     u EPA901.1 Modified       2.83E-01   2.0SE-01      2.0SE-01 3.68E-01     u EPA 901.1 Modified                 2.06E-01      2.27E-01 1.98E-01 EPA 901.1 Modified      1.20E-02   3.52E-02      3.53E-02 1.23E-01     u EPA 901.1 Modified                 5.89E-01      6.64E-01 1.82E-01 EPA 901.1 Modified                 2.71E-01      2.71E-01 2.20E-01     u 19-09001-12      TRG       L 1-10221A-FIGS-003-SS-A           06/11119 12:19                   9/3/2019   9/10/2019                                    EPA901.1 Modified                  2.14E-01      2.14E-01 1.12E-01     u
---------------*-*-            ---*---*---*---------*-*-*- '"' -*---------+-------*-*-----*-*
19-09001-12      TRG       L1-10221A-FIGS-003-SS-A            06/11119 12:19 ' ----            9/312019   9/10/2019                                    EPA901.1 Modified                  9.54E-02      9.54E-02 1.35E-01     u 19-09001-12      TRG       L 1-10221A-FIGS-003-SS-A           06/11/1912:19 i 9/3/2019                    9/10/2019        19-09001                    EPA 901.1 Modified                 1.07E-01      107E-01  9.10E-02     u 19-09001-12      TRG       L 1-10221 A-FIGS-003-SS-A          06/11/19 12:19                 ' 9/312019   9/10/2019        19-09001                    EPA 901.1 Modified                 9.56E-02      9.56E-02 3.75E-01     u 19-09001-12      TRG       L 1-10221A-FIGS-003-SS-A           06/11/1912~*+* 9/3/2019                     9/10/2019        19-09001       Potassium-40 EPA901.1 Modified                  2.45E+OO      2.52E+OO 1.44E+OO 19-09001-12                L 1-10221A-FIGS-003-SS-A           06111/19 12:19                   9/3/2019   9/10/2019        19-09001      Manganese-54                                     4.74E-02      4.74E-02 1.23E-01     u 19-09001-12                L1-10221A-FIGS-003-SS-A            06/11/19 12:19                   9/3/2019   9/10/2019        19-09001     Molybdenum-93                                                   5.44E-02 6.41E-02     u 19-09001-12                L 1-10221A-FIGS-003-SS-A           06/11/19 12:19                 ! 9/3/2019
                                                                                                                 ------------=-
9/10/2019        19-09001        Niobium-94                                                   7.0SE-02 9.56E-02     u 19-09001-12                L 1-10221A-FIGS-003-SS-A           06/11/1912:19                               9/10/2019        19-09001         Lead-210                                                             1.34E+OO     u L 1-10221A-FIGS-003-SS-A                                                       9/10/2019        19-09001
                                                                                                                                       --      Lead-212                                                             2.89E-01 9/10/2019        19-09001         Lead-214                                                             3.63E-01     u u
9/10/2019        19-09001     Promethium-145                                                           2.31E-01 9/10/2019   .,.. 19-09001        Radium-226                                                            3.68E-01     u L 1-10221 A-FIGS-003-SS-A                                           9/3/2019   9/10/2019        19-09001      Antimony-125                                                            4.07E-01     u L 1-10221A-FIGS-003-SS-A           06/11/1912:19                    9/3/2019 9/10/2019 _..._ 19-09001        Thorium-234                                                                        u L 1-10221A-FIGS-003-SS-A           06/11/1912:19                    9/3/2019   9/10/2019
* 19-09001            Thallium-208 L 1-10221A-FIGS-003-SS-A           06/11/1912:19                    9/3/2019   9/10/2019        19-09001       Uranium-235                                                                         u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(  ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                         865/481-0683             FAX 865/483-4621

Printed: 1012112019 11 :34 AM                                                                                                                                                                                                                                                                 Page 15 of 21 Report To:                                                                                                       Work Order Details:
Patricia Giza                                                                                                                  19-09001 Eberline Analytical                                                                                                                                                                                                                   SDG:
Final Report of Analysis Zion Solutions                                                                                                  ______         677118 Purchase Order: . __ --'-"""'-**-***-**-----*
                                                                                                            , __          2701 Deborah Ave                                                                   ..            Analysis Category:,           ENVIRONMENTAL Zion, IL 60099                                                                                      Sample Matrix.*            so Lab                  Sample                                         Client                              Sample                 Receipt         Analysis        Batch                                                                                                                                                Report Analyte                           Method               Result                 cu             CSU        MDA       Qualifier ID                    Type                                            ID                                  Date                   Date              Date          ID                                                                                                                                                 Units 19-09001-13 '                   TRG                  l 1-10221A-FIGS-004-SS-A                                06/11/19 12:21            9/3/2019
                                                                                                                                             ..            9/10/2019      19-09001      Actinium-228                       EPA 901.1 Modified       2.39E-01             3.74E-01      3.75E-01   6.21E-01         u              pCi/g
-*---*-----~----,"**                                                                                                                 --**-                                                                     **-**                                                                                                         &#xa5;*------*--*----
19-09001-13                     TRG                  L 1-10221A-FIGS-004-SS-A                                06/11/19 12:21            9/3/2019 __,_____
9/10/2019      19-09001       Silver-108m                       EPA 901.1 Modified      -3.87E-02             R96E-02       8.96E-02   U6E-01           u              pCi/g
                                                                      ' " '"'"""- *---~------------- a - * -                                                                                                                                                                                                      -**-* ---~---*-------
                                                                                                                                                                                            ,--"-*-    ,,_ _ _._,m_    ,
                                                                                                                                                                 "'"'"""'""*---~--"'
19-09001-13                     TRG                                               _______
l 1-10221 A-FIGS-004-SS-A "' ________                  06/11/19 12:21 9/3/2019        9/10/2019      19-09001    Americium-241
                                                                                                                                           ,------*- *---"----------,-.-~-~--- ----------
EPA 901. 1 Modified     -1.01E-01             1.23E-01
                                                                                                                                                                                                                                                                  *--~~~-*--"'
1.23E-01   1.70E-01         u              pCi/g u
                                                                                                                                                      -------*--*--*--*---.l-,---~--"-'' ,_, __ ' _.....
19-09001-13                     TRG                   l1-10221A-FIGS-004-SS-A                                06/11/1912:21             9/3/2019        9/10/2019      19-09001        Barium-133                       EPA901.1 Modified       -3.94E-02             4.61E-02      4.62E-02   1.96E-01                        pCi/g
                                          -----*-     '""" - ---*--*-----*--*--***~ *----*                                                                                                                                                       i                                                                        -* *-----------
19-09001-13                      TRG                  l1-10221A-FIGS-004-SS-A
                                                              ---**                               '" ___         06/11/1912:21             9/3/2019        9/10/2019      19-09001       Bismuth-214                       EPA 901.1 Modified       6.98E-01             2.03E-01      2.07E-01   1.08E-01                        pCi/g
,_ 19-09001-13               i' ________________
TRG                   l 1-10221
______ A-FIGS-004-SS-A                   -
06/11/19 12:21             9/3/2019        9/10/2019      19-09001 :        Cobalt-60
                                                                                                                                                                                                                     --,-  EPA 901.1 Modified      1.41E+OO              1.59E--01     1.74E-01   1.91E-01                        pCi/g 19--09001-13                    TRG                   l 1-10221 A-FIGS-004-SS-A                              06/11/19 12:21            9/3/2019        9/10/2019      19-09001       Cesium-134                        EPA901.1 Modified        4.20E-02             6.23E-02      6.23E-02   1.51E-01         u              pCi/g 19-09001-13                      TRG                  l 1-10221 A-FIGS-004-SS-A                              06/11/19 12:21            9/3/2019        9/10/2019      19-09001       Cesium-137                        EPA 901.1 Modified      5.83E+OO              6.94E-01      7.55E-01   2.15E-01                        pCi/g
                                                                                                                                                ----~- .                . ----
____________ ___                    TRG
                                      "'        ..., __ l 1-10221A-FIGS-004-SS-A 06/11/19 12:21            9/3/2019        9/10/2019      19-09001
                                                                                                                                                                                       ----""''"'""'-~--
LUl...-,...,.,.,11-1.JL             EPA 901.1 Modified       5.74E-02             3.21E-01      3.21E-01   3.12E-01          u             pCi/g 19-09001-13
-------------------,                 TRG
                                "---------~-"-'""                  _______
l 1-10221A-FIGS-004-SS-A
                                                                                 " _______                       06/11/19 12:21
                                                                                                         - f---,--,------,w,-*         '
9/3/2019 9/10/2019 19-09001   ________
Europium-154... ...               _ EPA901.1 Modified       -1.67E-01             2.20E-01      2 . 20E-01 1.60E-01          u             pCi/g 19-09001-13                     TRG                  l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21            9/3/2019        9/10/2019      19-09001 ,   :::u, -,*-* "- ,55                  EPA 901.1 Modified       5.04E-03             1.47E--01  i  1.47E-01   2.12E-01          u             pCi/g
-----------,.-------------------**-- ------------~--
19-09001-13                     TRG    ________________________
l 1-10221A-FIGS-004-SS-A     " ____                    06/11/19 12:21 i
9/3/2019        9/10/2019      19-09001 ; Holmium-166m                          EPA901.1 Modified        8.59E-02             8.90E-02      8.91E-02   1.12E-01         u              pCi/g 19-09001-13                     TRG                   l 1-10221A-FIGS-004-SS-A                               06/11/1912:21             9/3/2019        9/10/2019      19-09001  !      lodine-129                      EPA901.1 Modified     :  2.26E-01             1.09E-01      1.10E-01   1.69E-01         u              pCi/g
                                           --------,-~---------*---------------
f-*
19-09001-13                     TRG                   l 1-10221A-FIGS--004-SS-A
                                                       ---------~--                          '"'""""
06/11/19 12:21            9/3/2019        9/10/2019      19-09001 i   -                      ..4n         EPA901.1 Modified       9.33E+OO              1.70E+OO  i   1.77E+OO   1.15E+OO                        pCi/g 19-09001-13                      TRG                  l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21            9/3/2019        9/10/2019      19-09001 :    ...... ... .................
                                                                                                                                                                                              ,:,, ,                       EPA 901.1 Modified      -4.06E-03             1.10E--01     1.10E--01  1.73E-01          u             pCi/g 19-09001-13                      TRG                  l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21            9/3/2019        9/10/2019      19-09001 i " "1"h-<-n .. m               M       EPA 901.1 Modified       8.61E-04             8.53E-02  i   8.53E--02  7.90E-02          u             pCi/g 19-09001-13 i                   TRG           i       l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21            9/3/2019        9/10/2019      19-09001 i      Niobium-94                       EPA901.1 Modified        2.11E-02             9.58E-02      9.58E-02   1.27E-01          u             pCi/g 19-09001-13
* TRG                   l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21            9/3/2019        9/10/2019      19--09001 i        lead-210                      EPA901.1 Modified     : 1.05E+OO              1.01E+OO      1.01E+OO   1.53E+OO          u             pCi/g 19--09001-13 i                   TRG                  l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21       ; 9/3/2019           9/10/2019      19-09001
* Lead-212                      EPA 901.1 Modified       2.74E-01         :   2.0SE-01      2.09E-01   3.44E-01          u             pCi/g 19-09001-13 '                    TRG                  l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21 i
9/3/2019        9/10/2019 i 19-09001              Lead-214                      EPA 901.1 Modified       5 . 18E-01       i   2.82E-01  i   2.83E-01   4 . 55E-01 i pCi/g i                                                                                                                                                                                                                                                                 u 19-09001-13                      TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21            9/3/2019        9/10/2019      19-09001    Promethium-145                       EPA901.1 Modified        5.13E-02             8.22E-02  . 8.22E--02  1.88E--01                       pCi/g
                                                                                                                                       ! 9/3/2019                                                  ___,
19-09001-13                      TRG                  l 1-10221A-FIGS-004-SS-A                               06/11/1912:21 9/10/2019 i 19-09001          Radium-226                        EPA901.1 Modified        6.98E-01         :   2.03E-01   i  2.07E-01   1 . 08E-01 .                    pCi/g 19-09001-13 i                   TRG                   l 1-10221A-FIGS-004-SS-A                               06/11/1912:21        I    9/3/2019        9/10/2019      19-09001     Antimony-125                        EPA901.1 Modified       -2.18E-02         i   3.88E-01  i   3.88E-01   5.24E-01          u             pCi/g i---
19-09001-13                     TRG                   l 1-10221A-FIGS--004-SS-A                              06/11/1912:21             9/3/2019        9/10/2019 ' 19-09001         Thorium-234                        EPA 901.1 Modified    i 1.26E+OO          ;   1.13E+OO      1.13E+OO   1.71E+OO   !     u              pCi/g i
19-09001-13                      TRG                  L1-10221A-FIGS-004-SS-A                                06/11/19 12:21            9/3/2019
                                                                                                                                 ---~-------             i 9/10/2019
* 19-09001         Thallium-208                       EPA 901.1 Modified       3.28E-01         l   1.44E-01  i   1.45E-01   1.57E-01   :                    pCi/g 19-09001-13                     TRG                  l 1-10221A-FIGS-004-SS-A                               06/11/19 12:21            9/3/2019        9/10/2019    i 19-09001       Uranium-235                       EPA 901.1 Modified       2.46E-01         I   4.34E-01  i   4.34E-01   6.52E-01          u             pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                          865/481-0683                FAX       865/483-4621

Printed: 10/21/201911:34 AM                                                                                                                                                                                                                                                                                     Page 16 of 21 Report To:                                                                                                                               Work Order Details:
Patricia Giza                                                                                                                                       19-09001 Eberline Analytical                                                                      " ______ _____
Zion  ,   Solutions
_                                                                                         Purchase Order:
SDG.*
677118 Final Report of Analysis                                                                2701         ________
____ Deborah Ave--*--
                                                                                                       ,,,                                                                                        ~f1_a/ysis Cat'!J!ory:                          ENVIRONMENTAL Zion, IL 60099                                                                                             Sample Matrix:                           so Lab          Sample                         Client                                 Sample                 Receipt           Analysis          Batch                                                                                                                                                                             Report Date Analyte                        Method                              Result                      cu                           CSU         MDA     Qualifier ID           Type                            ID                                     Date                                                       ID                                                                                                                                                                               Units 19-09001-14       TRG              L1-10220!-FJGS-005-SS-A                        07 /09/19 08:30                                                19-09001           '"'_, ___________
Actinium-228                 EPA 901.1 Modified                        9.41E-01                2.58E-01                      2.63E-01      4.49E-01              pCi/g 19-09001-14       TRG              L1-102201-FJGS-005-SS-A                        07 /09/19 08:30                                                19-09001            Silver-108m                 EPA 901.1 Modified                        2.65E-02                6.04E-02                     6.04E-02       1.08E-01     u 19-09001-14       TRG              L1-10220!-FJGS-005-SS-A                        07 /09/19 08:30                                                                  Americium-241                 EPA 901.1 Modified                        1.72E-01                1.85E-01                      1.85E-01      2.55E-01     u
                              *-----**-**                  -----**- *****- **1--*-*******--**-****--,-----~---*---:**-*****                                                        --*****-i******--*--*****
19-09001-14 .. TRG              L1-10220!-FJGS-005-SS-A                        07/09/19 08:30                                                                     Barium-133                  EPA 901.1 Modified                        1.47E-04                6.39E-02                      6.39E-02      1.57E-01     u 19-09001-14       TRG              L1-10220!-FJGS-005-SS-A                        07/09/19 08:30                                                 19-09001            Bismuth-214 "W_WC _ _ _ _ _
EPA 901.1 Modified                                                2.26E-01                      2.33E-01      2.94E-01 19-09001-14        TRG             l 1-102201-FJGS-005-SS-A                                                                                      19-09001               Cobalt-60                EPA 901.1 Modified                                                                              1.14E-01      1.64E-01
                    -*--'"-...,."-'"m _ _ _ _ "'"'""' _ _ _ _ '"'"'' -*e'--                                                                                                                                                     ....,.......... .
19-09001-14        TRG             L1-10220!-FJGS-005-SS-A                                                                                       19-09001            Cesium-134                  EPA 901.1 Modified                                                                              3.0SE-02      9.89E-02     u 19-09001-14        TRG 19-09001-14 TRG L1-10220!-FJGS-005-SS-A L1-102201-FJGS-005-SS-A
                                                             "" ------------        07/09/19 08:30              9/3/2019 2019      19-09001            Cesium-137
                                                                                                                                  ----"-"''"'*----,----- -----~,,____________
9/10/20~- __1_9~-"..~99~ _ Europium-152
                                                                                                                                                                              ,, ____              EPA 901.1 Modified EPA 901.1 Modified 4.74E-01 2.35E-01 1.76E-01 3.00E-01 19-09001-14        TRG             l 1-10220!-FJGS-005-SS-A                       07/09/19 08:30           1_9_i3_i2_0_1_9__,__9_i1_0_i2_0_19 _ __1_9~~-001         Europium-154 ..J---E_P_A_9__0__1_.1__M_o__d_ifi_1e__   d _____ c******8_.__                                                  2.21E-01 64_E_-_02__ .. c.......2_.2_1_E_-0__1_____r*--*--****-**-*-**---------------'--..:::.         .._-1 1
19-09001-14        TRG             L1-102201-FJGS-005-SS-A                     -* 07/09/19_ 08:30          / ~!312_0_19---i_9i_1_0i_2_01_9__1_9_-09"._01_         -~-ur_op_iu_m_-_1s_s-+__       E_PA_9_01_._1__
M_o_d_ifi_1e_d___ 0                                  1.82E-01                     1.82E-01 19-09001-14       TRG              L1-10220I-FJGS-005-SS-A                        07/09/19 08:30              9/3/2019          9/10/2019        19-09001          Holmium-166m                  EPA 901.1 Modified                                                1.30E-01                      1.30E-01
                                                                                  -***---****                :-------+-*------**-*c-*-----....+-------*-**---***-**i--**--*----...;........_ _ ___:__________________________:___:::__-1 19-09001-14 .      TRG             L1-10220I-FJGS-005-SS-A                        Cl"i'/09/19 ".._8~~?        9/3/2019 : 9/10/2019 *--~ 9-~~--                         lodine_-1_2_9_+-_E_P_A_90_1_.1_M_od__ifi_1e__d_______ +-----                                                             7.19E+OO 19-09001-14                        L1-10220!-FJGS-005-SS-A                *** -~~?f_19_0_8~.9_             , 9/3/2019 , 9/1012_:>.1_9__ 19_:-_(_J~~- ---~-ot_a_ss_iu_m_~-t-----E_P__A__9_0_1_.1__M_o_d_ifi_e_d __..... _, ______ *****--*-i--*-*--*--r---------------*-*-_..;_ __:___:;:.__
 --------------*- .-----                                                                                                                                                                                                                                                                                                                         1 19-09001-14        TRG             L1-102201-FJGS-005-SS-A                        07/09/19 08:30           ' 9/3/2019           9/10/2019        19-09001          Manganese-54                  EPA901.1 Modified
--------~*"-----
19-09001-14        TRG             l 1-10220!-FJGS-005-SS-A 07/09/19 08:30          !   9/3/2019 ' 9/10/2019               19-09001
* Molybdenum-93*+****--E-P-*A***-9-0*1-.*1-*-M--o-d-ifi-ed-*-****;*-----*-**-'-*------*-*'------------c.--------'-**-::__---1 19-09001-14        TRG             l 1-102201-FJGS-005-SS-A                    ***07/09/1908:30T 9/3/2019                       9/10/2019        19-0900*1--N;;;;;;~;;:,-94                      EPA 901.1 Modified
                                                                                                                                                                    -----+----*--*-***--*--'-------*---*-----~,--*--------------,--*-*-'-__;;::___-I 19-09001-14        TRG             l 1-10220!-FJGS-005-SS-A                    -~&deg;-?/09/19 08:30           i  9/3/2019 ' 9/10/2019               19-09001               Lead-210                 EPA 901.1 Modified
                                                                                                                                                          *-**-"***--------j----:---------**-**---;---------~----:-:-::--:---c------------:---:--'--"---------*---:----t 19-09001-14        TRG             L1-102201-FJGS-005-SS-A                        07/09/19 08:30              9/3/2019          9/10/2019        19-09001               Lead-212                 EPA 901.1 Modified                                                                                            4.36E-01
                                  ----------------*-***-1--
19-09001-14        TRG             L1-10220!-FJGS-005-SS-A                        07/09/19 08:30              9/3/2019          9/10/2019        19-09001               Lead-214                 EPA 901.1 Modified 19-09001-14        TRG             L1-102201-FJGS-005-SS-A                        07/09/19 08:30              9/3/2019          9/10/2019        19-09001 ' Promethium-145                       EPA 901.1 Modified
                                   *-------------------1--------1--------:-                                                                                                  ----+------------***---i----------..:.----_..;.-----------'-------~-'--..::.._-1 TRG             L1-102201-FJGS-005-SS-A                        07/09/19 08:30              9/3/2019          9/10/2019        19-09001            Radium-226                  EPA 901.1 Modified
                                   ----------******---*----***-+--------,---------****-----                                                                      . -----+--*-**-------*---+--------L------+-----------i------*--'-,;:__--1 l 1-102201-FJGS-005-SS-A                                                                     9/10/2019        19-09001           Antimony-125                 EPA901.1 Modified                                                                               2.00E-01      3.26E-01
                                                                                                                ---19-t-9/_1_0/-20_1__        9    19-09001            Thorium-234 i*---_E--PA--9-01-_=-1-M-o-difi_e_d--+*---:-*~--~--;---:-1_=-69=-E=-+=-o-:o--c-1-.6=-9=-E-+=-oo----:=-:-:-t--:---:---:-----=---;
L1-10220!-FJGS-005-SS-A
                                                                                                                ---}-----------*.                                                -----+----------i-----*--+-----.;.-----------+-----;---'---=---1 l 1-10220!-FJGS-005-SS-A                                                                     9/10/2019        19-09001           Thallium-208                 EPA901.1 Modified                                                  1.61E-01                     1.64E-01      1.63E-01
                                                                                                                                                                   -----+---------;------l-------i---*---------'----**-c---'---=----1 L1-10220!-FJGS-005-SS-A                        07/09/19 08:30           !  9/3/2019          9/10/2019        19-09001            Uranium-235                 EPA 901.1 Modified                                                5.37E-01                      5.37E-01      6.90E-01     u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>       EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                               865/481-0683                              FAX         865/ 483-4621

Printed: 10/21/2019 11 :34 AM                                                                                                                                                                                                                                                                                                                                                                Page 17 of 21 Report To:                                                                                                                                                        Work Order Details:
Patricia Giza                                                                                                                                                                19-09001 Eberline Analytical                                                                                               --*-* ,_ ______________
Zion Solutions      _                                                                                                      Purchase Order:
SDG:
677118 Final Report of Analysis                                                                                           2701 Deborah Ave
_Analysis Category: __ _i:~Y!~Q-~~                                                   E~J:.A.!::_
Zion, IL 60099                                                                                                                Sample Matrix:                                 SO Lab                      Sample                                   Client                                          Sample              Receipt           Analysis                Batch                                                                                                                                                                                                                                      Report
                                      ,     Type                                                                                                          Date                  Date                 ID Analyte                                 Method                                  Result                       cu                        CSU                               MDA               Qualifier ID                                                                ID                                             Date                                                                                                                                                                                                                                                                                                     Units 19-09001-15                           TRG            L 1-102201-QJGS-005-SS-A                           *---           07/09/1908:30         : 9/3/2019            9/10/2019 ____1~-090~-                        Act~um-228 _                          EPA901.1 Modified                             6.54E-01                 : 2.39E-01                  2.41E-01                         4.40E-01                                     pCi/g 19-09001-15                           TRG            L 1-102201-QJGS-005-SS-A                         . __ -** 07/09/19 08:30 _ J .~'.3/202_\l ____ 9/10/2019___~0900.!._ ---~lver::_:?8..":...__,___ E_PA 901.1 Modified                                                                         -5.37E-03                  3.41 E-02                 3.41 E-02                        9.17E-02                   U                 pCi/g 19-09001-1*5**-**,,--*****T*--R*G*--*-*--*-L*-*1*--1--0*--2*2**01-QJGS-005-SS-A 07/09/19 08:30            9/31~&deg;.:.'.'..  .J1:1&deg;.~~0_19__ . __    19_-0_9_00_1        -~":'':._nc._iu_m._-2_4_1_+--*-E__P.A_ 9_0_1__.. 1     *._M_o_d_i.fi_,e___d***-----*-*8*_*2_8.*E....-.o.*.2.....~ __
1._51_E_-0__1_.____1__.51 E-01                              2.04E-01                  u                 pCi/g 19-09001-15 ,                         TRG            L 1-10220!-QJGS-005-SS-A                         ---*-**-**- _o_7!&#xa3;9!_19 08:30          , 9/312-?1.9**-***9!_1_~_01_9_ _            19_-~&deg;.0~              -~-~~um-~~--***-*--E__                  PA__ 9_0.1.1 Modified                   [     9.64E-03                  4.71E-02                  4.71E-02                          1.25E-o.1_.-**-***--*****-u*-*------***-*-*-p-Cil_g __ ,
19-09001-15                           TRG            L 1-10220!-QJGS-005-SS-A                                          07/09/19 08:30            9/3/2019          9/1012019             19-09001                 Bismuth-214                          EPA 901.1 Modified                       1     8.02E-01                  1.65E-01                  1.71E-01                          2.36E-01                                    pCi/g
   ""-""-"-""'"'-""""""""                _____               ,__,_____,.______,______* "---v-""""'""*--*-----*-**-**                                                                                          *********----*****                     I********            *********-**-***********---**-****+***----***-***-***-****-*******
19-09001-15                           TRG            L1-102201-QJGS-005-SS-A                                           07/09119 08:30        [ 9/3/2019            9/10/2019             19-09001 ,                  Cobalt-60                         EPA 901.1 Mo_d_ifi_,e_d_*--***"'****-5         __._47_E_-0_1__,___9_. _1..7_..E.._-_0_2..**.* , ..__
9_.5_9E_-_o.2_**--************1*****6*_0.E_.-_o._1 _____.__**--*-*---pCil_g____,
19-09001-15 :                         TRG            L1-102201-QJGS-005-SS-A                                           07/09/1908:30         : 9/3/2019            9/10/2019             19-09001 :               Cesium-134                           EPA901.1 Modified                         :    2.22E-02                ' 3.58E-02                  3.58E-02                          7.99E-02                  U                 pCi/g
   ----"-***--------------------,-,---------~*-----<--*---------+*-***-*---------------*-------!-**
19-09001-15                           TRG            L1-10220I-QJGS-005-SS-A                                           07/09/1908:30 I 9/3/2019                    9/10/2019             19-09001 : Cesium-137                                         EPA901.1        Modified                  :   2.65E+OO                 i 3.41E-01                  3.67E-01                          1.40E-01                                    pCi/g
  - - - - -                            , _ _ _ _ _ _ _ _ , _ _ _ _ _ _ _ _ , _ _ _ _ _ _ , _ _ ,w _ _ _ , , _          _,_****------*-***-*--*-------**-------e-***-------1-**---*******-***
19-09001-15 ,                         TRG            L1-10220I-QJGS-005-SS-A                                           07109/19 08:30        : 9/3/2019 , 9/10/2019                      19-09001 :             ;:"'-c*-*             152              EPA901.1 Modified                             -9.65E-03                  3.03E-01             '    3.03E-01                          2.87E-01                   U                pCi/g 1
, *..._1_._9_-._o.._9..0__0_1_-_1_5___,:___T_R_G__,,_.._L._.1..-.._1..o.*2._2_._rn_-o_J_G_s_-0_0_5-_s_s_-A*-***-----;--o_1_10.__9_1_1_9_o8_:3_o_,--;9_13_1_2_0_1_9_. ___._9_1__1__
01_20_1_9___1_9_-09_0.o_._1 __** _.:::__  "'-.-"*-_*_.1.54. __ ___         EP!'_.90_1_._1__M_o.d_ifi_,.e_d_***----+--1_.2_2E_-_0_1__,1__7_.8_7_E-_0_2___1_..8_9_E__                    -0_2*--*-**-*1__.e_1_E.__           -0_1______      u_._.____P_Ciig_ ___,
1
__ .1_~~001::.:~___                        T_RG
____~:_1_&deg;.2.~~~---Q__            JG_S.::."._Cl_5-_S_S:~....                   07/09/19 08:30 ; 9/3/2019                  9._1_1._0_12,_0_19__1_9_-o._9_00_1.__  1:::_"'_*--*._15._5            __...._ _E_P_A_9.01.1 Modified                               6.46E-02                  7.46E-02                  7.47E-02                          2.06E-01                   U                pCi/g 19-09001-15                           TRG            L1-10220I-QJGS-005-SS-A                                           07/09/1908:30 : 9/3/2019                    9/10/2019             19-09001 ! Holmium-166m                                       EPA901.1 Modified                              6.18E-02                  9.77E-02                  9.78E-02                          1.07E-01                  U                 pCi/g
      *19-:00001-1~-T-R--G-.,-1 -L-1--1-o-220~-Q-JG-S---ooS-"sS::-A _____,__0_7_/0_9_/1*-9*-o-8,-3o--*,-9--/3-l-20--1-9-**.-*-9-/1*-01-2--0*1-9--1-9--0-90-0--1-,-...l-1-od-in-e--1-2-9--**t-****-*--E**P--A-9_0_1_.-1--M--od-ifi-,e-d-*-********-4-.5._6_E_+_oo__,___1._93_E_+_0_1-.**--1.-93--E*-+--0--1-***--*-*-4*-.7-4..E--+*o***o*--*---***-*u****---*-----pCi/-g---:1 19-09001-15                           TRG       :    L1-102201-QJGS-005-SS-A                                           07/09/1908:30         : 9/3/2019 : 9/10/2019                      19-09001         ! - --- ...                  ,n              EPA901.1 Modified                             1.73E+01                   2.52E+OO                  2.67E+OO                         1.46E+OO                                     pCi/g 19-09001-15                           TRG            L1-10220I-QJGS-005-SS-A                                           07/09/1908:30         !   9/3/2019          9/10/2019             19-09001         ! Manganese-54                               EPA901.1 Modified                             -6.33E-03                : 7.17E-02                  7.17E-02                          1.10E-01                   U                pCi/g 19-09001-15                           TRG            L 1-10220!-QJGS-005-SS-A                                          07 /09/19 08:30       i   9/3/2.0_1_9__,_ __9_11_01_20_1_9_ 19-09001 : Molybdenum-93                                            EPA 901.1 Modified                             6.44E-03                  5.22E-02                  5.22E-02                          7 .83E-02                  U                pCi/g 19-09001-15 :                         TRG       '    L 1-10220!-QJGS-005-SS-A                                          07/09/19 08:30        1 9/3/2019            9/10/2019             19-09001 ,                Niobium-94                          EPA 901.1 Modified                            -6.73E-03                : 6.15E-02             :    6.15E-02                          8.52E-02                   U                pCi/g l-*-**-*******-******---*-**-*----*-*----~--*-----*------*----;--------;-------*-----**-
19-09001-15 ,                         TRG       :    L1-102201-QJGS-005-SS-A                                            07/09/1908:30        l 913/2019            9/10/2019             19-09001 j                   Lead-210                         EPA901.1 Modified                             6.90E+OO
                                                                                                                                                                                                                                             ---+-------*--**-*'-~----\.---_:..----*------_:..-::.:::__ _ _ _ ____:_______~:-::'.---1 l 3.20E+OO                  3.22E+OO                         4.86E+OO                                     pCi/g
___  19_-_o9__0_01_-1_5_~ ___ _!_RG_....,'_ _             L 1_-1_0_22__0_1-_o_JG_s_-0_~5-_s_s_-A_______ . _0_1_10_91_1__             9_o8_:_3o_ _9_J3_12_0__1_9._ _     9i.1_0_12_0_19___     19_-_o9_09~_-+!__L_e_ad_-_21_2__-+-*--E_PA_90_._1_....1__M_o_d_ifi_e_d--**-+--7_.5_2_E_-0_1___i-_1_A_6_E_-0_1___,__                                              1._51_E_-0_1______                3._17_E_-_01_ _     '_*---'---'p_C_ii-'-g--1 19-09001-15                           TRG            L1-102201-QJGS-005-SS-A                                            07/09/1908:30         [ 9/3/2019           9/10/2019             19-09001 :                   Lead-214                         EPA901.1 Modified                              8.38E-01                ( 1.99E-01             i    2.04E-01                          3.22E-01                                    pCi/g 1------------,-~-----*--------*-                                                                                         ---------i-----+--
l-1_9_-o._9_00_1_-1_5~,__                    TR_G_**-**+--L_1-_10_2_2rn     __-O_J__
G_S_-0_0_5-_s__s_-A__.,.. - - + 07/09/19 08:30                       9/3/2019          9/10/2019             19-09001 i Promethium-145                                     EPA 901.1 Modified                             1.38E+OO                  1.20E+OO             l    1.20E+OO                         1.48E+OO             '      U                pCi/g 19-09001-15                           TRG       ,    L1-10220I-QJGS-005-SS-A                                            07/09/1908:30         ; 9/3/2019           9J10i2019' 19-09001 I                           Radium-226                          EPA901.1 Modified                              8.02E-01                   1.65E-01                 1.71E-01                          2.36E-01                                    pCi/g 1---**------**---------*------*----t-------+-
19-09001-15 ,                         TRG            L1-102201-QJGS-005-SS-A                                           07/09/1908:30          / 9/3/2_0_19-_9_11_0_12_0:_!:._.._1_9_-0_9_00_1__An_1,_*m_o_ny_-_12_5-j-                                 EPA901.~~~~E~_n:'.;~117'..=::l=._n~?-i-__.!.:.1.:'.:6.'..'.1E:::-~01'._j-:__'_1::'.6.'.:1E:::-::'.o1_,_____ :_2_:.'.'.8'.:.1=:E-~0~1_'_~u~--c--!:'.':'.'pCi,g_ig_.
L11_:9~-0::9~00~1~--1::5'..;._T_l:R~G~~--L~1':::.~*M~on*::.cr:::1*-::-~-'.l!-*::-~~~~-:~*1_______J_0_7._I0_91_19_0_8_:3_0_i_9i~-2-01_9__,,_9_i1_0_i2_0_19__                                  ,1_9_-0_9_0o_1-+,_T_ho_n_*u_m_-2_3_4_4-__E__P_A                      __9_o_1._1_Mo_difi_e_d __;!__-_1.2._4E-_0_1--_1._46_E_+_o_o_-+__1_.4_6E_+_o_o_ _1_.8_9_E+_o_o____u                                                          _ _ __:_P_:.Ci/g'--*~
19-09001-15                           TRG       j    L1-10220I-QJGS-005-SS-A                                           07/09/19 08:30        ! 9/3/2019            9/10/2019 : 19-09001                   i      Thallium_-_20_8--j[--E_PA                 ___9o._1_.1_M_o__d_.i_fi_,e_d_-ri_5_.6_6_E_-o_1--t__1_.2_7_E_-o_1_-j1____1_._3_1E_-01_ _ _                                       1._29_E_-_01_,___ _-+__P--,--Cii_g_--1 19-09001-15                     I     TRG       !    L1-102201-QJGS-005-SS-A                                            07/09/1908:30        i   9/3/2019          9/10/2019             19-09001          J     Uranium-235                           EPA901.1 Modified                              2.43E-01                  4.39E-01             1 4.39E-01                          5.92E-01                  U
* pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                                  865/ 481-0683                                    FAX 865/ 483-4621

Printed: 1012112019 11 :34 AM                                                                                                                                                                                                                                    Page 18 of 21 Report To:                                                                                                       Work Order Details:
Patricia Giza                                                                                                            19-09001 Eberline Analytical                                                                           Zion Solutions SDG:
Purchase Order:               677118 cc,cc,,,c,c,,,_,, ,,,,,,,,
c,c,c,,,c,,,-------------c,,cccc ----  ------- --
Final Report of Analysis                                                                 2701 Deborah Ave                                                                       _Analysis Category* _____ENVIRONMENTAL Zion, IL 60099                                                                             Sample Matrix:               SO Lab                Sample                                 Client                     Sample            Receipt           Analysis             Batch                                                                                                                                     Report Analyte              Method                   Result                   cu           CSU       MDA     Qualifier ID                 Type                                     ID                        Date              Date               Date                  ID                                                                                                                                     Units 19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                   06/26/19 10:04        9/3/2019         9/10/2019           19-09001           Actinium-228      EPA 901.1 Modified           3,94E-01 __
_ _,,_,,c,cc,O,cc,_____                 1.76E-01       1.77E-01  3A9E-01              '"''"""''
pCi/g 19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                                                          9/10/2019           19-09001           Silver-108m       EPA 901.1 Modified                                               6,01E-02  7.38E-02     u
                                                                                                                     ----------------------------------cc, 19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                                                           9/10/2019          19-09001          Americium-241      EPA 901.1 Modified                                               8,90E-02  U1E-01       u
   '""""""""-"""""_'_"'""'""W""""" '"'"'" ~'"'""v-w" , - a - - - * " - " " " ' " ' - - "
19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                   06/26/1910:04                           9/10/2019          19-09001            Barium-133       EPA90U Modified                                                  V9E-02    1,22E-01     u ------         pCi/g _
1------------r---------'"          ------------------c -------*-*-*--*--*-               '"-~v -*---"'"-*----=-------***- : "'"----**-*-***-----**--~* --* _,,,,, -
19-09001-16               TRG                L1-10221 A-FIGS-003-SB-A                  06/26/19 10:04 ~9/3/20!~ _9,~1_?/2019 09001___ Bismuth-21~                                 EPA 901.1 Modified                                               U5E-01    1,52E-01 19-09001-16               TRG                                                          06/26/1910:04         9/3/2019          9/10/2019          19-09001             Cobalt-60       EPA 901.1 Modified                                               8.95E-02  1,50E-01      u
                                                                                                                                                                                 ---,1-,.----------------+------r----------------: - -------------------
19-09001-16                                                                            06/26/19 10:04        9/3/2019          9/10/2019
            '""''---+--------------,,,c__ ,,_,____,,_,_.____ +--------,c,,c,,-,,,,,,___,____-'-----------------+-*-*cc,-,,-----+----
EPA 901.1 Modified                                               9-22E-02  9.72E-02      u 19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                   06/26/19 10:04                                                                                  EPA 901.1 Modified           3,83E-01             9,54E-02       974E-02   U6E-01 19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                   06/26/19 10:04                                                                                  EPA 901-1 Modified           8,69E-02              1.20E-01      1.20E-01  1.73E-01      u 19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                                                                                                                                                                                    2,25E-01  8,98E-02      u 19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                                                                                                                                                                                    1,01E-01  1_62E-01 19-09001-16               TRG          C     L1-10221A-FIGS-003-SB-A                                                                                                                                                                                    8A2E-02   7-24E-02     u 19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                                                                                                                                                                                    2.16E-01  3,00E-01     u 19-09001-16               TRG                L 1-10221A-FIGS-003-S8-A                                                                                                                                                                                   3,09E+OO  2,01E+OO 19-09001-16               TRG                L1-10221 A-FIGS-003-SB-A                                                                                                                                                                                   5A6E-02   1.01E-01      u               pCi/g 19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                                                                                                                                                                                                            u 19-09001-16               TRG
                             *---*----=_,___,L________________
1-10221A-FIGS-003-S8-A 19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                                                                                                                                                                                                            u
                              -----~"--"------
19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                                                                                                                   EPA 901-1 Modified                                                         1.98E-01 19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                                                                                                                   EPA 901-1 Modified           3,28E-01                             U4E-01   2.37E-01 19-09001-16               TRG                L1-10221A-FIGS-003-SB-A                                                                                                                   EPA 901-1 Modified                                                1A1E-01  2.05E-01      u 19-09001-16                                                                                                                                                          Radium-226        EPA 901.1 Modified           4_31E-01                             L15E-01   1-52E-01 19-09001-16                                                                                                                                                                            EPA 901-1 Modified           2,39E-02              1,SOE-01       1_80E-01 2.51E-01      u               pCi/g 19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                                                                                                 Thorium-234       EPA 901-1 Modified           4,35E-01             7A4E-01        7A4E-01   U1E+OO        u               pCi/g 19-09001-16               TRG                L1-10221A-FIGS-003-S8-A                                                                                                 Thallium-208      EPA 901-1 Modified           4.75E-01              1,97E-01      1-99E-01  3.06E-01                      pCi/g 19-09001-16          i    TRG                L1-10221A-FIGS-003-SB-A                                                                                                 Uranium-235       EPA 901-1 Modified          91E-01             2.51E-01       2,51E-01  3A7E-01       u               pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>            EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                 865/481-0683                  FAX      865/483-4621

Printed: 10121/201911:34 AM                                                                                                                                                                                                                                     Page 19 of 21 Report To:                                                                     Work Order Details:
Patricia             Giza                                                                    19-09001 Eberline Analytical                                                                                                      . ,.,.,.,.,
Zion Solutions SDG:
Purchase Order:       677118 Final Report of Analysis                                                                                    2701 Deborah Ave                                                    Analysis Category:      ENVIRONMENTAL Zion, IL 60099                                                         Sample Matrix:       so Lab                           Sample                                   Client                            Sample                    Receipt     Analysis   Batch                                                                                                                     Report Analyte        Method           Result                   cu                     CSU        MDA     Qualifier ID                             Type                                    ID                                Date                        Date      Date       ID                                                                                                                       Units 19-09001-17                                 TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19 10:00              9/3/2019     9/10/2019 19-09001  Actinium-228 EPA 901.1 Modified  7.03E-01              3.18E-01                  3.20E-01   5.47E-01              pCVg 19-09001-17                                 TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19 10:00              9/3/2019     9/10/2019 19-09001   Silver-108m EPA 901.1 Modified  -5.84E-03             7.53E-02                  7.53E-02   1.12E-01     u
                                                                                                                                                                                                                              '". ---**--'"-''""''" -----------~-.. --------"""
19-09001-17                                 TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19 10:00                           9/10/2019          Americium-241 EPA 901.1 Modified                        1.24E-01                  1.24E-01
*-----****-******-*-***-**                                           ""-cc------------**"""__ _
19-09001-17                                 TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19                                 9/10/2019            Barium-133                                            4.23E-02                  4.23E-02 19-09001-17                                 TRG
...........................................................              L1-10221A-FIGS-001-SB-A
                                                           - ......... -----~---*-----------------<***               . 06/26/19 10:00
                                                                                                                       *****----..   -***-                      9/10/2019           Bismuth-214                                            2.00E-01                  2.02E-01   3.66E-01 19-09001-17                                 TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19 10:00                           9/10/2019             Cobalt-60                                            7.87E-02                  7.99E-02   1.20E-01 19-09001-17 19-09001-17 TRG TRG L1-10221A-FIGS-001-SB-A L1-10221A-FIGS-001-SB-A
___                   06/26/19 10:00                           9/10/2019 19-09001
                                                                                                       .........--;------***----,..**-----~..*---***---- ...-----*****......
9/10/2019 19-09001 Cesium-134 Cesium-137 EPA901.1 Modified EPA 901.1 Modified 6.99E-03             3.96E-02 1.54E-01 3.96E-02 1.59E-01
_____ _. .............................____________............-+..- -..........____;--..-*---..,.....**---*****-*-**-*-...---<-***-****----*--*---1-----*-******................. +----..--*-*--*--*---*--'-**----------*-----*....C--------*-**-*:........::.........~
1.38E-01 3.49E-01 u
19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A
___...............................- - - - - - - - - -..----*--+*--------*-----..*-*---;--*..................,.........
9/10/2019 19-09001  Europium-152 EPA 901.1 Modified   1.07E-02             1.82E-01                  1.82E-01   2.62E-01     u 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19                                 9/10/2019 19-09001               EPA 901.1 Modified  -4.59E-02             2.43E-01                  2.43E-01   1.37E-01     u
    --~-------,-,,.---,--------*'-**----*-------------*
19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19 10:00              9/3/2019     9/10/2019 19-09001               EPA901.1 Modified                                                   1.39E-01   2.17E-01     u
   --*------ --*- ................................-----------+-*-*--**----.....~---------------*------------'--'-----+***-*------------*-*
19-09001-17                                 TRG                   L1-10221A-FIGS-001-SB-A                       06/26/19 10:00                           9/10/2019 19-09001               EPA 901.1 Modified
  - - - - - - - ...---*----.----**--*-------..* - - - - + - - - - - - - - - ~ - - - * - - - ; - - - - - - - - * - * - - '..... - - - - + * * - - * * - - - * * * * - - - -..*****~------+---------,-------------**--......._________..:..... ...:::........-1 1.52E-01   1.01E-01     u 19-09001-17                                 TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001               EPA 901.1 Modified                                                  6.71E-02   1.24E-01     u 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001               EPA 901.1 Modified                                                             1.80E+OO 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001               EPA901.1 Modified                                                              1.24E-01     u 19-:0000--:i::;1* ...... TRG--L-1:102'i"1A-FIGS-001-SB-A                                                                                                          19-09001               EPA 901.1 Modified                                                             1.13E-01     u 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001               EPA901.1 Modified                                                              1.16E-01     u
  ------**----------... ----****-------**-*-*-l---**-***--+--*----*--*--*----*----....:....C---**---**---l**-*-----*-****-*-*-+--------'-------+----**-----;-----***'---=:.....-1 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001    Lead-210   EPA901.1 Modified                                                              1.43E+OO     u
                                                                                     ----*---**-**+------....:-------!-*--*--***---***---+-*-----**-**-+---------*.........--;----*-********---------------------*-**--*---*..:......::......--1 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001    Lead-212   EPA901.1 Modified                                                              2.83E-01 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001    Lead-214                                                                                  3.15E-01              pCi/g l------+--------
  ,_,   19-09001 -17 ________
________________                   ,         TRG                 , ______
L1-10221A-FIGS-001-SB-A                                                                          19-09001 19-09001   Radium-226 u        pCVg pCi/g 19-09001-17 j _ _!~G                                             L1-10221A-FIGS-001-SB-A         ---+*----------i------'-------'----+-----*+******--*------*,'**------+-------------*---'-------....:........;;:......--1 19-09001-17 .                              TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001                                                                                                           u
       -*--------*-*-*-""""""""\"" --*----.--
19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001  Thorium-234                                                                                              u 19-09001-17                                TRG                   L1-10221A-FIGS-001-SB-A                                                                          19-09001  Thallium-208 EPA901.1                                                                                             pCVg 19-09001-17                      i         TRG~10221A-FIGS-001-SB-A                                                                                               19-09001  Uranium-235                                                                                              u        pCVg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-<letect
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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                             865/481-0683          FAX       865/ 483-4621

Printed: 1012112019 11 :34 AM                                                                                                                                                                                                                             Page 20 of 21 Report To:                                                                                            Work Order Details:
Patricia                Giza                                                                                              19-09001 Eberline Analytical                                                                                .. ...
Zion Solutions SDG:
Purchase Order:              677118
                                                                                   *---*-------*---**-*m**--*,--****                                                      *---*-*--+ .-* ,.                     -*-*  -*-*----******-----***-***--
Final Report of Analysis                                                               2701 Deborah Ave Analysis Category:              ENVIRONMENTAL Zion, IL 60099                                                                                Sample Matrix:              SO Lab              Sample                             Client                         Sample                       Receipt      Analysis       Batch                                                                                                                          Report Date Analyte                    Method                                     cu            CSU     MDA     Qualifier ID               Type                                 ID                            Date                           Date                      ID                                                                                                                            Units 19-09001-18             TRG           L 1-10221A-FIGS-004-SB-A                       06/26/19 10:06                  9/3/2019     9/10/2019    19-09001        Actinium-228                                                         2.25E-01      2.26E-01 4.23E-01 19-09001-18             TRG           L 1-10221A-FIGS-004-S8-A                       06/26/19 10:06                  9/3/2019     9/10/2019     19-09001       Silver-108m                                                          6.72E-02      6.72E-02 7.04E-02    u
                                            -*--*----------*"'"'"'--,-* ----**     -------*------: *-*----*-------~--------*---*----*---------
19-09001-18             TRG           L 1-10221A-FIGS-004-S8-A                       06/26/19 10:06                  9/3/2019     9/10/2019     19-09001      Americium-241            EPA 901.1 Modified        -1.35E-01          9.03E-02      9.05E-02 1.19E-01     u
*------*-*---*----*-*-----*1'-*--------~~--~-*-                                     -------~---------*-------------- ***-~-----*-----                         "
19-09001-18             TRG           L 1-10221A-FIGS-004-S8-A                       06/26/19 10:06                  9/3/2019     9/10/2019     19-09001        Barium-133             EPA901.1 Modified         -8.22E-03          2.87E-02      2.87E-02 1.24E-01    u
                                                                                                                                                                --------*-*-+-------
19-09001-18             TRG           L 1-10221A-FIGS-004-SB-A                       06/26/19 10:06                  9/3/2019     9/10/2019     19-09001       Bismuth-214             EPA 901.1 Modified         3.22E-01          1.25E-01      1.26E-01 1.84E-01 L1-10221A-FIGS-004-S8-A                        06/26/19 10:06 m-----~-*--***-**---*-*.s*-*-*--'""V-~
9/3/2019     9/10/2019     19-09001         Cobalt-60             EPA 901.1 Modified         2.40E-01          7.SOE-02               1.39E-01 19-09001-18             TRG                                                                                                                                                                                                                       7.60E-02
 ----------*-                           -----~---*---**-*-*-----*--*
19-09001-18             TRG           L 1-10221A-FIGS-004-SB-A                       06/26/19 10:06                  9/3/2019     9/10/2019                                            EPA901.1 Modified          8.19E-03          3.50E-02      3.50E-02 1.0SE-01     u 19-09001-18             TRG           L 1-10221A-FIGS-004-S8-A                       06/26/19 10:06                                                                                    EPA 901.1 Modified         1.89E-01          8.86E-02      8.92E-02 1.33E-01
                                                                                                                                                                                                              -+-------------**-------*---*--*-*------*----*------------ ....-,
19-09001-18             TRG           L 1-10221A-FIGS-004-S8-A                       06/26/19 10:06                                                                                    EPA 901.1 Modified         3.38E-02          9.46E-02      9.46E-02 1.76E-01     u 19-09001-18             TRG           L1-10221A-FIGS-004-S8-A                                                                                                                          EPA 901 .1 Modified                          1.94E-01      1.94E-01 9.07E-02     u
    ---~------------------------A*A-,-a TRG           L1-10221A-FIGS-004-S8-A                                                                                                                          EPA 901.1 Modified                           8.59E-02      8.59E-02 1.30E-01     u 1.13E-01      1.13E-01 7.45E-02     u        pCi/g 2.18E-01               3.15E-01     u TRG           L1-10221A-FIGS-004-SB-A                                                                                   19-09001       Potassium-40            EPA901.1 Modified                                          3.50E+OO 1.34E+OO              pCi/g 1--------*-*--------:------'------*---*---------***--*+-------------+------------*--------------*-~-----+--*-------*****
TRG           L 1-10221A-FIGS-004-S8-A                                                                                  19-09001                                                                                          9.12E-02 1.41E-01              pCi/g TRG           L 1-10221A-FIGS-004-S8-A                                                                                                                                                                                             8.43E-02     u        pCi/g TRG           L 1-10221 A-FIGS-004-SB-A                                                                                                 Niobium-94                                                                                 8.08E-02     u L1-10221A-FIGS-004-S8-A                        06/26/19 10:06                                                              Lead-210                                                                                  1.33E+OO     u L1-10221A-FIGS-004-SB-A                        06/26/19 10:06                                                              Lead-212              EPA 901.1 Modified                                                  2.08E-01 Lead-214              EPA901.1 Modified                                                   2.09E-01              pCi/g 06/26/19 10:06                                                                                    EPA 901.1 Modified                                                  2.08E-01     u 06/26/19 10:06                                                                                    EPA901.1 Modified                                                   1.84E-01              pCi/g EPA901.1 Modified                                                   2.67E-01     u        pCi/g EPA901.1 Modified                                                   1.16E+OO     u EPA 901.1 Modified                                                  3.63E-01              pCi/g 06/26/19 10:06                                                                                    EPA 901.1 Modified                                         2.48E-01 3.87E-01     u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-<letect
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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601         SCARBORO ROAD OAK RIDGE,                          TN 37830                 865/481-0683                FAX      865/ 483-462!

Printed: 10/21/2019 11 :34 AM                                                                                                                                                                                                                     Page 21 of 21 Report To:                                                                              Work Order Details:
Patricia Giza                                                                                            19-09001 Eberline Analytical                                                                                Zion Solutions SDG:
Purchase Order                677118 Final Report of Analysis                                                                        2701 Deborah Ave
                                                                                                                                    ----------------                           Analysis Category: _______ ENVIRQt;J~_(~J*,J:r~~
Zion, IL 60099                                                              Sample Matrix:               SO Lab        Sample                                      Client                                Sample                Receipt     Analysis          Batch                                                                                                                 Report ID         Type                                           ID                                  Date                  Date         Date             ID Analyte         Method                  Result           cu             CSU       MDA    Qualifier Units 19-09001-19     TRG                 L1-10221A-FIGS-002-SB-A                                   06/26/19 10:02           9/3/2019    9/10/2019       19-09001    Actinium-228  EPA901.1 Modified           5.16E-01       2.76E-01        2.77E-01 5.44E-01     u             pCiig
                                                                                                                                                                                                                                                                       '""*----------,- ~-
19-09001-19     TRG                 L1-10221A-FIGS-002-S8-A                                   06/26/19 10:02           9/3/2019    9/10/2019       19-09001     Silver-108m  EPA901.1 Modified          -1.43E-03       3.25E-02        3.25E-02 9.18E-02     u
-------------- - ---- --- --------------------------------------------------+-*v*--,-.-,--,---                    *-,---,m-,,_,_   * ----------------                                      ---------****---------.----------------------------
19-09001-19     TRG                 L 1-10221A-FIGS-002-SB-A                                  06/26/1910:02            9/3/2019    9/10/2019       19-09001   Americium-241  EPA 901.1 Modlfied         -6.68E-02       1.03E-01        1.03E-01 1.42E-01     u 19-09001-19     TRG                 L1-10221A-FIGS-002-SB-A                                   06/26/19 10:02 **
* 9/3/2019         9/10/2019       19-09001 '   Barium-133   EPA 901.1 Modlfied          1.83E-02       3.57E-02        3.58E-02 1.67E-01     u 19-09001-19 . TRG*-----------L-1--1-02---2--1----A------F--IG--S--0-0-2--S--B--A---------- ---------------------=------------------------.-**--------------                            ----------,--***------------------------ -----------
06/26/19 10:02           9/3/2019    9/10/2019        19-09001    Bismuth-214
                                                                                               ,-~------"-- ____ _.,,., ---------------**---------------------,-------------"-
EPA 901.1 Modified                         1.72E-01        1.73E-01 3.06E-01     u 19-09001-19     TRG                 L1-10221A-FIGS-002-SB-A                                   06/26/19 10:02           9/3/2019    9/10/2019       19-09001      Cobalt-60   EPA 901.1 Modlfied                         6.94E-02        6.97E-02 1.63E-01     u
                        --------------------------------------------+--------------------------------
19-09001-19     TRG                 L1-10221A-FIGS-002-S8-A                                   06/26/1910:02            9/3/2019    9/10/2019       19-09001     Cesium-134   EPA 901.1 Modlfied                         4.18E-02       4.19E-02  1.21E-01     u
                         ---- ----------------------------------------+---------------------------,------------------------------+                                                       ----------,------l----------------------
19-09001-19     TRG                 L1-10221 A-FIGS-002-SB-A                                  06/26/1910:02     .
                                                                                                  ,____ ,, ___,___ ,,, _ 9/3/2019    9/10/2019
_ _,a_,_.,,_,_~            19-09001
___._., _ ______     Cesium-137
_ _ _ _ _, EPA 901.1 Modlfied                         1.45E-01        1.SOE-01 1.40E-01 19-09001-19     TRG                 L1-10221A-FIGS-002-SB-A                                   06/26/19 10:02           9/3/2019    9/10/2019       19-09001    Europium-152  EPA 901.1 Modlfied         -1.97E-02       1.89E-01        1.89E-01 2.27E-01     u 1-----------*-- '"'"~-------wmcos-------*~"'"'--l-**----------*-*-+
19-09001-19     TRG                 L1-10221A-FIGS-002-SB-A                                   06/26/19 10:02           9/3/2019    9/10/2019        19-09001                                             9.20E-02       1.98E-01        1.98E-01 1.16E-01     u 19-09001-19
-------------,--  TRG                ..__, _______________
L1-10221A-FIGS-002-S8-A L1-10221A-FIGS-002-SB-A 06/26/19 10:02 06/26/19 10:02 9/3/2019 9/3/2019 9/10/2019        19-09001                                             9.29E-02       1.20E-01        1.ZOE-01 1.81E-01     u u
19-09001-19     TRG                                                                            ---,-m,-,--,~ : _          _,_,__ ' 9/10/2019       19-09001                                             -2.42E-02       1.23E-01        1.23E-01 8.34E-02 19-09001-19     TRG                 L1-10221A-FIGS-002-SB-A                                   06/26/19 10:02           9/3/2019    9/10/2019       19-09001                                                             7.49E-02        7.49E-02 1.14E-01     u
----~--------~---------------------'"'"                                                             -------"----------
                                                                                                                  . 9/3/2019 .
19-09001-19     TRG                 L1-10221A-FIGS-002-SB-A                                   06/26/19 10:02                       9/10/2019       19-09001                                                             1.90E+OO       1.97E+OO  1.44E+OO 19-09001-19     TRG                                                                                                                                                                                                     8.44E-02                 1.33E-01     u 6.33E-02        6.33E-02 8.54E-02     u 6.86E-02        6.86E-02 1.06E-01     u             pCi/g 1.22E+OO     u 2.59E-01 u             pCi/g u             pCi/g u             pCi/g 1.41E+OO     u             pCi/g 3.15E-01     u 4.52E-01     u             pCiig CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect
(  ""M>
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601    SCARBORO ROAD OAK RIDGE,                         TN 37830      865/481-0683                  FAX 865/483-4621

         ~
ZS-WM-131 REC'D SEP O3 2019     Revision 0 Information Use ZIONSOLUTIONSrrc  An EnergySolu/ions Company                                             19:-oeoo1 Ll-12201A-AJGS-042-SS-A                NA   NA SOIL 500 ml                  5/9/2018            FULL SUITE MARINELLI     I                 1300            NA       697.25g L1-12202C-AJGS-042-SS-A                NA   NA SOIL 500 ml                  5/9/2018            FULLSUJTE MARINELLI     I                 1030            NA       633.95g Ll-1220IC-AJGS-042-SS-A                NA   NA SOIL 500 ml                  5/9/2018            FULL SUITE MARINELLI     I                1230             NA       671.0lg NA   NA SOIL 500 ml                  5/9/2018            FULL SUITE Ll-1220 IB-AJGS-042-SS-A                                   MARINELLI     I                1245             NA       782.55g Ll-1211IA-AJGS-040-SS-A                NA   NA SOIL 500 ml                 4/25/2018            FULL SUITE MARINELLI     I                0825             NA       746.35g Ll-1220IB-AJGS-040-SS-A                NA   NA SOIL 500 ml                 4/25/2018 MARINELLI     I                1013  FULL SUITE NA       931.94g Ll-122020-AJGS-040-SS-A                NA   NA SOIL 500 ml I
4/25/2018            FULL SUITE MARINELLI                      0830             NA       793.65g Ll-12201C-AJGS-040-SS-A                NA   NA SOIL 500 ml                 4/25/2018            FULL SUITE MARINELLI     I                1008             NA       625.83g L1-12202C-AJGS-039-SS-A                NA   NA SOIL 500 ml MARINELLI       4/18/2018            FULL SUITE I                 0825             NA       615.18g Ll-12201B-AJGS-039-SS-A                NA   NA SOIL 500 ml MARINELLI       4/18/2018            FULL SUITE I                 0950             NA       786.02g L1-1220IA-AJGS-039-SS-A                NA   NA SOIL 500 ml MARINELLI       4/18/2018            FULL SUITE I                 1005             NA       601.73g Ll-I220IC-AJGS-039-SS-A                NA   NA SOIL 500 ml MARINELLI       4/18/2018            FULL SUITE 1                 0935             NA       628.76g Ll-10221A-FSGS-004-SS-A                NA   NA SOIL 500 ml MARINELLI        6/6/2019            5ROC HTD 1                 1220             NA       698.04g Ll-10221A-FSGS-002-SS-A                NA   NA SOIL 500 ml MARINELLI        6/6/2019            5ROCHTD 1                 1210             NA       798.64g Ll-10221C-FSGS-012-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/11/2019            5ROCHTD    NA 0910                      823.06g Ll-10221C-FSGS-013-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/11/2019            5 ROC HTD  NA 0915                      774.57g Ll-10221C-FSGS-014-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/11/2019 0920 5 ROC HTD  NA 1013.99g Ll-10221A-FIGS-001-SS-A                NA   NA SOIL 500 ml MARINELLI    I  6/11/2019            5ROCHTD    NA 1215                      900.99g t  Ll-10221A-QIGS-001-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/11/2019 1215 5ROCHTD    NA 932.77g 3 of9

          . ~
REC'D SEP o3 2019    ZS-WM-131 Revision 0 Information Use ZIONSOLUTIONSuc   An EnergySo/uiions Company                                           1tf-0900 1 l(  Ll-10221A-FIGS-002-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/11/2019 1217 5ROCHTD   NA 922.34g Ll-10221A-FIGS-003-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/11/2019           5ROCHTD   NA 1219                    929.16g LI-1022IA-FIGS-004-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/11/2019           5 ROC HTD NA 1221                    925.96g Ll-102201-FJGS-005-SS-A                NA   NA SOIL 500 ml MARINELLI    1   7/9/2019           5ROCHTD   NA 0830                    572.09g Ll-102201-QJGS-005-SS-A                NA   NA SOIL 500 ml MARINELLI    1   7/9/2019           5 ROC HTD NA 0830                    648.58g L1-10221A-FIGS-003-SB-A                NA   NA SOIL 500 ml MARINELLI       6/26/2019           5 ROC HTD 1                 1004           NA       812.22g 17   L1-10221A-FIGS-001-SB-A                NA   NA SOIL 500 ml MARINELLI 1
6/26/2019 1000 5ROCHTD NA       677.47g Jg   Ll-10221A-FIGS-004-SB-A                NA   NA SOIL 500 ml MARINELLI 1
6/26/2019 1006 5ROCHTD NA       757.61g
{?   Ll-10221A-FIGS-002-SB-A                NA   NA SOIL 500 ml MARINELLI I
6/26/2019 1002 5 ROC HTD NA       756.86g Ll-I0221A-QIGS-001-SB-A                NA   NA SOIL 500 ml MARINELLI       6/26/2019           5 ROC HTD 1                 1000           NA       614.42g Ll-1022IA-FJGS-007-SS-A                NA   NA SOIL 500 ml MARINELLI       6/17/2019           5ROCHTD 1                 0856           NA       710.95g Ll-10221B-FJGS-002-SS-A                NA   NA SOIL 500 ml MARINELLI       6/17/2019           5ROCHTD 1                 0830           NA       714.12g Ll-1022IA-FJGS-002-SS-A                NA   NA SOIL 500 ml MARINELLI       6/17/2019           5ROCHTD I                 0846           NA       771.65g Ll-10221A-FJGS-00I-SS-A                NA   NA SOIL 500 ml MARINELLI    I  6/17/2019           5ROC HTD  NA 0844                    707.40g Ll-10221A-FIGS-005-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/13/2019           SROC HTD  NA 0745                    774.76g Ll-10221A-FIGS-006-SS-A                NA   NA SOIL 500 ml MARINELLI   1   6/13/2019           5ROCHTD   NA 0747                    783.08g Ll-10221A-FIGS-007-SS-A                NA   NA SOIL 500 ml MARINELLI    1  6/13/2019           5 ROC HTD NA 0749                    708.49g Ll-I0221A-FIGS-008-SS-A                NA   NA SOIL 500 ml MARINELLI   1   6/13/2019           5ROCHTD   NA 794.16g 0751 Ll-1022IA-FIGS-009-SS-A                NA   NA SOIL 500 ml MARINELLI   1   6/13/2019           5 ROC HTD NA 774.52g 0753 4 of9

REC'D SEP O5 2019
       ~
ZS-WM-131 Revision 0 Information Use ZIONSOLUTIONSru   An EnergySolutions Company 19*09001 Ll-1022ID-FIGS-021-SS-A               NA   NA  SOIL     500       ml  MARINELLI                                             5 ROC HTD Ll-10221D-FIGS-OOI-SS-A               NA   NA  SOIL     500       ml  MARINELLI                                             5 ROCHTD Laboratory:                                    Date Submitted To Lab:              Ship Container No.:   Cooler Temperature: FULL SUITE EBERLINE LABS                                                                             NA                         NIA Date              Time:                                                     Date: (mm/dd/yyyy):
                                                ~ft:        ):
Relinquished by:
l)vf)
Relinquished by:                               Date              Time:
(mm/dd/yyyy):
Comments 9 of9

EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD
* EBERLINE                                                                          OAK RIDGE, TENNESSEE 37830
  ~                       ANALYTICAL                                                        PHONE (865) 481-0683 FAX (865) 483-4621 EBS-OR-46231 October 22, 2019 Patricia Giza Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 CASE NARRATIVE Work Order# 19-09012-0R SAMPLE RECEIPT This work order contains sixteen soil samples received 09/03/2019. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.
CLIENT ID                            LAB ID             CLIENT ID                        LAB ID Ll-1022 lA-FJGS-002-SS-A              19-09012-04       Ll-10221 C-FIGS-103-SS-A         19-09012-12 Ll-1022 lA-FJGS-001-SS-A              19-09012-05       L 1-10221B-FIGS-102-SS-A         19-09012-13 Ll-1022 lA-FIGS-005-SS-A              19-09012-06       Ll-10221B-FIGS-103-SS-A          19-09012-14 Ll-1022 lA-FIGS-006-SS-A              19-09012-07       Ll-1022 lB-FIGS-l 04-SS-A        19-09012-15 Ll-1022 lA-FIGS-007-SS-A              19-09012-08       L 1-1022 lB-FIGS-105-SS-A        19-09012-16 Ll-1022 lA-FIGS-008-SS-A              19-09012-09       Ll-10221 D-FIGS-005-SS-A         19-09012-17 L 1-1022 lA-FIGS-009-SS-A             19-09012-10       Ll-1022 lD-FIGS-006-SS-A         19-09012-18 Ll-1022 lB-FIGS-l 00-SS-A             19-09012-11       Ll-1022 lD-FIGS-007-SS-A         19-09012-19 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.
Gamma Spectroscopy was performed using EPA Method 901.1 Modified.
Laboratory qualifiers are as follows:
U - Result is less than the MDA.
ANALYTICAL RESULTS Combined Standard Uncertainty is reported at 1-sigma value.
Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.
Page 1 of 3

ANALYTICAL RESULTS CONTINUED TOT AL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filters were reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.
Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are reported from Total Strontium assuming secular equilibrium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.
TRITIUM A representative aliquot of each sample was equilibrated with tritium free water. Equilibrates were transferred into a round-bottomed distillation flask and attached to a single stage still. A pottion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were counted by beta liquid scintillation.
Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.
NICKEL-63 A representative aliquot of each sample was prepared by leaching in acids. Aliquots were placed into an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion.
Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.
Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.
GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.
Page2of3

ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Actinium-228, Bismuth-214 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY I ce1tify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her desi~i::_ee to be accurate as verified by the following signature.
M.R. McDougall Laboratory Manager Date: 10/22/2019 Eberline Analytical wants and encourages your feedback regarding our perfonnance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services.
Page 3 of 3

Printed: 10/21/2019 12:02 PM                                                                                                                                                                                                                                             Page 1 of 21 Report To:                                                                                                     Worl< Order Details:
Patricia Giza                                                                                                     19-09012 Eberline Analytical                                                                                          Zion Solutions                                                                     Purchase Order:
SDG:
677118 Final Report of Analysis                                                                                2701 Deborah Ave
                                                                                                             *-----------,--~                                                                 __ Ana/ysis._Category: ___            ENV.1_.13Qt:-JMEt\J1~~---***
Zion, IL 60099                                                                       Sample Matrix:               SO Lab               Sample                                    Client                                   Sample                      Analysis          Batch                                                                                                                                Report Date Analyte                Method                   Result                   cu            CSU      MDA   Qualifier ID                 Type                                       ID                                      Date                                          ID                                                                                                                                  Units 19-09012-01                 LCS                KNOWN                                                                                    10/1/2019                              Tritium       LANL ER-210 Modified           2.08E+02            7.48E+OO                                        pCi/g 19-09012-01                LCS                SPIKE                                                                                    10/1/2019                              Tritium       LANL ER-210 Modified           2.04E+02            7.87E+OO          1.39E+01 5.89E+OO             pCi/g
                                                                                                                                                                               ********-------+-------,-,,-,--,,,,,,,,,.. ----------~-           ------------*-*-------~-----------~---------t 19-09012-02                MBL                BLANK                                                                                    10/1/2019                              Tritium       LANL ER-210 Modified           1.33E+OO            3.38E+OO          3.38E+OO 5.79E+OO    U        pCi/g
                                                                                                                           **-*,****-----* ------------*-*********--*--*,--* ******--*--***--***-+-----***-*--------+---*******----*-***********-*--*--*----**---*--------**** -----*--*-----
19-09012-03                DUP                L1-10221A-FJGS-002-SS-A                                   06/17/19 08:46                 10/1/2019       19-09012               Tritium       LANL ER-210                    3.24E+OO            3.47E+OO          3.48E+OO 5.82E+OO    U
                                                                    *******--****-----***** ____..,... l--*-*******-***---;.*-------***--****----------*-****-
19-09012-04 .               DO                L1-10221A-FJGS-002-SS-A                                   06/17/19 08:46                 10/1/2019       19-09012               Tritium       LANL ER-210 Modified           5.14E+OO            3.53E+OO          3.54E+OO 5.81E+OO    U
********-*--*-*****--************-**-------*-***                          -********----******* -*---1*---*-*------0----*------**-**-~-----*-..*---------+---***--*-****--*----********** **'*********-*-*******-****** ***'**---------+-**-*----------*---***-*****----**--*--*----1 19-09012-05                 TRG                L1-10221A-FJGS-001-SS-A                               ____o~~1_?~9 08:~- , 9/3/2019 .. __10/1/2~~ __19-09012 ____T                            LANL ER-210 Modified
__n_*t_iu_m*-****-+----*-***---------*---*+- 2.69E+OO            3.47E+OO          3.48E+OO 5.86E+OO    U        pCi/g 19-09012-06;_T._~_G*.-          ....-.* - _-_-_L*1=--_1*0_2_21_A_-_F_IG_S_-o_os_*:~~:~~=~~              06/13/19 07:45
* 9/3/2019
* 10/1/2019          19-09012               Tritium       LANL ER-210 Modified           3.03E+OO            3.44E+OO          3.44E+OO 5.78E+OO    U 19-09012-07                TRG                L1-10221A-FIGS-006-SS-A                                   06/13/19 07:47     9/3/2019    10/1/2019       19-09012               Tritium       LANL ER-210 Modified           4.00E+OO            3.50E+OO          3.SOE+OO 5.82E+OO    u 19-09012-08 '            . TRG                L1-10221A-FIGS-007-SS-A                                   06/13/1907:49                  10/1/2019       19-09012               Tritium       LANL ER-210 Modified           3.06E+OO            3.48E+OO          3.48E+OO 5.8SE+OO    u 19-09012:&deg;-9 *--- !~_9__ L1-1022:~_:~IGS-008-_SS-l:_______1___0_6_.*1_13_1_19_07__:5_1.__, _________1_0_11_12_0_1_9_0 _ _19-09012                       _ _ _ _ _ _. *, .
Tritium       LANL ER-210 Modified           -1.88E-01           3.30E+OO          3.30E+OO 5.73E+OO
                                                                                                                                                                              ----*---..J------********----****+-*-----*--;--,.-----**.--**--*-----*-*----**---"-**-------****---'-***    u 19-09012-10                TRG                L1-10221A-FIGS-009-SS-A                                   06/13/19 07:53                                 19-09012               Tritium       LANL ER-210 Modified           4.53E+OO            3.48E+OO          3.49E+OO 5.76E+OO    u 19-09012-11                TRG                L1-102218-FIGS-100-SS-A                                   05120119 09:55                                 19-09012               Tritium       LANL ER-210 Modified           2.99E+OO                              3.40E+OO 5.71E+OO    u        pc*
      ********-************-***-**--------------******-**-- **----*-**+--*---------+,-------*- -----*-*--***-*****; ... -----**-*--*+-----------*----+-----***--*-*-i-------'**-******---------*----------------..:..-
19-09012-12 ... *........:~~ __':.1_:.10221C-FIGS-!&deg;-~:SS-A __                                          07/08/19 12:47                                 19-09012               Tritium       LANL ER-210 Modified            1.86E-01                             3.28E+OO 5.68E+OO    u 19-09012-13                TRG                L1-102218-FIGS-102-SS-A                                   07/08/19 13:10                                 19-09012               Tritium       LANL ER-210 Modified           2.03E+OO            3.32E+OO          3.32E+OO 5.62E+OO    u 19-09012-14                TRG                L1-102218-FIGS-103-SS-A                                   07/08/19 13:12                 10/1/2019       19-09012               Tritium       LANL ER-210 Modified                                                          5.61E+OO    u 19-09012-15                                                                                             07/08/19 13:14                 10/1/2019       19-09012               Tritium       LANL ER-210 Modified                                                          5.SSE+OO    u 19-09012-16                                                                                                                            10/1/2019       19-09012               Tritium        LANL ER-210 Modified                                                         5.47E+OO    u 19-09012-17                                                                                                                            10/1/2019       19-09012               Tritium       LANL ER-210 Modified                                                          5.56E+OO    u 19-09012-18                TRG                L1-102210-FIGS-006-SS-A                                                                  10/2/2019       19-09012               Tritium       LANL ER-210 Modified                                                          S.57E+OO    u 19-09012-19                TRG                L1-102210-FIGS-007-SS-A                                                                  10/2/2019       19-09012               Tritium       LANL ER-210 Modified                                                          SASE+OO     u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                          865/481-0683                  FAX 865/ 483-4621

Printed: 10/21/201912:02 PM                                                                                                                                                                                                        Page 2 of 21 Report To:                                                                                   Work Order Details:
Patricia Giza                                                                                                 19-09012 Eberline Analytical                                                                     Zion Solutions SDG:
Purchase Order:       677118 Final Report of Analysis                                                          2701 Deborah Ave                                                               ..... AnalysisCategory:       ENVIRONMENTAL                                      ,_,,_,, ____
Zion, IL 60099                                                                          Sample Matrix:       so Lab                   Sample                  Client                            Sample            Receipt        Analysis            Batch                                                                                                              Report ID                    Type                     ID                               Date              Date            Date               ID Analyte                   Method            Result        cu            CSU      MDA   Qualifier Units 19-09012-01                     LCS    KNOWN                                        09/05/19 00:00       9/3/2019       10/1/2019          19-09012     Nickel-63                                                                                                pCi/g 19-09012-01                                                                         09/05/19 00 :00      9/3/2019 LCS    SPIKE                                                                            10/1/2019          19-09012     Nickel-63                                                                      3.29E+OO                   pCi/g 19-09012-02                            BLANK                                        09/05/19 00:00       9/3/2019       10/1/2019          19-09012     Nickel-63            ASTM 3500-Ni Modified  6.96E-01    1.86E+OO      1.86E+OO 3.17E+OO    u              pCi/g a-*,------
19-09012-03                            L1-10221A-FJGS-002-SS-A                      06/17/19 08:46       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified  1.85E+OO     2.01E+OO      201E+OO  3.37E+OO    u 19-09012-04                      DO    L1-10221 A-F JGS-002-SS-A                    06/17/19 08:46       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified  2.14E+OO     2.03E+OO      2.03E+OO 3.39E+OO 19-09012-05                     TRG    L1-10221A-FJGS-001-SS-A                      06/17/19 08:44       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified  1.18E+OO     1.95E+OO      1.95E+OO 3.30E+OO
             *------*-*---------------*------                                         --------'>------------------------------~--,----- -;--~-----------
19-09012-06                     TRG    L1-10221A-FIGS-005-SS-A                      06/13/19 07:45       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified  O.OOE+OO     1.84E+OO      1.84E+OO 3.17E+OO
___19-09012-07                      TRG    L1-10221A-FIGS-006--SS-A 06/13/19 07:47       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified               1.85E+OO      1.85E+OO 3.14E+OO 19-09012-08                     TRG    L1-10221A-FIGS-007-SS-A                      06/13/19 07:49       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified               1.93E+OO      1.93E+OO 3.30E+OO
      --------~-- -------"*------------------- ---------~-------------------                                                                    ----------
19-09012-09                     TRG    L1-10221A-FIGS-008-SS-A                      06/13/19 07:51       9/3/2019       10/1/2019          19-09012     Nickel-63            ASTM 3500-Ni Modified 1.12E+OO     2.01E+OO      2.01E+OO 3:40E+OO
-*----"--*-.,**---------,-,----------*-"~~-----
19-09012-10                     TRG    L1-10221A-FIGS-009-SS-A                      06/13/19 07:53       9/3/2019       10/1/2019          19-09012     Nickel-63            ASTM 3500-Ni Modified 2.51E+OO     1.97E+OO      1.98E+OO 3.27E+OO 19-09012-11                     TRG    L1-10221B-FIGS-100-SS-A                      06/20/19 09:55       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified  -3.27E-01    2.29E+OO      2.29E+OO 3.97E+OO -09012-12~ . TRG ' L1-10221C-FIGS-103-SS-A           --"'---*-* --------
07/08/19 12:47       9/3/2019       10/1/2019          19-09012     Nickel-63 ASTM 3500-Ni Modified  2:41E+OO     1.96E+OO      1.96E+OO 3.26E+OO
                                                          -----"',-----------,- -c--c 19-09012-13                     TRG    L1-10221 B-FIGS-102-SS-A                     07/08/19 13:10       9/3/2019       10/1/2019          19-09012     Nickel-63            ASTM 3500-Ni Modified                            2.14E+OO 3.61E+OO 19-09012-14                     TRG    L1-10221 B-FIGS-103-SS-A                     07/08/19 13:12       9/3/2019       10/1/2019          19-09012     Nickel-63            ASTM 3500-Ni Modified                            1.88E+OO 3.18E+OO
--~---,-------------------.                              *----*-
L1-10221B-FIGS-104-SS-A                      07/08/19             9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified                             1.93E+OO 3.34E+OO L1-10221 B-FIGS-105--SS-A                    07/08/19 13:16       9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified                             1.89E+OO 3.25E+OO L1-10221 D-FIGS-005-SS-A                     07/08/19 12:30       9/3/2019       10/1/2019          19-09012     Nickel-63            ASTM 3500-Ni Modified                            2.05E+OO 3:40E+OO
                                                                                          * - - - - - >----*-'*-------~ .                           --"--' ---*--
19-09012-18                     TRG    L1-102210-FIGS-006--SS-A                     07/08/19 12:32       9/3/2019       10/1/2019          19-09012     Nickel-63            ASTM 3500-Ni Modified                            1.96E+OO 3.34E+OO
                                                                                                                              ---------,-----*---~*--,-----
19-09012-19                     TRG    L1-102210-FIGS-007-SS-A                      07/08/19 12:34     ! 9/3/2019       10/1/2019          19-09012     Nickel-63           ASTM 3500-Ni Modified                             2.08E+OO 3.49E+OO   u              pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non--detect
(   ""M>
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601     SCARBORO ROAD OAK RIDGE,                         TN 37830                 865/481-0683          FAX    865/483-4621

Printed: 10/21/201912:02 PM                                                                                                                                                                                                                                                                                                                                                             Page 3 of 21 Report To:                                                                                                                                               Work Order Details:
Patricia Giza                                                                                                                                              19-09012 Eberline Analytical                                                                                                    Zion Solutions SDG:
Purchase Order:.. **-*--* .........               677118          ...... _.._.........- .................................
Final Report of Analysis                                                                                           2701 Deborah Ave                                                                       ....    . Analysis_Category: ......~_NV_IRONMENTAL Zion, IL 60099                                                                                              Sample Matrix:                                 SO Lab               Sample                                       Client                                           Sample             Receipt            Analysis           Batch                                                                                                                                                                                                                                   Report Analyte                                     Method                                                                                                     CSU                   MDA                    Qualifier ID                 Type                                          ID                                             Date                  Date             Date                ID                                                                                                                                                                                                                                    Units 19-09012-01               LCS                 KNOWN                                                                                     9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                                                                                                                                                              pCVg
                                                                                                                                                                                                                                                                                                                                                                                                                    'n,-w,,,--*
19-09012-01               LCS                 SPIKE                                                               09/05/19 00:00        9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                                               ........_ ..___.____ 1.78E+01                                7.98E-01                                          pCi/g 19-09012-02               MBL                 BLANK                                                               09/05/19 00:00        9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM
                                                                                                                                                                                            ...................-*+-........_ .....____    SRW01       Modified
                                                                                                                                                                                                                                                 ... ___    . _ _....... 5.10E-01                              3.02E-01                        3.50E-01..... ______    5.89E-01                      U                   pCi/g
------                                                                                                          ------*-"~--, '------                    '        ---.
19-09012-03               DUP.....-,_ ..L....1..-.:92_2_1A_-_F::l9S-~~~--s_s_-_A                                 _0~171~9-_o~:4_6_ .. _9-'.'.~/~~1.9-...._~0_12_12_0_1_9_1~.:~~91_~-     Strontium_-9_0-,_E__         1C__h._r..o..M_....s_R_w_o_1_M_o.*d...i_fi..e_d**-'<-------...............................3.*.3...o_E_-_o..._1........-3....:4
                                                                                                                                                                                                                                                                                                                                                    .._2_E
__-0_1______._6_.7._7_E__
                                                                                                                                                                                                                                                                                                                                                                                -0__1                u *----             pCVg L1-10221A-FJGS-002-SS-A                                             06/17/1908:46         9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified' -8.57E-02                                                         3.21E-01                        3.23E-01                6.96E-01                      U
                                                    ..... _________________ ........ *----*-**------*****----- ................................_. _ _ _ _ _ -*--** ---*                                                                                                                                                                                                           ................ ___ _. ......... _ .. ;.........C.-..J 19-09012-05               TRG                 L1-10221A-FJGS-001-SS-A                                             06/17/19 08:44        9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                   1.84E-01                         3.14E-01                        3.21E-01                6.52E-01                      U
                ---***---***--**-*--* ***** ------**-*-            ----------*******--- - -----*--**-----*******- ***---**--***----*---------..*-----** ................... ., ...... *- -                                                                                  *------* *-*------*---*--*-----**                                                                          -*~-*------*-***----**-**-*'---'--!
19-09012-06               TRG                 L1-10221A-FIGS-005-SS-A                                             06/13/19 07:45        9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                  3.72E-01                          2.98E-01                        3.25E-01                5.95E-01                      U
          - - - - - - - - - * - * - , '
* r n - . , . - , s s - * - * - " " " " " " - - - - - - - - " " " " " ,., _ _ _, , . _     * * - - - - - - - - = " " " ' ' " " ' - " " ' "_ _ _ _ mo,-*o*"''"~'~,--
19-09012-07               TRG                 L1-10221A-FIGS-006-SS-A                                             06/13/19 07:47        9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                   2.98E-01                         3.21E-01                        3.37E-01                6.52E-01                      U
 ---------***--*-- *-------------                                      -------*                               -----------~--,-.,---,~--                                  **------*----------------,------------------..----;-------------*----*-----------*----..*--+------------*-----*-**-***--*-****----..... _;___:_.......-1 19-09012-08               TRG                 L1-10221A-FIGS-007-SS-A                                             06/13/19 07:49        9/3/2019           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                   2.59E-02                         3.45E-01                        3:45E-01                7.33E-01                      U
                                                                                                                                                                                         -*--------+--------..-----**..**-*--.;.-..-                                                                      -------*----,-
19-09012-09               TRG                 L1-10221A-FIGS-008-SS-A                                             06/13/19 07:51                           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                  2.55E-01                          3.46E-01                        3.57E-01                7.11E-01                      U
 -*---*-*- .....................................-..                               .. .------J***-***-------*-*--****-*---*--*-------*---*--*-------..*-*--+---*-**--------*****-0---*--------*--..*-*--**---*-** ......----*-*-..*-*-*-**-**--*-- --------'--'-''----!
19-09012-10               TRG                 L1-10221A-FIGS-009-SS-A                                             06/13/19 07:53                           10/2/2019        19-09012     Strontium-90               EIChroM SRW01 Modified                                   3.39E-01                         4.09E-01                        4.26E-01                8.38E-01                      U
____... . -*-*-****...*. *****s----*-*------*. **--*-**----l---.. **--*-------*-<-*-***----------*----------****-*--**---*--*----+-------*---------**--+------*----*----*~-----***----..-*-----*-**-**-*--*---------'..-.C..:::..--1 19-09012-11               TRG                 L1-10221 B-FIGS-100-SS-A                                            06/20/19 09:55                           10/2/2019        19-09012     Strontium-90                                                                        1.42E-01                         3.82E-01                        3.85E-01                8.01E-01                      U 19-09012-12               TRG                 L1-10221C-FIGS-103-SS-A                                             07/08/1912:47                            10/2/2019        19-09012     Strontium-90                                                                        3.73E-01                         3.20E-01                        3.45E-01                6.40E-01 19-09012-13               TRG                 L1-10221 B-FIGS-102-SS-A                                            07/08/19 13:10        9/3/2019           10/2/2019                                                                                                                                          3.67E-01                        3.88E-01                7.44E-01                      u
                                                                                                              *-----------~-------
19-09012-14               TRG                 L1-10221B-FIGS-103-SS-A                                             07/08/19 13:12                           10/2/2019                                                                                                                                          3.58E-01                        3.63E-01                7:47E-01                      u 19-09012-15               TRG                 L1-10221B-FIGS-104-SS-A                                             07/08/19 13:14                           10/2/2019                                                                                                                                          2.86E-01                        2.87E-01                6.10E-01                      u 1----------*-*-*--,---*-
19-09012-16               TRG                 L1-10221B-FIGS-105-SS-A                                             07/08/19 13:16                           10/2/2019                                                                                                                                          3.12E-01                        3.17E-01                6.50E-01                      u 19-09012-17               TRG                                                                                                                                                                                                                                                                                 3.61E-01                        3.67E-01                7.52E-01                      u 6.01E-01                      u                   pCVg 5.52E-01                      u 19-09012-01               LCS                 KNOWN                                                                                                                                        Cobalt-60                                                                                                         5.10E+OO                                                                                                   pCi/g 19-09012-01                                   KNOWN                                                                                                                                      Cesium-137                                                                                                          3.39E+OO                                                                                                   pCi/g 19-09012-01               LCS                 SPIKE                                                                                                                                        Cobalt-60                                                                                                         1.02E+01                        1.25E+01                 9.61E-01 19-09012-01               LCS                 SPIKE                                                                                                                                       Cesium-137                                                                                                         9.07E+OO                        1.00E+01                 1.09E+OO                                          pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
("M>             EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                             865/481-0683                                      FAX 865/ 483-4621

Printed: 101211201912:02 PM                                                                                                                                                                                                                                                                                                                   Page 4 of 21 Report To:                                                                                                                                 Work Order Details:
Patricia Giza                                                                                                                                                    19-09012 Eberline Analytical                                                                                     Zion           Solutions ___ ,_ ----
Purchase___Order:
SDG:
677118
                                                                                                    --- ''""""------*------                                                         -                                 "'"-"'-' -----,-w,                  _
Final Report of Analysis                                                                           2701 Deborah Ave
                                                                                                                                                                                                             ....,. -*--      _ . , Analysis Category:                            ______
ENVIRONMENTAL Zion, IL 60099                                                                                                           Sample Matrix:                        so I                                                                                                                                                        '
Lab                  Sample                               Client                              Sample                       Receipt            Analysis                    Batch                                                                                                                  '                                                                            Report Analyte                        Method                            Result                 cu               CSU                 MDA                    Qualifier ID                   Type                                   ID                                  Date                ,        Date                Date                      ID                                                                                                                                                                                                  Units
__    1_9_:CJ_~12-,0_2_____,____M__B__L____ ,,B._LAN,     ____K*----------                            09/05/19 00:00             : 9/3/2019              9/10/2019                  19-09012           Actinium-228                EPA 90U Modified                        2.49E-02            7,21E-02      '   7,21E-02            U4E-01                           U                     pCi/g
                                                                                                                                                                                                      **sii;;~~:ios.;;-*                                                                                                                                            *u-----
1 19-09012-02                  MBL               BLANK                                            09,05,19 00:00                   91312019          9110,2019                  19-09012 -                                 ~-EP--A-901.1M~~'=-~-** ~-~-~9~~:_oi-:-_-_2_-:0_6_E_-0_2___2_:0                       __
6~~0~~~~-3.-31-E--02.~.                                               pci~
c-- *19-09012-02 .,                MBL               BLANK                                            09/05/19 00:*o--o*-*r***9,-/--3/*2*0-*1**-9*--c-*-9-/1*0*-,2-o-*1-9           19-09012          Amelicium-241                EPA 901.1 Modffied                     -5.66E-02            4.02E-02          4.03E-02            5.25E-02                         U                     pCi/g
                                               **------*------------*- --------*-+----*-------*-"'---------"""'"'"''""'''""Y""'**-----1----*-----*------*-------
_:1_~:Cl_~&deg;.2~:_CJ.~-- .         -~B~---~-K___ ---*-*-------------.._09_10~1_1_9 00:00 _                                              9/3/2019          91_19!~-~:9_ _ .: 9.::~~_CJ:1_2_ --- Ba~':':.!~-                          EPA 901. 1 Modifi<e~ _ --- -1 05E-02                        3.04E-02          3.04E-02            3.97E-02                         U                     pCi/g 19-09012-02                  MBL**--*----B_LA     ____N-K__________,,,.,,                       09/05/19 _o_o__:_o__o_,__9.i_3__,2_0_19__,-,_9_J_10_,_20.._1_9"'"" 19-09012                       Bismuth-214                EPA 901.1 Modified                      3.81E-02            4.31E-02          4.32E-02            7.73E-02                         U                     pCi/g
__1_9__ -o_9__0___
12,__-0_2~-------M*_B__L______,.______
B_LA_N_K____ -______,._________ -___ *------1-0-9--10__5_11_9_0_0:..o__o____+'_,9_13_12_0_1_9_, __9_11_0_,2_01_9_______1__9__ --0_90-__1_2_ -----c_o_b_a_tt-_6_0_ __~~~~:,'.,~-~!!ied _ "------1_.2__4__E,--o,_2,____ -_2_.1_3_E_-0_2_;_2_._13_E_-0_2__________3_,__               o7_E_-_0__2,______            u_____________.:,P_Ci/:.g____--1 1                                                                                                                                                                                                                              1                                                                              1 19-09012-02                  MBL               BLANK                                            09/05/1900:00              ; 9/3/2019
* 9/10/2019                             19-09012            Cesium-134                 EPA901.1 Modified                       3.48E-03
* 2.40E-02      1   2.40E-02            2.93E-02                         U                     pCi/g
    .. :1~:&deg;.~o~~~--*---~~~-,--BLA                       __ ~~ ----------------1--0_91_05__119                  __ __0,_o_:o_o___,* ..._91_3_120,,1__
9 ____9_1_11_o_,2__0
__1__9,, _____19-09012            Cesiu':1::2:3_~-- ___      EPA_901._:1 Modified___
* 2,99E-03
* 1.81 E-02         1,81 E-0__ 2_-,,_-___
3,9___1E__-0____2__*--------*--- u
__ __ ,_______,, _____P_Cii_g_____,
19-09012-02                  MBL               BLANK                                            09/05/1900:00 , 9/3/2019
* 9/10/2019                                          19-09012           Europium-152                EPA901.1 Modified                       1.79E-02
* 8.29E-02          8,29E-02            5.86E-02                         U                     pCi/g
                              --------------------------------------------,-l----------------*-+-----------------,----------------'-----1-----------------------------,,.,,,______________________________ , , _ _ _ _ _ ,,____---------------'---"----l 19-09012-02                  MBL               BLANK                                                                                                                                        1 09/05/19 00:00             ' 9/3/2019              9/10/2019                  19-09012           Europium-154                EPA 901. 1 rvl~~e.~4_.__6_9E___-_02______,.___              7_,o_7E_-_02_~,-7_.0_8_E-_o-2______2_ ..,9___4__E
__-__o-2_ _ _u                               pCi/g 19-09012-02                  MBL               BLANK                                            09/05/19 00:00             i 9/3/2019              9/10/2019                  19-09012           Europium-155                EPA901.1 Modified                      -1.52E-02            2.90E-02          2.91E-02            4.09E-02                         U                     pCi/g
   """" --------------*-*-**--" ----*--*-----------*---*-,.*----,---+----,-------+---,---+---                                                                                                                                                               __,_            ------*-*-**--0*------"---*--'--*-----"----------*--~---------,-----,,-----1 19-09012-02                  MBL               BLANK                                            09/05/19 00:00 : 9/3/2019                          9/10/2019                  19-09012          Holmium-166m                 EPA 901.1 Modified                     -1.47E-02            4.09E-02 ; 4.09E-02                   3.16E-02                         U                     pCi/g l--19--09_0_______,_M               ___B__L_____,___  B_LA,,,N--K------------ "" ,,,________ , __, __0,_9_/0-5/_1_9_00~-9/3~. 9110-,2-019 . 19-09012 '                                                    lodine-129,-t-__ ,___     E_P_A_9_01-.1-_M,o__d_ifi-,e--d*---,-G--6-.4_6,-E**--0-2~--1.-09-E--0-1---i---1-.1""0E"--01_______1___6_5E--'0"'1" -----"""u"'"'""'"___:__pC__i_/g"----l
 ,______                      ------"""'"**-*--~---,------*-----* ---*----~.-----+--                                                                                                  ----*--*----------1---------------------------------~----------i-----'---,,,____,,_ _ _ _,_
19-09012-02                  MBL               BLANK                                            09/05/1900:00 . 9/3/2019                           9/10/2019                  19-09012 I Potassium-40                        EPA901.1 Modffied                 1    4.95E-01             3,12E-01
* 3.13E-01                   7,81E-01                         U                     pCi/g
                                                                                                   --------                                                                                        .------1-----------------*+------------------+----+---------------'---------'-"----I 19-09012-02
* MBL               BLANK                                            09/05/1900:00                    9/3/2019          9/10/2019                  19-09012          Manganese-54                 EPA901.1 Modified                       3.56E-03
* 2.02E-02          2.02E-02            4,09E-02                         U                     pCilg
 ~---------*---- '. ,----*                                  ----*----------~                                          ~                                                                            ----'-------+----------,--'----------------0....-----',------------------------,----------'--_;;,_--'1 19-09012-02                  MBL               BLANK                                            09/05/1900:00 i 9/3/2019                           9/10/2019                  19-09012
* Molybdenum-93                       EPA901.1 Modified                 , -L02E-03                1.01E-02 ' 1.01E-02                   2.99E-02                         U                     pCi/g 19-09012-02                  MBL ____          B_LAN_K________________ --+-0-9-,0-51_19_00:00"'" 9/3/2019                                          9/1012019 "-19-09012 i--N:.io-b-iu-m--9-4-l------E-P_A__9_01___                       1 -M-od-ifi-,e*d----',--_-3_-8_2__E___
o3-,'----2.os-E--02--'-*--2-,o-8E'---02___.;;:3'-_2--5::.E_*-o-2----------u*------,-,__c:_pc"'i:..::/g:....-1
!----------*-                                                         --------------- -                                   -----<------'--------,- ---------~----------------------i------f---------------------*''"""'___:__:_;;:..__--'I 19-09012-02                  MBL               BLANK                                            09/05/19 00:00                   9/3/2019          9/10/2019                  19-09012              Lead-210                 EPA 901.1 Modffied                i 3.70E-01 ' 4,21E-01
* 4.21E-01                                6,60E-01                         U                     pCi/g
                                                                                                                                                                                                 --',-------+-------------~--------------,--r------+----------------'---"'--1 19-09012-02                  MBL         ,     BLANK                                            09/05/19 00:00                   9/3/2019 i 9/10/2019                         19-09012              Lead-212                 EPA 901.1 Modified                      3.27E-02       ,    2,93E-02      '   2.94E-02            5.17E-02                         U                     pCi/g J - - - - - - - - - - - , - - - - - - - ' - - - - - - - - - - - - - - - - - , - - , - - - - - - - - - - - - - - - , , - ~ - - - - - + - - - - - - - - - , - - - - - - - - * - - - - - - - - + * - - - - - - - - - - . . ; . . , , _ , ,______i----------+------------'------"--.:::____ ,
t--1_9_-0_9_0_12_-o-.2__,! ___      M_B_L_____+-__    B_LA_N_K--.--------------,--0-9.1_0_51_1_9_oo:oo i 9/3/2019                                         9/10/2019                  19-09012              Lead,-_2_14__     -+___E_P__A_9_0_1._1__M_o_difi_e_d__+-__11._06E_-02_i,___4.68_E-_02__-i---           4,6_8E-_02....._1_    ,5_1_  E-0_2-~__u__,_,.__ _,_PC'-il_;;g:__~
19-09012-02                  MBL               BLANK                                            09/05/19 00:00                   9/3/2019          9/10/2019 ; 19-09012 : Promethium-145                                     EPA901.1 Modified                      -4.08E-02
* 7.12E-02          7,12E-02         ,  1.01E-01                         U                     pCi/g 1--1-9--0--9-0-12--0-2--i)*--M-B_L_,______            B__LA_N_K____________+-_0_9_/0-5/_1__                      9_00-:0-0-<---9-/3-/2-0-1-9--;--9/-1-0/-20-1-9~--19-09012                               Radium-226                 EPA 90U Modified                        3.81E-02            4,31 E-02         4,32E-02            7,73E-02                         U                     pCi/g 1---------~*---------------------+--------+------+----,--- -"------+------------,,--------+----+---------------+------I 19-09012-02 ;                MBL               BLANK                                            09/05/1900:00                    9/3/2019          9/10/2019                  19-09012           Antimony-125                EPA901.1 Modified                       1.21E-02            2,75E-02          2,75E-02            R58E-02                          U                     pCi/g 19-09012-02           i MBL 1-----.:------,----------------"--I---------
BLANK                                            09/05/1900:00                    9/3/2019          9/10/2019                  19-09012           Thorium-234                 EPA901.1 Modified                      4,09E-01
                                                                                                                                                                                ------+---,--:--.:--t---:-:-:--:-:--:--------,-t---:::-:--:--:+----_;,_----,-------,------------'---=---'I 3,05E-01          3,06E-01            4,96E-01               '         U                     pCi/g 19-09012-02 ,                MBL
* BLANK                                            09/05/19 00:00                   9/3/2019 1 9/10/2019                         19-09_0_1_2_,-_Th_a_mu_m_-_20_8_,,1---E_PA_90_1_.1_M_o_d_ifi__        ,e_d_______1_1.1_0E_-02--._1.        __
                                                                                                                                                                                                                                                                                                 '.8_4E_-02_,_1_r,_85E_-02_ _ _       1,18_E-0_11_____u_____                      ._P_C_ii_g_--1 19-09012-02 ;                MBL         ,     BLANK                                            09/05/1900:00                    9/3/2019 i 9/10/2019                         19-09012           Uranium-235                 EPA901.1 Modified                      -3.29E-02            9,91E-02          9.91E-02            1.44E-01                         U                     pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(     ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601        SCARBORO ROAD OAK RIDGE,                                                TN 37830                     865/481-0683                            FAX       865/483-4621

Printed: 10/21/201912:02 PM                                                                                                                                                                                                                                     Page 5 of 21 Report To:                                                                         Worn: Order Details:
Patricia Giza                                                                                             19-09012 Eberline Analytical                                                                                        ** ****nm.-----*-----**v*n* *
* Zion         Solutions SDG:
Purchase****-*-----_,
Order:       _____________
677118
                                                                                                          '"""'"'"  _____""""~---*-                                                                                                                ,,_
                                                                                                                                                                                                                                                                   --------*----    ,,-rn _ _ _
Final Report of Analysis                                                                                     2701 Deborah Ave
                                                                                                                  "''"""=---------------
Analysis Category:_ . ENVIRONMENTAL v-v-  ---"-'
Zion, IL 60099                                                                    Sample Matrix:         so Lab           Sample                               Client                                             Sample                        Receipt       Analysis        Batch ID             Type                                  ID                                                  Date                          Date         Date           ID Analyte          Method             Result          cu             CSU      MDA    Qualifier 19-09012-03         DUP                L1-10221A-FJGS-002-SS-A                                        06/17/19 08:46                    9/3/2019     9/10/2019       19-09012    Actinium-228   EPA 901.1 Modified    5.38E-01       1.61E-01       1.64E-01 2.71E-01 19-09012-03         DUP                L1-10221A-FJGS-002-SS-A 06/17/19 08:46                    9/3/2019     9/10/2019       19-09012     Silver-108m   EPA 901.1 Modified                   4.82E-02       4.83E-02 5.ZOE-02     u 19-09012-03 19-09012-03 DUP DUP L 1-10221A-FJGS-002-SS-A L 1-10221 A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019     9/10/2019       19-09012   Americium-241
                                                                                                                                      ; 9/3/2019 _ 9/10/2019 ____ 19-09012 _, ___ Barium-133 EPA 901.1 Modified EPA 901.1 Modified 3.73E-02 O.OOE+OO 9.39E-02 3.09E-02 9.39E-02 3.09E-02 1.26E-01 8.53E-02 u
u 19-09012-03          DUP               L1-10221A-FJGS-002-SS-A                                                                          9/3/2019      9/10/2019                   Bismuth-214   EPA 901.1 Modified    4.0SE-01       1.06E-01       1.0SE-01 1.75E-01
 -----------,,*----*-*"""'""'        " ' " _ ,_ _ _ _ v v m " " " " - * - - - * - - v m e
* v ***-+-------~--**--*---*--
19-09012-03         DUP               L 1-10221A-FJGS-002-SS-A                                                                          9/3/2019     9/10/2019                                  EPA901.1 Modified      1.07E-01      4.63E-02       4.66E-02 8.72E-02 19-09012-03         DUP                L 1-10221A-FJGS-002-SS-A                                                                         9/3/2019     9/10/2019                                  EPA901.1 Modified                    2.29E-02       2.29E-02 5.49E-02     u 19-09012-03         DUP                L 1-10221A-FJGS-002-SS-A                                       06/17/19 08:46                    9/3/2019     9/10/2019                                  EPA 901.1 Modified    6.79E-01       1.11E-01       1.16E-01 7.96E-02 19-09012-03          DUP               L 1-10221 A-F JGS-002-SS-A                                     06/17/19 08:46                    9/3/2019     9/10/2019                                  EPA 901.1 Modified    3.53E-02       1.31E-01       1.31E-01 1.63E-01     u 19-09012-03          DUP               L1-10221A-FJGS-002-SS-A                                                                          9/3/2019      9/10/2019                                 EPA 901.1 Modified    8.96E-03       1.35E-01       1.35E-01 8.31E-02     u 19-09012-03 .        DUP               L1-10221A-FJGS-002-SS-A                                        06/17/19 08:46               : 9/3/2019         9/10/2019
                                                                                                                                                 ,v,m-*,-s-------,,m,_,.,
EPA901.1 Modified     4.04E-03       9.38E-02       9.38E-02 1.22E-01     u 19-09012-03         DUP                L 1-10221A-FJGS-002-SS-A                                       06/17/19 08:46                    9/3/2019     9/10/2019       19-09012   Holmium-166m    EPA 901.1 Modified    3.0SE-02                      6.SSE-02 6AOE-02      u 19-09012-03          DUP               L 1-10221A-FJGS-002-SS-A                                       06/17/19 08:46                    9/3/2019 9/10/2019
_,_,         19-09012      lodine-129   EPA901.1 Modified                                            3.02E+OO     u
 ------~---*
19-09012-03         DUP                L1-10221A-FJGS-002-SS-A                                        06/17/19 08:46               ! 9/3/2019 9/10/2019       19-09012    Potassium-40   EPA 901.1 Modified                                  1.82E+OO 7.40E-01 19-09012-03          DUP
,-------,----~--------------
L 1-10221A-FJGS-002-SS-                                        06/17/19 08:46                    9/3/2019     9/10/2019       19-09012    Manganese-54   EPA 901.1 Modified                                           7.40E-02     u 19-09012-03          DUP               L1-10221A-FJGS-002-SS-A                                        -06/17/19 08:46                   9/3/2019      9/10/2019      19-09012 ; Molybdenum-93__ EPA901.1 Modified                                            3.97E-02     u 19-09012-03          DUP                                                                              06/17/19 08:46                    9/3/2019      9/10/2019      19-09012      Niobium-94                                                                5.34E-02     u 19-09012-03                            L 1-10221A-FJGS-002-SS-A                                       06/17/19 08:46                    9/3/2019     9/10/2019       19-09012 Lead-210    EPA 901.1                                                    1.92E+OO     u L 1-10221A-FJGS-002-SS-A                                       06/17/19 08:46                    9/3/2019     9/10/2019       19-09012 j     Lead-212    EPA901.1                                                     1.69E-01 06/17/19 08:46                    9/3/2019      9/10/2019      19-09012!      Lead-214    EPA901.1                                                     2.06E-01 06/17/19 08:46                    9/3/2019      9/10/2019      19-09012 i Promethium-145 06/17/19 08:46                    9/3/2019      9/10/2019      19-09012     Radium-226 06/17/19 08:46                    9/3/2019      9/10/2019      19-09012    Antimony-125 06/17/19 08:46                    9/3/2019     9/10/2019       19-09012     Thorium-234 06/17/19 08:46                    9/3/2019     9/10/2019       19-09012 i  Thallium-208 06/17/19 08:46                    9/3/2019     9/10/2019 ' 19-09012         Uranium-235 CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;OUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>          EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                       865/481-0683            FAX    865/483-4621

Printed: 1012112019 12:02 PM                                                                                                                                                                                                                                                              Page 6 of 21 Report To.                                                                                                                  Worf< Order Details:
Patricia Giza                                                                                                                             19-09012 Eberline Analytical                                                          *-***---*-
Zion Solutions m*w 0
SDG:
Order:
677118 Final Report of Analysis                                                                   2701 Deborah Ave
                                                                                *--*~*-----** -*------***
Analysis Category:
                                                                                                                                                                                                                                ~------    ENVIRONMENTAL Zion, IL 60099                                                                                Sample Matrix:                              so Lab         Sample                             Client                                 Sample             Receipt        Analysis        Batch                                                                             :                                                                                 Report ID          Type                                ID                                     Date               Date          Date              ID
* Analyte                       Method                                 Result         cu             CSU                 MDA      Qualifier Units 19-09012-04 _.,    DO
                   ,,         l 1-10221A-FJGS-002-SS-A w, _ _ _ _ _ _ _ _ _ , _ _ _ _ _ _ _ _ -----*-****
06/17/19 08:46           9/3/2019      9/10/2019      19-09012            Actinium-228             EPA 901.1 Modified                           4.25E-01      1.78E-01        1.80E-01 3.45E-01 pCi/g 19-09012-04        DO        l 1-10221 A-F JGS-002-SS-A                              06/17/19 08:46           9/3/2019      9/10/2019      19-09012             Silver-108m             EPA901.1 Modified                            -2.10E-02     4.17E-02        4.18E-02            5.01E-02        u           pCi/g
~ - - - - '.---~-----*---------*----*---------**                             - -------=*" --***-------- **-*-* *-----*--*-----------,----,--****- **--- *----
19-09012-04        DO        L 1-10221A-FJGS-002-SS-A                                06/17/19 08:46           9/3/2019      9/10/2019      19-09012           Americium-241             EPA 901.1 Modified                           -1.28E-02     9.44E-02        9.44E-02            1.21E-01        u           pCi/g
                                                                                ------~--------.-----*---*- -*-----..----------~---- -*-- -*---=*                                    w                                                                                                                           **--"*---*----
19-09012-04        DO        l 1-10221 A-F JGS-002-SS-A                              06/17/19 08:46           9/3/2019      9/10/2019      19-09012             Barium-133              EPA 901.1 Modified                            1.48E-03     2.96E-02        2.96E-02            7.55E-02        u           pCi/g
                                                                                           *----""" _ _ _ ,
* m e " " " * * * - - * = = , - - - - - * - - -   --------*-----**
19-09012-04        DO        l 1-10221 A-FJGS-002-SS-A                               06/17/19 08:46           9/3/2019      9/10/2019      19-090               Bismuth-214             EPA901.1 Modified                             4.34E-01      1.19E-01       1.21E-01             1.75E-01
*-------- **-- "--**~-- -.,-.-----"------**
                        ""                                                                    --*--*-----*---;---.                                                                                                              i 19-09012-04        DO        l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46           9/3/2019      9/10/2019      19-09012 :             Cobalt-60             EPA901.1 Modified                             1.25E-01     4.98E-02        5.02E-02            9.17E-02                    pCi/g 19-09012-04        DO        l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46           9/3/2019      9/10/2019      19-09012             Cesium-134              EPA 901.1 Modified                           -1.51E-02     2.39E-02        2.40E-02            5.72E-02        u           pCi/g 19-09012-04       DO        l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46 9/3/2019      9/10/2019      19-09012        i    Cesium-137              EPA 901.1 Modified                            6.28E-01     1.04E-01        1.09E-01            7.49E-02                    pCi/g 19-09012-04       DO        l1-10221.         r -- -- ~'.::
* 06/17/19 08:46        ; 9/3/2019       9/10/2019      19-09012 *          =***--'**- :.s2          EPA901.1 Modified                            -2.94E-02   . 1.77E-01       1.77E-01            1.55E-01        u           pCi/g 19-09012-04 '      DO       l 1-10221 A-F JGS-002-SS-A                              06/17/19 08:46           9/3/2019      9/10/2019      19-09012        i   <=,*---'**- ~.s          EPA901.1 Modified                            -1.70E-02      1.28E-01       1.28E-01            8.06E-02        u          *pcitg        -
19-09012-04        DO    i  l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46        i 9/3/2019       9/10/2019      19-09012 ,          =~~--'**- "':            EPA 901.1 Modified                            1.10E-01     9.01E-02        9.02E-02            1.23E-01        u           pCi/g 19-09012-04        DO     '  l 1-10221 A-F JGS-002-SS-A                              06/17/19 08:46        i 9/3/2019      9/10/2019      19-09012 j Holmium-166m                      EPA901.1 Modified                            -8.47E-04   ! 6.76E-02        6.76E-02            6.37E-02        u           pCi/g 19-09012-04       DO        l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46        i  9/3/2019      9/10/2019      19-09012 ,            lodine-129             EPA901.1 Modified                            2.20E+OO    ' 9.51E+OO        9.51E+OO            3.02E+OO        u           pCi/g 19-09012-04        DO       l1-10221.         r---- ~'.::'                          06/17/19 08:46        i  9/3/2019      9/10/2019 , 19-09012 :             Potassium-40             EPA901.1 Modified                            1.29E+01      1.84E+OO    i   1.96E+OO            1.02E+OO                    pCi/g
                                                                                             **----~-~---
19-09012-04        DO    i l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46           9/3/2019      9/10/2019
* 19-09012           !  Manganese-54              EPA901.1 Modified                              r.78E-03  : 4.16E-02    !   4.16E-02            6.67E-02        u           pCi/g 06/17/19 08:46           9/3/2019      9/10/2019      19-09012 : Molybdenum-93                     EPA901.1 Modified                            -9.58E-03
                                                                                                                                                                                                                                                                .                                       u 19-09012-04        DO       l 1-10221A-FJGS-002-SS-A
                                                                                                       ----+-------- ;               ..                                        -*---                                                              : 3.50E-02        3.50E-02            5.14E-02  i                 pCi/g 19-09012-04 /      DO    i  l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46           9/3/2019      9/10/2019      19-09012              Niobium-94             EPA901.1 Modified                             3.13E-03   ! 3.07E-02    i   3.07E-02            5.57E-02        u           pCi/g
                                                                                                                            -             **-                                  --                                                                 :             i 19-09012-04 !     DO        l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46        '  9/3/2019
* 9/10/2019 , 19-0901                             -210           EPA 901.1 Modified                            3.64E-01     1.14E+OO        1.14E+OO            1.78E+OO        u           pCi/g
                                            ..                                                                                                                                                                                                    i 19-09012-04       DO        l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46        ! 9/3/2019 , 9/10/2019          19-0901                        212           EPA901.1 Modified                             3.70E-01     8.22E-02        8.44E-02            1.47E-01                    pCi/g 19-09012-04        DO       l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46        :  9/3/2019
* 9/10/2019         19-09012        t      lead-214              EPA901.1 Modified                            4.50E-01    i 1.25E-01    t 1.27E-01       i    1.98E-01                    pCi/g 19-09012-04  !     DO    i  l 1-10221 A-F JGS-002-SS-A                              06/17/19 08:46        l  9/3/2019      9/10/2019      19-09012        i Promethium-145             EPA901.1 Modified                             8.62E-01   ! 7.49E-01    !        iE-01          9.33E-01        u           pCi/g 19-09012-04        DO    I  l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46        1 9/3/2019       9/10/2019      19-09012 !
                                                                                                                                                     --+i Radium-226              EPA 901.1 Modified                            4.34E-01   i 1.19E-01        1.21E-01            1.75E-01                    pCi/g 19-09012-04        DO     i l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46        i  9/3/2019      9/10/2019 : 19-09012               Antimony-125             EPA901.1 Modified                            -8.35E-02   !  1.05E-01   i   1.05E-01            1.53E-01        u           pCi/g 19-09012-04        DO     '  l1-10221'         c1r::<:Jln?.<'<'
* 06/17/19 08:46        i  9/3/2019      9/10/2019      19-09012 i          Thorium-234              EPA 901.1 Modified                            3.60E-01   ! 9.21E-01        9.22E-01            1.24E+OO  i     u     :     pCi/Q 19-09012-04       DO     i  l 1-10221A-FJGS-002-SS-A                                06/17/19 08:46           9/3/2019
                                                                                                              -9/3/2019 9/10/2019      19-09012 jThallium-208                       EPA            .1 Modified                    1.43E-01   I 6.15E-02        6.19E-02            9.03E-02                    pCi/g 19-09012-04 !      DO       l 1-10221A-FJGS-002-SS-A                                06117/19 08:46 9/10/2019      19-09012        i    Uranium-235             EPA 901.1 Modified                           -1.06E-02   I 2.88E-01        2.88E-01            3.74E-01        u           pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(  ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                   865/481-0683                                 FAX    865/483-4621

Printed: 101211201912:02 PM                                                                                                                                                                                                                                                  Page 7 of 21 Report To:                                                                                                        Work Order Details:
Patricia Giza                                                                                                                    19-09012 Eberline Analytical                                                                       > , v* ---*-**---mm,m**"Sv-s*-
Zion Solutions SDG:
Purchase Order:                 677118
                                                                                            *--*------------*"-~-------"-                                                               -- -V*--------* *"''""' ""' --- **"'""'"-----*------.------*--**-*---*-*
Final Report of Analysis                                                              2701 Deborah Ave                                                                             . Analysis Category:                ENVIRONMENTAL
                                                                                                                                                                                                                      ""'' ---*-- ------*-"'"'""rn*--"' '"'- -*-*--,--,~---*-*
Zion, IL 60099                                                                                     Sample Matrix.*               so Lab               Sample                                Client                    Sample                   Receipt     Analysis                 Batch                                                                                                                                       Report Date         Date                     ID Analyte             Method                    Result                cu              CSU              MDA   Qualifier Units ID                  Type                                ID                         Date 19-09012-05               TRG                L1-10221 A-F JGS-001-SS-A             06/17/19 08:44              9/3/2019    9/10/2019               19-09012            Actinium-228      EPA901.1 Modified                                3.07E-01          3.09E-01        5.98E-01
                                                                                                        " -- -----*--*---                                                              ----------*-~-----*-*-
19-09012-05               TRG                L1-10221A-FJGS-001-SS-A               06/17/19 08:44              9/3/2019    9/10/2019               19-09012             Silver-108m      EPA 901.1 Modified                               8.26E-02          8.26E-02        9.82E-02   u 19-09012-05               TRG                L 1-10221A-FJGS-001-SS-A              06/17/19 08:44              9/3/2019    9/10/2019               19-09012           Americium-241      EPA 901.1 Modified           -8.15E-02           1.06E-01          1.06E-01        1.47E-01    u
                                                                                                                                                                                         ---------              **,-we~*----------,-~---------*--         -----*---*
19-09012-05               TRG                L 1-10221A-FJGS-001-SS-A              06/17/19 08:44              9/3/2019    9/10/2019               19-09012             Barium-133       EPA 901.1 Modified           -2.96E-02           2.85E-02          2.86E-02        1.63E-01    u 19-09012-05               TRG                L 1-10221A-FJGS-001-SS-A              06/17/19 08:44              9/3/2019    9/10/2019               19-09012            Bismuth-214       EPA901.1 Modified             3.39E-01            1.59E-01         1.60E-01        4.10E-01    u 19-09012-05               TRG                L1-10221A-FJGS-001-SS-A               06/17/19 08:44              9/3/2019                            19-09012              Cobalt-60
                                                                                                                                                        -------- _____ __ --*-*-            EPA901.1 Modified             1.39E-01           6.65E-02          6.69E-02        2.10E-01    u
----------=------------------------                                                                                                                                   _,
19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A              06/17/19 08:44           .                                                           Cesium-134       EPA 901.1 Modified            2.27E-02                                             1.30E-01    u
 -*-----*-** .................... *************-*--****--*--------** -**---+--**-------*-***--+----->----~--****-**.;.-***-***-**** ****---**----!-------*-**-*+-*-*----**---***----*****-***-**--+-------****----------*-****--*-**--**-,*--:........;:c..--t 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A                                                                                                                    EPA 901.1 Modified            3.14E-01                                             2.01E-01
                                                                    -**---* .......+----*-**----**-******si------***---,s*****-*----******-*--*--*-*****-*1-------------**-***_)**--**---**--*-*~*-**-*-*--*S--*--*----*-**************-**-***--*****---,.****,.***-*-****--'-=--***--1 19-09012-05                TRG                                                                                                                                                           EPA901.1 Modified             8.36E-02            1.28E-01         1.29E-01        2.29E-01    u 19-09012-05                TRG               L1-10221A-FJGS-001-SS-A               06/17/19                                                                                              EPA 901.1 Modified           -8.13E-02           2.12E-01          2.12E-01        1.16E-01    u
*----*---------*******--------*----**-**--+*-----***-***-----+--------*--..c._---*--*~--------*--***-'---_.:'-***--*--*+-*---****-*--*--------**-,***----*****-*s--
19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A                                                                                                                    EPA901.1 Modified             9.43E-03                             1.26E-01        1.85E-01    u 19-09012-05               TRG                L1-10221A-FJGS-001-SS-A                                                                                                                     EPA901.1 Modified             1.36E-01                             1.29E-01        8.26E-02   u 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A                                                                                                                    EPA901.1 Modified            -2.12E-02                                             1.16E-01   u 19-09012-05                TRG               L1-10221A-FJGS-001-SS-A                                                                                                                     EPA901.1                     1.36E+01                                              1.20E+OO 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A              06/17/19 08:44                                                                                        EPA 901.1 Modified           -9.68E-03                                             1.43E-01    u 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A                                                                                                                    EPA 901.1 Modified            1.29E-02                                             7.37E-02    u 19-09012-05                TRG               L 1-10221 A-F JGS-001-SS-A                                                                                                                  EPA901.1 Modified            -7.32E-02                                             7.84E-02    u 19-09012-05              ___----1--**
TRG     , _ ___ ______
_,,. " L 1-10221A-FJGS-001-SS-A                                                                                                    Lead-210        EPA901.1 Modified                                                                  1.30E+OO    u 19-09012-05                TRG               L1-10221A-FJGS-001-SS-A                                                                                                     Lead-212                                                                                           2.73E-01             pCi/g 19-09012-05                                  L1-10221A-FJGS-001-SS-A                                                                                                     Lead-214 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A                                                                                                   Radium-226       EPA901.1 Modified                                                                              u 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A                                                                                                  Antimony-125      EPA901.1 Modified                                                                              u 19-09012-05                TRG               L1-10221A-FJGS-001-SS-A                                                                                                   Thorium-234       EPA 901.1 Modified                                                                 2.35E+OO    u 19-09012-05                TRG               L 1-10221A-FJGS-001-SS-A                                                                                                  Thallium-208      EPA901.1 Modified                                                                  1.72E-01 19-09012-05                TRG               L1-10221A-FJGS-001-SS-A                                                                               19-09012            Uranium-235       EPA901.1 Modified                                                                  4.87E-01    u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
( ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601        SCARBORO ROAD OAK RIDGE,                                       TN 37830          865/481-0683                   FAX      865/ 483-4621

Printed: 10/21/201912:02 PM                                                                                                                                                                                   Page 8 of 21 Report To:                                                                          Work Order Details:
Patricia Giza                                                                                         19-09012 Eberline Analytical                                                *--------*-s--v-'**-*~*--**=---
                                                                         "     Zion Solutions SDG:
Purchase Order:               677118 Final Report of Analysis                                           2701 Deborah Ave v--""-""-"""-------~-~--m"-""v**
__ Analysis Category: __            ENVIRONMENTAL Zion, IL 60099                                                          Sample Matrix:                so Sample                  Client                Sample                  Receipt   Analysis     Batch                                                                                                          Report ID                                             Date      Date         ID Analyte            Method                   Result         cu            CSU     MDA    Qualifier Type                                         Date                                                                                                                                                          Units TRG     L 1-10221A-FIGS-005-SS-A                                                                     Actinium-228    EPA 901.1 Modified           5.92E-01    2.11E-01       2.13E-01 3.07E-01 19-09012-06                TRG     L1-10221A-FIGS-005-SS-A                                                                      Silver-108m     EPA 901.1 Modified          -2.27E-02    5.66E-02       5.66E-02 6.62E-02    u
 '""""~-----*-----*-------***----. ------*
19-09012-06                 TRG    L1-10221 A-Fl GS-005-SS-A                                                                                    EPA901.1 Modified            2.79E-03    2.97E-02       2.97E-02 1.09E-01    u
-*---*--*--"-*---------------""'"-'"--"""""'""*--m*"
19-09012-06                 TRG    L 1-10221A-FIGS-005-SS-A      06/13/19 07:45                                                  Barium-133     EPA 901.1 Modified           1.99E-02     3.05E-02      3.05E-02 1.17E-01    u 19-09012-06                 TRG    L 1-10221A-FIGS-005-SS-A       06/13/19 07 :45                                                               EPA901.1 Modified            4.07E-01     1.32E-01      1.34E-01 1.83E-01 19-09012-06                TRG     L1-10221A-FIGS-005-SS-A       06/13/19 07:45                                                                 EPA 901.1 Modified           8.58E-02    6.59E-02       6.61E-02 1.29E-01    u 19-09012-06                 TRG    L 1-10221A-FIGS-005-SS-A      06/13119 07:45                                                                                             -1.17E-02    3.52E-02       3.53E-02 9.32E-02    u        pCi/g 19-09012-06                        L 1-10221A-FIGS-005-SS-A      06/13119 07:45                                                                                              1.50E-01    7.32E-02       7.36E-02 1.10E-01 19-09012-06                TRG    L 1-10221A-FIGS-005-SS-A                                              9/10/2019                                                          -8.47E-02     1.74E-01      1.74E-01 1.64E-01    u 19-09012-06                TRG    L1-10221A-FIGS-005-SS-A                                               9/10/2019                                                          -1.42E-01     1.93E-01      1.94E-01 8.27E-02    u
     ~----**-*--"'*:.c--------------*-----------~--*
19-09012-06                TRG    L 1-10221A-FIGS-005-SS-A                                              9/10/2019                              EPA901.1 Modified            5.63E-02     6.93E-02      6.94E-02 1.17E-01    u 19-09012-06                TRG    L 1-10221 A-FIGS-005-SS-A                                             9/10/2019                              EPA 901.1 Modified          -5.87E-02                   9.25E-02 6.79E-02    u 19-09012-06                TRG    L 1-10221A-FIGS-005-SS-A                                                                                     EPA 901.1 Modified                                      2.00E-01 2.87E-01    u
                          .                                                                                                                         EPA901.1 Modified            1.40E+01                   3.02E+OO 1.83E+OO 19-09012-06                TRG 19-09012-06                                                                                                                                    EPA901.1 Modified            1.47E-02                   5.27E-02 9.03E-02    u 19-09012-06                                                                                                                                    EPA901.1 Modified                                                7.84E-02    u EPA901.1 Modified                                                7.75E-02    u Lead-210      EPA901.1 Modified                                                1.36E+OO    u Lead-212      EPA 901.1 Modified Lead-214 u        pCi/g pCi/g L 1-10221A-FIGS-005-SS-A                                              9/10/2019
* u 19-09012-06                TRG L1-10221 A-FIGS-005-SS-A       06/13/19 07:45               9/3/2019  9/10/2019                                                                                                                    pCi/g 19-09012-06                TRG    L1-10221A-FIGS-005-SS-A        06/13/19 07:45           ! 9/3/2019 ; 9110/2019    19-09012 I Thallium-208                                                                                          pCi/g
    ----~-                                                                                                 ---t---
Uranium-235                                                                                  u        pCi/g 19-09012-06                TRG    L 1-10221A-FIGS-005-SS-A       06/13/19 07:45               9/3/2019  9/10/2019   19-09012 I CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601     SCARBORO ROAD OAK RIDGE,               TN 37830         865/481-0683                  FAX   865/483-4621

Printed: 1012112019 12:02 PM                                                                                                                                                                                                                                             Page 9 of 21 Report To:                                                                                                                    Worl< Order Details:
Patricia Giza                                                                                                                    19-09012 Eberline Analytical                                                       ****-******
Zion Solutions SOG:
Purchase Order:           677118
                                                                                --                                                                                                     ---~--* "                                                                                                      ***---*-*
Final Report of Analysis                                                          2701 Deborah Ave                                                                          __ _ Analysis Category:*-             ENVIRONMENTAL so Zion, IL 60099                                                                                         Sample Matrix:
Lab                Sample                             Client                    Sample                Receipt    Analysis         Batch                                                                                                                                                    Report ID                Type                               ID                        Date                   Date       Date Analyte                                Method               Result                          cu            CSU      MDA     Qualifier ID                                                                                                                                                       Units 19-09012-07                TRG               L 1-10221A-FIGS-006-SS-A           06/13/19 07:47               9/3/2019   9/10/2019      19-09012 ;     Actinium-228                           EPA 901.1 Modified
                                                                                                                                                                                                                      '  -8.65E-02                     2.87E-01        2.87E-01 4.48E-01        u       pCi/g
-*-*
* w _ m_ _ _ ' " " "
                                                                                                                 '""*-*----,,-*-*---------**-------~*--~"'
19-09012-07                TRG               L1-10221A-FIGS-006-SS-A            06/13/19 07:47               9/3/2019   9/10/2019      19-09012        Silver-108m                           EPA901.1 Modified      -1.82E-02                     6.96E-02        6.96E-02 9.45E-02        u       pCi/g
*--*---------~*-'""i*"*-------**--***-------**-**--*--"""-----------~"---*- -*----------*---*-*                                                   ---- ,--------oc*--               ~
19.09012-07                TRG               L 1-10221A-FIGS-006-SS-A            06/13/19 07:47              9/3/2019   9/10/2019      19-09012      Americium-241                           EPA 901.1 Modified      -4.67E-02            ;       9.91E-02        9.92E-02 1.38E-01        u       pCi/g
                                                                                                 ----*----- * ----*------*------***---------*-*--*We*
19-09012-07 :              TRG               l 1-10221 A-F IGS-006-SS-A          06/13/19 07 :4 7            9/3/2019   9/10/2019      19-09012
* Barium-133                           EPA901.1 Modified       2.14E-01                     1.09E-01        1.09E-01 1.66E-01        u       pCi/g 19-09012-07                TRG               L1-10221A-FIGS-006-SS-A             06/13/19 07:47              9/3/2019   9/10/2019      19-09012        Bismuth-214                           EPA 901.1 Modified       4.52E-01                    1.52E-01        1.54E-01 2.73E.Q1                pCi/g
 ---*-*---*-*--*---*-*-~*~***-**------*----------                                                              '
19-09012-07 ,              TRG               L 1-10221A-FIGS-006-SS-A           06/13/19 07:47               9/3/2019   9/10/2019      19-09012           Cobalt-60                          EPA 901.1 Modified  l   2.92E-01                     8.31E-02        8.44E-02 1.24E-01                pCi/g 19-09012-07 ;              TRG               L 1-10221A-FIGS.006-SS-A
                                                                                       -"-----"---~ *-*----w='--
06/13/19 07:47              9/3/2019   9/10/2019 19-09012        Cesium-134                            EPA 901.1 Modified     -7.13E-03                     2.50E-02        2.50E-02 1.12E-01        u       pCi/g 19-09012-07                TRG               L 1-10221A-FIGS-006-SS-A            06/13/19 07:47              9/3/2019   9/10/2019      19-09012        Cesium-137                            EPA 901.1 Modified      9.35E-01                     1.62E-01        1.69E-01 1.75E-01                pCi/g
                                 ----- '"'"-------~-----------------
19-09012-07                TRG               L 1-10221A-FIGS-006-SS-A
                                       ""=*-,----------------------
__. 06/13/19 07:47     ,          9/3/2019   9/10/2019      19-09012 '.    -
L.Ul ..... l"',.,.,:1-1.JL             EPA 901.1 Modified 1.21E-01                    1.90E-01        1.90E-01 2.35E-01        u       pCi/g 19-09012-07                TRG               L1-10221A-FIGS-006-SS-A             06/13/19 07:47              9/3/2019   9/10/2019      19-09012   i   Cu, . . . l"' ..... 11- 54             EPA 901.1 Modified     -1.28E-01                     2.02E-01        2.03E-01 1.23E-01        u       pCi/g 19-09012.07 ,              TRG               L 1-10221A-FIGS-006-SS-A            06/13/19 07:47              9/3/2019   9/10/2019      19-09012 I     ~,..u ..... r--,-*11-   .55            EPA 901.1 Modified       2.50E-02                    1.16E-01        1.16E.01 1.72E-01        u       pCi/g 19-09012-07 ,              TRG               L 1-10221A-FIGS-006-SS-A           06/13/19 07:47            I 9/3/2019    9/10/2019      19-09012   !  Holmium-166m                            EPA 901.1 Modified     -4.86E-02                     1.31E-01        1.31E-01 8.13E-02        u       pCi/g 19.09012-07 '              TRG               L 1-10221A-FIGS-006-SS-A           06/13/19 07:47            ; 9/3/2019    9/10/2019      19-09012   i      lodine-129                          EPA 901.1 Modified       4.09E-03                    7.72E-02        7.72E-02 1.14E-01 ;      u       pCi/g 19-09012-07                TRG     """'""" ____ ________________
L 1-10221 ..A-FIGS-006-SS-A        06/13/19 07:47            ;  9/3/2019   9/10/2019 ' 19-09012          Potassium-40                           EPA901.1 Modified       8.63E+OO
                                                                                                                                                                                                                                               '      1.81E+OO         1.86E+OO 1.79E+OO pCi/g 19-09012-07           !    TRG               l 1-10221A-FIGS-006-SS-A            06/13/19 07:47           l  9/3/2019   9/10/2019 , 19-09012      i   .,_,  *~-* *--- ......                 EPA901.1 Modified        3.02E-02            '       8.64E-02        8.64E-02 1.46E-01 ;      u       pCi/g 19-09012.07 ;              TRG               L 1-10221A-FIGS-006-SS-A            06/13/19 07:47           ; 9/3/2019 , 9/10/2019       19-09012             *""-                --
M EPA901.1 Modified        2.85E-02            i 5.29E-02        5.29E-02 8.51E-02 ;      u       pCi/g 19-09012-07 i              TRG               L 1-10221A-FIGS-006-SS-A            06/13/19 07:47              9/3/2019 : 9/10/2019 ' 19-09012 :          Niobium-94                           EPA 901.1 Modified       3.27E-03                   7.25E-02         7.25E-02 1.05E-01        u       pCi/g 19-09012-07 :              TRG               L 1-10221A-FIGS-006-SS-A
                                                                                  -- 06/13/19 07:47   '---- : -----,
                                                                                                               ; 9/3/2019    9/10/2019 I 19-09012 .
                                                                                                                                                    --+------*--
Lead-210                           EPA901.1 Modified       9.95E-02             I       8.04E.01        8.04E-01 1.18E+OO u       pCi/g
                                            ;                                         06/13/19 07:47 --,
19-09012-07 ;              TRG               L 1-10221A-FIGS-006-SS-A                                        9/3/2019 9/10/2019      19-09012 I         Lead-212                           EPA 901.1 Modified      5.03E-01                     1.46E-01    :   1.48E-01 2.46E-01                pCi/g 19-09012-07                TRG L1-10221A-FIGS.006-SS-A             06/13/19 07:47           I 9/3/2019   9/10/2019      19-09012 1         Lead-214                           EPA 901.1 Modified      5.22E-01             i       1.53E-01    :   1.56E-01 2.49E-01                pCi/g 19-09012-07                TRG               L 1-10221A-FIGS-006-SS-A            06/13/19 07:47           !  9/3/2019   9/10/2019 I 19-09012      l Promethium-145                           EPA 901.1 Modified     -5.09E-02             l       9.38E-02    :   9.38E-02 1.32E-01 u       pCi/g 19-09012-07                TRG               L 1-10221A-FIGS.006-SS-A            06/13/19 07:47           f  9/3/2019   9/10/2019      19-09012 'i     Radium-226                            EPA901.1 Modified        4.52E-01            l       1.52E-01        1.54E-01 2.73E-01                pCi/g 19-09012.07 ;              TRG
                                              *-* L1-10221A-FJGS-006-SS-A       ~------
06/13/19 07:47   ___--4 ___  9/3/2019   9/10/2019      19-09012 _j Antimony-125                           EPA 901.1 Modified      -1.56E-01                    2.30E-01 2.30E-01 2.93E.01 I      u    ;  pCi/g
     """' /'\i'\I'\~: /'\~ ;    TRG               L1-10221 A-FIGS-006-SS-A                          ____
06/13/19 07:47 ......,,.__i 9/3/2019    9/10/2019      19-09012 i '   Thorium-234                            EPA901    Modified      2.90E-01             :       8.99E-01        8.99E-01 1.34E+OO I      u pCi/g 19-09012-07 [              TRG         '     l 1-10221A-FIGS-006-SS-A           06/13/19 07:47 T
9/3/2019   9/10/2019      19-09012 !     Thallium-208                           EPA 901.1 Modified      4.49E-01             i       1.42E-01        1.44E-01 1.58E-01                pCi/g 19-09012.07           i    TRG               L1-10221A-FIGS-006-SS-A            06/13/19 07:47               9/3/2019 l 9/10/2019 i 19-09012      I    Uranium-235                           EPA901.1 Modified       3.80E-01             i       2.98E-01        2.98E.01 4.75E-01 \      u    I  pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("MJ            EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601        SCARBORO ROAD OAK RIDGE,                       TN 37830                                860/481-0683            FAX           865/483-4621

Printed: 10/21/2019 12:02 PM                                                                                                                                                                                                                     Page 10 of 21 Report To:                                                                                             Wori< Order Details:
Patricia Giza                                                                                                    19-09012 Eberline Analytical                                                                     Zion Solutions                                                                    Purchase Order:
SDG:
677118 Final Report of Analysis                                                         2701 Deborah Ave Analysis _Category: _              ENVIRONMENTAL Zion, IL 60099                                                                       Sample Matrix:              so Lab                      Sample                      Client                   Sample           Receipt        Analysis             Batch                                                                                                                                 Report Analyte               Method                  Result             cu             CSU          MDA        Qualifier ID                       Type                       ID                       Date              Date            Date                ID                                                                                                                                   Units 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49      9/3/2019      9/11/2019            19-09012     Actinium-228                                                                   1.66E-01      3.42E-01                      pCi/g 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/1907:49       9/3/2019      9/11/2019            19-09012     Silver-108m      EPA901.1 Modified            2 07E-02          3.41E-02       3.41E-02      5.44E-02         u            pCi/g
    -------* -----,-* *-*"--*---------------                                             *-**------. ,,_,___,~*~"'-----=---------- -* ---- ,. ---- - - - - -
* 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49      9/3/2019      9/11/2019            19-09012    Americium-241     EPA901.1       Modified       1.14E-01         9.95E-02       9.96E-02      1.42E-01         u
                                                                                         -----=~---- --0------- -s----~---------,,,-*- *----------- ----------*+**-***--*********-***
19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49      9/3/2019      9/11/2019            19-09012      Barium-133      EPA 901.1 Modified            1.47E-02         3.84E-02       3.84E-02      7.25E-02         u            pCi/g 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49      9/3/2019      9/11/2019            19-09012     Bismuth-214      EPA 901.1 Modified            4.77E-01         1.08E-01       1.11E-01      1.67E-01
  ****-******-*********-*****-****** .. ********-*-*- ****--**-----*--*-**              *-*-****-*-*---****-*---------*------**---**-*----+----******
19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/1907:49       9/3/2019      9/11/2019            19-09012       Cobalt-60      EPA 901.1 Modified            5.65E-02         5.93E-02       5.93E-02      1.07E-01         u
                                                ***-*--***---**-----************---****+*----***-***---yo-**                                              **--*--**-**--*--+**---------
19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19            9/3/2019      9/11/2019            19-09012     Cesium-134       EPA 901.1 Modified           -8.23E-03         2.37E-02       2.37E-02      5.50E-02         u
.......*----~----------,----*<<--------------------,-----                                                                                                                                               *-*------------*-- "
19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49      9/3/2019      9/11/2019            19-09012      Cesium-137      EPA 901.1 Modified            2.87E-01         8.26E-02       8.39E-02      1.04E-01 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07 :49     9/3/2019      9/11/2019                                          EPA901.1 Modified            -2.92E-02         2.07E-01       2.07E-01      1.90E-01         u 19-09012-08 '                      TRG      . L1-10221A-FIGS-007-SS-A.     . 06/13/19 07:49      9/3/2019      9/11/2019                                          EPA 901.1 Modified            3.25E-02         1.16E-01       1.16E-01      9.49E-02         u
        ***--*----**-******------******-*****----*-----*****-----.+----~-----**---*-**-----,**-----*-----*-;...*-*****'***-**----+----*----***-**---+----*-******,***-**----*------*-----**----*--*--****---*******-**-*--*-*--.:.........:::...... -1 19-09012-08 **--** TRG ___ ~0221..J:FIGS-007:~~~---*                               06/13/19 07:49      9/3/2019      9/11/2019                                          EPA901.1                      5.71E-02         1.03E-01       1.03E-01      1.38E-01         u 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49      9/3/2019      9/11/2019                                          EPA 901.1 Modified           -4.26E-02         8.31E-02       8.31E-02      7.34E-02         u 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49      9/3/2019      9/11/2019                                          EPA 901.1 Modified           4.39E+OO         1.84E+01        1.84E+01     3.41E+OO          u 19-09012-08                        TRG          L1-10221A-FIGS-007-SS-A            06/13/19 07:49                    9/11/2019                                          EPA 901.1 Modified           9.29E+OO         1.51E+OO        1.58E+OO      8.40E-01
  ------------------~<<--------------
19-09012-08 .                      TRG       ,  L1-10221A-FIGS-007-SS-A            06/13/19 07:49                    9/11/2019                                          EPA 901.1 Modified           -1.83E-03         4.74E-02       4.74E-02      7.38E-02         u 19-09012-08                        TRG          l 1-10221A-FIGS-007-SS-A           06/13/19 07:49                    9/11/2019                                          EPA 901.1 Modified            1.60E-03         4.05E-02       4.05E-02      6.32E-02         u 06/13/19 07 :49                   9/11/2019                                          EPA 901.1 Modified                             4.04E-02       4.04E-02      6.33E-02         u L1-10221A-FIGS-007-SS-A                                                                                  Lead-210       EPA 901.1 Modified           1.99E+OO         1.08E+OO        1.09E+OO     2.29E+OO L1-10221A-FIGS-007-SS-A                                                                                  Lead-212       EPA901.1 Modified             3.67E-01         9.14E-02       9.34E-02      1.97E-01 L1-10221A-FIGS-007-SS-A                                                                                  Lead-214       EPA901.1 Modified             4.60E-01                        1.25E-01      1.93E-01 L1-10221A-FIGS-007-SS-A                                                                                                 EPA901.1 Modified             8.78E-01                        8.33E-01      9.63E-01         u L1-10221A-FIGS-007-SS-A                                                                                 Radium-226      EPA 901.1 Modified            4.77E-01                        1.11E-01      1.67E-01 L1-10221A-FIGS-007-SS-A                                                                                                                               5.54E-02                        1.00E-01      1.77E-01         u L1-10221A-FIGS-007-SS-A                                                                                Thorium-234                                                                                 1.40E+OO          u            pCi/g L1-10221A-FIGS-007-SS-A                                                                                                                                                                             1.41E-01 L1-10221A-FIGS-007-SS-A                                                                                                                                                2.89E-01                     3.80E-01         u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>                   EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                        865/481-0683                   FAX 865/483-4621

Printed: 10/21/2019 12:02 PM                                                                                                                                                                                                                        Page 11 of 21 Report To:                                                                                   Work Order Details:
Patricia Giza                                                                                            19-09012 Eberline Analytical                                                                             Zion Solutions                                                              Purchase Order:
SDG:
677118 Final Report of Analysis                                                                   2701 Deborah Ave                                                 .... ___ Analysis                       ENVIRONMENTAL Zion, IL 60099                                                               Sample Matrix:             so Lab             Sample                                Client                            Sample        Receipt        Analysis    Batch                                                                                                                                     Report ID                 Type                                 ID                              Date           Date           Date Analyte                Method                 Result          cu             CSU            MDA        Qualifier ID                                                                                                                                       Units 19-09012-09               TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012       Actinium-228                                                   2.83E-01       2.85E-01        5.19E-01 19-09012-09               TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012        Silver-108m                                                   6.72E-02        6.72E-02       8.93E-02        u 19-09012-09               TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012      Americium-241          EPA 901.1 Modified        -5.79E-02      9.74E-02        9.74E-02       1.36E-01        u
                                                                                                                                                                                    '""'"", *---v-,--,~----,--**-- '.---m----*-"-**-------*------------
19-09012-09                TRG           L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012        Barium-133           EPA 901.1 Modified      . -2.25E-03      3.53E-02  . 3.53E-02       1.SOE-01        u 19-09012-09                TRG           L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012       Bismuth-214           EPA 901.1 Modified         4.29E-01      1.29E-01        1.31E-01       2.02E-01
*--**----*-""'"'""""""' ---*-*--*---*---------* -*------*----*---*-- . -*-------***-***-*-----**-****----**---*--**-***-*-*-*****-**---*--***-** ****--*----+-*-----*---------***--**********-*-i***--*--**-**
19-09012-09               TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012          Cobalt-60          EPA 901.1 Modified         5.09E-02      9.40E-02        9.40E-02       1.59E-01        u
                            "'"""*----*-<----                 *--*--*-"""""'         "*-**- ---*-~-----*--<*-----------*----*- *-----~--------------*-~t--- mn,-,---*--*---*--v---*,
19-09012-09               TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012        Cesium-134           EPA901.1 Modified          7.34E-03      3.64E-02        3.64E-02       1.07E-01        u 19-09012-09                TRG           L1-10221A-FIGS-008-SS-A                          _________________
06/13/19 07:51                    ----------
9/3/2019___.___9/11/2019  19-09012                             EPA 901.1 Modified         3.48E-01      1.22E-01        1.23E-01       1.72E-01 19-09012-09               TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51   9/3/2019       9/11/2019  19-09012                             EPA 901.1 Modified        -7.16E-02      1.90E-01        1.90E-01       2.23E-01        u 19-09012-09                TRG       ~-L1_-_10_2_2'.~_::'.I_G_s_-o_o_s-.s_s_-_A_ _ __ _ 06/13/19 07:~/3/2019 . 9/1112019             -~~?.~.1.~-' ,.                       EPA901.1 Modified          7.57E-02      2.02E-01 Euro_p*_,u_m_-1_5_4_+-**-**-*-*-----**-**-**---,--------*-**--*-**--*---       2.02E-01
__ .___________                     u 1_.1_3_E_-_0_*1**-******-*---*----...:.---''--I
 . 19-09012-09 .              TRG           L1-10221A-FIGS-008-SS-A                           06/13/19 07:51 ; 9/3/2019       9/11/2019  19-09012       Europium-155          EPA 901.1 Modified         1.25E-01      1.10E-01        1.10E-01       1.82E-01        u
                            *******---*-*-*-------                                            06/13/19 07:51 : 9/3/2019 . 9/11/2019                ' Holmium-1._66-m-;----***-*---******---*---*,*--*----*****-,---**---*--*----*-***-**--***-******7****-.9-6*-E**_**o-2***--*--------*-***--f 19-09012-09               TRG            L1-10221 A-FIGS-008-SS-A                                                                                                          EPA 901.1 Modified         3.24E-02      1.29E-01        1.29E-01                       u TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51                  9/11/2019                   lodine-129          EPA901.1 Modified         -3.70E-02      7.48E-02       7.49E-02                        u 19-09012-09 -t-- TRG                 :   L1-10221A-FIGS-008-SS-A                    .      06/13/19 07:51                  9/11/2019                 Potassium-40          EPA901.1 Modified         1.32E+01      2.11E+OO        2.21E+OO
           --,--,,~-,     "
                                                                       *--**--*--+*---*-*-----i----~***-----+-----.;--------**--+*---********--*----+***-*-**-*---i---------*-'--
TRG           L1-10221A-FIGS-008-SS-A                           06/13/19                        9/11/2019                                       EPA 901.1 Modified                       8.14E-02        8.14E-02                       u TRG           L1-10221A-FIGS-008-SS-A                           06/13/19 07:51                                                                  EPA 901.1 Modified         6.11E-03      6.58E-02        6.58E-02                       u TRG                                                                                                                                             EPA 901.1 Modified                                       6.14E-02                       u TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51                                                                                                                                         1.16E+OO         u TRG            L1-10221A-FIGS-008-SS-A                           06/13/19 07:51                                                                                                                                          2.06E-01                       pCi/g L1-10221 A-FIGS-008-SS-A                          06/13/19 07 :51                                                                                                                                         2.34E-01                       pCi/g u              pCi/g pCi/g u              pCi/g EPA901.1 Modified                                        9.06E-01      1.35E+OO                        pCi/g EPA 901.1 Modified                                       1.63E-01       1.48E-01                       pCi/g 9/3/2019       9/11/2019                                       EPA 901.1 Modified                                       3.09E-01      4.49E-01         u              pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
("M>             EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                   865/481-0683                FAX 865/483-462!

Printed: 10/21/201912:02 PM                                                                                                                                                                                                                                                 Page 12 of 21 Report To:                                                                                                            Work Order Details:
Patricia Giza                                                                                                                                 19-09012 Eberline Analytical                                                                Zion Solutions                                                                                               Purchase Order:
SDG:
677118
                                                                     **-------- *-----*"*--*"""*---~---*                                                                                            ****--*---**------*--"=* ----*------------ ---**                                                                ..
Final Report of Analysis                                                        2701 Deborah Ave                           ..             .. "'"*--                           ***-     - . Analysis Category: ...             ENVIRONMENTAL
                                                                     - - * - - " ~ - - - - - - - * - - - - "'""&deg;'"' - * - * *
* Zion, IL 60099                                                                                                Sample Matrix:                  so Lab            Sample                  Client                              Sample                         Receipt             Analysis          Batch                                                                                                                                              Report ID             Type                     ID                                  Date                             Date               Date             ID Analyte                     Method                    Result                  cu           CSU      MDA      Qualifier Units 19-09012-10 :        TRG      L 1-10221A-FIGS-009-SS-A 06/13/19 07:53                       9/3/2019           9/11/2019        19-09012           Actinium-228              EPA 901.1 Modified        '   6.87E-01             1.91E-01      1.95E-01 2.91E-01 19-09012-10 ,        TRG      L 1-10221 A-FIGS-009-SS-A                   06/13/19 07,53                       9/3/2019           9/11/2019                      ! Silver-108m                  EPA901.1 Modified             5.28E-03             2.16E-02      2.16E-02 7.48E-02         u             pCi/g
                                                         *****-**     --~--------*-                     ***----**---*-*--*-- .. - -**----*-** -~--- ***--------*- *- ***------~- ,...                                                                                                                           ----
19-09012-10 ;        TRG      L1-10221 A-FIGS-009-SS-A                    06/13/19 07 ,53                      9/3/2019           9/11/2019        19-09012         Americium-241               EPA 901.1 Modified            2.41E-02             4.32E-02  :   4.32E-02 1.03E-01         u             pCi/g 19-09012-10          TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                       9/3/2019           9/11/2019        19-09012            Barium-133               EPA 901.1  Modified          -9.57E-03             4.20E-02      4.20E-02 1.11E-01         u             pCi/g
                                                           -**-       ***-----------*---*-,,,-----:--------**.---~---------------- ,---                                                                                                                                                                            **-
19-09012-10 :        TRG      L 1-10221A-FIGS-009-SS-A
                                                           *******-*   _,,,_  _________~-----------------------------*"---
06/13/19 07:53                       9/3/2019           9/11/2019        19-09012            Bismuth-214              EPA 901.1  Modified       !   4.58E-01             1.43E-01      1.45E-01 1.59E-01                       pCi/g 19-09012-10 '        TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                       9/3/2019           9/11/2019        19-09012              Cobalt-60              EPA901.1 Modified         l   1.20E-01             5.91E-02      5.94E-02 1.05E-01                       pCi/g 19-09012-10          TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                       9/3/2019            9/11/2019       19-09012 :          Cesium-134               EPA901.1 Modified         i -1.45E-02              1.SOE-02  :   1.SOE-02 8.67E-02         u             pCi/g 19-09012-10 :        TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                       9/3/2019            9/1112019       19-09012            Cesium-137               EPA901.1 Modified             5.42E-01             1.20E-01      1.23E-01 1.43E-01                       pCi/g 19-09012-10          TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                   '   9/3/2019            9111/2019       19-09012          -~v, *c        --*-        EPA901.1 Modified             3.93E-02          '  1.78E-01      1.78E-01 1.58E-01         u             pCi/g 19-09012-10 TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                       9/3/2019            9/11/2019       19-09012          -~"'"~'""' ,v
                                                                                                                                                                                     -           EPA901.1 Modified         :   2.43E-02             2.06E-01      2.06E-01 8.30E-02         u             pCi/g 19-09012-10       ! TRG       L 1-10221A-FIGS-009-SS-A                    06/13/19 07 :53                      9/3/2019            9/11/2019       19-09012      i    ~"'-c -*
                                                                                                                                                                                    *ss          EPA901.1 Modified             4.18E-02          :  8.19E-02      8.19E-02 1.23E-01         u
------~----------*--*-*-----------                                                                                                                                1                                                                                                                                                 --
19-09012-10 ,        TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07 :53                      9/3/2019            9/11/2019       19-09012         Holmium-166m                EPA901.1 Modified         i  -4.02E-02             7.00E-02      7.00E-02 7.33E-02         u             pCi/g
                                                                             -------                        '-*-=,-                                                  *-----
19-09012-10          TRG      L1-10221A-FIGS-009-SS-A                     06/13/19 07:53                   :   9/3/2019            9/11/2019       19-09012             lodine-129              EPA901.1 Modified             2.44E-01          '  2.17E-01      2.17E-01 3.14E-01         u             pCi/g 19-09012-10          TRG      L1-10221A-FIGS-009-SS-A                     06/13/19 07:53                       9/3/2019            9/11/2019       19-09012 ,         Potassium-40              EPA901.1 Modified         i  9.01E+OO           i 2.02E+OO       2.07E+OO 7.16E-01                       pCi/g 19-09012-10 \        TRG      L1-10221A-FIGS-009-SS-A                     06/13/19 07:53                       9/3/2019            9/11/2019       19-09012         Manganese-54                EPA 901.1 Modified            5.02E-02             6.55E-02  :   6.55E-02 1.18E-01         u             pCilg 19-09012-10 l        TRG      L1-10221A-FIGS-009-SS-A                     06/13/19 07:53                   f 9/3/2019            9/1112019       19-09012      i ....,       ""'
no EPA 901.1 Modified           -1.65E-02          '  4.50E-02      4.50E-02 6.98E-02         u             pCi/g 19-09012-10 ,        TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07 :53                  i   9/3/2019 ' 9/11/2019                19-09012            Niobium-94               EPA901.1 Modified             5.78E-03             4.51E-02  ;   4.51E-02 6.65E-02         u             pCi/g 19-09012-10 :        TRG      L1-10221A-FIGS-009-SS-A                     06/13/19 07:53                       9/3/2019            9/11/2019       19-09012              Lead-210               EPA 901.1 Modified            1.20E+OO             8.25E-01      8.28E-01 1.29E+OO         u             pCi/g 19-09012-10          TRG      L 1-10221 A-FIGS-009-SS-A                   06/13/19 07 :53                  f   9/3/2019 ' 9/1                      19-09012              Lead-212               EPA 901.1 Modified            3.06E-01             9.00E-02  i   9.14E-02     19E-01                     pCi/g 19-09012-10          TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                       9/3/2019            9/11/2019       19-09012              Lead-214               EPA 901.1 Modified
                                                                                                                                                                                                                           '   4.18E-01             1.18E-01  i   1.19E-01 1.82E-01                       pCi/g 1: ---* 1,* .. c    TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                   1 9/3/2019              9/11/2019       19-09012        Promethium-145               EPA 901.1 Modified        :   1.58E-02             1.36E-01      U6E-01   2.01E-01         u             pCi/g 19-09012-10         TRG   :  L 1-10221A-FIGS-009-SS-A                    06/13/19 07 :53                      9/3/2019 , 9/11/2019                19-09012 i          Radium-226               EPA 901.1 Modified            4.58E-01             1.43E-01      1.45E-01 1.59E-01                       pCilg 19-09012-10          TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                       913/2019 '                          19-09012 '         Antimony-125
                                                                                                                                                                                          .. EPA901.1 Modified            -9.24E-02          ,  1.68E-01      1.68E-01 2.15E-01         u             pCi/g 19-09012-10          TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07 :53                      9/3/2019 ~9/11/2019 : 19-09012 '                       Thorium-234               EPA901.1 Modified             5.84E-01             6.28E-01      6.29E-01 1.05E+OO         u             pCilg 19-09012-10          TRG      L 1-10221A-FIGS-009-SS-A                    06/13/19 07:53                   :   9/3/2019 i 9/11/2019 ) 19-09012                        Thallium-208              EPA901.1 Modified             3.03E-01             2.23E-01  '   2.23E-01 3.SOE-01         u          '  pCilg 19-09012-10          TRG      L1-10221A-FIGS-009-SS-A                     06/13/19 07:53                       9/3/2019       i    9/11/2019 : 19-09012               Uranium-235               EPA 901.1 Modified            2:07E-01
                                                                                                                                                                                                                                                 '  2.39E-01  !   2.40E-01 3.74E-01         u
* pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(  ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                 865/481-0683                   FAX          865/483-4621

Printed: 1012112019 12:02 PM                                                                                                                                                                                                                                                                                                                                         Page 13 of 21 Report To:                                                                                                                                                        Work Order Details:
Patricia Giza                                                                                                                                                                     19-09012 Eberline Analytical                                                                                              Zion Solutions....... .._____                     ,,,    ,,,,, ..........., ........... ..                           Purchase Order:
SDG:
___ , __ , a _ , _ , _ * * * * ' - ' ' ' ' " - ' , _ , , '
677118 Final Report of Analysis                                                                                2701 Deborah Ave                                                                                              __ Analysis Category:                                              ENVIRONMENTAL Zion, IL 60099                                                                                                            Sample Matrix:                                         so Lab                       Sample                              Client                               Sample                                Receipt           Analysis                   Batch                                                                                                                                                                                                 Report ID                      Type                               ID                                      Date                                 Date               Date                       ID Analyte                       Method                                          Result                              cu                     CSU           MDA          Qualifier Units 19-09012-11                    _ TRG                    L1-102218-FIGS-100-SS-A
                                                            '-*-------""""""~---------*-
06/20/19 09:55                               9/3/2019          9/11/2019 19-09012           Actinium-228         EPA 901.1 Modified                                       2.62E-01                            2.16E*01                2.16E-01       3.86E-01 19-09012-11 19-09012-11 TRG TRG L1-102218-FIGS-100-SS-A L1-102218-FIGS-100-SS-A 06/20119 09:55 06/20/19 09:55 9/3/2019 9/3/2019 9/11/2019 9/11/2019        .;,_
19-09012 19-09012 Si1ver-108m Arnericium-241 EPA 901.1 Modified EPA 901.1 Modified
                                                                                                                                                                                                                                                                                                 -3.45E-02 2.68E-02
__   ""-~'
5.69E-02 1.18E-01 5.70E-02 1.18E-01 5.63E-02 1.58E-01
,__........... , ___________ ,,,,,,,_,,,,.. **--- ..- ------------- '"'"-----~----------* ''"
m,,,_, _ _ _ _ _ _ _ _ _ _ _ _ ,="" _ _ ,,,
19-09012-11                          TRG                L1-102218-FIGS-100-SS-A                    06/20/19 09:55                               9/3/2019           9/11/2019               19-09012             Barium-133         EPA 901.1 Modified                                      -4.23E-03                            4.60E-02                4.60E-02       9.SOE-02 19-09012-11                          TRG                L1-102218-FIGS-100-SS-A                    06/20/19 09:55                                9/3/2019          9/11/2019               19-09012            Bismuth-214         EPA 901.1 Modified                                       4.53E-01                            1.31E-01                1.33E-01       2.01E-01
*-----------------                                           ---------*----*---,-----------***-- -------------" --------------~----~-------~-- --------*---
19-09012-11                          TRG                L1-102218-FIGS-100-SS-A                    06/20/19 09:55                               9/3/2019           9/11/2019               19-09012              Cobalt-60         EPA901.1 Modified                                        8.15E-02                            4.67E-02                4.69E-02       1.02E-01
      ------+-------~----,-------------------,                                                                                                                                                                                                                                                                   ..................------------,-----..----------------------------C---"---..----J 19-09012-11
    ----------0--*----,------              TRGV               L1-102218-FIGS-100-SS-A
                                                     ,-,-~,,,________________                 , __ _ 06/20/19 09 :55                                  9/3/2019           9/11/2019               19-09012             Cesium-134         EPA901.1 Modified                                         1.02E-02                           2.82E-02                2.82E-02
                                                                                                                                                                                                                                                                       - - - -..+,..--..-------- *--.... ----------*-------------*-------~---------------------------1 7.01E-02 19-09012-11                          TRG                L1-10221B-FIGS-100-SS-A                    06/20/19 09:55                               9/3/2019           9/11/2019               19-09012             Cesium-137         EPA 901.1 Modified                                       2.66E-01                            9.61 E-02               9.70E-02       1.35E-01 19-09012-11                          TRG***--*"* L-1--1-o-22-18~FiG_s___1_00---s-S--A              06120119 09:55                           1   9/3/2019           9/11/2019                                                ---E-P-A   ____9__0**---1--_--1---M-o_d_ifi_,e__d____ _,_ ___5____  2_5E---02________ -----9-.2**-7-E--o-2*-'--9-_2_7_E--o-2_____          1_-99_E___
o_1---------
                                    --~A--------,-------
19-09012-11                          TRG                 L1-102218-FIGS-100-SS-A                   06/20/19 09:55                                9/3/2019          9/11/2019                                                       EPA 901.1 Modified                                      -1.70E-01                            1.97E-01                1.97E-01       1.00E-01
 -----------~-------------------------*--------+*---*-----------***------~-------..*--------------.."--------------+---------------*-*--'------...... -----------------.--------------------------------------------1 19-09012-11                          TRG                 L1-10221B-FIGS-100-SS-A                   06/20/1909:55                                 9/3/2019          9/11/2019                                                       EPA901.1 Modified                                         5.79E-03                            1.13E-01               1.13E-01       1.46E-01 19-09012-11                          TRG                L1-10221B-FIGS-100-SS-A                    06/20/19 09:55                               9/3/2019           9/11/2019                                                       EPA 901.1 Modified                                       O.OOE+OO                            8.09E-02                8.09E-02       8.63E-02
                                                                                                        ------------~-------
19-09012-11                          TRG                L1-102218-FIGS-100-SS-A                    06/20/19 09:55                               9/3/2019                                                                           EPA901.1 Modified                                        2.04E+OO                            9.54E+OO               9.54E+OO       3.87E+OO 1------i---------------*--*------------------------*+-*---*------------~--- *----*---*--'-----------,-----*-------+---*-*-*--
19-09012-11                          TRG                 L1-10221B-FIGS-100-SS-A                   06/20/1909:55                                 9/3/2019                                                                          EPA901.1 Modified                                        1.15E+01                            1.79E+OO                1.89E+OO       7.20E-01
_ _ _,______________ ,___________-----~-----~------i----------------l----------*--------~----------"-***-*-------------------*-*-----------------*----'----"---1 19-09012-11                          TRG                 L1-102218-FIGS-100-SS-A                   06/20/1909:55                                 9/3/2019                                                                          EPA901.1 Modified                                       -1.14E-02                            6.08E-02                6.0SE-02       9.10E-02
                                                                                             --+------*---*--                                   -:........... ____c,_________;._, _______ .........CC--------*-*l---------.                                                .--..--+---*--------+--
19-09012-11                          TRG                 L1-10221B-FIGS-100-SS-A                   06/20/1909:55                                 9/3/2019                                                                          EPA901.1 Modified                                         5.18E-02                           4.12E-02                4.12E-02       6.30E-02
                                                                                                                                                                                                                                                                                                                                                       ---------------------'-----*'-----1
_1_9_-0_9_01_2_-1_1--j-_ TRG                                  L1-10221B-FIGS-100-SS-A               -!--0-__6:.;/2~-0=-/1:_;9_0:.;9_:_:5:__5:__;~9-/3_12=-0=-1-:9_.__;__;_ _____;_:_:__:_;__;__:,.._ ______________ --J----E_P_A              ______9___0___
1._1_M_o_d_ifi_ed___           +__-3_._25_E_-_02_________ , ....            4.30E-02                4.30E-02       5.78E-02 19-09012-11                          TRG                L1-10221B-FIGS-100-SS-A                    06/20/1909:55                                                                                                                   EPA901.1 Modified                                        2.18E+OO                            1.60E+OO                1.61E+OO
                                   ,-------,--.. ----*-*----------*-J.-----------*-*-------*--*----,-*-----i-------..L .. - ....----+------*-*--*--*-*--*------i-----*----------------~-----------'-*---------'--.::._-----1 19-09012-11                          TRG                L1-10221B-FIGS-100-SS-A                    06/20/19 09:55                                                                                                                  EPA 901.1 Modified                                       4.67E-01                            1.03E-01                1.06E-01 1-------------i-------------------------------*+*---------;----------'-------+*-----,-------------+---------
19-09012-11                          TRG                 L1-10221 B-FIGS-100-SS-A                  06/20/19 09:55                                                                                                                  EPA 901.1 Modified                                                                            1.33E-01               1.35E-01 1.12E+OO 2.01E-01 2.05E-01 L1-10221B-FIGS-100-SS-A                                                                                                                                                   EPA901.1                                                                                     1.17E+OO                               1.58E+OO
                           -i------
19-09012-11              --4-___~~~221B-FIGS-100-SS-A                                                                                                                                                         Thallium-208         EPA 901.1                                                                                    1.05E-01                               1.22E-01 19-09012-11                  i       TRG            i    L1-10221B-FIGS-100-SS-A                                                                                                                              Uranium-235                                                                                                       3.07E-01                3.0SE-01       4.47E-01          u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>                   EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                      865/48!-0683                                               FAX 865/ 483-4621

Printed: 10/21/2019 12:02 PM                                                                                                                                                                                                                                  Page 14 of 21 Report To:                                                                                           Work Order Details:
Eberline Analytical                                                                                        Patricia Giza
                                                                                                                     -*---'-'""~'*--,****"=--*------
SDG:        19-09012 Zion Solutions                                                    ~- .. ---*-----         Purchase Order:              677118
                                                                                                           *--*-***-~-                        "--*-*-------                                                          -*-                  ----------------------~-----*
Final Report of Analysis 2701 Deborah Ave                                                   "''"' ____      ____ Analysis_Category: __          ENVIRONMENTAL Zion, IL 60099                                                                             Sample Mattix:              so Lab                       Sample                   Client                                     Sample                                  Analysis     Batch                                                                                                                           Report ID                          Type                      ID                                      Date                                     Date          ID Analyte                 Method                 Result               cu          CSU       MDA    Qualifier Units 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                                                                          9/11/2019  19-09012          Actinium-228           EPA901.1 Modified          6.27E-01          1.88E-01      1.91E-01 3.77E-01 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                                                                          9/11/2019  19-09012           Silver-108m           EPA 901.1 Modified         3.54E-02          5.90E-02      5.91E-02 7.24E-02    u 19-09012-12                              TRG   L1-10221C-FIGS-103-SS-A                                                                           9/11/2019  19-09012         Americium-241           EPA 901.1 Modified        -5.64E-02          8.37E-02      8.37E-02 1.16E-01    u
-------~-------------~*-, ""*-*----*-*=--
19-09012-12                              TRG   L1-10221C-FIGS-103-SS-A                                                                           9/11/2019  19-09012           Barium-133            EPA901.1 Modified          1.47E-02          3.60E-02      3.60E-02 1.33E-01     u
  -*--*-**-----"-""------.,-------*"*-----~-------------*--------*-*-**                                 ------------*----*:                            "'--*----.~-*--- -*-- --*-*-*--*----           ---------*---~---
19-09012-12                              TRG   L1-10221C-FIGS-103-SS-A
*-*------------...,..,---**-----*--~--~--*-*------ ----------**---~-                                    _,,,,, __________'""\''"----------*'"'"
07/08/19 12:47                9/3/2019        9/11/2019  ""'. __       ,,
_________ ___ --------,,0--,---,,---~--
19-09012 , ___ , Bismuth-214,            EPA 901.1 Modified         3.35E-01          1.47E-01      1.48E-01 2.80E-01 19-09012-12                              TRG   L1-10221C-FIGS-103-SS-A                             07/08/19 12:47                9/3/2019        9/11/2019  19-09012             Cobalt-60           EPA 901.1 Modified         9.13E-02          6.23E-02      6.25E-02 1.12E-01    u
  -----------J-----'""----,-------------..----**--*~,
______ 19-09012-12         "'                  ______________ _____
             .. _____ ____........-, .......... TRG                   , __ ...
l 1-10221C-FIGS-103-SS-A         ,___,,, ____. -*   07/08/19 12:47                9/3/2019        9/11/2019  19-09012           Cesium-134            EPA 901.1 Modified
                                                                                                                                                                                                      -----*----*---~----
1.66E-02          2.41E-02      2.41E-02 1.04E-01     u 19-09012-12                              TRG L 1-10221C-FIGS-103-SS-A ___________      ,,,       07/08/19 12:47                9/3/2019        9/11/2019  19-09012           Cesium-137            EPA901.1 Modified                                          8.33E-02 1.26E-01 19-09012-12 TRG   L 1-10221C-FIGS-103-SS-A 07/08/19 12:47                9/3/2019        9/11/2019  19-09012          Europium-152           EPA 901.1 Modified
                                                                                                                                                                                                                     .......-*----*-~
7.34E-02 1.87E-01     u 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A 07/08/19 12:47                                                                                    EPA901.1 Modified                                          1.53E-01 9.92E-02     u u
                 ..- ...........--~***-*-----*----..* - - - - * - - - ,.. ..._,__,-,,-----
19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                            07/08/19 12:47                                           19-09012          Europium-155           EPA 901.1 Modified                                         9.91E-02 1.49E-01 19-09012-12                              TRG   L1-10221 C-FIGS-103-SS-A                            07/08/19 12:47                                           19-09012         Holmium-166m            EPA901.1 Modified                                                   6.88E-02    u 19-09012-12                              TRG   L 1-10221 C-FIGS-103-SS-A                                                                                    19-09012            lodine-129           EPA901.1 Modified                                                   9.90E-02    u 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                                                                                     19-09012          Potassium-40           EPA 901.1 Modified                                                  1.10E+OO              pCi/g 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                                                                                     19-09012         Manganese-54            EPA 901.1 Modified                                                  1.04E-01     u 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                                                                                     19-09012         Molybdenum-93           EPA901.1 Modified                                                                u
----------..*-*--..--~                                                *-*--------*-"
19-09012-12                              TRG   L 1-10221 C-FIGS-103-SS-A                                                                                    19-09012            Niobium-94           EPA 901.1 Modified                                                               u 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                                                                                     19-09012             Lead-210                                       1.01E-01                                              u 19-09012-12                              TRG   L1-10221C-FIGS-103-SS-A                                                                                      19-09012             Lead-212                                       2.71E-01 19-09012-12                              TRG   L 1-10221 C-FIGS-103-SS-A                           07/08/19 12:47                             '  9/11/2019  19-09012             Lead-214            EPA 901.1 Modified 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A 07 /08/19 12:47               9/3/2019        9/11/2019  19-09012     i Promethium-145            EPA 901.1 Modified                                                                        pCi/g TRG    L1-10221 C-FIGS-103-SS-A                           07/08/19 12:47                9/3/2019        9/11/2019  19-09012           Radium-226            EPA 901.1 Modified TRG   L 1-10221 C-FIGS-103-SS-A                           07/08/19 12:47                9/3/2019        9/11/2019  19-09012 . Antimony-125                  EPA901.1 Modified                                                                u TRG   L 1-10221C-FIGS-103-SS-A                            07/08/19 12:47            i   9/3/2019        9/11/2019  19-09012 :        Thorium-234            EPA901.1 Modified                                                   1.16E+OO    u         pCi/g 9/11/2019 19-09012 '
Thallium-208           EPA 901.1 Modified                                                  2.02E-01 19-09012-12                              TRG   L 1-10221 C-FIGS-103-SS-A                           07/08/19 12:47                9/3/2019 19-09012-12                              TRG   L 1-10221C-FIGS-103-SS-A                            07/08/19 12:47            i 9/3/2019          9/11/2019  19-09012          Uranium-235            EPA901.1 Modified          2.98E-01                                 3.96E-01     u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
(        ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                865/481-0683                FAX 865/ 483-4621

Printed: 10/21/2019 12:02 PM                                                                                                                                                                                                                                                                                                                     Page 15 of 21 Report To:                                                                                                                                         Work Order Details:
Patricia Giza                                                                                                                                                           19-09012 Eberline Analytical                                                                   '""'''''"'""'""""""'
Zion       Solutions                                                                                                      Purchase Order:
SDG:
677118
                                                                                              ---- ,,----~------*-------                                                                                            ----                                                    -------------.---              -
Final Report of Analysis                                                                        2701 f"""'-----*-*----.------~-
Deborah Ave e - - - - - - -----------*--*------ e**-*--~--1***
                                                                                                                                                   ,cw-*
Analysis,Category: _ ___E_N_V_IR_O_N_I\J1_ENTAL Zion, IL 60099                                                                                                               Sample Matrix:                             SO Lab                 Sample                         Client                                  Sample                   Receipt               Analysis                Batch                                                                                       '                                                                                                      Report Analyte                          Method                                Result                  CU                      CSU                MDA            Qualifier ID              , Type                              ID                                      Date                      Date                    Date                   ID                                                                                      \                                                                                                       Units 19-09012-13                  TRG         L1-10221 B-FIGS-102-SS-A                            07/08/19 13:10                9/3/2019             9/11/2019              19-09012                 Actinium-228                  EPA 901.1          Modified                 3.53E-01         '   275E-01                2,75E-01             5,65E-01             U            pCi/g
 '"'"'"'"'""'""""''"''''"'""""""" _____________   ,____________''""'''"'"'___ ------+--------,----"''""''""                                     ______        ""--,------"'*""'""'""'""'--'""''"'"!"' ''""
19-09012-13                  TRG         L1-102218-FIGS-102-SS-A                             07/08/1913:10            , 9/3/2019                9/11/2019              19-09012 :                Silver-108m                  EPA901,_1___       M_od_ifi_,e_d_+___-_3,_93     __E_-_02__, ___6_,_6S__E 02_         6.66E-02             8-77E-02             U            pCi/g
_1_9_-o_90_1_2-_13-____ _:_F:_~---L_1_-1_02~1~-:~1Gs-_102-~~;:;-----                            07/08/1913:10                 91_3_1_2_0_1__9___ ,-9___11_1_12_0_19__,_1_9"_-0_9_01_2-+_Am_e__n_ci__u_m_-_2___        4_1_       EPA 90U Modified                           -1A4E-01          '   8.57E-02               8-60E-02             U2E-01               u            pCi/g      __ _
19-09012-13                  TRG         L1-102218-FIGS-102-SS-A                             07/08/1913:10                 9/3/2019
-------------------------------------'"'-----l---.:;_                                                      _________;,._"_"          _______9/11/2019                       19-09012
                                                                                                                                                        ,____,_,,_,,_--~-------*""''"                 Barium-133                   EPA 901-1 Modified                         -3,11E-02
                                                                                                                                                                                                                                           '"'"'''"'""'"-""-"T''"----i--'"'""""""
9,87E-02                9,87E-02            125E-01
                                                                                                                                                                                                                                                                                                                   """"""'""''"""''"'---------*---,-----C---,C"'"""-1 U            pCi/g
_}_9-:~9-~2:1~~3-. ~R~"----~1:_1022-1B_-_Fl~~~:_?_2-_S-S:_.t; ______ I- __                        0_7i_08_i_19_1_3_:1_0___ ,'___9i__3__i2__
0_1"9______9_1,1__1_12_0_19---'-__1_9_-_o__9_0__1__12--"'__B_is_m_u_th_-_2__1_4____ +    EPA 901-1 Modified                          5.30E-01             1-52E-01                1,SSE-01            1.60E-01        ,                 pCi/g      --
  ,,,,1,9,:!_9012-1 ~-- __":i:~~--L_1-_10_2~~--F_IG~_:1_?2:_~~-~-- .,,.,                          07/08/19 13:10            : 9/3/2019               9/11/2019              19-09012                    Cobalt-60             *_   EPA 901-1 Modified                          5,0SE-01             1,08E-01                1.11 E-01 ____      1_.8_2_E_-_01______________;__pC__i _g_0 ___---1 19-09012-13                 TRG         L1-102218-FIGS-102-SS-A                             07/08/1913:10                 9/3/2019              9/11/2019             19-09012 ; Cesium-134                                  EPA90U Modified                               '22E-03            1-96E-02                1,96E-02            9.82E-02             U            pCi/g
-       ___,___ "" *"""' -'-"'-""" - - - - -                          '"""'"--,-,_m-+-*----------+-""'"""""-""'___ "__________+-----*-"'"'"'"' ""'"""'
__19_-_09_0_12_-~~" " _L_1-_10_2_21_B:~G_s_-1_0_2-_s_s:;:;________ -1 __0_1___10__8_11._9_1 __3__:"1__            0 _____9_13_1_20_,_1__9"_____9_11_1_12_01_9,_____1_9_-o_90_1_2_,l+-_c_e_s__i__        um----1_37_ _, ___E_P_A ___9_0--1_____1____
M__o__
difi_,e_d____ _;__9__  82_E_-0_1_ _  ,_1._s_oE__-_0"__1_ ---"- ____
1__s1__E___-_01_____1_,s,_sE_-"0___
1 _______,____:__pCi-'-ig_-1 1
19-09012-13                 TRG         L1-10221B-FIGS-102-SS-A                              07/08/1913:10                9/3/2019              9/11/2019             19-09012                :::v,ve,v .. , ,52             EPA90U Modified                             2,64E-01         ;   1,93E-01                1,93E-01            1,96E-01              U           pCi/g 0
1-19-09012-13
* TRG""" -c;-.:-10-22_1_s_-FIGS--10-2--s-s;_*------,-1---07-/0-8--/1_9_1_3*:*1--o---~-9/_3_/2-01-9-~--9--/1_1_1_2_0_19_____1_9_,__0_9_0-12-+-                    1-Eu_r.op-iu_m___   154---1----E-P-A"'"9"01 1 Modified                        3.38E-02             2_ 10E-01               2_ 10E-01           1 _02E-01             u           pCi/g
,------------------+--------,--------------*"""'---;----------- ---------
19-09012-13 '               TRG         L1-102218-FIGS-102-SS-A                              07/08/1913:10                9/3/2019              9/11/2019             19-09012 , Europium-155                                EPA901.1 Modified                           1.58E-04             8.83E-02                8.83E-02            1.29E-01              U           pCi/g 1 - - - - ' - ' " ' " ' " " ' ' " " " ' " " - ' - - - - - - - - - - - - - - - - - - - - - - - - - - i - - - - - - - * - - ---------"-- -----                                                    t--------+-*-"""'""'""""'                            ------------+------r--------'""''"'"'""*-*--*------------------'---"-------1 19-09012-13                 TRG         L1-102218-FIGS-102-SS-A                             07/08/1913:10             : 9/3/2019                9/11/2019, 19-09012 \ Holmium-166m                                           EPA90U Modified                            -7AOE-02 ; UOE-01                             UOE-01              7.63E-02              U           pCi/g 1-------,-----------------------*""'"--j-'------+-----------                                                                                                                                     i---------------               "'""'"'"'''""'"'-------+---,--i----------,."_______________:_ _ _ _ _ __, ___ ,:;"''----1
__ 1S-v,v "-~::; ! __:R~-"-- L1-10221~~1GS-102-~~---- __ 07/08/19 13:10---~~-0~ __ ?111/20:_9-_                                                                            19-09012 l                 lodine-129 ---l------E__P__A   ___9_0_1__,1_M_o_d_ifi_1e_d__+-_2__2_o_E_-0_1__,__ ""2_.34       __E__ -o_1_-_____2   ___34_E__-0_1___3_,_4__  1E_-0_1_~__u_______"p_Ci/-'-g--1 l--~9-09012-13                    TRG _       L1-102218-FIGS-102-SS-A                  '""'       07/08/1913:10                 9/3/2019              9/11/2019 __ 19-09012 [                        Potassium-40                  EPA9"0"_1_",_1__   M_od_ifi_e_d_+_1_1.s_oE_+o1___3_._1s_E___              +_o_o________3___-_26_E_+_oo_ _ _  8_.2_4E__-0_1__* _ _ _"'C"""""'_pCi_ig___-t 19-09012-13                 TRG         L1-102218-FIGS-102-SS-A                              07/08/1913:10                9/3/2019              9/11/2019             19-09012                Manganese-54                   EPA901.1 Modified                           8A8E-02              8-87E-02                8,89E-02            1A7E-01               U           pCi/g
 -~--"---
19-09012-13                 TRG
                                     ----*-L1-102218-FIGS-102-SS-A 07/08/1913:10                9/3/2019              9/11/2019             19-09012                Molybdenum-93                  EPA901,1 Modified                           4.85E-02         !   5,26E-02                5.27E-02            9,10E-02              U           pCi/g 19-09012-13 ;               TRG         L1-102218-FIGS-102-SS-A                              07/08/1913:10                9/3/2019              9/11/2019             19-09012 ,                Niobium-94                   EPA901.1 Modified                          -4.31E-02             6A8E-02                 6A8E-02             8.65E-02              U           pCi/g 19-09012-13 ;               TRG    ,    L1-102218-FIGS-102-SS-A                              07/08/1913:10                9/3/2019              9/11/2019             19-09012                    Lead-210                   EPA90U Modified                             6A2E-01          ,   8.90E-01          ,     8,91E-01            1,35E+OO              U           pCi/g 19-09012-13 t               TRG         U-102218-FIGS-102-SS-A                               07/08/1913:10                9/3/2019              9/11/2019             19-09012 i                  Lead-212                   EPA90U Modified                             4,56E-01             1.18E-01                1,20E-01            2,54E-01                          pCi/g 19-09012-13 :               TRG         U-102218-FIGS-102-SS-A                               07/08/1913:10            ! 9/3/2019                9/11/2019         i 19-09012                      Lead-214                   EPA 901-1 Modified                          4,20E-01         f   1.24E-01                1.26E-01            2.31E-01 19-09012-13 I               TRG     ,   L1-102218-FIGS-102-SS-A                              07/08/19 13:10               9/3/2019              9/11/2019 i 19-09012                         -,v, ,v::,v,      ,- ~:         EPA 901.1 Modified                          5,61E-02         !   1.52E-01                1,52E-01            2,26E-01              U           pCi/g 19-09012-13 :               TRG   -----~1-102218-FIGS-102-SS-A                               07/08/1913:10            ! 9/3/201_9-1,__9_1_1_11_20_1_9_ '_19_-_o9_0_1_2+_Ra_d_iu_m_-_22_s_l-__E_PA                               __  90____1___1_M_od_ifi_,e_d_+__s__3_o_E_-0_1--i1-1__s-::2E~-0_1_, __                1__s_s_E_-0_1" _ _,1__ s_oE'CC"-,01--c-T"''--c-:-----P'-C:-cii::g_-l 0
19-09012-13 :               TRG         L1-102218-FIGS-102-SS-A                              07/08/191                                  9 ' 9/11/2019                 19-09012                 Antimony-125                  EPA901.1 Modified                           1.63E-01             2.02E-01          /     2.02E-01            3.03E-01        ,     U           pCi/g
                                                                                                                                                    -----+---\-----'---+---------+----:-+--~~~-+-----~---~-:-'----:~--'-:c:_--1 19-09012-13 [               TRG         L1-102218-FIGS-102-SS-A                              07/08/1913:10                9/3/2019              9/11/2019             19-09012 +---Th_o_ri_um_-_2_34_+-__E_P_A_9_0_1.__                       1_M_o_difi_,e_d_+-__       9.7__1_E-0_1___      7'._36E_-o1_':""_7',,_38E       __-o__1 ____1_,1_4E_+_o_o_,___u   ______      pCii_g_""'1 19-09012-13            I    TRG    '    L1-10221B-FIGS-102-SS-A                              07/08/1913:10                9/3i2?_1_9-4-_91_1_11_20_1_9_;,__19_-_o9_o_1_2+_T_h_a_lliu_m_-_20_8__ ___
1 E_PA_90_1_.1_M     ____
od_ifi_e_d--+_4_,.o~-2~Ec_-O     n1,--l_2_.21_1E_-0___1__',---2._21_E_-0__1_____        3._s_oE_-_01_ _ ._----'---P,__Cii_::;_g----i 19-09012-13 i               TRG    '. L,-.~;:;:;;:;-FIGS-102-SS-A                          07/08/1913:10                9/3/2019              9/11/2019             19-09012                 Uranium-235                   EPA901.1 Modified                           1'-"~c-v,            2.60E-01          [     2,61E-01            3.97E-01        '     U           pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>               EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601      SCARBORO ROAD OAK RIDGE,                                                     TN 37830                       865/481-0683                                 FAX        865/483-4621

Printed: 10/21/201912:02 PM                                                                                                                                                                                                                                                                                       Page 16 of 21 Report To:                                                                                                                                        Work Order Details:
Patricia Giza                                                                                                                                                            19-09012 Eberline Analytical                                                                                                                                                                                                                                                    SOG:
Zion         Solutions
                                                                                                                       ,,, *-----~"*--,                                                                                                                    Purchase Order:         677118 Final Report of Analysis                                                                             2701 Deborah Ave
                                                                                                       ------------*--,---*--------- -                                                                                                   . . . Analysis Category<.                 ENVIRONMENTAL Zion, IL 60099                                                                                                                                       Sample Matrix:     so Lab           Sample                                     Client                                 Sample                     Receipt       Analysis                      Batch                                                                                                                                                      Report ID             Type                                         ID                                     Date                     Date            Date Analyte                                              Method        Result        cu            CSU      MDA    Qualifier ID                                                                                                                                                      Units 19-09012-14         TRG              L 1-10221 B-FIGS-103-SS-A                                07/08119 13:12                   9/3/2019     9/1112019                   19-09012                     Actinium-228                                  EPA 901.1 Modified         2.23E-01    1.85E-01      1.85E-01 3.29E-01 19-09012-14         TRG              L 1-102218-FIGS-103-SS-A                                 07108119 13:12                   9/312019     9/11/2019                   19-09012                       Silver-108m                                 EPA 901.1 Modified        -1.18E-02    4.49E-02      4.49E-02 5-76E-02
                                                                                                     --------"""-~------------
19-09012-14 19-09012-14 TRG TRG L1-10221 B-FIGS-103-SS-A L1-102218-FIGS-103-SS-A 07/08119 13:12
                                                                                                *---'""'""'_m_,,_.,,,, _ _ _ _ _
0710811913:12 91312019 913/2019 "S-____ .----,----
9/11/2019 9111/2019 19-09012 19-09012
                                                                                                                                                                                                 =
Americium-241 Barium-133 EPA 901.1 Modified EPA901.1 Modified
                                                                                                                                                                                                                                                                               -1.36E-01    1.09E-01
                                                                                                                                                                                                    ,,_ -----~-+------*----*-**--*----*------***+-----**--------*------*--***---------**------
2.80E-02      2.80E-02 1.26E-01 7.83E-02 u
u
               ,_._ _ _ _   ""- " ' " " " " ' " " " ' " _ _ , _ , _ ,_ _ _ _ _ _ _, _ , _ _ e
                                                                                              - - - . ~ - - - - - - - - - - * "'"m,_, _ _ _ _ , - , - - = - - - ' " " " ' - " " " " ' - " " " , . , . , , . . , _ , , , . . , , . , _ ,..... , , . , , ,. .. , , , . ,
19-09012-14         TRG              L1-102218-FIGS-103-SS-A                                  07/0811913:12                    9/3/2019     9/1112019                   19-09012                      Bismuth-214                                   EPA901.1 Modified                     1.20E-01      1.21E-01 2.04E-01 19-09012-14         TRG              L1-102218-FIGS-103-SS-A
                    ----------,-=-,--------*----------------
07108/19 13:12
                                                                                                  ----------------*0 913/2019 9/1112019                   19-09012   ____ , ___ --~         Cobalt-60                                EPA901.1 Modified                      5.51E-02      5.63E-02 9.50E-02 19-09012-14 :       TRG              L 1-102218-FIGS-103-SS-A                                 07/08/1913:12                    9/3/2019     9/11/2019                   19-09012                       Cesium-134                                  EPA 901.1 Modified                     4.08E-02      4.09E-02 5.63E-02    u
*--*--------~------***----*------------------------                                           - - * - - - - " - " " , ----m"""'                                                                 +~- -~-~-w-                 --""'
19-09012-14         TRG              L1-102218-FIGS-103-SS-A                                  07108119 13:12                   91312019     9/11/2019                   19-09012                       Cesium-137                                  EPA901.1 Modified                      1.52E-01      1.62E-01 7.67E-02 19-09012-14         TRG              L 1-102218-FIGS-103-SS-A                                 07108/19 13:12                   9/312019     9111/2019                   19-09012                                                                                                          1.92E-01               1.77E-01     u 19-09012-14         TRG              L1-10221 B-FIGS-103-SS-A                                 07/08119 13:12                   9/3/2019     911112019                   19-09012                                                                                                          1.49E-01      1.49E-01 9.42E-02     u 07108/19 13:12                   9/3/2019     9111/2019                   19-09012                                                                                                          9.62E-02      9.63E-02              u 19-09012-14         TRG              L 1-102218-FIGS-103-SS-A                                 07108119 13:12                                9/11/2019                   19-09012                                                                                                                        2.46E-02 6.93E-02    u 19-09012 :                                                                                                                      8.55E+OO 3.43E+OO    u 1.76E+OO 1.56E+OO 19-09012-14          ___________L1-10221 TRG                     ,_          B-FIGS-103-SS-A                       07/08119                                                                                                                                                                                                  3.41E-02 6.96E-02    u 19-09012-14         TRG              L1-10221 B-FIGS-103-SS-A                                                                                                                                                                                                                                           3.40E-02 5.59E-02    u TRG              L 1-10221 B-FIGS-103-SS-A                                07108/19 13:12                                                                                                                                                                                            3.62E-02 5.55E-02    u 19-09012-14         TRG              L 1-10221B-FIGS-103-SS-A                                 07108119 13:12                                                                                                                                                                                            1.38E+OO 2.29E+OO    u 19-09012-14         TRG              L 1-10221 B-FIGS-103-SS-A                                07108/19 13:12                                                                                                                                       EPA 901.1 Modified                                            1.83E-01 19-09012-14         TRG              L 1-102218-FIGS-103-SS-A                                 07/08119 13:12                                                                                                                                        EPA 901.1 Modified 19-09012-14         TRG              L 1-102218-FIGS-103-SS-A                                 07/08119 13:12                                                                                                                                        EPA 901.1 Modified 19-09012-14         TRG              L1-10221 B-FIGS-103-SS-A                                                                                                                                                                                       EPA901.1 Modified 19-09012-14         TRG              L 1-10221 B-FIGS-103-SS-A                                                                                                                                                                                     EPA901 . 1 Modified                                  1.08E-01              u 19-09012-14         TRG              L 1-10221 B-FIGS-103-SS-A                                                                                                                                                                                                                                          9.58E-01 1.30E+OO    u         pCi/g 19-09012-14         TRG              L 1-10221 B-FIGS-103-SS-A                                07108119 13:12                                                                                          Thallium-208                                                                                      7.63E-02 9.85E-02              pCi/g 19-09012-14         TRG              L1-10221 B-FIGS-103-SS-A                                 07108119 13:12                                                                                          Uranium-235                                                                                       2.79E-01 3.92E-01    u         pCilg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>         EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                                                      865/481-0683            FAX    865/483-4621

Printed: 10/21/2019 12:02 PM                                                                                                                                                                                   Page 17 of 21 Report To:                                                                                  Work Order Details:
Eberline Analytical                                                     Patricia Giza                                                                  SDG:             19-09012 Zion Solutions                                                      Purchase
                                                                                                                                               ~,- -~-,~- Order:
                                                                                                                                                            ----------   ___ 677118
                                                                           **---*---------m                                                               '            ,    ,_,                       ,          , __
Final Report of Analysis                                          2701 Deborah Ave                           *-**--------1        Analysis Category:              ENVIRONMENTAL Zion, IL 60099                                                       Sample Matrix:
Lab               Sample                Client                 Sample         Receipt   Analysis       Batch                                                                                                                     Report ID                Type                  ID                      Date          Date        Date          ID Analyte              Method                 Result              cu            CSU          MDA    Qualifier Units 19-09012-15              TRG    L 1-102218-FIGS-104-SS-A          07/08/19 13:14              9/11/2019    19-09012    Actinium-228                                                    2.22E-01      2.23E-01     3.59E-01
   ---------- - ,,--*----~-------------""=--------
19-09012-15              TRG    L1-10221B-FIGS-104-SS-A           07/08/19 13:14              9/11/2019    19-09012     Si1ver-108m                                                    5.80E-02      5.80E-02     8.18E-02 19-09012-15              TRG                                      07/08/19 13:14              9/1112019    19-09012   Americium-241                                                    8.90E-02      8.91E-02     1.21E-01 19-09012-15              TRG    L 1-10221B-FIGS-104-SS-A          07108/19                    9/11/2019    19-09012     Barium-133                                                     2.56E-02      2.56E-02     1.35E-01 19-09012-15              TRG    L1-10221 B-FIGS-104-SS-A          07108/19 13:14              9/11/2019    19-09012    Bismuth-214                                   3.11E-01          1.22E-01      1.23E-01     2.56E-01 19-09012-15              TRG    L1-10221 B-FIGS-104-SS-A          07/08/19 13:14              9111/2019                  Cobalt-60       EPA 901.1 Modified        -1.42E-02           7.83E-02      7.83E-02     1.17E-01
                                                                                                                                                          --*******-'********---********-*---~---------********-----*-**********---'-__;'---1 19-09012-15              TRG    L 1-10221 B-FIGS-104-SS-A                                     9/11/2019                                  EPA 901.1 Modified        -1.58E-01           1.05E-01      1.06E-01     1.01E-01 19-09012-15              TRG    L 1-102218-FIGS-104-SS-A                                                                                                                               9.07E-02      9.14E-02     1.31E-01 1.53E-01      1.53E-01     1.86E-01 1.06E-01      1.06E-01     9.22E-02 19-09012-15              TRG                                                                                                                                                           1.03E-01      1.03E-01     1.43E-01 19-09012-15              TRG                                                                                                                                                           9.73E-02      9.73E-02     6.56E-02 19-09012-15              TRG                                                                                                                                                           6.44E-02      6.44E-02     9.15E-02 19-09012-15              TRG                                                                                                                                                                         1.66E+OO     9.19E-01 19-09012-15              TRG                                                                                                                                                                         7.16E-02     1.13E-01 19-09012-15              TRG                                                                                                             EPA901.1 Modified                                                        8.24E-02 19-09012-15              TRG                                                                                                             EPA 901.1 Modified                                                       8.28E-02 EPA 901.1 Modified                                                       1.06E+OO    u EPA 901.1 Modified                                                       1.79E-01 EPA 901.1 Modified                                                       2.44E-01 EPA901.1 Modified                                                        1.14E-01    u L1-10221B-FIGS-104-SS-A                                                                                  EPA 901.1 Modified                                                       2.56E-01 TRG    L 1-10221 B-FIGS-104-SS-A                                                                                EPA901.1 Modified                                                        2.54E-01    u 19-09012-15              TRG    L1-102218-FIGS-104-SS-A                                                                                  EPA901.1 Modified           9.64E-01                                     1.78E+OO    u 19-09012-15              TRG    L1-10221 B-FIGS-104-SS-A                                                                                 EPA 901.1 Modified          2.91E-01                                     2.76E-01              pCi/g 19-09012-15              TRG    L 1-102218-FIGS-104-SS-A                                                                                 EPA901.1                    1.34E-01                                     4.14E-01    u         pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect

Printed: 10/21/201912:02 PM                                                                                                                                                                                              Page 18 of 21 Report To:                                                                                        Work Order Details:
Patricia Giza                                                                                              19-09012 Eberline Analytical                                                    Zion    Solutions                                                        Purchase Order:
SDG:
677118
                                                                 "'____""----------*-"            ~--*-*"                                                       --'"""*----*-----  ---~---------
Final Report of Analysis                                           2701 Deborah Ave                                                     Analysis Category:____                ENVIRONMENTAL __________________ ........-----*-*-------*-- ______ _
Zion, IL 60099                                                               Sample Matrix:                SO Lab        Sample                   Client                      Sample        Receipt   Analysis                                                                                                                                            Report ID         Type                     ID                           Date          Date       Date Method                    Result         cu              CSU       MDA        Qualifier Units 19..09012-16     TRG        L1-10221 B-FIGS-105-SS-A              07/08/19 13:16   9/3/2019  9/11/2019                                        EPA901.1 Modified                3.60E-01     2.35E-01         2.36E-01  4.73E-01        u 19-09012-16      TRG        L1-10221 B-FIGS-105-SS-A              07/08/19 13:16   9/3/2019  9/11/2019                                        EPA 901.1 Modified              -1.53E-03     3.55E-02         3.55E-02  8.25E-02        u
                                                                                                                        -------------"""'"'1"'"""""'"''                 -----\------------**-'-----*-*-*-.. -**-*
19-09012-16      TRG        L1-10221B-FIGS-105-SS-A               07/08/19 13:16   9/3/2019  9/11/2019                                        EPA 901.1 Modified              -1.21E-01     8.16E-02         8.19E..02 1.05E-01        u 19-09012-16      TRG        L1-10221B-FIGS-105-SS-A               07/08/19 13:16
: 9/3/2019  9/11/2019
                                                                                           --,~-. cm-.--.*~---*------------                      EPA 901.1 Modified               2.07E-02     2.44E-02         2.44E-02  1.08E-01        u 19-09012-16      TRG        L1-102218-FIGS-105-SS-A               07/08/19 13:16   9/3/2019  9/11/2019  19-09012    Bismuth-214               EPA 901.1 Modified               2.93E..01    1.34E-01         1.35E-01  1.62E-01
                              ---*--------*-*-*--*-----*           ----------*.-*--------*----*------- . -*-------*-------------+-*-----*-----*----------------;-----*-*-----:----------*,*---*-----------*------
19-09012-16      TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16    9/3/2019  9/11/2019  19-09012 . Cobalt-60                EPA901.1 Modified                2.64E-02     7.89E-02         7.89E-02  1.35E..01       u
 . 19-09012-16 ~    TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16  : 9/3/2019  9/11/2019  19-09012    -----+--E--P----A--9-0__1___1_M_o*d--ifi*,-e-d----**----------------*-*--**-----------------
3.00E-02         3.00E-02  8.99E-02        u 19-09012-16      TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16  '           9/11/2019           -                            EPA901.1 Modified                1.58E-01     8.22E-02         8.26E-02  1.25E-01 19-09012-16      TRG        L1-10221 B-FIGS-105-SS-A              07/08/19 13:16             9/11/2019                                        EPA 901.1 Modified                            1.03E-01         1.03E-01  1.61E-01        u TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16              9/11/2019                                        EPA901.1 Modified                2.03E-01                      2.07E-01  8.50E-02        u
                                                    ---*--*-------*--+----------;-------+-----*---*--------------+--'-----*----~------*-----------*---+-'*------'-------------------------*--
TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16              9/11/2019                                        EPA901.1 Modified                1.71E-01                      1.19E-01  1.64E-01
                                                         '""'""'"'+------+------*---------*,*-----*-----*--*-----,*-
19-09012-16      TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16                                                               EPA901.1 Modified                                              9.83E-02  6.69E-02        u
---*----*---------~--      '        ----------
19-09012-16      TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16                                                                                                                                        2.92E-01        u
 ---*----*------*-*--+------*--*----*-----*-----**---*--ls---*----+----**-*-*-------*---*----*--*i--------+--*--**-------*--i--**-*------*---*-*----*+-----**-*--~----
19-09012-16      TRG        L1-102218-FIGS-105-SS-A               07/08/1913:16                                                                                                                                        3.83E-01
    -*--------~-----------*---*--**-----+--------*---------'-*--*------+---*------l---*-------*---!-------+*--------~--------*--
19-09012-16 '    TRG        L1-10221 B-FIGS-105-SS-A                                                                                                                                                                   1.37E-01        u 19-09012-16 ;    TRG    ~2218-FIGS-105-SS-A              .                                                                                                                                                                             u TRG        L1-10221B-FIGS-105-SS-A                                                                                                                                                                                    u TRG        L1-102218-FIGS-105-SS-A                                                                                                                                                                                    u 19-09012-16      TRG        L1-102218-FIGS-105-SS-A                                                                                                                                                          1.08E..01 2.10E-01 19-09012-16                 L1-10221B-FIGS-105-SS-A                                                                                                                                                          9.67E..02 2.12E..01 19-09012-16                                                                                                                                                                                                  1.33E-01  1.82E-01        u 19-09012-16                                                                                                                                                                                                  1.35E-01  1.62E-01 19-09012-16                                                                                                                                                                                                  1.90E-01  2.24E-01        u 1.02E+OO        u 3.11E-01 3.76E-01        u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>      EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                 865/481-0683                    FAX 865/483-4621

Printed: 10/21/201912:02 PM                                                                                                                                                                                                                                              Page 19 of 21 Report To:                                                                                                                    Work Order Details:
Patricia Giza                                                                                                                             19-09012 Eberline Analytical                                                                                  -
Zion Solutions                                                                                     Purchase Order:
SDG:
677118
                                                                                                                                                                                                                                                       ,_ >SW  .
                                                                                                                                                                                                          --------*- ------------ ''""-~---*--                                                          ,,,.
Final Report of Analysis                                                             2701 Deborah Ave                                                                                Analysis Category:
                                                                                                                                                                                    'r'----*-A ENVIRONMENTAL
                                                                                                                                                                                                                                               ,-.o--~--**-* -----'-' *--                                  ...
so U   A-                             s* _ _ _ _ _._, --- m -------
Zion, IL 60099                                                                                       Sample Matrix:
Lab              Sample                                 Client                   Sample            Receipt    Analysis       Batch                                                                                                                                                       Report ID               Type                                       ID                    Date              Date       Date           ID Analyte                                      Method                          Result          cu              CSU      MDA      Qualifier Units 19-09012-17             TRG                  L______________
1-10221 D-FIGS-005-SS-A           07/08/19 12:30       9/312019   9/11/2019     19-09012        Actinium-228                             EPA 901.1 Modified                   7.04E-01       2.10E-01        2.13E-01 4.77E-01                pCilg 19-09012-17             TRG
-------------- -------v------------- ___,____ ---------         "'"' _____________
L 1-102210-FIGS-005-SS-A              07/08/19 12:30
                                                                                   -------~-*-**-
91312019
                                                                                                         ----~---**
9/11/2019     19-09012         Silver-108m
                                                                                                                                          -----=-------~-~- .. ,--**----
EPA901.1 Modified                    -7.90E-02      6.59E-02        6.60E-02 7.20E-02       u        pCi/g 19-09012-17             TRG                  L1-102210-FIGS-005-SS-A               07/08/19 12:30       9/3/2019   9111/2019     19-09012      Americium-241                              EPA 901.1 Modified                    4.43E-03      1.37E-01        1.37E-01 1.80E-01       u        pCi/g
"'"''"'*---------------,*---*-"'*------------**------------------- -               --------,-----------------------,- ------------------.-----~----
19-09012-17             TRG                  L 1-10221 D-FIGS-005-SS-A             07/08/19 12:30       9/3/2019   9111/2019     19-09012          Barium-133                             EPA 901.1 Modified                 i  2.37E-02      3.51E-02        3.51E-02 1.03E-01       u        pCi/g
                                "'""'"'""'---~----,-----*------------ -------- - - - , ----,-=--------, --------------,-'O'                     ---------'          ~-~~             >-**-**
19-09012-17             TRG                  L1-102210-FIGS-005-SS-A
~ ------>--------- ------ "'"""'-"""**----------------------
07/08119 12:30       9/3/2019   911112019     19-09012         Bismuth-214                             EPA 901.1 Modified                 :  6.09E-01      1.50E-01        1.54E-01 2.45E-01                pCi/g 19-09012-17             TRG                  L1-10221 D-FIGS-005-SS-A              07/08/19 12:30       9/312019   9/11/2019     19-09012 i         Cobalt-60                             EPA 901.1 Modified                    2.58E-01      6.06E-02        6.20E-02 4.98E-02                pCi/g
----------~------- --------------**                                                 ------------*-------~---                     . - - - * . ------~"-
19-09012-17       :     TRG                  L 1-10221 D-FIGS-005-SS-A             07108/19 12:30       9/312019   9/11/2019     19-09012         Cesium-134                              EPA901.1 Modified                  !
                                                                                                                                                                                                                                  -8.27E-03
                                                                                                                                                                                                                                             '   2.05E-02        2.05E-02 6.88E-02       u        pCi/g 19-09012-17 ,           TRG                  L 1-102210-FIGS-005-SS-A              07/08/19 12:30       9/3/2019   9111/2019     19-09012 '       Cesium-137                              EPA 901.1 Modified                 ! 1.39E+OO       2.09E-01        2.21E-01 1.48E-01                pCi/g 19-09012-17             TRG                  L 1-10221 D-FIGS-005-SS-A             07/08/19 12:30       9/3/2019   9/11/2019     19-09012  !    -
cu1                      <CO
                                                                                                                                                        ..... '"', ... ,:1-,...,.._          EPA 901.1 Modified                   -7.00E-02      2.21E-01        2.21E-01 2.24E-01       u        pCi/g 19-09012-17             TRG                  l 1-102210-FIGS-005-SS-A              07/08/19 12:30       9/3/2019   9/11/2019     19-09012 '     cu, ... '"''"''11-1..>"t                  EPA 901.1 Modified                   -2.42E-02      1.90E-01        1.90E-01 1.19E-01       u        pCi/g
--------------------s-------------*---**--------                                -
19-09012-17             TRG                   L 1-102210-FIGS-005-SS-A             07/08/19 12:30       9/3/2019   9/11/2019     19-09012 :     Europium- .55                             EPA 901.1 Modified                    7.09E-02      6.61E-02        6.62E-02 1.88E-01       u        pCi/g -*-
19-09012-17 i           TRG                  L 1-10221 D-FIGS-005-SS-A             07108/19 12:30   :   9/3/2019   9111/2019 ' 19-09012        Holmium-166m                               EPA 901.1 Modified                    1.00E-01
                                                                                                                                                                                                                                             '   8.52E-02        8.53E-02 9.56E-02       u        pCilg 19-09012-17 ;          TRG                  L 1-10221 D-FIGS-005-SS-A             07/08119 12:30       9/3/2019   9111/2019     19-09012  i       lodine-129                             EPA 901.1 Modified                   3.29E+OO       1.43E+01        1.43E+01 4.26E+OO       u        pCi/g 19-09012-17       i     TRG                   L1-102210-FIGS-005-SS-A              07/08/19 12:30   :   913/2019   9/11/2019     19-09012 :     Potassium-40                              EPA 901.1 Modified                   1.35E+01
                                                                                                                                                                                                                                             '  2.00E+OO         2.12E+OO 5.20E-01                pCi/g 19-09012-17 [           TRG                   L1-10221 D-FIGS-005-SS-A             07/08/19 12:30       9/312019   9/11/2019     19-09012 ; Manganese-54                                  EPA 901.1 Modified                    5.61E-02      5.73E-02        5.74E-02 9.37E-02       u        pCi/g 19-09012-17       !     TRG                   L 1-10221 D-FIGS-005-SS-A            07108/19 12:30       9/312019   9/11/2019     19-09012   ! ""''"'"""''-                    M           EPA 901.1 Modified                    6.43E-03  !
4.61E-02        4.61E-02 7.16E-02       u        pCi/g
                                 --"--*-----------------                                                                                                                                                                                                      i 19-09012-17             TRG                   L 1-10221 D-FIGS-005-SS-A            07/08119 12:30   i   9/3/2019   9/11/2019     19-09012          Niobium-94                             EPA 901.1 Modified                    3.61E-02      5.09E-02
                                                                                                                                                                                                                                                              '  5.09E-02 8.14E-02       u        pCi/g 19-09012-17 ;           TRG                  l 1-10221 D-FIGS-005-SS-A             07/08119 12:30       9/3/2019   9/11/2019     19-09012 ,         Lead-210                              EPA 901.1 Modified                   2.87E+OO      2.30E+OO         2.30E+OO 3.72E+OO       u        pCi/g 19-09012-17 t           TRG                  L 1-102210-FIGS-005-SS-A              07/08/19 12:30       9/3/2019 , 9/11/2019     19-09012 :         Lead-212                              EPA 901.1 Modified                    6.53E-01  i   1.36E-01 1.40E-01 2.29E-01 :              pCi/g i
19-09012-17 ,           TRG                   L1-10221 D-FIGS-005-SS-A             07/08/19 12:30       9/3/2019 i 9/11/2019 , 19-09012             Lead-214                              EPA 901.1 Modified                 i  7.25E-01      1.78E-01        1.82E-01 2.84E-01                pCi/g 19-09012-17       i     TRG                   L 1-10221 D-FIGS-005-SS-A            07/08/19 12:30       913/2019   9/11/2019 ' 19-09012 i Promethium-145                                  EPA901.1 Modified                  i 6.59E-01  i   9.07E-01        9.07E-01 1.30E+OO       u        pCi/g
                                  ---,-----------**---*                                                                                        1 19-09012-17 ;           TRG                   L 1-10221 D-FIGS-005-SS-A            07/08/19 12:30       9/3/2019   9111/2019     19-09012         Radium-226                              EPA 901.1 Modified                    6.09E-01      1.50E-01     '  1.54E-01 2.45E-01                pCi/g 19-09012-17       i     TRG                  L 1-102210-FIGS-005-SS-A              07108119 12:30       9/3/2019   9/11/2019     19-09012       Antimony-125                              EPA901.1 Modified                     4.16E-02      1.48E-01        1.48E-01 2.47E-01       u        pCi/g i
19-09012-17       J     TRG                  L 1-102210-FIGS-005-SS-A              07/08119 12:30       9/3/2019   9/11/2019     19-09012 '       Thorium-234                             EPA901.1 Modified                     3.82E-01      1.28E+OO        1.28E+OO 1.71E+OO       u        pCi/g
                                                                                                                                ''O'----r--
19-09012-17       i     TRG                   L1-102210-FIGS-005-SS-A              07/08/19 12:30       9/3/2019   9/11/2019     19-09012  !      Thallium-208                            EPA 901.1 Modified                    4.04E-01      1.17E-01     l  1.19E-01 2.12E-01                pCi/g 19-09012-17       i     TRG                   L 1-10221 D-FIGS-005-SS-A            07108/19 12:30   i   9/3/2019   9/11/2019 i 19-09012    !      Uranium-235                             EPA 901.1 Modified                   -8.1           4.07E-01     :  4.07E-01 5.21E-01 i     u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
(  ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601   SCARBORO ROAD OAK RIDGE,                        TN 37830                                 865/ 481-0683                          FAX   865/ 483-4621

Printed: 10/21/201912:02 PM                                                                                                                                                                                   Page 20 of 21 Report To:                                                                         Work Order Details:
Patricia Giza                                                                                      19-09012 Eberline Analytical                                                           Zion Solutions
                                                                                                   **----.-**w*--**--***
SDG:
Purchase Order:         677118 Final Report of Analysis                                                 2701 Deborah Ave                                                         Analysis Category:  ____ ENVIRONMENTAL Zion, IL 60099                                                              Sample Matrix:         so Lab             Sample                   Client                       Sample        Receipt          Analysis     Batch                                                                                                        Report Analyte                    Method            Result       cu            CSU      MDA    Qualifier ID              Type                      ID                          Date           Date              Date        ID                                                                                                          Units 19-09012-18            TRG       L1-10221 D-FIGS-006-SS-A               07/08/19 12:32    9/3/2019         9/11/2019   19-09012 Actinium-228            EPA 901.1 Modified    6.21E-01   3.16E-01      3.17E-01 7.23E-01     u        pCi/g
                                                                        --------------------------------~-----------
19-09012-18            TRG       L 1-10221 D-FIGS-006-SS-A              07/08/19 12:32    9/3/2019         9/11/2019   19-09012                         EPA 901.1 Modified               1.00E-01      1.00E-01 1.22E-01    u         pCi/g 19-09012-18             TRG      L1-10221D-FIGS-006-SS-A                07/08/19        -                  9/11/2019                                    EPA 901.1 Modified               1.50E-01      1.50E-01 2.14E-01     u
*-----------"""""'" *-**--*~--------------*-
19-09012-18             TRG      L1-102210-FIGS-006-SS-A                                                                                                EPA901.1 Modified                6.89E-02      6.89E-02 2.51E-01     u        pCi/g 19-09012-18             TRG      L1-10221 D-FIGS-006-SS-A                                                                                               EPA901.1 Modified                2.78E-01      2.79E-01 4.89E-01 19-09012-18             TRG      L 1-102210-FIGS-006-SS-A               07/08/19 12:32                                                                  EPA 901.1 Modified    2.01E-01   1.39E-01      1.39E-01 2.37E-01     u
       ---**----- .-------* *--*-------"'---------*------1---------------------------------------------------------,-----------------------~--------------------------
19-09012-18             TRG      L1-102210-FIGS-006-SS-A                07/08/1912:32                                                                   EPA 901.1 Modified
--*----*-*-------------, -*-*---*--------------- ----+--------------;-----------i---**--------------:----------------+--- -------------------------------------------------
5.54E-02   5.45E-02      5.46E-02 1.79E-01     u 19-09012-18             TRG      L1-102210-FIGS-006-SS-A                07 /08/19 12:32                                                                 EPA901.1 Modified     8.30E-01   1.70E-01      1.76E-01 1.40E-01 19-09012-18             TRG       L1-10221D-FIGS-006-SS-A               07/08/1912:32                                                                   EPA 901.1 Modified
                                              -----------**-------*--+----------------r---*----'*-------------------------o,*****----;_________________ +-----*------
1.73E-01   2.16E-01      2.17E-01 3.13E-01     u 19-09012-18             TRG       L1-10221D-FIGS-006-SS-A               07/08/1912:32                                                                   EPA901.1 Modified    -3.02E-02   3.04E-01      3.04E-01 1.SSE-01     u        pCi/g
             -------c -------------****--------------
19-09012-18             TRG       L1-10221D-FIGS-006-SS-A               07/08/1912:32                                                                   EPA 901.1 Modified    8.28E-02   1.SOE-01      1.SOE-01 2.68E-01     u 19-09012-18             TRG       L1-102210-FIGS-006-SS-A               07/08/19 12:32                                                                  EPA 901.1 Modified    6.06E-02   1.83E-01      1.83E-01 1.22E-01     u 19-09012-18             TRG       L1-10221 D-FIGS-006-SS-A                                                                                              EPA 901.1 Modified   -6.17E-02   1.40E-01      1.40E-01 1.99E-01     u 19-09012-18             TRG       L1-10221 D-FIGS-006-SS-A                                                                                              EPA 901.1 Modified   1.24E+01    2.52E+OO      2.60E+OO 2.16E+OO
    - - - * : -*-*--      TRG       L1-102210-FIGS-006-SS-A                                                                                               EPA 901.1 Modified   -3.66E-02   1.19E-01      1.19E-01 1.86E-01     u TRG       L1-10221 D-FIGS-006-SS-A                                                                                              EPA 901.1 Modified    5.62E-02   9.28E-02      9.28E-02 1.46E-01     u TRG       L1-102210-FIGS-006-SS-A                                                                                               EPA901.1 Modified     1.61E-02   9.14E-02      9.14E-02 1.35E-01     u TRG       L1-102210-FIGS-006-SS-A                                                                                               EPA 901.1 Modified    1.81E+OO   2.02E+OO      2.03E+OO 3.38E+OO     u L1-10221 D-FIGS-006-SS-A                                                                                              EPA 901.1 Modified    9.85E-01   2.35E-01      2.41E-01 3.32E-01              pCi/g EPA901.1 Modified     8.92E-01   2.30E-01      2.34E-01 3.63E-01              pCi/g EPA901.1 Modified     3.52E-03   1.37E-01      1.37E-01 2.26E-01     u EPA901.1 Modified     5.20E-01   2.78E-01      2.79E-01 4.89E-01 L1-10221 D-FIGS-006-SS-A                                                                                              EPA 901.1 Modified    2.40E-01                 2.65E-01 L1-10221 D-FIGS-006-SS-A                                                                                              EPA 901.1 Modified   1.22E+OO    1.40E+OO      1.40E+OO L1-10221 D-FIGS-006-SS-A                                                                                              EPA901.1 Modified     5.24E-01   2.12E-01      2.14E-01 L1-10221 D-FIGS-006-SS-A                                                                      Uranium-235             EPA 901.1 Modified    1.0SE-01   4.53E-01      4.53E-01 6.81E-01 CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
("M>          EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                  865/481-0683           FAX   865/483-4621

Printed: 10/21/2019 12:02 PM                                                                                                                                                                                                                                                                       Page 21 of 21 Report To:                                                                                                                    Work Order Details:
Patricia Giza                                                                                                                    19-09012 Eberline Analytical                                                                                 Zion Solutions                                                                            Purchase Order:
SOG:
677118 Final Report of Analysis                                                                     2701 Deborah Ave                                                          ___,.....___A__n_alysis Category:              ---~f'J_~l-~Q-~~-E_N_T~~
Zion, IL 60099                                                                             Sample Matrix:                        SO Lab                       Sample                                       Client              Sample        Receipt    Analysis           Batch                                                                                                                                                                                    Report Type                                       10                   Date          Date       Date               ID Analyte                        Method                          Result                  cu                   CSU                 MOA             Qualifier 10                                                                                                                                                                                                                                                                                                                             Units 19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A             07/08/19 12:34   9/3/2019  9111/2019         19-09012           Actinium-228
                                                                                                                     ~-----**-*--*------~-----*---**-----
19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A             07/08/19 12:34   9/3/2019  9/1112019         19-09012            Silver-108m 19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A             07/08/1912:34    9/312019  9/11/2019         19-09012         Amelicium-241
**-*-****-****-***---*****--******--'**--*******-******** ***--------------*--***---                OA'----,----~-~- *-*----0-~----"'--"' * ------"'"''""
19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A             07/08/1912:34    9/312019  911112019         19-09012            Balium-133 19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A 19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A 19-09012-19 '                         TRG              . L1-10221D-FIGS-007-SS-A TRG                   L 1-102210-FIGS-007-SS-A TRG                   L1-10221 D-FIGS-007-SS-A                                                                                                         EPA 901-1 Modified                  9 . 37E-04                                 1. 82E-01           3.04E-01                 U
                ""'""'""""-"' **--"'""'""_ _ _ _ ,___________________,,_,,, + - - - - - - - - - - - - * - * - - - - - - * * * - - * * * - * - - - - * " - * - - - - - - - - - + - - - + - - - - - l - - - - - - * - - - - - - - - - - - - - - ~ - - - * * * * - * * - - - - * . - - - - - - - ~ - - - - - - - - - - * - * - - - - - - - - - - - - - - - * - - f 19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A                                                                                                          EPA 901.1 Modified                 -2.29E-01             3.44E-01              3.44E-01            1.56E-01                 U
                                                                                                                                                                                                                      -*----**"--t-----*--*----~-----~---*-***------------**--**----**-*-------*-----*----***--1 19-09012-19                           TRG                   L1-10221 D-FIGS-007-SS-A                                                                                                         EPA901.1 Modified                   3.25E-01             1.68E-01              1.69E-01            3.00E-01
                                                                                                                                                                                                                                   --*------*--r--**---"--
19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A             07108/1912:34                                                                                EPA901.1 Modified                                                              1.52E-01            1.26E-01                 U
                                                                            -----****--------***-**+----------'----**-------------..;.....        _________-i---------+-----------*-+-----*--*------------------------------_;,..-;;_                                                                                                                     __....
19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A             07108119                                                                                     EPA901.1 Modified                  -7.26E-01             6.10E-01              6.11E-01            7.74E-01                 U
    --------------*--------""'"""---~------------t-*---------~---***--*----------*-*---*--***--*----------i------------------+----*----4-->*-------*---------------------------
19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A                                                                                                          EPA901.1 Modified                                       4.87E+OO               5.03E+OO            1.81E+OO
                                   ----------------*----------1---------*-*l---------------*-----'--*----+----**--*------*---* --+---------~------'--------------------------------~---_;,.._c_--1 19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A                                                                                                          EPA901.1 Modified                                        9.08E-02              9.08E-02            1.48E-01                 U
                                                                             ----------*-*+--*-----+-------------------+-_;;;_________+---*-*-*------*-------**-+-----'-----------------------------'-_;__.;;.__.........
19-09012-19                           TRG                   L1-102210-FIGS-007-SS-A                                                                                                          EPA901.1 Modified                                        7.68E-02              7.68E-02            1.20E-01                 U                pCilg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MOA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;OUP=Ouplicate;TRG=Normal Sample;DO=Ouplicate Original;U=Non-detect
(     ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                 865/481-0683                          FAX 865/483-4621

ZS-WM-131
      . ~                                                    REC'D SEP O3 2019                               Revision 0 Information Use ZIONSOLUTIONSLLC   An EnergySolutions Company
                                                                                 ., 9 :a- O9 0 1 2 Ll-10221A-FIGS-002-SS-A                 NA   NA SOIL 500 ml   MARINELLI     l 6/11/2019           5 ROC HTD NA 1217                      922.34g Ll-10221A-FIGS-003-SS-A                 NA   NA SOIL 500 ml   MARINELLI     l 6/11/2019           5ROCHTD   NA 1219                      929.16g L 1-10221 A-FIGS-004-SS-A               NA   NA SOIL 500 ml   MARINELLI    1  6/11/2019           5ROC HTD  NA 1221                      925.96g LJ-102201-FJGS-005-SS-A                NA   NA SOIL 500 ml   MARINELLI     I  7/9/2019           5ROC HTD  NA 0830                      572.09g I
Ll-102201-QJGS-005-SS-A                 NA   NA SOIL 500 ml   MARINELLI    I   7/9/2019           5 ROC HTD NA 0830                      648.58g Ll-1022IA-FIGS-003-SB-A                 NA   NA SOIL 500 ml   MARINELLI       6/26/2019           5ROC HTD l              1004             NA       812.22g L1-1022JA-FIGS-001-SB-A                 NA   NA SOIL 500 ml   MARINELLI       6/26/2019           5ROCHTD J               1000             NA       677.47g LI-10221A-FIGS-004-SB-A                 NA   NA SOIL 500 ml   MARINELLI       6/26/2019           5 ROC HTD l               1006             NA       757.61g Ll-I0221A-FIGS-002-SB-A                 NA   NA SOIL 500 ml   MARINELLI       6/26/2019           5ROCHTD J               1002             NA       756.86g Ll-10221A-QIGS-OOI-SB-A                 NA   NA SOIL 500 ml   MARINELLI       6/26/2019           5ROC HTD l               1000             NA       614.42g Ll-1022IA-FJGS-007-SS-A                 NA   NA SOIL 500 ml   MARINELLI       6/17/2019           5ROCHTD 1               0856             NA       710.95g LI-102218-FJGS-002-SS-A                 NA   NA SOIL 500 ml   MARINELLI       6/17/2019           5ROC HTD l               0830             NA       714.12g Ll-I0221A-FJGS-002-SS-A                 NA   NA SOIL 500 ml   MARINELLI       6/17/2019           5ROCHTD l               0846             NA       771.65g Ll-10221A-FJGS-00I-SS-A                 NA   NA SOIL 500 ml   MARINELLI       6/17/2019           5 ROC HTD NA 0844                      707.40g Ll-I0221A-FIGS-005-SS-A                 NA   NA SOIL 500 ml   MARINELLI    I  6/13/2019           5 ROCHTD  NA 0745                      774.76g Ll-1022IA-FIGS-006-SS-A                 NA   NA SOIL 500 ml   MARINELLI    I  6/13/2019           5 ROC HTD NA 0747                      783.08g LI-10221A-FIGS-007-SS-A                 NA   NA SOIL 500 ml   MARINELLI    l  6/13/2019           5ROC HTD  NA 0749                      708.49g Ll-10221A-FIGS-008-SS-A                 NA   NA SOIL 500 ml   MARINELLI   1   6/13/2019           5ROCHTD   NA 0751                      794.16g Ll-10221A-FIGS-009-SS-A                 NA   NA SOIL 500 ml   MARINELLI    l  6/13/2019           5 ROC HTD NA 0753                      774.52g 4 of9

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ZS-WM-131 Revision 0 Information Use ZIONSOLUTIONSrrc    An EnergySo/utions Company
\   \    Ll-10221B-FIGS-100-SS-A                  NA      NA SOIL    500 ml MARINELLI     1 6/20/2019 0955 5 ROCHTD            NA-  '
627.14g
   ;;l   Ll-10221C-FJGS-103-SS-A                  NA      NA SOIL   500  ml MARINELLI     l 7/8/2019         5ROC HTD            NA 1247                                860.24g LI-10221B-FIGS-102-SS-A                  NA      NA SOIL   500  ml MARINELLI     l 7/8/2019         5 ROC HTD           NA 3                                                                                                   1310                                680.87g l '"f    LI-1022IB-FIGS-103-SS-A                  NA      NA SOIL   500  ml MARINELLI     l 7/8/2019 1312 5ROC HTD            NA 723.59g rs       L 1-10221 B-FIGS-104-SS-A                NA      NA SOIL   500  ml MARINELLI     1 7/8/2019 1314 5 ROC HTD           NA 824.34g J IP     L 1-1022 IB-FIGS-105-SS-A                NA      NA SOIL   500  ml MARINELLI    1  7/8/2019 1316 5 ROCHTD            NA 703.93g LI-10221D-FIGS-005-SS-A                   NA      NA SOIL   500  ml MARINELLI    l  7/8/2019         SROCHTD             NA 1230                                 626.47g Ll-1022ID-FIGS-006-SS-A                  NA      NA SOIL   500  ml MARINELLI    1  7/8/2019         5ROC HTD            NA 1232                                 649.53g Ll-10221D-FIGS-007-SS-A                   NA      NA SOIL   500  ml MARINELLI    l  7/8/2019         5 ROC HTD           NA 1234                                 485.57g Ll-1022ID-FIGS-008-SS-A                  NA       NA SOIL   500  ml MARINELLI    1  7/8/2019         5 ROC HTD           NA 1236                                 530.46g Ll-10221C-AJGS-109-SB-A                  NA       NA SOIL   500  ml MARINELLI    1  6/5/2019        FULL SUITE           NA 1236                                 920.33g Ll-10221C-AJGS-102-SB-A                  NA       NA SOIL   500  ml MARINELLI    l  6/5/2019        FULL SUITE           NA 1222                                 868.46g L l-10209C-AJGS-110-SB-A                 NA       NA SOIL   500  ml MARINELLI    1  6/6/2019        FULL SUITE           NA 0738                                 730.63g LI-10209C-AJGS-109-SB-A                  NA       NA SOIL   500  ml MARINELLI    1  6/6/2019        FULL SUITE           NA 0736                                 782.82g LI-10209C-AJGS-108-SB-A                  NA       NA SOIL   500  ml MARINELLI    l  6/6/2019        FULL SUITE           NA 0734                                 897.48g Ll-10209C-AJGS-107-SB-A                  NA       NA SOIL   500  ml MARINELLI    l  6/6/2019        FULL SUITE           NA 0732                                 654.16g Ll-10209C-AJGS-104-SB-A                  NA       NA SOIL   500  ml MARINELLI    l  6/6/2019        FULL SUITE           NA 0726                                 782.70g LI-10209C-AJGS-103-SB-A                  NA       NA SOIL   500  ml MARINELLI    1  6/6/2019        FULL SUITE           NA 0724                                 806.24g Ll-I0209C-AJGS-102-SB-A                  NA       NA SOIL   500  ml MARINELLI    I  6/6/2019        FULL SUITE           NA 0722                                 787.15g
:I<-                            '"'   - C       {&#xa3;i 5 of9

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ZS-WM-131 REC'D SEP O3                                             Revision 0 ZIONSOLUTIONSrrc                                                         *-gr*-
                                                                         ., r-- O9 0 1 2 2079                            Infonnation Use An EnergySolulio!Js Company Ll-10221D-FIGS-021-SS-A                NA   NA  SOIL     500       ml  MARINELLI                                          5 ROC HTD L1-1022ID-FIGS-001-SS-A                NA   NA  SOIL     500       ml  MARINELLI                                          5 ROCHTD Laboratory:                                     Date Submitted To Lab:             Ship Container No.: Cooler Temperature: FULL SUITE EBERLINE LABS                                                                                                      NIA
                                                 ~s Date              Time:                                                   Date: (mm/dd/yyyy):
                                                             ):
Relinquished by:
                                                                                                                                                       /oDf)
Relinquished by:                                Date              Time:
(mm/dd/yyyy):
Comments 9 of9

EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TENNESSEE 37830 ANALYTICAL                                                        PHONE (865) 481-0683 FAX (865) 483-4621 EBS-OR-46288 November 6, 2019 Patricia Giza Zion Solutions, LLC 2701 Deborah Avenue Zion, IL 60099 CASE NARRATIVE Work Order# 19-09014-0R SAMPLE RECEIPT This work order contains sixteen soil samples received 09/03/2019. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.
CLIENT ID                            LAB ID             CLIENT ID                        LABiD L 1-10220A-FSGS-006-SS-A              19-09014-04       Ll-10220H-FJGS-001-SS-A          19-09014-12 L 1-10220A-FSGS-O 16-SS-A             19-09014-05       L 1-10221 D-FIGS-004-SS-A        19-09014-13 L 1-1022 lB-FSGS-006-SS-A             19-09014-06       Ll-10220H-FJGS-004-SS-A          19-09014-14 L 1-1022 lD-FJGS-007-SS-A             19-09014-07       Ll-1022 lD-FIGS-O 10-SS-A        19-09014-15 L 1-10221C-FIGS-101-SS-A              19-09014-08       Ll-1022 lD-FIGS-O 14-SS-A        19-09014-16 L 1-10220I-FJGS-001-SS-A              19-09014-09       L 1-1022 lD-QIGS-013-SS-A        19-09014-17 L 1-10220I-FJGS-002-SS-A              19-09014-10       L 1-10221D-FIGS-013-SS-A         19-09014-18 L 1-102201-FJGS-004-SS-A              19-09014-11       L 1-10221D-FIGS-018-SS-A         19-09014-1 9 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.
Gamma Spectroscopy was performed using EPA Method 901.1 Modified.
Laboratory qualifiers are as follows:
U - Result is less than the MDA.
ANALYTICAL RES UL TS Combined Standard Unce1tainty is reported at I-sigma value.
Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.
Page l of 3

ANALYTICAL RES UL TS CONTINUED TOT AL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and selectively extracted and precipitated. Precipitates were mounted on 4 7mm filters. Filters were reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.
Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are repmted from Total Strontium assuming secular equilibrium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated an acceptable relative percent difference and normalized difference.
Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.
TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A pmtion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were counted by beta liquid scintillation.
Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.
NICKEL-63 A representative aliquot of each sample was prepared by leaching in acids. Aliquots were placed into appropriately sized beakers. Stable elemental Nickel carrier was added to each sample prior to digestion.
Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.
Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.
GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.
Page 2 of 3

ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as repo1ied. The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Actinium-228 and Bismuth-214 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY I ce1iify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her ee to be accurate as verified by the following signature.
M.R. McDougall Laboratory Manager Date: 11/6/2019 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services.
Page 3 of 3

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                 Page 1 of 21 Report To:                                                                    Work Order Details:
Patricia Giza                                                                               19-09014 Eberline Analytical                                                  Zion Solutions SDG:
677118                                 *----"*_, _______
                                                                       "-'-'"---------~~-                                                                           -------------*--"*--*                                       ,_,_, ____
Final Report of Analysis 2701 Deborah Ave                                                                            ENVIRONMENTAL Zion, IL 60099                                                           Sample Matrix:     so Lab        Sample                    Client                    Sample           Receipt     Analysis        Batch                                                                                                           Report ID         Type                      ID                         Date             Date         Date           ID Analyte            Method         Result         cu            CSU      MDA            Qualifier Units 19-09014-01       LCS       KNOWN                             09/05/19 00:00                     1017/2019      19-09014       Tritium   LANL ER-210 Modified               7.56E+OO 19-09014-01       LCS       SPIKE                             09/05/19 00:00                     1017/2019      19-09014       Tritium    LANL ER-210 Modified              7.99E+OO      1.48E+01 5.58E+OO 19-09014-02 . MBL       BLANK                              09/05/19 00:00                    1017/2019      19-09014       Tritium    LANL ER-210 Modified              3.31E+OO      3.32E+OO 5.58E+OO             u
                                                                                  -~-~---~-------~*------"  --~ *~*---*---. **-*-*-~~*-
19-09014-03       DUP       L 1-10220A-FSGS-006-SS-A           06/03/19 06:55        9/3/2019    1017/2019      19-09014       Tritium    LANL ER-210 Modified              3.19E+OO      3.19E+OO 5.38E+OO             u 06/03/19                          1017/2019      19-09014       Tritium    LANL ER-210 Modified              3.17E+OO      3.18E+OO 5.37E+OO             u
                                                                                                                                        ~----"'*---- -~
1017/2019      19-09014       Tritium   LANL ER-210 Modified               3.29E+OO      3.29E+OO 5.71E+OO            u 1017/2019      19-09014       Tritium                                                    3.35E+OO 5.59E+OO            u 1017/2019      19-09014       Tritium                                                    3.19E+OO 5.58E+OO            u 1017/2019      19-09014       Tritium                                                             5.48E+OO             u 19-09014-09     TRG                                                                                            19-09014       Tritium    LANL ER-210 Modified                                     5.53E+OO             u 19-09014-10     TRG                                                                                            19-09014       Tritium    LANL ER-210 Modified                                     5.47E+OO             u 19-09014-11      TRG                                                                                            19-09014       Tritium   LANL ER-210 Modified                                      5.45E+OO            u 19-09014-12      TRG                                                                                                           Tritium    LANL ER-210 Modified                                     5.41E+OO            u 1017/2019                     Tritium    LANL ER-210 Modified                            3.20E+OO 5.59E+OO             u 19-09014-14                                                                                     1017/2019                     Tritium    LANL ER-210 Modified                            3.07E+OO 5.30E+OO             u 19-09014-15                                                                                     1017/2019                     Tritium                                                    3.23E+OO 5.58E+OO             u 19-09014-16      TRG       L 1-10221 D-FIGS-014-SS-A                                            1017/2019                     Tritium                                                    3.19E+OO 5.52E+OO             u 1-----------*****'"----------*--**--+-----*********-+*****---*-+--*********-----*****>***-*--*---*+
19-09014-17      TRG        L 1-102210-QIGS-013-SS-A           07/09/19 08:51                    1017/2019                     Tritium                                                    3.12E+OO 5.36E+OO            u
    ---**----*******-------****--+----...;********--*-*........;-*-*****-:*-**--*******;*******-*--+**-**---****-*-----i-----'.,----****-------=-----..;___ _:...::...::..... -J 19-09014-18      TRG        L 1-102210-FIGS-013-SS-A           07/09/19 08:51                    10/8/2019                     Tritium                                                    3.17E+OO 5.39E+OO             u TRG        L1-10221D-FIGS-018-SS-A            07115/19 13:45        9/3/2019    10/8/2019                     Tritium                                                    3.16E+OO 5.49E+OO             u         pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601     SCARBORO ROAD OAK RIDGE,                   TN 37830        865/481-0683         FAX 865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                                                    Page 2 of 21 Report To:                                                                                                                           Work Order Details:
Patricia Giza                                                                                                                                      19-09014 Eberline Analytical                                                                   Zion       Solutions                                                                                  Purchase Order:
SDG:
677118
                                                                                 ----"---------~-,mm,-
Final Report of Analysis                                              -------**
2701 Deborah Ave Analysis Category:                      ~'ll'IRONMENTAL _________________________ _
Zion, IL 60099                                                                                            Sample Matrix:                           SO Lab          Sample                          Client                          Sample               Receipt    Analysis                   Batch                                                                                                                                                 Report ID           Type                             ID                              Date                Date          Date                      ID Analyte                            Method                              Result         cu              CSU         MDA   Qualifier Units 19-09014-01           LCS           KNOWN                                      09/05/19 00:00          9/3/2019   10/23/2019                 19-09014           Nickel-63                ASTM 3500-Ni Modified                        1.48E+03      4.44E+01                                         pCi/g 19-09014-01           LCS           SPIKE                                      09/05/19 00:00          9/3/2019   10/23/2019
* 19-09014                         Nickel-63                ASTM 3500-Ni Modified                        1.47E+03      1.28E+01       8.75E+01     3.23E+OO 19-09014-02           MBL           BLANK                                      09/05/19 00:00       , 9/3/2019    10/23/2019                 19-09014           Nickel-63                ASTM 3500-Ni Modified                       -2.24E+OO      1.85E+OO        1.85E+OO    3.29E+OO    u 19-09014-03           DUP           L 1-10220A-FSGS-006-SS-A                   06/03/19 06:55          9/3/2019   10/24/2019                 19-09014       ________________
Nickel-63     ,          ASTM 3500-Ni Modified                       -1.49E+OO      1.90E+OO        1.91E+OO    3.36E+OO    u
                                                                                       -------= -------,
19-09014-04            DO           L 1-10220A-FSGS-006-SS-A                   06/03/19 06:55          9/3/2019   10/24/2019. 19-09014                          Nickel-63                ASTM 3500-Ni Modified                        -3.48E-01     1.92E+OO        1.92E+OO    3.33E+OO    u
                    ------*------*-*-----"-------*                              ---------------------,-0,-~-----------: ------
19-09014-05          TRG            L 1-10220A-FSGS-016-SS-A                   06/03/19 07:15          9/3/2019   10/24/2019                 19-09014           Nickel-63                ASTM 3500-Ni Modified                       -6.21E-01      1.95E+OO        1.95E+OO    3.40E+OO    u 1--****------------+-**-----------**--****-----*----***---+--------------,-----------*-*-----------*****-c-*------*-***-***------+**-*
19-09014-06 ,_     _:i:i'<.<3______ L1-1022_1,8-.:.~~GS-006-SS-A    ----+-0_61__   1o_,_19_1_3_:3_5  --~3!2.&deg;-19  10/24/2019                 19-0901_~--, ___ __f:li_:~':_l-6_3_-l-****A_S_T_M_____35__o_o_-.N                       -1.50E+OO      1.92E+OO        1.92E+OO
____i _M_od_i_fie_d___,----------**-*-*-*--**-****'*--*-*--*-*-**-- 3.38E+OO    u
,__1_9_-0_9_0_14-_0_7___T_R_G_____ ~_1_:_1_ 0221.~:~~_G_S_-_00_7~_s_-_A____ ''' _ 06/1~/1912:3~_!)~3.:~1?, _1_0,_2_41_2_01_9__1_9-_0_90_1_4                         Nickel-63                                                                                          2.14E+OO     3.52E+OO    u L 1-10221C-FIGS-101-SS-A                   06/24/19 09:00          9/3/2019   10/24/2019                 19-09014           Nickel-63                                                                                          2.03E+OO     3.46E+OO    u
,----------------*--**--*--------*-*-----*-----*---+-----                                                             - - - - + - - - - :..---~-----
L1-102201-FJGS-001-SS-A                    06/27/19 09:40          9/3/2019   10/24/2019. 19-09014                          Nickel-63                                                                                          2.06E+OO     3.51E+OO    u L 1-102201-FJGS-002-SS-A                   06/27/19 09:42                     10/24/2019                                                                                                                        1.87E+OO        1.87E+OO    3.30E+OO    u L 1-102201-FJGS-004-SS-A                   06/27/19 09:46                     10/24/2019                                    Nickel-63                                                                           1.96E+OO        1.96E+OO    3.40E+OO    u L 1-10220H-FJGS-001-SS-A                   06/27/19 09:48                     10/24/2019                                    Nickel-63                                                                           1.98E+OO        1.98E+OO    3.43E+OO    u L 1-102210-FIGS-004-SS-A                   06/27/19 09:36                                                                   Nickel-63                                                                           2.14E+OO       2.14E+OO     3.65E+OO    u
          ----r-----
19-09014-14           TRG
                                ----    L 1-10220H-FJGS-004-SS-A                   07/09/19 08:20                                                                   Nickel-63                                                                           2.03E+OO        2.03E+OO    3.50E+OO    u 19-09014-15           TRG           L 1-102210-FIGS-010-SS-A                   07 /09/19 08:45                                                                  Nickel-63                                                                           2.12E+OO        2.13E+OO    3.53E+OO    u 19-09014-16           TRG           L 1-10221 D-FIGS-014-SS-A                  07 /09/19 08:53                                                                  Nickel-63                                                                           1.92E+OO        1.92E+OO    3.37E+OO    u 1 19-09014-17                           L 1-102210-QIGS-013-SS-A                   07/09/19 08:51                                                19-09014           Nickel-63                                                                           1.93E+OO        1.94E+OO    3.39E+OO    u
     - - - - - - ~ - - - ,. . . _, _________________
19-09014-18           TRG           L 1-10221 D-FIGS-013-SS-A 07/09/19 08:~           9/3/2019   1_0_,2_4_12_0_1_9-*-19-09014--
                                                                                                                                                           -+   -----------
Nickel-63                                                                           2.07E+OO       2.07E+OO     3.61E+OO    u 19-09014-19           TRG           L1-10221D-FIGS-018-SS-A                    07/15/19 13:45       i  9/3/2019 , 10/24/2019, 19-09014 ;                        Nickel-63                                                                           2.12E+OO       2.12E+OO     3.66E+OO    u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601     SCARBORO ROAD OAK RIDGE,                                   TN 37830                      865/481-0683                                 FAX   865/ 483-4621

Printed: 1013012019 3:09 PM                                                                                                                                                                                                                                                                                                                                                                                                      Page 3 of 21 Report To:                                                                                                                                                               Work Order Details:
Patricia Giza                                                                                                                                                                                  19-09014 Eberline Analytical                                                                                                           Zion                   Solutions                                                                                                          Purchase Order:
SDG:
677118
                                                                                                                 "~~~-*~------,--",m'""=---*~-= -**** -****,.                                                                                                                                                                                          --..--*-**---..-*********-****---*-
Final Report of Analysis                                                                           " " ' , ,_,,,_ ._ . ___
2701     ------~,-     Deborah Ave                           __ '"'"**----
                                                                                                                                                                                                                                                   ....- ...., ...... Analysis Category:                                          ENVIRONMENTAL Zion, IL 60099                                                                                                                                Sample Matrix:                                   so Lab                 Sample                                   Client                                                Sample                                Receipt             Analysis         Batch                                                                                                                                                                                                                                                  Report ID                  Type                                      ID                                                       Date                                Date         ,     Date              ID Analyte                                     Method                                  Result                             cu                            CSU                        MDA                     Qualifier Units
 ~9-09,914:.&deg;-~--L_c_s __ **- K!'_o_w_N______________                                                          ___0~1&#xa3;5-l:1:1.&#xa3;&deg;-&deg;-~--~3/2019                                       10/11/2019       19-&#xa3;~&deg;-1*~-                 ~:ro_nt_iu_m-_9<!___               EIChroM SRW01 Modified ,                            5.02E+01                       2.81E-01                                                                                                pCi/g
__'.?-09&#xa3;.14:.?1- *. -~~s~~----*--*----*-- - - * - - _?_9!&deg;-5-11~&#xa3;???.~_!!!_3!~?.'.?__1_0_11_11_20_:~--_'1~90~----S!ro~t~um-90                                                                                                                                     EIChroM SRW01 Modified T' .._4_-*8_9_E                         __+_o_1_______2_.65E+OO                              1.72E+01                   1.14E+OO                                    pCi/g
:?:?.~?.~~2-           *---~~L********. *---~~!':~----*----******-*-1-*-o__                                        9i_0_5_/19 00:00                          9/3/2019           10/11/2019       19-09014                   -~tron_~-~':'1.:.??*.*,_E_IC_h_ro__M            __s_R __w
__o1__ _M_od_ifi_,_e__d..........5__._7__4__E_-_0__2___________3
____._4_3
_____E___-___0___1_________3_.44_E_-_0
____1_*******--8*_.7__3___E__*__0__1_ *.**.*......u___________
pCi_ig ___ _,
19-09014-03                DUP              L1-10220A-FSGS-006-SS-A                                             06/03/19 06:55                           . 9/3/2019             10/11/2019       19-09014                    Strontium-90                       EIChroM SRW01 Modified                               3.09E-01                      3.75E-01                         3.90E-01                   9.22E-01                          U         pCi/g
~'.4:.&deg;-~--- :- ..... __l?_~----~-'..:.~?220A-FSGS-006-~~:~--- _____0_6__10__3__11____                                                9 __ 0_6___:_ _5__5___0 i___9__1_3_1_2_0_1_9__
                                                                                                                                                                                  ,10_11_1_12_0_19___1_9_-o
__9__0_1__4____ "......s___t_r_o___n__t_iu_m_-9_o....., __E_I_C
__hr_o_M_S_R_W_0_1_M_o_d_ifi_ed__~*-_2_.5_1_E_-0_1 __________3_.6_5_E_-_0_1 _____3__.7_6_E_-0_1_________                                    9._04_E_-0_1____u_______ *-****-***---p_Cii_g__,
19-09~-- , ..*. TRG _                       L1-10220A-FSGS-016-SS-A **-**-*                                     06/03/19 07:15                               9/3/2019           10/11/2019 : 19-09014                    __s_t_r_o__n___n__u_m_-_9_0-+-E_IC_h_r_o__M        ____s__
Rw__o_1_M_o_difi_,e__d_~____5_._4__        1E_-_02___,* _____3__._5_1E        ___-_0_1_____3_.5_1_E-_0_1________8__._9__1_E-_0_1_______u_________P_Ciig___ __,
19-09014-06                TRG              L1-102218-FSGS-006-SS-A                                             06/10/19 13:35                           : 9/3/2019             10/11/2019       19-09014                    Strontium-90                       EIChroM SRW01 Modified ,                             5.69E-02                      3.44E-01                     :   3.44E-01                   8.75E-01                          U         pCi/g
 ~~=TRG-                                      *;:1--1-02-2-1D:F--JG-S--0-07--S-S---A-****--*-*-~/1912:30                                                     i   9/3/2019           10/11/2019       19-09014                    Strontium-90                       EIChroM SRW01 Modified                               7.41E-01                      3.63E-01                         4.45E-01                   8.34E-01                          U         pCi/g
 .. '.~=~-~~-4-~---< .*..*:r.~~----*-'::.1:10~2~C_-_FI_G_s_-1_01_-s_s_-1>;_________, __0                            ___6_t__2___4___
                                                                                                                                  ,1__9____o
___9_:oo          !   9/3/2019            10/11/2019      19-09014 :                  Strontium-90                       EIChroM SRW01 Modified .                             3.55E-01                      3.07E-01                         3.31E-01                   7.39E-01                          U         pCi/g 19-09014-09                TRG              L1-102201-FJGS-001-SS-A                                             06/27/1909:40                            ' 9/3/2019              10/11/2019      19-09014                    Strontium-90                       EIChroM SRW01 Modified                               1.50E-01                      3.24E-01                         3.28E-01                   8.12E-01                          U         pCi/g
 *-**----- ******---**-*****-**-**------*---------*-+------**-*-'----+-*--**---,-**--*---,----*-****--**--~--------------f*--******-*----****-**********-**--*---'---*-----------**-***--*-*****-**--*..:..--'~-- -*-1 19-09014-10                TRG              L1-102201-FJGS-002-SS-A                                             06/27/19 09:42                               9/3/2019 i 10/11/2019 19-09014 : Strontium-90                                                      EIChroM SRW01 Modified ; 6.18E-01                                                  3.44E-01                         4.06E-01                   8.02E-01                          U         pCi/g 1--------------------------------------***                                                                                                                                                                                        -------l--------***----....l.---**-****--***1---*-**-------------*-**-----*-*-*****-***--***-****----....:c.......;:____,
19-09014-11                TRG              L1-1022DI-FJGS-004-SS-A                                             06/27/19 09:46                           !   9/3/2019 ' 10/11/2019: 19-09014                                 Strontium-90                       EIChroM SRW01 Modified                        i     -2.22E-01                      3.35E-01                         3.43E-01                   8.90E-01                          U         pCi/g 1                                     1 19-09014-12                TRG              L1-10220H-FJGS-001-SS-A                                             06/27/1909:48                                9/3/2019            10/11/2019      19-09014                    Strontium-90                       EIChroMSRW01 Modified                                1.73E-01                      2.97E-01                     i   3.03E-01                   7.40E-01                          U         pCi/g 19-09014-13                TRG              L1-10221 D-FIGS-004-SS-A                                            06/27/19 09:36 j 9/3/2019                                        10/11/2019 19-09014 1 Strontium-90                                             EIChroM SRW01 Modified                               1.98E-01                      3.63E-01 ; 3.69E-01                                         9.06E-01                          U         pCi/g
 --------------'~-----*------------------1-----**--**+-------*+----*-----****-****-*****----**-----*---+---*--***-----*---*-**********--*-*-*~---------------*-*---------*******--------..
19-09014-14                TRG              L1-10220H-FJGS-004-SS-A                                             07/09/19 08:20 : 9/3/2019 : 10/11/2019 19-09014 : Strontium-90                                                                                  EIChroM SRW01 Modified , 1.14E-02                                                  4.30E-01                         4.30E-01                   1.10E+OO                          U         pCi/g 1 - - - - - - ~ -~----s,,---------*-----------
19-09014-15                TRG              L1-102210-FIGS-010-SS-A                                             07/09/19 08:45                            i 9/3/2019             10/11/2019      19-09014                    Strontium-90                       EIChroM SRW01 Modified '                             4.57E-01                '     4.70E-01                         4.96E-01                   1.14E+OO                           U        pCi/g 19-09014-16 :              TRG              L1-10221D-FIGS-014-SS-A                                             07/09/190~9/3/2019 . 10/11/2019                                                  19-09014              !      Strontium-90                      EIChroMSRW01 Modified                                3.49E-01                ,     3.29E-01                     ,   3.50E-01                   7.96E-01                           U        pCi/g
!-***--*---*-**-*****-***-,***--*--*-------*------------------;--*--**-****-------                                                                                                                                           *--*------1-----------+------!-----+----------------'-*-*-''--.::....--1
__ 19-090'.4:.17 ' ___ :i:_~c::;     ____L_1-_10_2_2_10     __-_0_1G_s_-__0_1_3-_s_s_-A ______......_0_11~~~.?_8:5-_1_ _9_t3_12_o___                                        19.12?.':.:.:2.~-       19-09014                 -~~.'.'~u_m_-9_0~-!-E1C_hro                    __M__s_Rw  __o1_1_M_od_ifi__  e_d-+--2__        .54_E-0_11______*____4_._1o_E_-0__1_-';_4_._1_9_E_-0_1_ _ _                           1._08_E_+_oo_.;...._u__________....:Pc..C_ii.c.g_
4 19-09014-18          1     TRG              L1-10221D-FIGS-013-SS-A                                             07/09/19 08:51                           i 9/3/2019 , 10/11/2019                 19-09014                    Stron_~~--m_-9_0___,_E_IC_h_r_o_M_S_R_w_o_1__M                ____o_d_ifi_1e"d" *,-....-2._._s_1_E_-0_1__ ~*.__3__._8__5_E__-_0__1_,_3_._95_E_-0__1______                         1._0_2_E_+_oo_ _ _u____________p_Cii_g_..
:=1=9=-0=9=01=4-=1=9==l==T=R=G===----*-----~--1-=--1_0-=2-2_~1_0*-=--F_1-G:s_--_o-=1*8_--s_-s:-A:_*:=*=---~-T::*_0*1_=1_1-5_i_1_-9_1_3_:4_5_-~:_91_3_t2_01_9__,_'_1_0,_1_1,_20_1_9_____1_9_:o9014 1                              Strontium-90                       EIChroM SRW01 Modified                               2.38E-01                :     3.78E-01                         3.87E-01                   9.38E-01                          U         pCi/g 1-------*--*-+-*----**--*-------------------1---------~------~'---~-----*""<-----**- + - - - - - - - - - - - ~ - - - - - - - - - - - - - ~ - - - - - - - - * - * * * - - - * - * * * * - - - - - - - - - 1
,__1_9__
       -o_9_01__4_-0_1__+*--*L_c_s____          K_N__o__w_N______________________, ___0_9_10_51_19 00:00                                                         9/3/2019            9/13/2019       19-09014 _____c_o_b_a_1t_-6_0_..,._ __E                              __P__A_9__0_1_.1_M_o_d_ified_~__               11._31_1E_+o__2___..___s_.1_0E_+_o_o~j_____________________P_C_i1g_......
14-01             LCS              KNOWN                                                               09/05/19 00:00                            : 9/3/2019             9/13/2019       19-09014              i      Cesium-137                             EPA 901.1 Modified                              8.26E+01                      3.39E+OO                     /                                                                          pCi/g 14-01            LCS              SPIKE                                                               09/05/1900:00 ~ 0 1 9 I 9/-13-/2-0-19___1_9_-0_90_1_4~,--*C;;-balt-60                                                                                EPA901.1 Modified                               1.42E+02 i 1.03E+01 : 1.26E+01                                                            8.42E-01                                    pCi/g
,__19--0-9-0-14--0-*1-"'1*--L-C-s*---.....--S-P-IK-E*-***--------***-*-<--o-9*10*5-,1-9*0*0,-oo-l 9/3/2019                                                                           9/13/2019 --19-09014                         Cesium*---13*7--<c---E-PA_9_0_1__1*-M-*o-d-ifi*-,e-d-+--8-.5-2.-E+--o-1*-*1-9___3_3_E_+o*o~-1-.0-3_E_+_o1----1.-06_E_+_o_o__________p_C_i/_g___,
CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Ouplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
(     ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                                            865/481-0683                                       FAX           865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                     Page 4 of 21 Report To:                                                                                                        Work Order Details:
Patricia Giza                                                                                                       19-09014 Eberline Analytical                                                              Zion    Solutions                                               Purchase Order:
SDG:
677118
                                                                              ~~~-,-*---"--~-~-----*------"                                                   ,,, ._ " r n V O - - A , o ' - ,_ _. _ _ , _ ,__ ,____________     *---------
Final Report of Analysis                                                    2701 Deborah Ave                                             Analysis Category:                                    ENVIRONMENTAL Zion, IL 60099                                                    Sample Matrix:                                   SO Lab               Sample                   Client                         Sample        Receipt    Analysis   Batch                                                                                                                                             Report 10                 Type                    10                             Date           Date        Date      10 Analyte              Method                                    Result                     cu              CSU      MOA    Qualifier Units 19-09014-02                MBL       BLANK                                   09/05/19 00:00   9/3/2019                         Actinium-228                                                                                              2.37E-02 1.44E-01   u 19-09014-02                MBL       BLANK                                   09/05/19 00:00   9/3/2019
                                                                              -------------- ,.--------*-------~----
Silver-108m                                                                                               2.38E-02 3.47E-02    u 19-09014-02                MBL       BLANK                                   09/05/19 00:00              9/13/2019 19-09014   Americium-241      EPA 901.1 Modified                                                                      3.62E-02 4.79E-02    u
  ------*---- -------~ *--*-----***------- ___ ----*--*-*
19-09014-02                MBL       BLANK                                   09/05/19 00:00              9/13/2019 19-09014     Barium-133       EPA 901.1 Modified                                                                      1.33E-02 3.53E-02   u 19-09014-02                MBL       BLANK                                   09/05/19 00:00              9/13/2019 19-09014    Bismuth-214       EPA 901.1 Modified                                                                      5.74E-02 8.51E-02    u
"" ~-------*----~--*--------*---*-*-*-----
19-09014-02                MBL       BLANK                                   09/05/19 00:00              9/13/2019 19-09014      Cobalt-60       EPA 901.1 Modified                                                                      2.23E-02 4.21E-02    u 19-09014-02                 MBL      BLANK                                                               9/13/2019 19-09014    Cesium-134        EPA 901.1 Modified                                                                      3.00E-02 4.13E-02    u
. --------***-------*---*..... -------------                  -*-------*--                                                                     -*-----*~------"'------*
19-09014-02                MBL       BLANK                                   09/05/19                    9/13/2019 19-09014    Cesium-137        EPA 901.1 Modified                                                     2.18E-02         2.19E-02 4.69E-02   u
                                                                              -----c--------- ---------------,---*-*            -"'----~--
19-09014-02                 MBL      BLANK                                   09/05/19 00:00   9/3/2019   9/13/2019 19-09014 : Europium-152       EPA 901.1 Modified                                                     6.SOE-02         6.SOE-02 6.10E-02    u
 ---------------------' ---------  .    ---------*----*--------------                ----~.~----------------
19-09014-02                 MBL      BLANK                                   09/05/19 00:00              9/13/2019 19-09014                      EPA901.1 Modified                                                      1.07E-01         1.07E-01 3.11E-02    u 19-09014-02                 MBL      BLANK                                   09/05/19 00:00              9/13/2019 19-09014                      EPA 901.1 Modified                                                     2.92E-02         2.92E-02 4.33E-02    u
   ---------------,------=----------------,---
19-09014-02                MBL       BLANK                                   09/05/19 00:00              9/13/2019 19-09014   Holmium-166m       EPA901.1 Modified                                                      4.01E-02         4.01E-02 3.07E-02    u 19-09014-02                 MBL      BLANK                                                               9/13/2019              lodine-129       EPA 901.1 Modified                                                     1.11E-01                  1.58E-01    u 19-09014-02                 MBL                                                                          9/1312019             Potassium-40                                                                             3.50E-01         3.50E-01 4.67E-01    u 19-09014-02 .,_             MBL      BLANK                                                               9/13/2019                                                                                                      1.33E-02         1.33E-02 1.85E-02    u 19-09014-02                MBL       BLANK                                                                                                                                                                              1.89E-02         1.89E-02 3.19E-02    u 19-09014-02                 MBL      BLANK                                                                                      Niobium-94       EPA901.1 Modified                                                      1.86E-02         1.86E-02 3.40E-02    u 19-09014-02                 MBL      BLANK                                                                                       Lead-210        EPA 901.1 Modified                                                     4.00E-01         4.00E-01 6.21E-01    u
      ---------                                  *-----------------~
19-09014-02                 MBL      BLANK                                                                                       Lead-212        EPA 901.1 Modified                                                                      3.84E-02 6.37E-02    u 19-09014-02                 MBL      BLANK                                                                                       Lead-214        EPA901.1 Modified                                                                       3.66E-02 6.35E-02    u 19-09014-02                 MBL      BLANK                                                                                                       EPA 901.1 Modified                                                                      7.26E-02 1.06E-01    u 19-09014-02                 MBL      BLANK                                                                                                       EPA 901.1 Modified                                                                      5.74E-02 8.51E-02    u 19-09014-02                MBL       BLANK                                                                                                       EPA901.1 Modified                                                                       7.32E-02 1.06E-01    u 19-09014-02                 MBL      BLANK                                                                                                       EPA901.1 Modified                           2.20E-01                   2.84E-01         2.84E-01 4.46E-01    u 19-09014-02                 MBL      BLANK                                                                                                       EPA901.1 Modified                            1.93E-02                  6.39E-02         6.39E-02 1.03E-01    u 19-09014-02                 MBL      BLANK                                                                                                       EPA901.1 Modified                                                      9.55E-02         9.55E-02 1.47E-01    u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MOA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;OUP=Ouplicate;TRG=Normal Sample;OO=Ouplicate Original;U=Non-detect
(  ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                       865/481-0683                                      FAX 865/ 483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                     Page 5 of 21 Report To:                                                                                              Work Order Details:
Patricia Giza                                                                                                   19-09014 Eberline Analytical                                                  Zion Solutions                                                       ......
SDG:
Purchase Order:         677118 Final Report of Analysis                                          2701 Deborah Ave Analysis Category:           ENVIRONMENTAL so Zion, IL 60099                                                                            Sample Matrix:
Lab          Sample                         Client             Sample         Receipt    Analysis         Batch                                                                                                                                 Report
:                                                                                                                Analyte                            Method           Result           cu            CSU          MDA      Qualifier ID       :   Type                             ID                Date           Date        Date           ID                                                                                                                                   Units 19-09014-03 ;      DUP           L 1-10220A-FSGS-006-SS-A       06/03119 06:55    9/312019   9/1312019      19-09014        Actinium-228                 EPA 901.1 Modified      2.63E-01        1.89E-01      1.90E-01     3.60E-01      u          pCi/Q 19-09014-03 :      DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/13/2019      19-09014         Silver-108m
                                                                                                                                                    - *-- ---*-* -~*
EPA 901.1 Modified       1.36E-02      5.48E-02       5.48E-02     5.68E-02      u          pCi/g
~----*----*---------------*-*---------------~--"---------------
19-09014-03        DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/13/2019      19-09014     j Americium-241                 EPA 901.1 Modified      -7.23E-02       8.08E-02      8.09E-02     1.11E-01       u         pCi/g 19-09014-03 :      DUP           L 1-10220A-FSGS-006-SS-A       06/03119 06:55    9/312019   9/13/2019      19-09014         Barium-133                  EPA 901.1 Modified      -1.00E-02       1.58E-02      1.58E-02     1.18E-01       u         pCilg
                                       ----~----*"*-*-*------* -----*-*--=*----*-*------------*-----*---------,, ------*- - --
19-09014-03 ;      DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/1312019      19-09014        Bismuth-214                  EPA 901.1 Modified       3.07E-01       1.38E-01      1.39E-01     2.55E-01                 pCi/g 19-09014-03 :      DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9113/2019      19-09014          Cobalt-60                  EPA 901.1 Modified
                                                                                                                                                                                 ' 5.68E-02       6.0SE-02       6.0SE-02     6.81E-02       u         pCilg
                                                                -   *------------'---~~~ *-**--------'""'"'"--                             -----*
19-09014-03        DUP           L 1-10220A-FSGS-006-SS-A       06103119 06:55    9/3/2019   9/1312019      19-09014         Cesium-134                  EPA 901.1 Modified      4.14E-03       2.18E-02       2.18E-02     8.21E-02       u         pCi/g
                                                                       --*---,;*--*------*-*-------~-----*---*---*-----                                                          '
19-09014-03 '. DUP           L 1-10220A-FSGS-006-SS-A       06/03119 06:55    9/3/2019   9113/2019      19-09014         Cesium-137                  EPA 901.1 Modified       5.03E-02       6.22E-02      6.22E-02     9.83E-02       u         pCilg 19-09014-03    i   DUP           L 1-10220A-FSGS-006-SS-A       06103/19 06:55    9/3/2019
                                                                    ----------0------*--*
9/13/2019      19-09014 '     Europium-152 EPA 901.1 Modified       8.87E-03       9.18E-02      9.18E-02     1.71E-01       u         pCilg 19-09014-03    i   DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55  : 9/3/2019 , 9/13/2019      19-09014 :     Europium-154                  EPA 901.1 Modified       3.58E-02       1.57E-01      1.57E-01     8.78E-02       u         pCi/g 19-09014-03 i      DUP           L 1-10220A-FSGS-006-SS-A       06/03119 06:55 ;  9/3/2019   9/13/2019      19-09014 :     !:***--'**-  155              EPA 901.1 Modified    :  6.44E-02       9.02E-02      9.03E-02     1.36E-01       u         pCi/g 19-09014-03 '      DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/13/2019  !   19-09014 : Holmium-166m                      EPA901.1 Modified     i  1.41E-02  :    9.84E-02      9.84E-02     6.12E-02       u         pCi/g 19-09014-03        DUP        '  L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/13/2019      19-09014 :        lodine-129                 EPA 901.1 Modified      -5.87E-02       5.95E-02      5.95E-02     8.19E-02       u         pCi/g 19-09014-03 ,      DUP        :  L 1-10220A-FSGS-006-SS-A       06/03/19 06:55 :. 9/3/2019   9/13/2019      19-09014 !      Potassium-40                 EPA901.1 Modified     ; 7.14E+OO       1.23E+OO 1.28E+OO     2.83E-01                 pCi/g 19-09014-03        DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/13/2019      19-09014 i          *o C
EPA 901.1 Modified      -2.38E-02  '    7.39E-02       1.40E-02    1.14E-01       u         pCi/g 19-09014-03 :      DUP        . L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    913/2019   9113/2019      19-09014     I          "UO M
EPA 901.1 Modified       2.52E-02  :    4.51E-02      4.52E-02     6.20E-02       u         pCi/g
                                                                                  '                                        I 19-09014-03        DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/13/2019      19-09014         Niobium-94                  EPA901.1 Modified     i  1.75E-02       3.89E-02      3.89E-02     6.96E-02       u         pCi/g 19-09014-03        DUP           L1-10220A-FSGS-006-SS-A        06/03/19 06:55    9/3/2019   9/13/2019      19-09014 /         Lead-210                                                          6.32E-01      6.33E-01     9.95E-01       u         pCi/g
: 9/3/2019                                                               EPA9011t;H-~-01 19-09014-03 [      DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55               9/13/2019 ' 19-09014        i     Lead-212                  EPA 901.1                     -01       1.16E-01      1.18E-01     1.45E-01                 pCilg 19-09014-03    f   DUP        :  L1-1   *-  -.... -.... - ~~.
06/03/19 06:55    9/3/2019   9/13/2019 ' 19-09014 :            Lead-214                  EPA901.1                  . 1E-01  i    1.27E-01      1.28E-01     2.43E-01                 pCilg 19-09014-03    !   DUP        :  L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9113/2019      19-09014 : Promethium-145                    EPA 901.1 Modified       1.48E-02  l    7.13E-02      7.13E-02     1.06E-01       u         pCi/g 19-09014-03 :      DUP           L1-1   *-  -.... -
                                                    ~~      ~~
06/03/19 06:55    9/3/2019 : 9/13/2019      19-09014 :       Radium-226                  EPA901.1 Modified        3.07E-01  :    1.38E-01   :  1.39E-01     2.55E-01                 pCi/g 19-09014-03 I      DUP           L1-10220A-FSGS-006-SS-A        06/03/19 06:55  ! 9/3/2019   9/13/2019      19-09014     i  Antimony-125                 EPA 901.1 Modified       3.34E-02       1.29E-01      1.29E-01     1.88E-01       u         pCi/g 19-09014-03 i      DUP           L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019   9/13/2019      19-09014        Thorium-234                  EPA 901.1 Modified      1.04E+OO   i    7.09E-01      7.11E-01     1.11E+OO       u
* pCilg 19-09014-03    i   DUP_,,_, ___: L 1-10220A-FSGS-006-SS-A       06/03/19 06:55    9/3/2019 : 9/13/2019      19-09014 j      Thallium-208                 EPA 901.1 Modified       3.39E-01  . 1.41E-01   :  1.42E-01     1.11E-01                 pCi/g 19-09014-03    l   DUP           L1-10220A-FSGS-006-SS-A        06/03/19 06:55  ! 9/3/2019 , 9/13/2019      19-09014     J  Uranium-235                  EPA 901.1 Modified    l  1.94E-02 2.18E-01      2.18E-01     3.25E-01       u         pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
(  ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                              865/481-0683            FAX   865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                                                                                         Page 6 of 21 Report To:                                                                                                                    Work Order Details:
Patricia Giza                                                                                                                                  19-09014 Eberline Analytical                                                                                Zion Solutions SDG:
Purchase Order                677118 Final Report of Analysis                                                                        2701 _____
Deborah
                                                                                                                           "  ___, _____ __ Ave       ,
                                                                                                                                                                                                  -------------- _Analysis Category:..                  ENVIRONMENTAL Zion, IL 60099                                                                                                    Sample Matrix:               SO Lab                Sample                                 Client                             Sample               Receipt             Analysis                 Batch                                                                                                                                                                       Report ID                  Type                                   ID                                 Date                 Date                 Date                     ID Analyte                     Method                   Result                cu                     CSU             MDA            Qualifier Units 19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55          9/3/2019            9/13/2019
                                                                                                                                            ---------,m,_,,_
19-09014               Actinium-228              EPA 901.1 Modified           4.09E-01            2.16E-01               2.17E-01        4.37E-01               u               pCi/g
     -----------------w                                                                                                                                                                   ~
19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55          9/3/2019            9/13/2019               19-09014                Silver-108m              EPA901.1 Modified            3.50E-03                                                    6.64E-02
 ""_, _ _ _ """'      '""'"'"""""w - - ~ - *-, _ _ _, - * - - - - - - - - - - - - , _ ,_ _ _ ,,_                                              ',w., - * * - - * - - - - - ~ - - - - - " 'W __ , SWw,_"""'""""' "" ___ ,
______ 19-09014-04 .. . ____D()           ....... -~:~~~~:FSGS-006--~~_+/-:___ _                      06/03/19 06:55           9/3/2019           9/13/2019               19-09014              Americium-241              EPA 901.1 Modified          -5.86E-02                                                    1.11E-01
                                                                                                                                                                                            ----~-------*-
19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55 9/3/2019            9/13/2019               19-09014 Barium-133               EPA 901.1 Modified          -3.15E-03 2.97E-02        '         _______________
_____2.97E-02
                                                                                                                                                                                                                                                                                                  '"               1.31 E-01 19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55          9/3/2019            9/13/2019               19-09014                Bismuth-214              EPA901.1 Modified            4.84E-01            1.37E-01               1.39E-01         2.04E-01 19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55          9/3/2019            9/13/2019               19-09014                 Cobalt-60               EPA 901.1 Modified           3.65E-02            5.87E-02               5.87E-02         9.00E-02              U
,------ *-------                                                                                   ----------------~    ____ ,_____           .   ----'-""----~                         ,,_  --------                   . _____    ,_,_____        ,-----~,-,---      ,_________   ,_,, - ,-,,-----------."'-""'_________           ---*------*----------------------!
19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55           9/3/2019           9/13/2019               19-09014                Cesium-134               EPA 901.1 Modified           1.14E-03            2.70E-02               2.70E-02         1.04E-01              U 19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55                              9/13/2019                                                                                             5.87E-02            6.90E-02               6.91E-02         1.09E-01              U
 "'---------"'----~---,-------------------                                                       -+----*-------------------*---*----*-----------*---*---------,-----------------------,--
19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55                                                                                                                                                        6.59E-02               6.59E-02         1.78E-01              U
 --.-,------~-''"'"'"-""''"-"""'_____                                             -------1-------*-**---+... ---------.----.*---------.,.-.-;.__.___,____.__._,-j ....-.._ _.____._._,-.,_,_ _ .___-:.._ _ _ _ _._,._._.__ _,.__._,_,,~--*---*-*-*--*--.-,-.------.---.-.---.--.,--,-**--*
19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55           9/3/2019                                                                                    EPA 901.1 Modified                               1.00E-01               1.00E-01         9.05E-02              U
                                                                                        ---+------------*--------C---------------------*-------:-----'-----l------*----*------------------*-+-------*---*---------**--c-----------------**---*------------
19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55                                                                                                       EPA901.1 Modified                                1.21E-01                                1.84E-01              U 19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55                                                                                                       EPA 901.1 Modified                               1.15E-01               1.15E-01         6.79E-02              U 19-09014-04                DO 19-09014-04                DO
                              "'""""' ______        L1-10220A-FSGS-006-SS-A                                                                                                                                                                                                                                                              u 19-09014-04                DO               L1-10220A-FSGS-006-SS-A                                                                                                                                                                                                                                                              u DO               L1-10220A-FSGS-006-SS-A                                                                                                                                                                                                                                                              u DO               L1-10220A-FSGS-006-SS-A                                                   9/3/2019
                                                                -------*--------+--------------,-----~------------~-----*----+---
9/13/2019                                                                EPA901.1Modified                                                                        1.22E+OO   ,..,_, ________
u               pCi/g DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55           9/3/2019           9/13/2019                                                                EPA901.1 Modified                                                       1.26E-01         1.80E-01                              pCi/g DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55           9/3/2019           9/13/2019                                                                EPA 901.1 Modified                                                      1.05E-01         1.95E-01 DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55 , 9/3/2019                   9/13/2019                                                                EPA 901.1 Modified                                                                       1.04E-01              u DO               L1-10220A-FSGS-006-SS-A
                                                                                                    ----*---~-----------
06/03/19 06:55           9/3/2019           9/13/2019               19-09014                Radium-226               EPA 901.1 Modified                                                                       2.04E-01                              pCi/g 1---------*---------*-----D--O---L--1---1-0-2--2-*0-A---F-SG-S----00--6--S-S---A------+---06/03/19 06:55 -- : 9/3/2019                           9/13/2019               19-090141;-_An_ti_m-on-y*--1-2-5--+--*--------------,------------,--------,--*----~----2--.3-8-E--0*1-~--------,----
u 00               L1-10220A-FSGS-006-SS-A                          06/03/~~~~:55 -i ~_312019
* 9/13/2019                               19-09014 !--Thoriu-;;;:2-34-;----*------~---*-------------,-------1-.-11_E_+_00--------                                                                         u 19-09014-04 ,              DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55     ' 9/3/2019               9/13/2019               19-09014          i Thallium-208
                                                                                                                                                                                --+------*+-------------+----                                                                                     1.46E-01
                                                                                                                                                                                                                                                                     -+-----__;____________________                2.56E-01 1-------+-------'-------------*
19-09014-04                DO               L1-10220A-FSGS-006-SS-A                          06/03/19 06:55     I     9/3/2019           9/13/2019               19-09014 '              Uranium-235                                                                                      2.51E-01         3.64E-01              u               pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                       865/481-0683                  FAX 865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                          Page 7 of 21 Report To:                                                                                    Work Order Details:
Patricia Giza Eberline Analytical                                                       Zion          Solutions                                                        Purchase Order:
SDG:
                                                                      -- --~--------"-----,-.-,
Final Report of Analysis                                          -**
2701 Deborah Ave
                                                                             - * -
* w,_,, _ _ _ _ _ _ _ _ _
* _,_                                   Analysis. Category: .. _...
Zion, IL 60099                                                                    Sample Matrix:
Lab              Sample                       Client             Sample                    Receipt     Analysis    Batch                                                                                                                            Report Date        Date Analyte                  Method                  Result             cu           CSU           MDA      Qualifier ID               Type                         ID                  Date                                              ID                                                                                                                              Units 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                9/3/2019    9/13/2019  19-09014     Actinium-228                                                                     3.42E-01     5.00E-01       u 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                9/3/2019    9/13/2019  19-09014     Silver-108m                                                                      7.15E-02     6.71E-02        u
  --*----------*-~---------------*-*
19-09014-05             TRG           L 1-10220A-FSGS-016-SS-A    06/03/19 07:15                9/3/2019    9/13/2019  19-09014                                                                                      9.87E-02     1.32E-01        u 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                9/3/2019    9/13/2019                                                                                                9.04E-02     9.82E-02        u
                                 ----------------------~--~--
19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                9/3/2019    9/13/2019  19-09014     Bismuth-214         EPA 901.1 Modified                             1.13E-01      1.14E-01     2.07E-01
                                                                                           *---0--------------*-----*-----*--*---*--***-- -*-------------+--* -**---------------------*-*--***-
19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                9/3/2019    9/13/2019  19-09014       Cobalt-60         EPA 901.1 Modified           5.75E+OO          4.53E-01      5.41 E-01    1.52E-01 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                9/3/2019    9/13/2019  19-09014     Cesium-134          EPA 901.1 Modified           9.15E-03          3.89E-02      3.90E-02     7.68E-02       u 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/1907:15                 9/3/2019    9/13/2019  19-09014     Cesium-137          EPA901.1 Modified            4.39E-02          7.07E-02      7.07E-02     1.10E-01        u
                                                                 ---------                        ------                "www*--~*--            --+----**-**--------,----**--*-*-**.:____,,__ _
19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                9/3/2019    9/13/2019  19-09014                         EPA901.1 Modified             3.99E-02         1.90E-01      1.90E-01     1.89E-01        u 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                            9/13/2019  19-09014                         EPA901.1 Modified            -8.82E-03         1.33E-01      1.33E-01     9.91E-02        u 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/1907:15                                        19-09014                         EPA901.1 Modified 1.34E-01         1.01E-01      1.02E-01     1.35E-01        u 19-09014-05             TRG           L 1-10220A-FSGS-016-SS-A    06/03/19 07:15                                       19-09014    Holmium-166m         EPA901.1 Modified
_________. ,________________,________________________ _,________________f-------+-----------------*--*-----------t------------------+-------------------------------------    6.93E-02          1.17E-01      1.17E-01     6.81E-02        u 19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                                                     lodine-129         EPA901.1 Modified            2.68E+OO          1.14E+01      1.14E+01     3.11E+OO        u
    ------------,,------------------------,--+-----------;------------------------------------*-----+---------------------------------------*-,-------------------------------------------
19-09014-05             TRG           L1-10220A-FSGS-016-SS-A     06/03/1907:15                                                                         EPA901.1 Modified                              1.42E+OO      1.48E+OO     1.15E+OO 19-09014-05            TRG           L1-10220A-FSGS-016-SS-A     06/03/19 07:15                                                                                                     -5.09E-02         9.84E-02      9.84E-02      1.39E-01       u 19-09014-05            TRG           L1-10220A-FSGS-O16-SS-A     06/03/19 07:15                                                                                                      3.59E-02         5.77E-02      5.78E-02     6.00E-02        u 19-09014-05            TRG           L1-10220A-FSGS-016-SS-A                                                                                                                                                                                     u 19-09014-05            TRG           L1-10220A-FSGS-016-SS-A                                                                                           EPA 901.1 Modified            3.24E-01                                    2.03E+OO        u 19-09014-05            TRG           L1-10220A-FSGS-016-SS-A                                                                                           EPA901.1 Modified                                                         2.33E-01 19-09014-05            TRG           L1-10220A-FSGS-016-SS-A                                                                                           EPA 901. 1 Modified                            1.49E-01      1.50E-01     3.02E-01 19-09014-05            TRG           L1-10220A-FSGS-016-SS-A                                                                                           EPA901.1 Modified                              5.96E-01      5.96E-01     8.82E-01        u       pCi/g 19-09014-05            TRG           L1-10220A-FSGS-016-SS-A                                                                                                                                          1.13E-01      1.14E-01     2.07E-01 TRG           L1-10220A-FSGS-016-SS-A                                                                                                                                          1.30E-01      1.30E-01     2.15E-01        u TRG                                                                                                                                                                            9.50E-01      9.50E-01     1.26E+OO        u TRG                                                                                                                                                                            8.34E-02      8.39E-02     1.21E-01 TRG                                       06/03/19 07:15                                                                                                                       3.21E-01      3.21E-01     4.22E-01        u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                   865/481-0683                   FAX 865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                            Page 8 of 21 Report To:                                                                        Work Order Details:
Patricia Giza                                                                                                 19-09014 Eberline Analytical                                                                      Zion Solutions SDG:
Purchase Order:          677118 Final Report of Analysis                                                              2701 Deborah Ave
                                                                                       * * - - = ' - ' " = N e N , _ , , _ _ """"""'"
_l\naty~!s C_a_te_qory:      ENVIRONMENTAL Zion, IL 60099                                                                         Sample Matrix:          so Lab             Sample                       Client                            Sample                         Receipt         Analysis         Batch                                                                                                  Report Type                         ID                                  Date                           Date            Date            ID Analyte           Method             Result       cu            CSU     MDA    Qualifier ID                                                                                                                                                                                                                                                    Units 19-09014-06            TRG         L 1-10221 B-FSGS-006-SS-A                     06/10/19 13:35                    9/3/2019        9/13/2019       19-09014    Actinium-228  EPA 901-1 Modified      5,11E-01   1,87E-01      1-89E-01 3,85E-01 19-09014-06            TRG         L1-102218-FSGS-006-SS-A                       06/10/19 13:35                    9/3/2019        9/13/2019       19-09014    Si1ver-108m                           1-76E.02   2,91E-02      2_92E-02 5,69E-02   u
                                                                                 -----------~*~                    ,, --"-----* ---"''""'*-------~---"'---*-----
19-09014-06            TRG         L 1-10221 B-FSGS-006-SS-A                     06/10/19 13:35                    9/3/2019        9/13/2019       19-09014   Americium-241   EPA 901-1 Modified    -8,90E-02   6,88E-02      6_89E-02 9.10E-02    u 19-09014-06            TRG         L 1-10221 B-FSGS-006-SS-A                     06/10/19 13:35                    9/3/2019        9/13/2019       19-09014     Barium-133    EPA 901-1 Modified     5_52E-02   6,72E-02      6.72E-02 9A1E-02     u
 ----------......:---*-""-*-*-------------*-*---*~-, ~--                         --------------------0-- -------*"-**--                   ~'  ,_ ,,,,,~---****-----,----------
19-09014-06            TRG         L 1-10221 B-FSGS-006-SS-A                     06/10/19 13:35                    9/3/2019        9/13/2019       19-09014    Bismuth-214    EPA 901 _1 Modified    3,0SE-01   1-31E-01      1-32E-01 2,18E-01 19-09014-06            TRG         L1-102218-FSGS-006-SS-A                       06/10/19 13:35                    9/3/2019        9/13/2019       19-09014      Cobalt-60   EPA901_1 Modified       2,72E-02   7.0SE-02      7_05E-02 USE-01     u 19-09014-06            TRG
--------------*----"-'"\"'_'          L 1-10221 B-FSGS-006-SS-A
_______________     =------------------                06/10/19 13:35                    9/3/2019        9/13/2019       19-09014    Cesium-134     EPA 901-1 Modified    -1.37E-01   7.81E-02      7_84E-02 773E-02     u 19-09014-06            TRG     .________
L 1-10221---<-*-------
B-FSGS-006--SS-A                   06/10/19 13:35                    9/3/2019        9/13/2019       19-09014                                          2,83E-01   8,00E-02      8.13E-02 1-05E-01 19-09014-06            TRG         L 1-10221 B-FSGS-006-SS-A                     06/10/19 13:35                    9/3/2019        9/13/2019       19-09014                                          7_03E-03   USE-01        1-35E-01 1.45E-01    u
                                        ----------------------=-'='
19-09014-06            TRG         L 1-102218-FSGS-006-SS-A                      06/10/19 13:35                    9/3/2019        9/13/2019                                  EPA 901.1 Modified    -7.31E-02   2.04E-01      2,04E-01 7.30E-02    u 19-09014-06            TRG         L 1-102218-FSGS-006-SS-A                      06/10/19 13:35                    9/3/2019        9/13/2019                                  EPA 901-1 Modified     1.15E-01   6.86E-02      6.88E-02 1.30E-01    u L 1-10221 B-FSGS-006-SS-A                     06/10/19 13:35                    9/3/2019        9/13/2019                                  EPA901.1 Modified                 7,81E-02      7.81E-02 5.61E-02    u L 1-102218-FSGS-006-SS-A                      06/10/19 13:35                                    9/13/2019                                  EPA 901.1 Modified     1,89E-01   1.76E-01      1.77E-01 2,55E-01    u l 1-102218-FSGS-006--SS-A                     06/10/19 13:35                                    9/13/2019                                  EPA 901.1 Modified     1.15E+01   2.44E+OO      2,52E+OO 1.54E+OO L 1-10221 B-FSGS-006-SS-A                     06/10/19 13:35                                    9/13/2019                                  EPA 901.1 Modified     1.63E-02                 4_87E-02 8.39E-02    u        pCi/g L1-102218-FSGS-006--SS-A                      06/10/19 13:35                                    9/13/2019                                  EPA 901.1 Modified    -1.84E-02                 4,0SE-02 6.24E-02    u        pCi/g L1-10221 B-FSGS-006--SS-A                                                                                                                  EPA 901-1 Modified     8.98E-03                 4.19E-02 6,52E-02    u L1-10221 B-FSGS-006-SS-A                                                                                                                   EPA 901-1 Modified     1,02E+OO                 8.63E-01 1A2E+OO     u L 1-10221 B-FSGS-006-SS-A                                                                                                                  EPA 901-1 Modified     3.75E-01                 8,06E-02 1.43E-01 L 1-10221 B-FSGS-006-SS-A                                                                                                                  EPA90U                 2.43E-01                 1.00E-01 1.77E-01             pCi/g L 1-10221 B-FSGS-006-SS-A                                                                                                                  EPA 901.1 Modified     1.55E-01   1.09E-01      1_09E-01 1.68E-01    u 19-09014-06            TRG         L 1-102218-FSGS-006--SS-A                                                                                                                  EPA 901.1 Modified     3,0SE-01   1-31E-01      1.32E-01 2.18E-01 i                                                                                                                                                                                                                                u 19-09014-06 ;
--------'              ___TRG L 1-10221 B-FSGS-006-SS-A                                                                                                                  EPA 901.1 Modified     6.40E-02   1.34E-01      1.34E-01 1.99E-01 19-09014-06 ,          TRG         L 1-10221 B-FSGS-006-SS-A                                                                                                   Thorium-234    EPA 901-1 Modified     6,57E-01   5.63E-01      5_64E-01 8.70E-01    u 19-09014-06 +. TRG                 L1-102218-FSGS-006--SS-A                                                                                                    Thallium-208   EPA 901,1 Modified     3.32E-01   1.65E-01               2.56E-01 19-09014-06            TRG         L 1-102218-FSGS-006--SS-A                                                                                                   Uranium-235    EPA 901-1 Modified     1.02E-01   1.91E-01      1.91E-01 2,94E-01    u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect (1fJ;          EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                        865/481-0683            FAX 865/ 483-4621

Printed: 1013012019 3:09 PM                                                                                                                                                                                                                    Page 9 of 21 Report To:                                                                     Wolk Order Details:
Patricia Giza                                                                                               19-09014 Eberline Analytical                                                                                 Zion Solutions
                                                                                                             " ' _ _ _ _ _ _w _ _ u , o r n SDG:
Purchase Order:        677118 Final Report of Analysis                                                                         2701 Deborah Ave                                                                  Analysis Category: ___ ENVIRONMENTAL Zion, IL 60099                                                                       Sample Matrix:        so Lab          Sample                                   Client                                  Sample                    Receipt        Analysis       Batch                                                                                                   Report ID             Type                                   ID                                       Date                       Date          Date           ID Analyte             Method            Result      cu            CSU      MDA   Qualifier Units 19-09014-07         TRG              L 1-102210-FJGS-007-SS-A                                06/18/19 12 :30                9/3/2019       9/13/2019                                   EPA 901.1 Modified   1.13E+OO   5.38E-01      5.41E-01 1.00E+OO 19-09014-07         TRG              L1-102210-FJGS-007-SS-A                             ---""'"' __________
06/18/19 12:30                 9/3/2019
                                                                                                                      -'.---,-w~,
9/13/2019    19-09014      Silver-108m
                                                                                                                                                        ---*---*-----=- ____,__ ,"_ -- - EPA 901 .1 Modified   1.01E-01  1.31E-01      1.31E-01 2.22E-01    u 19-09014-07         TRG              L 1-102210-FJGS-007-SS-A                                06/18/19 12:30                 9/3/2019       9/13/2019    19-09014    Americium-241      EPA901.1 Modified    -2.62E-01  2.00E-01      2.00E-01 2.68E-01    u
                                                                                                                                       --~---&#xa5;*---------*--------,--
19-09014-07         TRG              L 1-10221 D-F J GS-007 -SS-A                            06/18/19 12:30                 9/3/2019       9/13/2019    19-09014       Barium-133      EPA 901.1 Modified    3.76E-03  9.79E-02      9.79E-02 3.25E-01    u 19-09014-07
    -----~--------*
TRG            _________          , ________________ '----------------*~--------~~---------------
                            "" " ' " ' " - - - - ' r n = - - - " ' " " " ' " - - ~ , - - ,
L 1-10221 D-F JGS-007 -SS-A                             06/18/19                       9/3/2019       9/13/2019    19-09014      Bismuth-214      EPA 901.1 Modified   1.33E+OO   3.56E-01      3.63E-01 5.62E-01 19-09014-07         TRG              L 1-10221 D-FJGS-007-SS-A                               06/18/19 12:30                 9/3/2019       9/13/2019    19-09014        Cobalt-60      EPA 901.1 Modified   2.16E+OO   2.38E-01      2.63E-01 2.65E-01 19-09014-07         TRG              L1-10221 D-F JGS-007-SS-A                               06/18/19 12:30                 9/3/2019       9/13/2019    19-09014      Cesium-134       EPA901.1 Modified     3.45E-02  9.81E-02      9.81E-02 2.43E-01    u 19-09014-07          TRG             L 1-10221 D-F JGS-007 -SS-A                             06/18/19 12:30                 9/3/2019       9/13/2019                                   EPA 901.1 Modified   1.06E+01   1.22E+OO      1.34E+OO 4.28E-01 19-09014-07 TRG
                         ~----*--------              """'" _______________
L 1-102210-FJGS-007-SS-A                                06/18/19 12:30                 9/3/2019       9/13/2019                                   EPA 901.1 Modified    9.64E-02  4.29E-01      4.29E-01 4.73E-01    u 19-09014-07          TRG              L1-102210-FJGS-007-SS-A                                06/18/19 12:30                                9/13/2019                                   EPA 901.1 Modified   -5.54E-03  3.40E-01      3.40E-01 2.46E-01    u 19-09014-07          TRG              L 1-10221 D-FJGS-007-SS-A                              06/18/19 12:30                                9/13/2019                                   EPA 901.1 Modified    1.18E-01  2.38E-01      2.38E-01 3.47E-01    u
----------- ,------------------- .              -------*'"''""' -~"'"--------*-.-
19-09014-07         TRG              L 1-10221 D-F JGS-007 -SS-A                             06/18/19 12:30                                9/13/2019                                   EPA901.1 Modified    -4.99E-02  2.50E-01      2.50E-01 1.76E-01    u 19-09014-07          TRG              L1-102210-FJGS-007-SS-A                                06/18/19 12:30                                9/13/2019                                   EPA 901.1 Modified    2.72E-01  1.70E-01      1.70E-01 2.58E-01    u 19-09014-07          TRG              L1-10221 D-F JGS-007-SS-A                              06/18/19 12:30                                9/13/2019                                   EPA 901.1 Modified   2.04E+01   3.08E+OO      3.26E+OO 1.58E+OO
  ----          :   -*----       .    ----------~---------.
TRG              L1-10221 D-F JGS-007-SS-A                              06/18/19 12:30                                9/13/2019                                   EPA 901.1 Modified    2.28E-01  2.00E-01      2.00E-01 3.28E-01    u TRG              L 1-10221 D-F JGS-007-SS-A                             06/18/19 12:30                                                                            EPA 901.1 Modified    5.87E-02  1.33E-01      1.33E-01 1.44E-01    u TRG              L 1-10221 D-F JGS-007 -SS-A                                                                                                                      EPA 901.1 Modified   -6.49E-02  1.38E-01      1.38E-01 1.89E-01    u 19-09014-07         TRG              L 1-10221 D-FJGS-007-SS-A                                                                                                          Lead-210       EPA 901.1 Modified              1.61E+OO      1.61E+OO 2.68E+OO    u 19-09014-07          TRG             L 1-10221 D-FJGS-007-SS-A                                                                                                          Lead-212       EPA 901.1 Modified              4.04E-01      4.13E-01 6.09E-01 19-09014-07          TRG              L 1-102210-FJGS-007-SS-A                                                                                                                         EPA 901.1 Modified              3.53E-01      3.59E-01 6.33E-01 19-09014-07          TRG              L 1-10221 D-F J GS-007-SS-A                                                                                                                      EPA 901.1 Modified              1.29E-01      1.29E-01 2.92E-01    u 19-09014-07          TRG              L 1-102210-FJGS-007-SS-A                                                                                                                                                         3.56E-01      3.63E-01 5.62E-01 19-09014-07         TRG              L 1-10221 D-F JGS-007 -SS-A                             06/18/19 12:30                                                                                                            5.91E-01      5.91E-01 7.98E-01    u 19-09014-07         TRG              L 1-102210-FJGS-007-SS-A                                06/18/19 12:30                                                                                                            1.78E+OO      1.78E+OO 2.67E+OO    u 19-09014-07         TRG               L1-102210-FJGS-007-SS-A                                06/18/19 12:30                                                           Thallium-208     EPA 901.1 Modified              3.05E-01      3.07E-01 4.94E-01 19-09014-07          TRG              L1-10221 D-FJGS-007-SS-A                               06/18/19 12:30                                                           Uranium-235      EPA901.1 Modified    -9.70E-02  5.90E-01      5.90E-01 9.50E-01    u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
( "'M>
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                           865/481-0683           FAX 865/ 483-4621

Printed: 1013012019 3:09 PM                                                                                                                                                                                                                  Page 10 of 21 Report To:                                                                                  Work Order Details:
Patricia Giza                                                                                        19-09014 Eberline Analytical                                                                      Zion Solutions SDG:
Purchase Order:        677118
                                                                                                                                                                                                     -~-----,m"""--,=--**-*--------*-*
Final Report of Analysis                                                              2701 Deborah Ave                                                           Analysis Category:       ENVIRONMENTAL Zion, IL 60099                                                                Sample Matrix:        so Lab                  Sample                       Client                           Sample        Receipt   Analysis    Batch                                                                                                                                  Report ID                    Type                         ID                              Date           Date      Date        ID Analyte                      Method            Result         cu             CSU               MDA        Qualifier Units 19-09014-08                TRG        L1-10221C-FIGS-101-SS-A                      06/24/19 09:00    9/3/2019  9/13/2019 19-09014          Actinium-228              EPA 901.1 Modified    2.38E-01     1.61E-01       1.61E-01          3.01E-01         u
                                                                                  -------------------------------------------------- -               '"'"''""'+*-----                                   ---------~------s---              "' """""'-'"
L1-10221 C-FIGS-101-SS-A                     06/24/19 09:00    9/3/2019  9/13/2019 19-09014          Silver-108m               EPA 901.1 Modified
                                                                                                                                                                - ----~,--wrne-_,___,~,    -3A9E-02      4.12E-02       4.13E-02          5.38E-02         u 19-09014-08                 TRG       L1-10221C-FIGS-101-SS-A
---~-----------"*~---------~----*-*-*-*---------*
06/24/19          9/3/2019  9/13/2019 19-09014        Americium-241               EPA 901.1 Modified
                                                                                                                                    "'"''' ,,,,----------+-------------------
9.80E-02       9.80E-02           1.25E-01        u 19-09014-08                TRG L1-10221C-FIGS-101-SS-A                      06/24/19 09:00 , 9/3/2019 , 9/13/2019 19-09014
                                      -----------------------------*"""'___ --~-------~~-----------~---' -*-----~--" ----------~*-------
Barium-133                                                  3.10E-02       3.10E-02          7.91E-02        u 19-09014-08                TRG        L1-10221 C-FIGS-101-SS-A                     06/24/19 09:00    9/3/2019  9/13/2019 19-09014          Bismuth-214               EPA 901. 1 Modified   3.04E-01     1.08E-01       1.09E-01           1.84E-01
                                                                                  """-""""          ,----------------------------------------+-----
19-09014-08                TRG        L1-10221C-FIGS-101-SS-A                      06/24/19 09:00    9/3/2019  9/13/2019 19-09014            Cobalt-60               EPA 901. 1 Modified   2A5E-01      5.59E-02       5.73E-02          6.76E-02 19-09014-08                 TRG       L1-10221 C-FIGS-101-SS-A                     06/24/19 09:00    9/3/2019  9/13/2019 19-09014          Cesium-134                EPA 901.1 Modified    1.30E-02     2.24E-02       2.24E-02           5.57E-02        u 19-09014-08                TRG        L1-10221C-FIGS-101-SS-A                      06/24/19 09:00    9/3/2019  9/13/2019 19-09014          Cesium-137                EPA 901.1 Modified   1.06E+OO      1A8E-01        1.58E-01           1.07E-01 19-09014-08                TRG        L1-10221C-FIGS-101-SS-A                      06/24/19 09:00    9/3/2019  9/13/2019 19-09014                                    EPA 901.1 Modified    1.06E-01     1.78E-01                          1.67E-01        U
  -------------------------------------------------- ------1-----------------+-----~------------------------------1------------------------- -----------------c------------s-----------------------------------'-__;;'---1 19-09014-08                 TRG       L1-10221C-FIGS-101-SS-A                                                  9/13/2019 19-09014                                    EPA 901.1 Modified   -4.58E-02     1.26E-01       1.26E-01          8.65E-02         U
  --------"4" ___,________.------------------'"------,-----------------------+-------------------------------+------------------------------ -i----------------------------------------------------1 TRG       L1-10221C-FIGS-101-SS-A                                                  9/13/2019 19-09014                                    EPA 901. 1 Modified   UOE-01       9.50E-02       9.52E-02           1.30E-01        u TRG        L1-10221C-FIGS-101-SS-A                                                  9/13/2019 19-09014                                    EPA 901. 1 Modified  -7.37E-03     7.15E-02       7.15E-02          6.64E-02        u TRG       L1-10221C-FIGS-101-SS-A                                                  9/13/2019 19-09014                                    EPA 901.1 Modified    1.28E-01     3.64E+OO      3.64E+OO           3.38E+OO         u 19-09014                                   EPA 901.1 Modified   7.85E+OO      1A6E+OO        1.51E+OO          1.35E+OO 19-09014                                   EPA 901.1 Modified    6.31E-04     4.73E-02       4.73E-02           7A2E-02 19-09014                                    EPA 901.1 Modified   -3.75E-03                    3.59E-02          5.52E-02
_________          ,"" _________                                                                                                             Niobium-94               EPA 901.1 Modified    2A4E-02      3A3E-02        3A3E-02           5A1E-02 19-09014-08                 TRG       L1-10221 C-FIGS-101-SS-A                                                                                                       EPA 901.1 Modified                                1A3E+OO           2.27E+OO 19-09014-08                 TRG       L1-10221C-FIGS-101-SS-A                                                                                Lead-212                EPA 901.1 Modified                                                   1.53E-01 19-09014-08                 TRG       L1-10221C-FIGS-101-SS-A                                                                                Lead-214                EPA 901.1 Modified                                                  2.14E-01 19-09014-08                 TRG       L1-10221 C-FIGS-101-SS-A                                                                                                       EPA 901.1 Modified                                                  9.89E-01        u 19-09014-08                 TRG       L1-10221C-FIGS-101-SS-A                                                                                                        EPA 901.1 Modified                                                   1.84E-01 19-09014-08                TRG        L1-10221C-FIGS-101-SS-A                                                                                                        EPA 901.1 Modified                                                   1.80E-01        u 19-09014-08                 TRG       L1-10221C-FIGS-101-SS-A                                                                                                                                                                            1.20E+OO         u        pCi/g 19-09014-08                 TRG       L1-10221C-FIGS-101-SS-A                      06/24/19 09:00                                                                    EPA90U                                                              9.59E-02 19-09014-08                           L1-10221C-FIGS-101-SS-A                       06/24/19 09:00   9/3/2019                              Uranium-235                                                                                   3.74E-01         u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(    "'M>
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                    865/481-0683           FAX 865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                        Page 11 of21 Report To:                                                                                  Work Order Details:
Patricia Giza                                                                                                  19-09014 Eberline Analytical                                                                       Zion Solutions SDG:
Purchase Order:    677118
                                                                                         ,oc,--,--"--"'*--'"'"'"'""""'"-"
Final Report of Analysis                                                          2701 Deborah Ave                                                                        Analysis Category:_     ENVIRONMENTAL Zion, IL 60099                                                                                Sample Matrix:    so Lab                Sample                          Client                       Sample             Receipt      Analysis       Batch                                                                                                                 Report ID                Type                             ID                           Date               Date         Date           ID Analyte                        Method         Result      cu           CSU       MDA    Qualifier Units 19-09014-09                  TRG             L 1-10220l-FJGS-001-SS-A                06/27/19 09:40                                                    Actinium-228                                                                      7_55E-01 19-09014-09                  TRG             L 1-10220l-FJGS-001-SS-A                                                                                   Silver-108m                                                                      1_25E-01    u TRG             L 1-102201-FJGS-001-SS-A                                                                                                                                                                    1_59E-01    u 1.81E-01    u 19-09014                                                                   2_35E-01      2_37E-01  3.66E-01 19-09014-09                  TRG             l 1-102201-FJGS-001-SS-A                06/27/19 09:40                     9/13/2019     19-09014                                                                   1.31E-01      1_34E-01
                                                                                                                                           --------------------------------------t--------
19-09014-09 TRG l 1-102201-FJGS-001-SS-A                06/27/19 09:40                     9/13/2019
                                                       ,w*--=--"-'""''""m",-~,-,"*m*-+-------------*---*-------0***-----------**-*-*---*-
3_91E-02      3_91E-02  1.51E-01    u 19-09014-09                  TRG             L1-10220l-FJGS-001-SS-A                 06/27/19                           9/13/2019                                                                                                        1_91E-01 19-09014-09                  TRG             L 1-10220l-FJGS-001-SS-A                                                                                                                                                                    2.43E-01    u
                                          '  ~---------"--------------
TRG             L 1-10220l-FJGS-001-SS-A                                                                                                                                                                    1.24E-01    u TRG             l 1-102201-FJGS-001-SS-A                                                                                                                                                                    2.31E-01 TRG             l 1-10220l-FJGS-001-SS-A                                                                                                                                                                    1_06E-01    u TRG             L 1-102201-FJGS-001-SS-A                                                                                                                                                                    4.43E-01    u TRG             l 1-10220l-FJGS-001-SS-A                                                                                                                                                                    1.45E+OO TRG             L 1-10220l-FJGS-001-SS-A                                                                                                                                                                    1.38E-01    u TRG             L 1-10220I-FJGS-001-SS-A                                                                                                                                            6.31E-02      6.31E-02  1.0SE-01    u TRG             L1-10220I-FJGS-001-SS-A                                                                                                                                             7.41 E-02     7.41 E-02 1_07E-01    u TRG             L 1-102201-FJGS-001-SS-A                                                                                                                                            1 _63E+OO     1.64E+OO  2.56E+OO TRG             l 1-10220I-FJGS-001-SS-A                                                                                                                                            1_54E-01      1_58E-01  2_90E-01 TRG             l 1-102201-FJGS-001-SS-A                                                                                                                                            1.92E-01      1 _95E-01 3.48E-01 TRG             L 1-10220I-FJGS-001-SS-A                                                                                                                                            1.30E-01      1.30E-01  2_84E-01 L 1-102201-FJGS-001-SS-A                                                                                                              EPA901_1 Modified             2.35E-01      2_37E-01  3_66E-01 l 1-102201-FJGS-001-SS-A                                                                                                              EPA901_1 Modified                                     3_97E-01 l 1-10220l-FJGS-001-SS-A                                                                                                              EPA901_1 Modified EPA 901 _1 Modified EPA901_1 Modified CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(     ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                   865/481-0683      FAX 865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                                                  Page 12 of 21 Report To:                                                                                                           Work Order Details:
Patricia Giza                                                                                                                              19-09014 Eberline Analytical                                                                     Zion Solutions SDG:
Purchase Order:             677118 Final Report of Analysis                                                **-******
2701___ Deborah ,
Ave
__.. ,-,*-"'-"'"-*~~---------                                                              Analysis ca.regory_:_ ..      ENVIRONMENTAL so Zion, IL 60099                                                                                                  Sample Matrix:
Lab            Sample                              Client                        Sample                        Receipt    Analysis     Batch                                                                                                                                                        Report ID             Type                                  ID                          Date                           Date       Date          ID Analyte                                      Method                Result             cu              CSU         MDA     Qualifier Units 19-09014-10           TRG                 L 1-102201-FJGS-002-SS-A               06/27/19 09:42                     9/3/2019   9/16/2019   19-09014    Actinium-228                                   EPA 901.1 Modified        3.87E-01         1.39E-01        1.41E-01    2.55E-01
 -----~-"""' ----
19-09014-10           TRG                              ____ ____ ___
L 1-102201-FJGS-002-SS-A
                                                                 "_"   ,            06/27 /19 09:42 9/3/2019   9/16/2019   19-09014
                                                                                                         ------,.--------~----------~-----~-----*
Silver-108m
                                                                                                                                                                                                   '"-'      m,,*mm,-,--------*=""-"'"---
* EPA 901.1 Modified       -3.57E-02 4.51E-02 4.51E-02    4.05E-02 0--------------------*** ""'
u ''"'"
pCi/g
                                                                                                                                                                                                                                                                                                        ""*_,_,_,,~----
19-09014-10           TRG                 L 1-102201-FJGS-002-SS-A               06/27 /19 09:42                    9/3/2019   9/16/2019   19-09014   Americium-241                                   EPA 901.1 Modified        6.09E-02         8.95E-02        8.96E-02    1.22E-01        u            pCi/g
                                                                                             ---*-*-*-*- "'""''**-*--------=~---------~"~---~---*--                                                                           '
19-09014-10           TRG                 L 1-10220!-FJGS-002-SS-A               06/27/19 09:42                     9/3/2019   9/16/2019   19-09014       Barium-133                                  EPA 901.1 Modified       -9.67E-02         6.87E-02                                    u
                                                                                *---------------------------.-*--------,-----**-*--*---*--*=* ,-
6.89E-02    6.41E-02                     pCi/g 19-09014-10           TRG                 L 1-10220!-FJGS-002-SS-A
                   =*"'""--*-*--~---""_"_.,,_____" ' ' - - - * - - * - -          ___ ____
06/27/19 09:42 9/3/2019   9/16/2019   19-09014     Bismuth-214
_______ "'---~----------*--,,.-,.--~-,-,,                        .. ,_,,   --- I***-* EPA 901.1 Modified   ;    3.79E-01         1.06E-01         1.0SE-01   1.50E-01                     pCilg __
19-09014-10 ,         TRG                 L 1-10220!-FJGS-002-SS-A               06/27/19" 09:42
                                                                                           --    ___ ,,          .,.,. 9/3/2019   9/16/2019   19-09014         Cobalt-60 EPA 901.1 Modified   :    1.04E-01         3.38E-02        3.42E-02    5.0SE-02                     pCi/g 19-09014-10           TRG                 L 1-10220!-FJGS-002-SS-A 06/27/19 09:42                     9/3/2019   9/16/2019 , 19-09014      Cesium-134                                   EPA 901.1 Modified       -6.60E-03         1.92E-02        1.92E-02    4.42E-02        u            pCi/g 19-09014-10 *-----*=---"
-----*---<               TRG ____________    L1-10220!-FJGS-002-SS-A
                                                            .,_____________         06/27/19 09:42                     9/3/2019   9/16/2019   19-09014      Cesium-137                                   EPA 901.1 Modified        3.70E-01         8.50E-02        8.70E-02    9.95E-02                     pCi/g 19-09014-10           TRG L 1-10220!-FJGS-002-SS-A
                                                  , ____.                           06/27/19 09:42 i
9/3/2019   9/16/2019   19-09014    Cui .... ,., ..... 11-152                      EPA901.1 Modified    :    1.11E-01         1.14E-01        1.14E-01    1.50E-01        u            pCi/g 19-09014-10           TRG                 L1-10220!-FJGS-002-SS-A                06/27/19 09:42                     9/3/2019   9/16/2019 : 19-09014 . Eu,~~*~*,,_ 54                                 EPA901.1 Modified    I   -2.09E-02         6.50E-02        6.50E-02    7.64E-02        u            pCi/g 19-09014-10 '         TRG                 L 1-102201-FJGS-002-SS-A
                          *- "'"'"'------~---*---*----,_-,
06/27 /19 09:42 9/3/2019 : 9/16/2019   19-09014
* Eu,~~*~* ,,_ , 55                               EPA 901.1 Modified   :    1.02E-01         8.47E-02        8.48E-02    1.15E-01        u            pCi/g 19-09014-10 i         TRG                 L 1-10220!-FJGS-002-SS-A 06/27/19 09:42                     9/3/2019   9/16/2019   19-09014 i Holmium-166m                                    EPA 901.1 Modified   i   -1.41E-03         5.68E-02        5.68E-02    5.78E-02        u            pCi/g 19-09014-10           TRG                 L1-102201-FJGS-002-SS-A                06/27/19 09:42                     9/3/2019   9/16/2019   19-09014        lodine-129                                 EPA901.1 Modified         6.91E-01  ; 4.19E+OO             4.19E+OO    2.73E+OO        u            pCi/g 19-09014-10      !    TRG                 L 1-10220!-FJGS-002-SS-A               06/27/19 09:42                     9/3/2019   9/16/2019   19-09014 i  Potassium-40                                   EPA 901.1 Modified       1.04E+01         1.48E+OO         1.57E+OO    5.00E-01                     pCi/g 19-09014-10      !    TRG                 L 1-102201-FJGS-002-SS-A               06/27/19 09:42                     9/3/2019   9/16/2019   19-09014 ,  , ....... !,1 ................... 5" EPA901+~;1~:02 3.64E-02        3.64E-02    6.34E-02        u            pCi/g 19-09014-10 i         TRG                 L 1-10220!-FJGS-002-SS-A               06/27/19 09:42                     9/3/2019
                                                                                                                --~-----*-,-
9/16/2019 , 19-09014 , Molybdenum-93                                   EPA901.                     .   -03 .      3.39E-02        3.39E-02    5.00E-02        u            pCi/g 19-09014-10      j    TRG                 L 1-10220!-FJGS-002-SS-A               06/27/19 09:42                     9/3/2019   9/16/2019   19-09014 :     Niobium-94                                  EPA 901.1 Modified        4.72E-03         3.54E-02     . 3.54E-02    4.SOE-02        u            oCi/q 19-09014-10           TRG                 L1-10220!-FJGS-002-SS-A                06/27/19 09:42               i     9/3/2019   9/16/2019 ! 19-09014         Lead-210                                  EPA 901.1 Modified       2.32E+OO         1.68E+OO         1.68E+OO    2.69E+OO        u            pCi/g 19-09014-10           TRG                 L 1-102201-FJGS-002-SS-A               06/27/19 09:42               I     9/3/2019   9/16/2019   19-09014 ;       Lead-212                                  EPA901.1 Modified         3.85E-01         8.99E-02        9.20E-02    1.87E-01                     pCi/g 19-09014-10 :         TRG                 L 1-102201-FJGS-002-SS-A               06/27 /19 09:42                    9/3/2019   9/16/2019   19-09014         Lead-214                                  EPA 901.1 Modified   i    4.61E-01         1.11E-01        1.14E-01    1.67E-01                     pCi/g 19-09014-10      !    TRG                 L 1-102201-FJGS-002-SS-A               06/27 /19 09:42               i    9/3/2019   9/16/2019   19-09014   Promethium-145                                  EPA 901.1 Modified        5.14E-01  i      6.15E-01        6.16E-01    7.71E-01        u            pCi/g i
19-09014-10 j         TRG                 L 1-10220!-FJGS-002-SS-A               06/27 /19 09:42                    9/3/2019 : 9/16/2019   19-09014      Radium-226                                   EPA 901.1 Modified        3.79E-01         1.06E-01         1.DSE-01   1.50E-01                     pCi/g 19-09014-10 I         TRG                 L1-102201-FJGS-002-SS-A                06/27/19 09:42               i     9/3/2019 i 9/16/2019   19-09014    Antimony-125                                   EPA 901.1 Modified        7.84E-02  ;      8.25E-02        8.26E-02    1.53E-01        u            pCi/g 19-09014-10           TRG                 L 1-10220!-FJGS-002-SS-A               06/27/19 09:42               i     9/3/2019   9/16/2019   19-09014 ,  Thorium-234                                    EPA901.1 Modified         1.07E-01         8.71E-01     ;  8.71E-01    1.14E+OO        u            pCi/g 19-09014-10           TRG                 L 1-10220!-FJGS-002-SS-A               06/27/19 09:42               i     9/3/2019 , 9/16/2019   19-09014    Thallium-208                                   EPA901.1 Modified         2.57E-01  i      7.41E-02        7.52E-02    8.21E-02                     pCi/g i
19-09014-10      i    TRG                 L 1-102201-FJGS-002-SS-A               06/27/19 09:42               I     9/3/2019   9/16/2019 ; 19-09014     Uranium-235                                   EPA 901.1 Modified        4.63E-02  i      2.54E-01        2.54E-01    3.37E-01        u            pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
("M>          EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                   865/481-0683                FAX 865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                                                                   Page 13 of 21 Report To:                                                                                                              Worl< Order Details:
Patricia Giza                                                                                                                   19-09014 Eberline Analytical                                                                                             Zion Solutions Purchase Order:
SDG:
677118 Final Report of Analysis                                                                   ,..... __  ,    2701___Deborah Ave
                                                                                                                                             ---*,                                   *-*--    -        __ Analysis Category-.                        ENVIRONMENTAL Zion, IL 60099                                                                           Sample Matrix:                        so Lab                  Sample                               Client                                      Sample           Receipt     Analysis      Batch                                                                                                                                                           Report Type                               ID                                            Date            Date        Date          ID Analyte                         Method                            Result             cu                   CSU         MDA     Qualifier Units ID 19-09014-11                   TRG               L 1-10220!-F  JGS-004-SS-A                              06/27/19 09:46       9/3/2019 : 9/16/2019    19-09014            Actinium-228                             ___________
EPA901.1,,, Modified                   5.86E-01        1.87E-01              1.89E-01     3.28E-01                pCi/g
                                                        """'"' _ _ _ _ , _ _ .,,_,n _ _ , , ,
19-09014-11                   TRG               L 1-102201-FJGS-004-SS-A                                06/27/19 09:46     i 9/3/2019    9/16/2019   19-09014             Silver-108m                 EPA901.1 Modified 1.90E-02        4.81E-02              4.81E-02     7.75E-02     u          pCi/g f*-                           **-ue,*-----*----------~,m* ,__ -----"                                                                                                          ~-**---,-*---*--*                                                   -----*-*----*
19-09014-11                    TRG              L 1-102201-FJGS-004-SS-A                                06/27/19 09:46       9/3/2019    9/16/2019    19-09014         Americium-241                  EPA 901.1 Modified                    -172E-02         7.08E-02              7.08E-02     1.00E-01     u          pCi/g
 ---------*--- *-------~--------*-------------~-                                                                                                                                                        *----*-----**--~
19-09014-11                    TRG              L1-102201-FJGS-004-SS-A                                  06/27 /19 09:46     9/3/2019    9/16/2019    19-09014            Barium-133                  EPA901.1 Modified                      2.12E-03        2.98E-02         . 2.98E-02     1.04E-01     u          pCi/g 19-09014-11                    TRG              L 1-10220!-FJGS-004-SS-A                                 06/27/19 09:46    : 9/3/2019    9/16/2019    19-09014            Bismuth-214                 EPA 901.1 Modified                     5.65E-01        1.26E-01              1.30E-01     1.63E-01                pCi/g
 ----                                        '' --~--------*---                ------------"" -
19-09014-11                    TRG              L1-102201-FJGS-004-SS-A
                                           -*,w----,-~,-,_"
06/27/19 09:46     : 9/3/2019    9/16/2019   19-09014               Cobalt-60                 EPA 901.1 Modified                     1.04E-01        7.27E-02              7.29E-02     1.36E-01    u           pCi/g f.,,-""'"'""'"' """'_'_'='"')'"-'' ___,_,,
19-09014-11                                     L 1-102201-FJGS-004-SS-A                                 06/27/19 09:46                  9/16/2019                        Cesium-134
                                                                                                                                                                                          "---"-'          EPA901.1 Modified                      2.22E-03        3.15E-02 3.15E-02     8.46E-02     u TRG                                                                                         : 9/3/2019                 19-09014                                                                                                                                                          pCi/g
 ****-***-*-*-                    --------"-~---**-------------- --                                                             :
19-09014-11                    TRG              L 1-10220!-FJGS-004-SS-A                                06/27/19 09:46       9/3/2019 : 9/16/2019     19-09014            Cesium-137                  EPA 901.1 Modified                     5.35E-01    i   9.81E-02              1.02E-01     9.68E-02                pCi/g
   --*--""'<-~----*-----------                                                  ------~---"'*
19-09014-11                    TRG              L 1-10220!-FJGS-004-SS-A                                 06/27/19 09:46    i 9/3/2019    9/16/2019    19-09014           Europium-152                 EPA 901.1 Modified              i     -5.58E-02    i   1.86E-01              1.86E-01     1.56E-01     u          pCi/g
  ----------------*-----..--*-------,---..-------*--~--*-
19-09014-11                    TRG              L1-102201-FJGS-004-SS-A                                  06/27 /19 09:46   : 9/3/2019    9/16/2019    19-09014           Europium-154                 EPA 901.1 Modified              i 3.40E-02    :   1.65E-01              1.65E-01     7.95E-02     u        - pCi/g 19-09014-11                    TRG              L 1-102201-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019    9/16/2019    19-09014.. .,..,.. Europium-155                 EPA901.1 Modified                      1.60E-01        9.57E-02              9.60E-02     1.47E-01                pCi/g
-**---*---- -------*-------------..---------*---                                                                                                     ----*~-.--,
19-09014-11                    TRG              L 1-102201-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019 , 9/16/2019     19-09014         Holmium-166m                   EPA 901.1 Modified                     4.06E-02        4.08E-02         i    4.09E-02     6.87E-02     u          pCi/g
~~*--*-**-*-'-*----                                                              *--*-----~----,
19-09014-11                    TRG              L1-102201-FJGS-004-SS-A                                  06/27/19 09:46      9/3/2019    9/16/2019    19-09014             lodine-129                 EPA 901.1 Modified              :     -7.51E-02    i   1.89E-01              1.89E-01     2.69E-01     u          pCi/g
 - --*-------              '    ----------~---*..-*                                  --------~-                                                                                                                                            i 19-09014-11                    TRG              L1-10220!-FJGS-004-SS-A                                  06/27/19 09:46      9/3/2019    9/16/2019    19-09014 '         Potassium-40                 EPA901.1 Modified                     1.35E+01     i   2.70E+OO              2.79E+OO     1.22E+OO                pCi/g
  ---------*--,,._,,,,-, -~---------..---                                                  ------                                                                                                                                                                                  i 19-09014-11                    TRG              L 1-102201-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019    9/16/2019    19-09014               *s-*         <           EPA901.1 Modified                      1.54E-02    !   5.48E-02         i    5.48E-02     9.22E-02     u          pCi/g 19-09014-11           :        TRG              L 1-10220!-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019 ' 9/16/201      19-09014                     .. _,   M EPA 901.1 Modified              i      5.SOE-03    i   2.SOE-02              2.SOE-02     6.35E-02     u          pCi/g 19-09014-11                    TRG              L 1-102201-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019
* 9/16/2019     19-09014 '          Niobium-94                  EPA 901.1 Modified                     1.67E-02        4.24E-02              4.24E-02     6.62E-02     u          pCi/g u
19-09014-11                    TRG              L1-10220!-FJGS-004-SS-A                                  06/27 /19 09:46     9/3/2019    9/16/2019    19-09014    1 Lead-210                  EPA901.1 Modified               i      9.63E-01        8.22E-01         . 8.24E-01     1.36E+OO                pCi/g
 """'"'-"'"-"'"''"'""'-*"'--"*-------"--------*,wm,,_
19-09014-11                    TRG              L 1-10220!-FJGS-004-SS-A                                 06/27/19 09:46      9/312019 !  911612019    19-09014 :            Lead-212                  EPA901.1 Modified                      4.52E-01    i   9.76E-02              1.00E-01     1.79E-01                pCi/g 19-09014-11           i     ______
TRG ___   ,      L 1-102201-FJGS-004-SS-A      __..                       06/27/19 09:46      9/3/2019 i  9/16/2019    19-09014              Lead-214                  EPA 901.1 Modified                     4.0SE-01    i   1.06E-01              1.08E-01     1.80E-01                pCVg 9-09014-11                   TRG              L 1-10220!-FJGS-004-SS-A                                 06/27/19 09:46    i 9/3/2019 : 9/16/2019     19-09014       Promethium-145                   EPA 901.1 Modified                     3.58E-02        1.22E-01         i     1.22E-01    1.81E-01     u          pCi/g 19-09014-11           i        TRG              L 1-10220!-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019 i  9/16/2019    19-09014            Radium-226                  EPA 901.1 Modified                     5.65E-01        1.26E-01         :     1.30E-01    1.63E-01                pCi/g 19-09014-11           i        TRG              L 1-10220I-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019    9/16/2019 , 19-09014 i          Antimony-125                 EPA 901.1 Modified                    -2.81E-02    /    1.64E-01        i     1.64E-01    2.23E-01     u          pCi/g 11              TRG              L1-10220!-FJGS-004-SS-A                                  06/27/19 09:46      9/3/2019    9/16/2019 : 19-09014            Thorium-234                  EPA 901.1 Modified              i      5.31E-01    . 6.38E-01         :    6.39E-01     9.63E-01     u          pCi/g i
19-09014-11           i        TRG L 1-102201-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019 i 9/16/2019     19-09014           Thallium-208                 EPA901.1 Modified                      3.76E-01    i   1.73E-01              1.74E-01     2.63E-01                pCi/g 19-09014-11           i        TRG              L 1-102201-FJGS-004-SS-A                                 06/27/19 09:46      9/3/2019    9/16/2019    19-09014 \         Uranium-235                  EPA 901.1 Modified                     1.12E-01    !   2.36E-01         :    2.36E-01   . 3.54E-01     u      i   pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
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EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                               865/481-0683                           FAX     865/483-4621

Printed: 10130/2019 3:09 PM                                                                                                                                                                                                                                                                            Page 14 of 21 Report To:                                                                                                                                            Work Order Details:
Patricia Giza                                                                                                                                                       19-09014 Eberline Analytical                                                                       Zion Solutions                                                                                                                   Purchase Order:
SDG:
677118 Final Report of Analysis
                                                                                                                   -- v, 2701 Deborah Ave                                                                                              .... .. .. Analysis Category: __ ..                   ENVIRONMENTAL Zion, IL 60099 Sample Matrix:                  so Lab           Sample                           Client                           Sample          Receipt       Analysis                   Batch                                                                                                                                                                               Report ID Analyte                                    Method                     Result         cu            CSU         MDA            Qualifier ID         : Type                                                                Date            Date          Date                         ID                                                                                                                                                                               Units 19-09014-12            TRG           L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019      9/16/2019
                                                                                                                             ,. _________ ,,,    19-09014                           Actinium-228                              EPA 901.1 Modified                4A5E-01      2.69E-01      2.70E-01     4.80E-01            u             pCi/g
                                                                                     "" ----------*---                                        , e ' " - " _,,_, _ _ _ _ . _ . _ _ _ _ , _  _.,___.----~*
19-09014-12             TRG          L1-10220H-FJGS-001-SS-A                         06/27/19 09:48     9/3/2019      9/16/2019              19-09014                             Silver-108m                             EPA 901.1 Modified               -4A2E-02      6.63E-02      6.63E-02     1.11E-01       __   u
                                                                                        *-*-*--*----,.,   ~---*--* *----*-~*-~*~=------*----*---,mvrn,,                                           '"-""""*--                                                                                        --------*-   ,,,_,
19-09014-12             TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019      9/16/2019              19-09014                        Americium-241                                EPA 901.1 Modified             ' -8.38E-02     U7E-01        1.17E-01     L63E-01             u             pCi/g 19-09014-12
                          --*---~
TRG
                                             *---- -*---* -~----*****---*
L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48
                                                                                                          . 9/3/2019      9/16/2019              19-09014 ,                            Barium-133
                                                                                                                                                                                                                  ---1--,,-,.
EPA901.1 Modified                 1.08E-02
                                                                                                                                                                                                                                                                          . 4.26E-02      4.26E-02     1.90E-01            u             pCi/g 19-09014-12             TRG          L1-10220H-FJGS-001-SS-A                         06/27/19 09:48     9/3/2019      9/16/2019              19-09014                            Bismuth-214                              EPA 901.1 Modified                3.89E-01     2.18E-01      2.19E-01     3.38E-01                          pCi/g 19-09014-12             TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48   . 9/3/2019      9/16/2019              19-09014                                  Cobalt-60                          EPA 901.1 Modified                2.03E-01     9.54E-02      9.60E-02     2.09E-01            u             pCi/g
----------*-*-- *-*------*--                    wwOV-o""
                                                                                          *-*==*-----,,.--~,,.--e-,~~--------.;"""                                                  --------------------              t...-.--~- - - - - - - - - - - - - - -
19-09014-12             TRG --------------_,,_         __________ -------------
L 1-10220H-FJGS-001-SS-A                        06/27 /19 09:48    9/3/2019      9/16/2019              19-09014 ;                           Cesium-134 EPA 901.1 Modified             :  1.77E-02     4.73E-02      4.73E-02     1.34E-01            u             pCi/g 19-09014-12             TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019      9/16/2019              19-09014                             Cesium-137                              EPA 901.1 Modified               1.00E+OO      1.88E-01      1.95E-01     1.71E-01                          pCi/g
-----------,-.,-----~-*----                                               *-----
19-09014-12 TRG         ,L,1-10220H-FJGS-001-SS-A
                                            ,,_,,,,,,,-----------~                       06/27/19 09:48
                                                                                     ----~------
9/3/2019      9/16/2019
                                                                                                                                              -------~"-----------
Europium-152                               EPA 901.1 Modified             !  7.19E-02 2.42E-01      2.42E-01     2.54E-01            u             pCi/g 19-09014-12             TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48   ; 9/3/2019      9/16/2019              19-09014                          ~u1 .... ~, .. ,11-      l54               EPA 901.1 Modified               -4.35E-02     2.40E-01      2.40E-01     1.33E-01            u             pCi/g 19-09014-12 i           TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48   . 9/3/2019      9/16/2019              19-09014 ,                        Europium-EPA 901.1 Modified 1.05E-01     1.38E-01      1.38E-01     2.06E-01            u             pCi/g 19-09014-12             TRG          L 1-10220H-FJGS-001-SS-A                        06/27 /19 09:48  : 9/3/2019      9/16/2019              19-09014                   !    Holmium-166m                                 EPA 901.1 Modified                6.91E-03     1.22E-01      1.22E-01     9.65E-02            u             pCi/g 19-09014-12             TRG          L1-10220H-FJGS-001-SS-A                         06/27/19 09:48     9/3/2019      9/16/2019              19-09014 :                               lodine-129                          EPA 901.1 Modified                2.90E-02     9.04E-02      9.04E-02     1.36E-01            u             pCi/g
-*----------~ . -----                           ---------------------                                                                                                                                                                                                                                                              :
19-09014-12             TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019      9/16/2019              19-09014 ;                         Potassium-40                              EPA 901.1 Modified                1.05E+01     1.99E+OO      2.06E+OO     1.49E+OO                          pCi/g
                                                                                                                                                                                                                                                                          'i 19-09014-12 ;           TRG          L 1-10220H-FJGS-001-SS-A                        06/27119 09:48     9/3/2019      9/16/2019
                                                                                                         -{--*------,----*, ---*-------=-
19-09014                   i     Manganese-54                                EPA 901.1 Modified                5.01E-04     9.53E-02      9.53E-02     1.50E-01            u             pCi/g 19-09014-12             TRG          L1-10220H-FJGS-001-SS-A                         06/27/19 09:48     9/3/2019      9/16/2019              19-09014                   ! Molybdenum-93                                   EPA901.1 Modified              ;  9.30E-03   : 5.48E-02      5.48E-02     9.86E-02            u             pCi/g 19-09014-12 ;           TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48
                                                                                                          ; 9/3/2019      9/16/2019              19-09014                               Niobium-94                            EPA 901.1 Modified             : -1.66E-02  ;  7.06E-02      7.06E-02     1.10E-01            u             pCi/g 19-09014-12
* TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019      9/16/2019              19-09014                                  Lead-210                           EPA 901.1 Modified             i 2.49E+OO   '  1.34E+OO      1.34E+OO    2.16E+OO             u             pCi/g 19-09014-12             TRG          L 1-10220H-FJGS-001-SS-A                        06/27 /19 09:48    9/3/2019      9/16/2019              19-09014                                  Lead-212                           EPA 901.1 Modified             i  6.94E-01     1.95E-01      1.99E-01     2.90E-01                          pCi/g 19-09014-12
* TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48   ; 9/3/2019      9/16/2019              19-09014 '                                Lead-214                           EPA 901.1 Modified             i  4.05E-01     1.61E-01      1.63E-01     3.06E-01                          pCi/g 19-09014-12         i   TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48
                                                                                                          ' 9/3/2019      9/16/2019              19-09014                   !       ...... ''"" ......... 11- -,-...,         EPA 901.1 Modified               -1.18E-01     1.13E-01      1.14E-01     1.56E-01            u             pCi/g 19-09014-12 ;           TRG          L 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019      9/16/2019              19-09014 :                           Radium-226                              EPA 901.1 Modified             i  3.89E-01     2.18E-01      2.19E-01     3.38E-01                          pCi/g 19-09014-12 :           TRG          l 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019      9/16/2019              19-09014 i                        ,-,,.::, .. _ .. , .:::                    EPA 901.1 Modified               -1.84E-02  . 2.65E-01      2.65E-01     3.64E-01            u             pCi/g 19-09014-12         i   TRG L .rn??m        c '""'.flfl1-SS-A               06/27/19 09:48     9/3/2019      9/16/2019              19-09014 ;                          Thorium-234                              EPA 901.1 Modified                1.58E+OO  ;  1.89E+OO  . 1.89E+OO    3.16E+OO             u             pCi/g 19-09014-12             TRG          L1-10220H-FJGS-001-SS-A                         06/27/19 09:48     9/3/2019
* 9/16/2019                 19-09014                   J       Thallium-208                              EPA901.1 Modified                 1.97E-01     1.59E-01      1.60E-01     3.40E-01            u             pCi/g 19-09014-12         !   TRG          l 1-10220H-FJGS-001-SS-A                        06/27/19 09:48     9/3/2019 i 9/16/2019                 19-09014                   i u _,,,_,,, ::::                                 EPA 901.1 Modified                8.79E-02  !  3.62E-01  :   3.62E-01     5.46E-01            u             pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                                                        865/481-0683                      FAX   865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                                     Page 15 of 21 Report To:                                                                                                         Wotk Order Details:
Patricia Giza                                                                                                                        19-09014 Eberline Analytical                                                   _ _ ,__ w ---
Zion Solutions Purchase Order:
SDG:
677118
                                                             --~-----------------"                                                                                 ------'"'""'"''"-*----------~----                        --*----- - ----------*-*-*----
Final Report of Analysis
                                                             -*=* , _ _2701         Deborah Ave
_ _,, ______________                          -------                                Analysis_Category: _____ E                      _____N
______V
____ IRONMENTAL Zion, IL 60099                                                                             Sample Matrix:                           SO Lab          Sample                   Client                  Sample             Receipt                         Analysis  Batch                                                                                                                                                Report Analyte                Method                              Result                         cu                  CSU      MDA     Qualifier ID           Type                     ID                      Date                   Date                           Date    ID                                                                                                                                                  Units 19-09014-13       TRG        L1-102210-FIGS-004-SS-A         06127/19 09:36          9/3/2019                       9/16/2019 19-09014  Actinium-228       EPA 901 .1 Modified                     9.53E-01                                          4.23E-01 1.08E+OO     u
                                                               --------~-------,-------------*----*="=~-~----,--,
19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A        06/27/19 09:36          9/3/2019                       9/16/2019 19-09014  Silver-108m        EPA901.1 Modified                                                                         6.28E-02 1.42E-01      u I--------+-*****-----------******-------------------***-+******************--**** ..
19-09014-13       TRG        L1-102210-FIGS-004-SS-A                                                                9/16/2019 19-09014 Americium-241       EPA 901.1 Modified                     -2.23E-01                                          2.47E-01 2.97E-01      u
 *-*--,.-*-'"""-**-*--* c*" _,,-,,m*------*-*-------"'""                                                                                                ,_ ,------*-*-----*---------*
19-09014-13       TRG        L 1-102210-FIGS-004-SS-A                                                               9/16/2019 19-09014   Barium-133        EPA901.1 Modified                       1.86E-02                                          1.09E-01 2.12E-01      u EPA 901.1 Modified                                                                        2.70E-01 4.01E-01 EPA901.1 Modified                       2.28E+OO                                          2.72E-01 2.29E-01 19-09014-13       TRG        L1-102210-FIGS-004-SS-A         06/27/19 09:36                                                                                EPA 901.1 Modified                      7.64E-03                      4.93E-02            4.93E-02 1.10E-01      u
                 *--------------------------------------------------1------------+-----+----------"**---------------+----------------------i--*--------------------
19-09014-13       TRG        L1-102210-FIGS-004-SS-A         06/27/19 09:36                                                                                EPA 901.1 Modified                                                   1.12E+O              1.23E+OO 2.84E-01 19-09014-13       TRG        L1-10221D-FIGS-004-SS-A         06/27/19 09:36                                                                                EPA901.1 Modified                       1.57E-01                      4.31E-01            4.31E-01               u 19-09014-13       TRG        L1-10221D-FIGS-004-SS-A                                                                                                       EPA 901.1 Modified                      1.46E-01                      2.74E-01            2.74E-01 2.04E-01      u
                   ------*****--*--**-------***-J----***---i*-*--*----f----'-*****---'---;_**-*---+-*----*****-**--***-**--****~--------**<****---
19-09014-13   I   TRG        L1-102210-FIGS-004-SS-A                                                                                                       EPA 901.1 Modified                       1.27E-01                     1.14E-01            1.15E-01 3.12E-01      u l------~-----------------------
19-09014-13       TRG        L1-10221D-FIGS-004-SS-A                                                                                                       EPA901.1 Modified                      -1.35E-01                      1.74E-01            1.75E-01 1.66E-01      u 19-09014-13       TRG        L1-102210-FIGS-004-SS-A                                                                                                       EPA 901.1 Modified                     -1.25E+01                     5.20E+01             5.20E+01 6.69E+OO      u 19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A        06/27/19 09:36                                                                                EPA 901.1 Modified                      2.28E+01                     3.41E+OO             3.61E+OO 2.35E+OO 19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A        06/27/19 09:36                                                                                EPA901.1 Modified                                                     1.15E-01            1.15E-01 2.02E-01      u 19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A        06/27/19 09:36                                                                                EPA901.1 Modified                       7.31E-02                      7.86E-02            7.87E-02  1.14E-01     u        pCi/g 19-09014-13       TRG        L1-102210-FIGS-004-SS-A         06/27119 09:36                                                                                EPA 901.1 Modified                                                    8.63E-02                      1.33E-01     u
                          --<--~-,--**-----*
19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A                                                                                                      EPA 901.1 Modified                                                   4.59E+OO            4.61E+OO  7.14E+OO 19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A                                                                                                                                                                            2.27E-01            2.34E-01 4.30E-01 19-09014-13       TRG        L1-102210-FIGS-004-SS-A                                                                                                                                                                             3.26E-01                     5.07E-01 1
19-09014-13       TRG    -,- L1-102210-FIGS-004-SS-A                                                                                                                                                                        :    1.70E+OO            1.70E+OO 2.02E+OO      u 19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A                                                                                                                                                                            2.60E-01            2.70E-01 4.01E-01 19-09014--13      TRG        L1-102210-FIGS-004-SS-A                                                                                                                                                                             2.04E-01                     4.86E-01      u 19-09014-13       TRG        L1-10221 D-FIGS-004-SS-A                                                                                                                                                                                                2.0SE+OO 2.85E+OO      u 19-09014-13       TRG                                                                                                                                                                                                                                2.06E-01  1.71E-01              pCi/g 19-09014-13       TRG                                                                                                                                                                                                                                6.SOE-01 8.76E-01      u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
( "'M> EBERLINE                     ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                              865/481-0683                             FAX 865/483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                                                                                                 Page 16 of 21 Report To:                                                                                                                                      Work Order Details:
Patricia Giza                                                                                                                                                 19-09014 Eberline Analytical                                                                                                                                                                                                               SDG:
Final Report of Analysis Zion Solutions
                                                                                          -~--------------------"--- -****'
2701 Deborah Ave
                                                                                                                                                                          ------ - -                    Purchase Order:
                                                                                                                                                                                             - - Analysis Category: ____ ENV_IRQt.iMENIAL__ _ ___ _
___  677118
                                                                                                                                                                                                                                                                    "'"-'""'"""*-------------- -----~------
                                                                                        '*--,-,"-" "---*--"-""""-"""-*-"-~--mm-Zion, IL 60099                                                                                        Sample Matrix:                                         SO Lab                 Sample                         Client                              Sample                   Receipt     Analysis        Batch                                                                                                                                                                                            Report ID                  Type                          ID                                   Date                     Date         Date            ID Analyte                       Method                                              Result               cu                  CSU                   MDA          Qualifier Units 19-09014-14                 TRG            L1-10220H-FJGS-004-SS-A 07/09/19 08:20 9/3/2019     9/16/2019      19-09014
                                                                                                                       '-------~-----------""'""'"""'"'""'-, ,, _,        ________
Actinium-228             EPA 901.1 Modified                                         6.33E-01            2.40E-01           2.42E-01               5.09E-01
_1~-090_~~->-* TRG                        ___l:!.:.~~~20H-FJc:;_S-004-SS~---*-*--** - -- 07/091_~ 08:20 . ' -~0-~_()1~-~/2019                    _19-09:'.~~.         -- ~jlV_:'~:2~~m           EPA 901.1 Modifi__,e_d____ _,_.....*-8.99E-03                                  6.83E-02
_ _ _~---****--*-*-***--               6.83E-02               1.01E-01 19-09014-14                 TRG            L1-10220H-FJGS-004-SS-A                      07/09/1908:20                9/3/2019     9/16/2019      19-09014            Americium-241             EPA901.1 Modified                                          -4.22E-02           9.58E-02           9.59E-02               1.35E-01 19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                      07/09/1908:20                9/3/2019     9/16/2019      19-09014               Barium-133             EPA901.1 Modified                                          -7.34E-03           4.33E-02           4.33E-02               1.43E-01
 ----*----****-* *-***************-**-*-----**---------*-********-*                       -*-*------*                                   -----------****---------..,-------1-----------------*-***-*----*-***---*--*-----*-***-*>-*
19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                      07/09/19 08:20               9/3/2019     9/16/2019      19-09014              Bismuth-214             EPA 901.1 Modified                                          5.90E-01           1.77E-01           1.SOE-01               2.74E-01
                                                                                                                                                --,-"-"'"'" __ ,._m,.,,
19-09014-14                 TRG            L1-10220H-FJGS-004-SS-A                      07/09/19 08:20           f             , 9/16/2019       19-09014                Cobalt-60             EPA 901.1 Modified                                          1.72E-01           8.67E-02           8.71E-02               1.69E-01 19-09014-14                 TRG            L1-10220H-FJGS-004-SS-A                                                                               19-09014              Cesium-134              EPA901.1 Modified                                          -1.14E-02           3.18E-02           3.18E-02               1.25E-01           u 19-09014-14                  TRG
                                     -~---     L1-10220H-FJGS-004-SS-A                                                                                                                                                                                        1.37E+OO            1.88E-01           2.01E-01               1.22E-01
"'"""'""'"*---------*---~
19-09014-14                  TRG                                                                                                                                                                                                                           9.46E-03           2.75E-01           2.75E-01               2.14E-01 19-09014-14                  TRG
--------------~:_-1_02_2_0H_-f'.::!G_s_-0_0_4-~~~---**-+-o_1_1_09_1                                 __
19_o_s_:2__0__..;.**.* _. _ _ _ _ _ _ _ _       19-
__o_9__0__1_4_-+*-*****-'------l---E        ___P__A
__9_0__1__.1__;_M                                                        1.63E-01
__ _;_o:..:d_;__ifi_;__ed;____..c,.--......c=--- 4*--*__.___;:_.....;  __1.63E-01
_;__:..::::....:__ ____  __::..:.;._ _..:u 1.09E-01 19-09014-14                  TRG___,____________
L1-10220H-FJGS-004-SS-A                      07/09/19 _
                                                                      ****--**-l*-_;___;__:__           08:20  _i--__;:-: _ _ _ _ __;__:__ __                        +---.:..                      EPA 901.1 Modified
                                                                                                                                                                             -,'.----:...:..:.....i-.::..----:..::                                                                9.15E-02
                                                                                                                                                                                                                               ..:::.::..:....__-i'***--_;__...:..:....*+-----_;__:_-:..:_:-:..,-._:.:..:_;_::..:.::        2.03E-01 _____U 9.17E-02____..::__.:..:.::__:.:           -:.
19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                            1.0SE-01           1.0SE-01               9.32E-02           U        pCi/g 19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                            2.63E-01           2.63E-01               3.91E-01           u        pCi/g
-            *------,--            ~      -r---*---------
19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                            3.45E+OO          3.55E+OO                2.13E+OO 19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                            7.89E-02           7.89E-02               1.27E-01 19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                                               5.43E-02               8.51E-02 19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                                               6.45E-02                1.01E-01 19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                                               1.07E+OO               1.69E+OO 19-09014-14                  TRG           L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                                               1.32E-01               2.14E-01 L1-10220H-FJGS-004-SS-A                                                                                                                                                                                                                               1.42E-01               3.68E-01 1.83E-01 1.SOE-01               2.74E-01 9/3/2019 9/16/2019 I 19-09014                Antimony-125                                                                                                               2.30E-01               3.15E-01 19-09014-14                                                                                                          9/3/2019
                                                                                                                                     -9/16/2019      19-09014 !            Thorium-234 19-09014-14                                                                                                          9/3/2019     9/16/2019 ! 19-09014                 Thallium-208                                                                                                                                                                 pCi/g 19-09014-14                                L1-10220H-FJGS-004-SS-A                      07/09/19 08:20               9/3/2019     9/16/2019      19-09014 ;            Uranium-235             EPA 901.1 Modified                                                                                                                          u        pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(   ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                          865/ 481-0683                                             FAX 865/ 483-4621

Printed: 10/30/2019 3:09 PM                                                                                                                                                                                                                                          Page 17 of 21 Report To:                                                                                                                Work Order Details:
Patricia Giza                                                                                                                        19-09014 Eberline Analytical                                                                           Zion Solutions SDG.
Purchase Order:               677118
                                                                                                                                             -~------,----*                          ..    """'"""'''"*"""                     ---*"-*--*------------*-*---**--**----*                                      *****----**
Final Report of Analysis 2701 Deborah Ave                                                                                   Analysis Category:                ENVIRONMENTAL ____             ,
Zion, IL 60099                                                                                          Sample Matrix:
so Lab                   Sample                         Client                            Sample         Receipt       Analysis             Batch                                                                                                                                               Report ID                    Type                            ID                                Date           Date            Date               ID Analyte                                Method                   Result           cu            CSU      MDA    Qualifier Units 19-09014-15                   TRG          L1-102210-FIGS-010-SS-A                       07/09/19 08:45     9/3/2019      9/16/2019          19-09014        Actinium-228                                                     :
                                                                                                                                                                                                ,, ___ EPA901.1 Modified            1.52E+OO       6.43E-01       6.48E-01 1.36E+OO                      pCi/g
                                                                                          -* --**---~----"                                      ------------- ,---~-----
19-09014-15 1---*-"'"""""---*----*-* __,___
TRG          L 1-10221 D-FIGS-010-SS-A 07 /09/19 08:45 . 9/3/2019      9/16/2019          19-09014          Silver-108m                  ,,, __________________
EPA 901.1 Modified
                                                                                                                                                                                                                       ,,,,       i  2.39E-02  :    1.36E-01      1.36E-01 2.19E-01    u                 pCi/g 19-09014-15                   TRG L1-10221D-FIGS-010-SS-A                       07/09/19 08:45     9/3/2019      9/16/2019          19-09014       Americium-241
                                                                                          ~-~------------- :---*------- --. --*---------.----~------ --------*-------*
EPA901.1 Modified           -1.83E-02   :   1.87E-01      1.87E-01 2.67E-01    u                 pCi/g 19-09014-15                   TRG          L 1-10221 D-FIGS-010-SS-A                     07/09/19 08:45     9/3/2019      9/16/2019          19-09014           Barium-133                          EPA 901.1 Modified        i  5.07E-02       1.10E-01      1.10E-01 3.18E-01    u                 pCi/g
    "                                                                 "'""" --------~-- *---------*- '-----,--""---------                                     *-----                                                                                                                            .
19-09014-15 ;                 TRG          L 1-102210-FIGS-010-SS-A                      07/09/19 08:45     9/3/2019      9/16/2019          19-09014         Bismuth-214                           EPA 901.1 Modified           1.17E+OO      3.05E-01       3.11E-01 1.60E-01                      pCi/g
                                                                                          ---~-----------------,,,,,,*---*----- ,,,--------*--*-*
19-09014-15 j                 TRG          L1-102210-FIGS-010-SS-A                       07 /09/19 08:45    9/3/2019      9/16/2019          19-09014            Cobalt-60                          EPA 901.1 Modified          1.90E+OO       2.34E-01       2.54E-01 2.06E-01                      pCi/g 19-09014-15                   TRG          L 1-10221 D-FIGS-010-SS-A                     07/09/19 08:45  ;  9/3/2019      9/16/2019          19-09014          Cesium-134                           EPA 901.1 Modified        : -2.08E-02   i  8.0SE-02       8.0SE-02 2.41E-01    u                 pCi/g 19-09014-15                   TRG          L 1-10221 D-FIGS-010-SS-A                     07/09/19 08:45  ;  9/3/2019      9/16/2019          19-09014
* Cesium-137                           EPA901.1 Modified           8.29E+OO       9.SOE-01       1.07E+OO 4.18E-01                      pCi/g 19-09014-15                   TRG          L 1-102210-FIGS-010-SS-A
                                  -----,.........,,---*----------,---,                       07/09/19 08:45     9/3/2019      9/16/2019          19-09014 '      C,*---:**- """""
                                                                                                                                                                 --* *r-*-*** 1'-'"-                    EPA901.1 Modified           -7.94E-02      2.81E-01       2.81E-01 4.76E-01    u                 pCi/g 19-09014-15 :                 TRG          L 1-102210-FIGS-010-SS-A                      07/09/19 08:45     9/3/2019      9/16/2019          19-09014        C,*---:**-
                                                                                                                                                                        *r-*-*** *1..,..,.              EPA901.1 Modified           -3.57E-01      3.84E-01       3.84E-01 2.43E-01    u                 pCi/g TRG          L 1-102210-FIGS-010-SS-A                      07/09/19 08:45   ! 9/3/2019      9/16/2019          19-09014        C,      -: .. -
                                                                                                                                                                 --*-r-*-***'1'-''-'
                                                                                                                                                                                      "'"'""            EPA901.1 Modified         i 2.57E-01      2.28E-01       2.28E-01 3.78E-01    u                 pCi/g
 *----*--r------*-----*----------                                                                                                                                                                                                              :
19-09014-15                   TRG          L 1-102210-FIGS-010-SS-A                      07/09/19 08:45     9/3/2019      9/16/2019          19-09014 , Holmium-166m                                EPA 901.1 Modified           6.47E-02      2.37E-01       2.37E-01 1.66E-01    u                 pCi/g 19-09014-15            1 TRG          L 1-10221 D-FIGS-010-SS-A                     07/09/19 08:45  i  9/3/2019      9/16/2019          19-09014     i     lodine-129                          EPA 901.1 Modified           2.76E-01       1.65E-01      1.66E-01 2.54E-01    u                 pCi/g 19-09014-15 :                 TRG          L 1-102210-FIGS-010-SS-A 07/09/19 08:45  i  9/3/2019      9/16/2019          19-09014     j  Potassium-40                           EPA 901.1 Modified        : 2.01E+01   .. 3.19E+OO       3.35E+OO 1.94E+OO                      pCi/g 19-09014-15                   TRG          L1-10221D-FIGS-010-SS-A                       07/09/19 08:45  ;  9/3/2019
* 9/16/2019             19-09014     i .. *-* -~-* *-- :                       EPA901.1 Modified            1.25E-01       1.64E-01      1.64E-01 2.74E-01    u                 pCi/g 19-09014-15                   TRG          L1-10221D-FIGS-010-SS-A                       07/09/19 08:45     9/3/2019      9/16/2019          19-09014     i Molybdenum-93                           EPA901.1 Modified           -4.00E-02       1.47E-01      1.47E-01 1.37E-01    u                 pCi/g 19-09014-15                   TRG          L1-10221D-FIGS-010-SS-A                       07/09/19 08:45  i  9/3/2019      9/16/2019
* 19-09014
* Niobium-94                          EPA 901.1 Modified           1.56E-01       1.38E-01      1.38E-01 1.79E-01    u                 pCi/g 19-09014-15                   TRG          L1-10221D-FIGS-010-SS-A                       07 /09/19 08:45
                                                                                                             'i 9/3/2019      9/16/2019 ' 19-09014            i      Lead-210                           EPA 901.1 Modified          1.94E+OO       1.81E+OO       1.81E+OO 3.01E+OO    u                 pCi/g 19-09014-15 TRG          L1-10221D-FIGS-010-SS-A 07/09/19 08:45     9/3/2019      9/16/2019          19-09014            Lead-212                           EPA 901.1 Modified        . 1.10E+OO    i  2.53E-01       2.59E-01 5.51E-01                      pCi/g 19-09014-15                   TRG          L 1-10221 D-FIGS-010-SS-A                     07/09/19 08:45  i  9/3/2019      9/16/2019          19-09014 i          Lead-214                           EPA 901.1 Modified           1.04E+OO      3.51E-01       3.55E-01 6.40E-01                      pCi/g 19-09014-15 ;                 TRG          L 1-102210-FIGS-010-SS-A                      07/09/19 08:45  i  9/3/2019      9/16/2019          19-09014     j Promethium-145                          EPA901.1 Modified            7.61E-02       1.54E-01  i   1.54E-01 2.88E-01    u                 pCi/g
                                                                                                                                            ----              1 19-09014-15                   TRG L 1-102210-FIGS-010-SS-A
                                                           -*--------                        07/09/19 08:45  i  9/3/2019 : 9/16/2019             19-09014          Radium-226                           EPA901.1 Modified         i  1.17E+OO      3.05E-01   . 3.11E-01 1.60E-01                      pCiig 19-09014-15            :      TRG          L 1-102210-FIGS-010-SS-A                      07/09/19 08:45     9/3/2019      9/16/2019          19-09014 ;      Antimony-125                           EPA 901.1 Modified           6.02E-02      5.62E-01       5.62E-01 7.65E-01    u                 pCi/g 19-09014-15                  TRG           L 1-10221D-FIGS-010-SS-A                      07/09/19 08:45  i  9/3/2019 . 9/16/2019             19-09014 i       Thorium-234                          EPA 901.1 Modified            9.41E-01      1.76E+OO       1.76E+OO 2.62E+OO    u
                                                                                                                                                                                                                                                                                                .        pCi/g 19-09014-15                   TRG i    L 1-10221 D-FIGS-010-SS-A                     07/09/19 08:45  : 9/3/2019
* 9/16/2019              19-09014     i   ,: __:::__        --                 EPA901.1 Modified            1.03E+OO
                                                                                                                                                                                                                                               . 3.54E-01       3.57E-01 4.86E-01                      pCi/g 19-09014-15                   TRG     l    L 1-10221 D-FIGS-010-SS-A                     07/09/19 08:45  i  9/3/2019 i 9/16/2019             19-09014     i   Uranium-235                           EPA 901.1 Modified          -1.64E-01      6.42E-01       6.42E-01 9.20E-01    u                 pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
(    ~
EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830                                                              865/481-0683                 FAX   865/483-4621

Printed: 1013012019 3:09 PM                                                                                                                                                                                                                                                               Page 18 of 21 Report To:                                                                                              Work Order Details:
Patricia Giza                                                                                                     19-09014 Eberline Analytical                                                                                                                 Zion Solutions SDG:
Purchase Order:           677118 Final Report of Analysis                                                                                                     2701 Deborah Ave                                                                   . Analysis. Category:_        ENVIRONMENTAL so w -------*---
Zion, IL 60099                                                                          Sample Matrix:
Lab                              Sample                                       Client                                     Sample         Receipt       Analysis              Batch                                                                                                                                  Report Analyte                      Method               Result          cu            CSU            MDA       Qualifier ID                                 Type                                        ID                                         Date           Date           Date                 ID                                                                                                                                   Units 19-09014-16                                   TRG                    L1-10221D-FIGS-014-SS-A                                   07/09/19 08:53     9/3/2019     9/16/2019            19-09014      Actinium-228              EPA 901.1 Modified      4.27E-01       1.59E-01       1.60E-01      3.0SE-01                      pCi/g 19-09014-16                                   TRG                    L1-10221D-FIGS-014-SS-A                                   07/09/19 08:53     9/3/2019     9/16/2019             19-09014     Silver-108m               EPA 901.1 Modified      9.65E-04       1.67E-02       1.67E-02      4.61E-02         u
      ------------~- .. ~"-**------h-----*""-""'_________ _
19-09014-16                                   TRG                    L 1-102210-FIGS-014-SS-A                                  07/09/19 08:53     9/3/2019     9/16/2019             19-09014    Americium-241              EPA 901.1 Modified      5.99E-03       9.94E-02       9.94E-02      1.30E-01         u
                                                                                                                                     -*"--*-----*- *'">***-*--*----- ow'""'~-------*-**----
19-09014-16                                   TRG                    L1-10221D-FIGS-014-SS-A                                   07/09/19 08:53     9/3/2019     9/16/2019             19-09014      Barium-133               EPA901.1 Modified        1.13E-02      2.67E-02       2.67E-02      7.36E-02         u
***-**1****9*-_*0*9**-0***1*4*-_*1**6*-*-'***********TR*****-*G**- -*---*-L1**-*10**-2_2_10 F__
IG-s*-*0-*1**4*---s-S--A-*-****-- --+--0-7 /0.9/19 08:53 : 9/3/2019     9/16/2019             19-09014 . . Bismuth-214               EPA 901.1 Modified       5.19E-01                     1.11E-01      1.47E-01 19-09014~                                     TRG                    L 1-102210-FIGS-014-SS-A                                  07/09/19 08:53     9/3/2019     9/16/2019             19-09014       Cobalt-60               EPA 901.1 Modified       6.43E-02      4.09E-02       4.10E-02      1.01E-01         u
                                                                    * * * * - - * - - - - - - - - - - - - - - - * * - - * - - * -------*****-*-- - - - - * - - - * - - - - - - - * * - * - - - - - * * - - * - - - * * * * .. +***--------*----*----,-----*-*---****,**-*----*-***-*****-**-****-----------*-***********************--*---**---I 19-09014-16                                   TRG                    L1-10221D-FIGS-014-SS-A                                   07/09/19 08:53     9/3/2019     9/16/2019             19-09014     Cesium-134                EPA 901.1 Modified       7.17E-03      2.18E-02       2.18E-02      5.12E-02         u 4~~-                                                                                             ----*----> - -          -
19-09014-16                                   TRG                    L1-10221D-FIGS-014-SS-A                                   07/09/19 08:53     9/3/2019     9/16/2019             19-09014     Cesium-137                EPA 901.1 Modified       4.74E-01      9.73E-02       1.00E-01      1.02E-01
      ~~------->---*---*--*--*--*-*                                                                                                    --------***--*-~-*-------
19-09014-16                                  TRG                    L1-10221 D-FIGS-014-SS-A                                  07/09/19 08:53     9/3/2019     9/16/2019             19-09014                               EPA901.1 Modified        1.60E-02      1.0SE-01       1.0SE-01      1.67E-01         u
  ------*"*--- :-~----- .                                               "
19-09014-16                                  TRG                    L1-10221 D-FIGS-014-SS-A                                  07/09/19 08:53                  9/16/2019             19-09014                               EPA 901.1 Modified      -5.66E-02      1.23E-01       1.23E-01      8.59E-02         u 19-09014-16 19-09014-16
                             ------;--*-----*-"*----""TRG TRG L 1-10221 D-FIGS-014-SS-A L 1-102210-FIGS-014-SS-A 07/09/19 08:53 07/09/19 08:53 9/16/2019 9/16/2019 19-09014 19-09014    Holmium-166m EPA 901.1 Modified EPA 901.1 Modified 1.58E-01      1.03E-01 6.94E-02 1.04E-01 6.94E-02 1.38E-01 7.04E-02 u
u pCi/g 19-09014-16                                   TRG                    L 1-10221D-FIGS-014-SS-A                                  07/09/19 08:53                  9/16/2019             19-09014      lodine-129               EPA901.1 Modified                      9.58E+OO      9.58E+OO       3.02E+OO         u 19-09014-16 ...., _______ TRG                                        L1-102210-FIGS-O 14-SS-A                                  07/09/19 08:53                  9/16/2019             19-09014     Potassium-40              EPA 901.1 Modified                     1.57E+OO      1.66E+OO       1.07E+OO EPA 901.1 Modified                     4.14E-02                     6.59E-02         u EPA 901.1 Modified                     3.59E-02       3.59E-02      5.0SE-02         u EPA 901.1 Modified                     3.76E-02       3.77E-02      5.71E-02         u 1.94E+OO       1.94E+OO      3.18E+OO         u L 1-102210-FIGS-014-SS-A                                  07/09/19 08:53                                                                                                                      1.02E-01       1.0SE-01      1.65E-01 L 1-10221 D-FIGS-014-SS-A                                 07/09/19 08:53                                                                                                                                     1.45E-01      2.20E-01 L1-10221 D-FIGS-014-SS-A                                  07/09/19 08:53                                                                                                                                                   9.29E-01         u L 1-102210-FIGS-014-SS-A                                  07/09/19 08:53                                                                                                                                                   1.47E-01 L 1-10221 D-FIGS-014-SS-A                                 07/09/19 08:53                                                                                                                                                   1.63E-01         u 19-09014-16                                  TRG                    L 1-102210-FIGS-014-SS-A                                                                                                                                                                                                   1.32E+OO         u 1------+--- - ~ - -
* 19-09014-16                                  TRG                    L1-10221D-FIGS-014-SS-A                                                                                                      Thallium-208                                                                                  1.30E-01 1--------...l..-----
19-09014-16                                  TRG                    L 1-102210-FIGS-014-SS-A                                                                                                     Uranium-235                                                                     2.67E-01      3.72E-01         u            pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
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Patricia Giza                                                                                                                             19-09014 Eberline Analytical                                                                Zion      Solutions                                                                       Purchase Order:
SDG:
677118
                                                                                       ----------~-,-,~-                                                                                                                                                       *--**-****-*----------------
Final Report of Analysis                                                       2701 Deborah Ave                                                              _ _ Analysis Category: __ _                                 ENVIRONMENTAL Zion, IL 60099                                                                               Sample Matrix:                               so Lab                        Sample                  Client                    Sample             Receipt   Analysis               Batch                                                                                                                                                                                     Report ID                         Type                     ID                       Date                Date       Date                   ID Analyte                    Method                                  Result                             cu                CSU              MDA           Qualifier Units 19-09014-17                     TRG      L1-10221 D-QIGS-013-SS-A "m--"-~,---------,--.-                -07/09/19 08:51      '
9/3/2019 9/16/2019
                                                                                                                              -         19-09014
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